Scanning ferromagnetic resonance (FMR) for wafer-level characterization of magnetic films and multilayers
11092661 · 2021-08-17
Assignee
Inventors
- Santiago Serrano Guisan (San Jose, CA, US)
- Luc Thomas (San Jose, CA, US)
- Son Le (Gilroy, CA, US)
- Guenole Jan (San Jose, CA, US)
Cpc classification
H01P5/18
ELECTRICITY
G01R33/30
PHYSICS
International classification
G01R31/00
PHYSICS
Abstract
A ferromagnetic resonance (FMR) measurement system is disclosed with a waveguide transmission line (WGTL) connected at both ends to a mounting plate having an opening through which the WGTL is suspended. While the WGTL bottom surface contacts a portion of magnetic film on a whole wafer, a plurality of microwave frequencies is sequentially transmitted through the WGTL. Simultaneously, a magnetic field is applied to the contacted region thereby causing a FMR condition in the magnetic film. After RF output is transmitted through or reflected from the WGTL to a RF detector and converted to a voltage signal, effective anisotropy field, linewidth, damping coefficient, and/or inhomogeneous broadening are determined based on magnetic field intensity, microwave frequency and voltage output. A plurality of measurements is performed by controllably moving the WGTL or wafer and repeating the simultaneous application of microwave frequencies and magnetic field at additional preprogrammed locations on the magnetic film.
Claims
1. A scanning ferromagnetic resonance (FMR) measurement system, comprising: a controller in communication with a radio frequency (RF) generator, a power generator that is connected to a magnet, and one or both of a mounting plate, to which a flat waveguide transmission line (WGTL) is attached, and a wafer chuck configured to hold an overlying wafer under test (WUT) having a magnetic film with an exposed upper surface, the mounting plate or wafer chuck being programmed to move laterally and vertically in a step and repeat fashion, wherein: the RF generator is configured to provide a sequence of RF input signals each comprising a different microwave frequency through a RF input cable to the flat WGTL; the flat WGTL is attached to the mounting plate through a first RF connector that is affixed to a top surface of the flat WGTL proximate to a first end thereof, and through a second RF connector affixed to a top surface of the flat WGTL proximate to a second end thereof, the flat WGTL has a bottom surface below a mounting plate opening and is configured to contact a predetermined region on the exposed upper surface of the magnetic film, and to sequentially transmit a plurality of microwave frequencies thereto; and the magnet includes a magnetic pole piece aligned above the flat WGTL and providing a magnetic field through the mounting plate opening on the predetermined region of the magnetic film such that a FMR condition is established in the predetermined region thereby causing a unique microwave absorbance for each frequency that results in a RF power loss for each combination of microwave absorbance and microwave frequency and is detected from a RF output signal that passes from the flat WGTL to a RF power diode, wherein the RF power diode is configured to convert the RF output signal to a voltage signal and to send the voltage signal to the controller such that one or more magnetic properties are determined for the magnetic film.
2. The scanning FMR measurement system of claim 1, wherein the flat WGTL and mounting plate are installed in an electrical probe station.
3. The scanning FMR measurement system of claim 1, wherein a vertical movement of the mounting plate or wafer chuck causes the bottom surface of the flat WGTL to contact the predetermined region of the exposed upper surface of the magnetic film.
4. The scanning FMR measurement system of claim 1, wherein the first and second RF connectors do not contact the exposed top surface of the magnetic film or extend below a plane of contact between the flat WGTL and exposed upper surface of the magnetic film.
5. The scanning FMR measurement system of claim 1, wherein the mounting plate and flat WGTL are moved with respect to the WUT and magnetic film, which are held stationary.
6. The scanning FMR measurement system of claim 1, wherein the WUT and magnetic film are moved with respect to the flat WGTL and mounting plate, which are held stationary.
7. The scanning FMR measurement system of claim 1, wherein the flat WGTL and the magnetic film are separated after the FMR measurement by a vertical movement to establish a gap therebetween before a lateral movement is performed to align the flat WGTL over another predetermined region in the magnetic film.
8. The scanning FMR measurement system of claim 1, wherein the flat WGTL includes a top conductor layer, a rigid substrate layer, a bottom ground plane layer including a signal layer, and a dielectric layer between the rigid substrate layer and bottom ground plane layer.
9. The scanning FMR measurement system of claim 1, wherein the FMR measurement is performed with a transmission mode, wherein the RF input signal passes through the first RF connector, and the RF output signal passes through the second RF connector.
10. The scanning FMR measurement system of claim 1, further comprising a directional coupler, power divider, or bias tee that receives the RF input signal from the RF generator and then transmits the RF input signal through the RF input cable to the flat WGTL, the directional coupler, power divider, or bias tee also receives a reflected RF output signal from the WGTL through the RF input cable, and transmits the reflected RF output signal to the RF power diode in a reflectance mode for performing the FMR measurement.
11. The scanning FMR measurement system of claim 1, wherein the first and second RF connectors are end launch connectors.
12. A scanning ferromagnetic resonance (FMR) measurement system, comprising: a mounting plate including an opening extending through the mounting plate; a flat waveguide transmission line (WGTL) including a planar bottom surface extending through at least a portion of the opening of the mounting plate; a magnetic pole piece arranged over a central region of the flat WGTL, the magnetic pole piece being configured to generate a magnetic field; a magnetic film disposed below the planar bottom surface of the flat WGTL; a radio frequency (RF) generator configured to provide an RF signal to the flat WGTL, wherein the RF signal in the flat WGTL and the magnetic field generated by the magnetic pole piece interact with the magnetic film, wherein the RF signal includes a plurality of microwave frequencies; and a controller configured to move at least one of the magnetic film or the flat WGTL through a sequence of positions, each position corresponding to a plurality of measurements indicative of an interaction of the magnetic film with the RF signal in the flat WGTL and the magnetic field generated by the magnetic pole piece.
13. The scanning FMR measurement system of claim 12, wherein the flat WGTL includes: a dielectric layer; a rigid substrate disposed on the dielectric layer; a conductive element including: a planar conductive element extending along a bottom surface of the dielectric layer, a bottom surface of the planar conductive element forming the planar bottom surface of the flat WGTL; a first via element extending through the dielectric layer and the rigid substrate to contact a first end of the planar conductive element; and a second via element extending through the dielectric layer and the rigid substrate to contact a second end of the planar conductive element.
14. The scanning FMR measurement system of claim 13, wherein the flat WGTL further includes a ground plate disposed on the dielectric layer and encapsulated in the rigid substrate.
15. The scanning FMR measurement system of claim 13, wherein a signal path for the RF signal in the flat WGTL is defined by the first via element, the planar conductive element, and the second via element.
16. The scanning FMR measurement system of claim 12, wherein the controller is in communication with the RF generator, the power generator that is connected to a magnet, and one or both of the mounting plate, to which the flat WGTL is attached, and the wafer chuck configured to hold an overlying wafer under test (WUT) having the magnetic film, the mounting plate or wafer chuck being programmed to move laterally and vertically in a step and repeat fashion.
17. A scanning ferromagnetic resonance (FMR) measurement system, comprising: a wafer under test including a magnetic film; a flat waveguide transmission line (WGTL) including a planar bottom surface disposed over the magnetic film, the planar bottom surface of the flat WGTL being spaced apart from the magnetic film; a radio frequency (RF) generator coupled to a first end of the flat WGTL, the RF generator being configured to provide an input RF signal including a plurality of microwave frequencies to the flat WGTL; a magnetic pole piece arranged over the flat WGTL such that the planar bottom surface of the flat WGTL is arranged between the magnetic film and the magnetic pole piece, the magnetic pole piece being configured to generate a magnetic field simultaneous to provision of the input RF signal to the flat WGTL, wherein the input RF signal in the flat WGTL and the magnetic field generated by the magnetic pole piece interact with the magnetic film; and an RF detector coupled to a second end of the flat WGTL, the RF detector being configured to measure an output RF signal indicative of an interaction of the input RF signal in the flat WGTL and the magnetic field generated by the magnetic pole piece interact with the magnetic film.
18. The scanning FMR measurement system of claim 17, further comprising: a controller configured to move the flat WGTL through a sequence of positions, each position corresponding to a plurality of measurements indicative of the interaction of the input RF signal in the flat WGTL and the magnetic field generated by the magnetic pole piece interact with the magnetic film; and a mounting plate including an opening extending through the mounting plate, wherein at least a portion of the flat WGTL extends through at least a portion of the opening of the mounting plate.
19. The scanning FMR measurement system of claim 17, wherein flat WGTL includes a waveguide selected from the group consisting of a microstrip, a grounded coplanar waveguide, a coaxial waveguide, and combinations thereof.
20. The scanning FMR measurement system of claim 17, wherein the input RF signal has a frequency in a range from about 1 GHz to about 100 GHz, and wherein the magnetic field is less than or equal to about 3 Tesla.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION
(14) The present disclosure is a scanning FMR system that is designed to measure magnetic properties including H.sub.K and α for magnetic films or multilayers on a whole wafer at a plurality of locations identified by their (x, y) coordinates. The scanning FMR system is fully automated and features a mounting plate with a center opening in which a waveguide transmission line (WGTL) is suspended from two ends that are attached to RF connectors rigidly held on a mounting plate. It should be understood that the term “RF connector” encompasses various types of RF connectors including end launch RF connectors mentioned in the exemplary embodiments. However, other embodiments may comprise other types of RF connectors used in the art but not described herein. X-axis and y-axis coordinates on the wafer under test (WUT) are in a plane that is aligned parallel to and below the plane of the mounting plate. Each FMR measurement site on a magnetic film has a pair of coordinates (x.sub.n, y.sub.n) where n is an integer. The z-axis direction in the drawings is orthogonal to the plane of the WUT. The present disclosure also encompasses a FMR test method for measuring magnetic properties of one or more films on patterned or unpatterned wafers.
(15) Referring to
(16) The RF detector may be a power diode 55 that detects a RF output signal from the WGTL corresponding to a RF power loss caused by the FMR condition where a certain amount of microwave power is absorbed and excites the magnetic film to a resonance state. After the FMR measurement is performed at the (x.sub.n, y.sub.n) coordinate, the wafer chuck and WUT are lowered 50d via a signal through link 41c to reestablish a gap below the WGTL. Subsequently, the wafer chuck and WUT are moved to another predetermined (x.sub.n, y.sub.n) coordinate and the chuck is raised 50u to enable the WGTL to contact magnetic film top surface 43t for another FMR measurement.
(17) The controller 40 has a first link 41a to a power generator 47 that is responsible for providing an appropriate magnetic field from the magnetic field pole 83 so that an applied microwave frequency and the applied field induce a FMR condition in the magnetic film 43f when the probe chuck 42 and WUT 43 are raised 50u to enable contact of the magnetic film with a WGTL bottom surface (not shown) that is suspended through and below an opening in the mounting plate 46. Meanwhile, the controller has a second link 41b to a RF generator 49 that provides a plurality of microwave frequencies through RF input cable 51a to one end of the WGTL.
(18) In a preferred operating mode, the applied magnetic field is varied (swept from a minimum to a maximum value) at constant microwave frequency. The FMR measurement may be repeated for a plurality of different microwave frequencies. The RF power diode converts the power output to a voltage signal that is transmitted through an output cable 51b to the controller. Thereafter, the controller calculates H.sub.k and α based on each pair of applied magnetic field value and applied microwave frequency used to establish a FMR condition, and on voltage output data from the RF power diode for each (x.sub.n, y.sub.n) coordinate used in the FMR measurement sequence.
(19) The present disclosure anticipates that layouts other than the one illustrated in
(20) According to various embodiments of the present disclosure, FMR measurements are performed by analyzing a RF signal transmitted through a WGTL as described with respect to
(21) In some embodiments, the RF input and output signals pass through an end launch RF connector (not shown) positioned between the second input cable and the WGTL. In particular, the directional coupler receives reflected RF signals (output signals) from the WGTL through cable 51a2 and then directs the signals to the RF power diode 55 where a conversion occurs to a voltage output signal for each pair of applied magnetic field and applied microwave frequency (H.sub.R, f.sub.R) as previously described. The output signal is then transmitted to the controller 40 through output cable 51b.
(22) Referring to
(23) During intervals when no FMR measurements are being performed, the tip portion 45b is a gap distance k>0 from the top surface 43t of magnetic film 43f on WUT 43. As indicated previously, when the FMR system is programmed to perform a FMR measurement at a certain (x.sub.n, y.sub.n) coordinate, the wafer chuck is raised so that k=0 until the FMR measurement is completed. In an alternative embodiment, k is proximate to 0 and sufficiently small, preferably less than 100 micrometers, to enable efficient transmission of microwaves from the WGTL to the magnetic film. It is important that the magnetic pole tip 83b is above opening 46a and aligned over the (x.sub.n, y.sub.n) coordinate where tip portion 45b makes contact with top surface 43t so that the same region proximate to the (x.sub.n, y.sub.n) coordinate is exposed to both of the magnetic field and microwave frequency.
(24) Referring to
(25) The entire WGTL assembly (WGTL and end launch RF connectors) is affixed to the mounting plate 46 by two removable and retractile clamps 56. Opening 46a may be formed therein by a conventional method and has an x-axis dimension of sufficient length to enable a bent WGTL to be suspended between the two clamps, and have a middle tip portion below the plane of the mounting plate.
(26) The present disclosure also encompasses a second embodiment of an FMR measurement system similar to the scheme depicted in
(27) Referring to the top view of the second embodiment in
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(29) During a FMR measurement when a magnetic field is applied to an area around an (x, y) coordinate of the magnetic film contacted by the WGTL, a microwave frequency passes through end launch connector 54c and the top conductor layer 61t, and then through via 61v1 and into the signal path layer 61b. A portion of the microwave power is absorbed by the magnetic film 43f during a FMR condition so that the output RF signal carried through via 61v2 and out through end launch connector 54d has reduced power compared with the input RF signal. The RF power diode (not shown) converts the output RF power signal for each (H.sub.R, f.sub.R) pair to a voltage measurement that is relayed to the controller.
(30) Referring to
(31) As a result of the simultaneous application of microwave frequency F1 and the magnetic field, the magnetic film achieves a FMR condition and absorbs a portion of the microwave power that depends on the magnetic properties of the magnetic film, F1, and the applied field (H.sub.R). Accordingly, in step 112, the RF power diode detects a reduced power value in the RF output signal compared with the value specified by the controller in the RF input signal from step 111.
(32) In step 113, the RF power diode converts the RF output signal to a voltage measurement that is transmitted to the controller and indicates the microwave absorbance by the magnetic film for applied microwave frequency F1 and applied magnetic field H.sub.R.
(33) Step 114 comprises a repetition of steps 111-113 except the RF input signal has a second frequency F2 that is applied to the magnetic film at the previously selected (x, y) coordinate after F1 is applied. In some embodiments, steps 111-113 are repeated a plurality of times at each (x, y) coordinate used for the FMR measurement method. In other words, a third frequency F3 that differs from F1 and F2 may be applied during an interval of time after F2, and so forth up to an “nth” frequency Fn after F3 is applied. Note that the applied magnetic field is swept between a minimum and a maximum value when each frequency F1 up to Fn is applied according to a preferred embodiment. Thus, a FMR condition occurs with each applied frequency, and each FMR condition has a unique microwave absorbance that is translated into a corresponding voltage signal by the RF power diode. In an alternative embodiment, the applied magnetic field is held constant while the microwave frequencies are varied (swept) from F1 up to Fn to establish a FMR condition.
(34) Referring to step 115, the controller commands the wafer chuck and overlying magnetic film to be lowered (movement 50d in
(35) Thereafter, steps 111-114 are repeated to complete a FMR measurement at the second location. Note that each location may comprise a contact area of a plurality of square millimeters, and each (x, y) coordinate may be a center point in the area contacted by the WGTL.
(36) Depending on the size of the magnetic film area to be contacted by the WGTL, and the number of different positions desired for an FMR measurement, step 116 indicates that steps 111-115 may be repeated a plurality of times to yield a plurality of FMR measurements involving “m” different (x, y) coordinates each with a plurality of (H.sub.R, f.sub.R) pairs where f.sub.R is one of F1 up to Fn. At step 117, a decision is made whether or not all of the pre-selected (x, y) coordinates on the magnetic film have been tested. If “no”, another FMR measurement is taken at a different (x, y) coordinate. If “yes”, step 118 indicates the FMR measurement process is complete.
(37) As mentioned earlier, the controller is capable of determining magnetic properties in the magnetic film at each location corresponding to a different (x, y) coordinate. Each FMR measurement yields one or more pairs (frequency, field) also referred to as (H.sub.R, f.sub.R) pairs in equation (1) corresponding to each FMR condition. The controller uses FMR measurement data and one or more of equations (1)-(3) described previously to determine Hk, α, and in some cases γ and inhomogeneous broadening (L.sub.0).
(38) An experiment was performed using the FMR system with a bent WGTL shown in
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(40) In a second experiment, the same MTJ stack of layers was retained from the first experiment. However, the free layer thickness was purposely varied from 17 Angstroms in the upper left portion of the wafer by small increments to 18.5 Angstroms in the lower right corner to demonstrate how the FMR measurement system and method of the present disclosure may be advantageously used as a tool to explore H.sub.K dependence on free layer thickness. The experimental results are mapped in
(41) RF connectors, the probe station (platform), RF generator, RF power diode, input and output cables, as well as alternative RF devices such as vector network analyzers, pulse generators, and time-resolved oscilloscopes are commercially available. A suitable magnet comprising a magnetic pole piece that delivers the required magnetic field to induce a magnetic resonance according to the present disclosure is also commercially available or may be custom built by one skilled in the art.
(42) While this disclosure has been particularly shown and described with reference to, the preferred embodiment thereof, it will be understood by those skilled in the art that various changes in form and details may be made without departing from the spirit and scope of this disclosure.