SPECIMEN PREPARATION METHOD FOR ELIMINATING MEMBRANE PENETRATION EFFECT ON HIGHLY-WEATHERED ROCK
20210190649 · 2021-06-24
Assignee
Inventors
- Xianwei Zhang (Wuhan, CN)
- Xinyu Liu (Wuhan, CN)
- Chao Ma (Wuhan, CN)
- Jijun Du (Wuhan, CN)
- Ruiduo Li (Wuhan, CN)
- Cheng CHEN (Wuhan, CN)
Cpc classification
G01N2203/0256
PHYSICS
G01N1/286
PHYSICS
G01N1/28
PHYSICS
International classification
Abstract
A specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock, wherein the method makes an originally uneven surface of a specimen smooth using a cured liquid latex as a filler, thereby eliminating a membrane penetration effect on a highly-weathered rock, and comprises the following specimen preparation steps: specimen cutting, pit filling, surface smoothing, specimen shaping and specimen loading.
Claims
1. A specimen preparation method, comprising: (1) taking a soil specimen out of a soil specimen tube or a packaging bag, removing a soil layer on a surface of the soil specimen by cutting to obtain a standard cylindrical triaxial specimen, and testing a diameter of the specimen with a slide caliper and recording the diameter as d.sub.1; (2) laying a wet filter paper on upper and lower surfaces of the specimen, smearing a liquid latex on a peripheral surface of the specimen for packaging and leveling with a cutter to make the peripheral surface of the specimen smooth, and placing the packaged specimen in a moisture preservation vat and letting it stand until the liquid latex on the peripheral surface of the specimen is cured; (3) disposing a membrane tube around a membrane, turning two ends of the membrane outwards to be attached to an outside of the membrane tube and the portions located outside the membrane tube of the membrane are banded with rubber bands; inserting a pointed end of a plastic suction bulb into a suction hole of the membrane tube, and pressing the plastic suction bulb to exhaust air between the membrane and the membrane tube; and dipping the liquid latex with a finger wearing a latex glove into the liquid latex and smearing in the membrane, wherein an average thickness of the liquid latex smeared in the membrane is 0.1 mm; (4) placing the specimen processed in step (2) into the membrane sleeve prepared in step (3) and integrally curing with the membrane sleeve, wherein an inner surface of the membrane sleeve is coated with the liquid latex, and a thickness of the membrane sleeve is d.sub.0; (5) instantly placing the specimen processed in step (4) in a triaxial confining pressure chamber after porous stones are placed in an upper portion and a lower portion of the specimen, respectively, applying a confining pressure to press the liquid latex into the specimen, and letting the specimen stand until the liquid latex is cured, wherein the confining pressure is 10 kPa; and (6) releasing the confining pressure, removing the membrane sleeve, measuring an outer diameter d.sub.2 of the specimen with a slide caliper, and loading a specimen meeting d.sub.2/d.sub.1<1.01 for a triaxial shear test.
2. The specimen preparation method according to claim 1, wherein the diameter of the specimen is 50.00 mm, a height of the specimen is 100.0 mm, the soil specimen contains 15.0 wt % of gravel particles, 50.0 wt % of sand particles and 35.0 wt % of clay particles in step (1); and a thickness of the liquid latex smeared in the membrane is 0.1 mm during step (3).
3. The specimen preparation method according to claim 1, wherein the liquid latex stands in the moisture preservation vat for 5 hrs to be cured during step (2).
4. The specimen preparation method according to claim 1, wherein the liquid latex stands in the confining pressure chamber for 5 hrs to be cured during step (4).
Description
BRIEF DESCRIPTION OF THE SEVERAL VIEWS OF THE DRAWINGS
[0027]
[0028]
[0029]
[0030]
[0031]
[0032]
[0033]
[0034]
[0035]
[0036]
[0037]
[0038] Reference numerals in the drawings are used to refer to the following structures: 1.sub.a—first filter paper; 1b—second filter paper; 2—clay particle; 3—sand particle; 4—liquid latex; 5—membrane; 6—membrane tube; 6b—second outer cylinder; 7—suction hole; 8—plastic rubber suction bulb; 9a—first rubber band; 9b—second rubber band; 10—cylindrical specimen.
DETAILED DESCRIPTION OF THE INVENTION
[0039] To make the objective, contents and advantages of the invention clearer, a specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock provided by the examples of the invention will be explained below in further detail in conjunction with the accompanying drawings.
Example 1
[0040] In the example, a test material is highly-weathered granite in Xiamen and contains 15.0 wt % of gravel particles, 50.0 wt % of sand particles and 35.0 wt % of clay particles, a specimen is a standard triaxial specimen (with a diameter of 50.0 mm and a height of 100.0 mm) and undisturbed, the thickness d.sub.0 of a membrane adopted is 0.3 mm, and a confining pressure for consolidation is 500 kPa.
[0041] As shown in
[0042] (1) Specimen Cutting
[0043] A soil column with sizes a bit larger than the sizes (diameter 50.0 mm, height 100.0 mm) of a triaxial specimen is obtained; the soil column is cut with a soil cutter at first until the height of the specimen reaches 102.0 mm; then, the side face of the specimen is cut with a wire saw until the specimen is cut into a cylinder with a diameter of 50.0 mm; and finally, the specimen is cut with the wire saw until the height of the specimen reaches 100.0 mm, so that a cylindrical specimen 10 with standard sizes is obtained, as shown in
[0044] (2) Pit Filling
[0045] Wet first filter paper 1a and wet second filter paper 1b are pasted on the upper surface and the lower surface of the specimen 10 respectively; then the first filter paper 1a, the specimen 10 and the second filter paper 1b are sequentially placed on a horizontal test stand; a liquid latex 4 to be filled in pits in the surface of the specimen is scrapped with a small blade, the liquid latex 4 adopted in the example is No.C1204 produced by Woodland Scenics, is up to the quality standard of American Society for Testing and Materials (abbreviated as ASTM), is non-toxic, and has a relatively density of 0.98, a viscosity of 15 mPa.Math.s and a pH of 7.1, and the liquid latex 4 is filled in pits between the clay particles 2 and the sand particles 3; after that, the liquid latex 4 is carefully leveled with the soil cutter to make the specimen 10 as smooth as possible; when all the pits are filled with the liquid latex 4, the first filter paper 1a, the specimen 10 and the second filter paper 1b are placed in a moisture preservation vat and stand for 5 h until the liquid latex 4 is cured, and the cylindrical specimen 10 obtained after pit filing is shown in
[0046] (3) Surface Smoothening
[0047] As shown in
[0048] (4) Specimen Shaping
[0049] The plastic suction bulb 8, the first rubber band 9a, the second rubber band 9b and the membrane tube 6 are removed sequentially, a porous stone is placed in each of upper and lower portions of the specimen 10 wrapped with the membrane 5, then the specimen 10 is instantly placed in a triaxial confining pressure chamber, a 10 kPa confining pressure is applied to press the liquid latex 4 into voids of particles on the surface of the specimen until the voids are full of the liquid latex, and the specimen 10 stands for 5 h under the 10 kPa confining pressure to cure the liquid latex 4.
[0050] (5) Specimen Loading
[0051] The confining pressure is released; the specimen 10 wrapped with the membrane 5 is taken out, and the outer diameter d.sub.2 of the specimen 10 is measured with the slide caliper, wherein d.sub.2 is equal to the sum of d.sub.0, d.sub.1 and the thickness of the cured liquid latex 4. The influence of the thickness of the membrane having the liquid latex 4 cured thereon on the triaxial test is evaluated by calculation according to the following formula:
M=d.sub.2/d.sub.1.
[0052] If M is less than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon will not exert an additional constraint force on the specimen, and the prepared specimen will be loaded in terms of Standard for Soil Test Method (GB/T50123-1999) for the triaxial test; or, if M is greater than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon may exert an additional constraint force on the specimen, which will increase the intensity of the specimen; and in this case, specimen preparation and loading need to be carried out again according to Step (1)-Step (4) until M is less than 1.01, and then the triaxial shear test will be carried out.
[0053] M obtained by the specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock according to the invention is 1.008.
[0054] The triaxial shear test is carried out in terms of Standard for Soil Test Method (GB/T50123-1999), a TSZ30-2.0 bench triaxial instrument produced by Nanjing Soil Instrument Co., Ltd. is used as test equipment, and the triaxial shear test comprises the following specific steps:
[0055] {circle around (1)} Specimen loading: the specimen is loaded according to Step (1)-Step (5);
[0056] {circle around (2)} Installation of the confining chamber: a piston at the top of the confining chamber is lifted, the pressure chamber is lowered, the position is aligned to the center of the specimen, base connecting nuts are uniformly tightened, pure water is injected into the pressure chamber, an exhaust hole is tightened when water overflows from the exhaust hole in the top of the pressure chamber, and the piston is aligned to a forcemeter and the top of the specimen;
[0057] {circle around (3)} Installation of the forcemeter: a clutch is adjusted to a rough adjustment gear, and a rough adjustment hand wheel is rotated; when a specimen cap and the piston are close to the forcemeter, the clutch is adjusted to a fine adjustment gear, and a fine adjustment hand wheel is used to make the specimen cap and the piston contact with the forcemeter; a deformation indicator is installed, and the forcemeter and the deformation indicator are adjusted to zero;
[0058] {circle around (4)} Application of a consolidation pressure: a drain valve is closed, a pressure valve around is opened, and a 500 kPa consolidation pressure is applied;
[0059] {circle around (5)} Shearing: a motor is started and the clutch is closed to start shearing, and the shear strain rate is controlled to 0.5% per minute; and when a reading on the forcemeter reaches a peak value, shearing should be continuously carried out until the axial strain reaches 20%;
[0060] {circle around (6)} End of the test: when the test ends, the motor is stopped, the pressure valve around is closed, the clutch is opened and is adjusted to the rough adjustment gear, and the rough adjustment hand wheel is rotated to lower the pressure chamber, the exhaust hole is opened, water in the pressure chamber is drained, the pressure chamber cover is disassembled, and the specimen is unloaded.
Example 2
[0061] To better verify the reliability and practicability of the specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock of the invention, a test material containing particles different from those in Example 1 is selected, and the test material in Example 2 is highly-weathered granite in Shenzhen and contains 10.0 wt % of gravel particles, 45.0 wt % of sand particles and 45.0 wt % of clay particles. In addition, to check the influence of the sizes of the specimen, the thickness of the membrane and the confining pressure for consolidation on the specimen preparation method, the sizes of the specimen and the thickness of the membrane are different from those in Example 1, wherein the diameter of the specimen is 38.0 mm, the height of the specimen is 80.0 mm, the thickness d.sub.0 of the membrane is 0.2 mm, and the confining pressure for consolidation is 500 kPa.
[0062] As shown in
[0063] (1) Specimen Cutting
[0064] A soil column with sizes a bit larger than the sizes (diameter 38.0 mm, height 80.0 mm) of a triaxial specimen is obtained; the soil column is cut with a soil cutter at first until the height of the specimen reaches 82.0 mm; then, the side face of the specimen is cut with a wire saw until the specimen is cut into a cylinder with a diameter of 40.0 mm; and finally, the specimen is cut with the wire saw until the height of the specimen reaches 80.0 mm, so that a cylindrical specimen 10 with standard sizes is obtained, as shown in
[0065] (2) Pit Filling
[0066] Wet first filter paper 1a and wet second filter paper 1b are pasted on the upper surface and the lower surface of the specimen 10 respectively; then the first filter paper 1a, the specimen 10 and the second filter paper 1b are sequentially placed on a horizontal test stand; a liquid latex 4 to be filled in pits in the surface of the specimen is scrapped with a small blade, and the liquid latex 4 adopted in Example 1 is No.C1204 produced by Woodland Scenics and is filled in pits between the clay particles 2 and the sand particles 3; after that, the liquid latex 4 is carefully leveled with the soil cutter to make the specimen 10 as smooth as possible; when all the pits are filled with the liquid latex 4, the first filter paper 1a, the specimen 10 and the second filter paper 1b are placed in a moisture preservation vat and stand for 5 h until the liquid latex 4 is cured, and the cylindrical specimen 10 obtained after pit filing is shown in
[0067] (3) Surface Smoothing
[0068] As shown in
[0069] (4) Specimen Shaping
[0070] The plastic suction bulb 8, the first rubber band 9a, the second rubber band 9b and the membrane tube 6 are removed sequentially, a porous stone is placed in each of upper and lower portions of the specimen 10 wrapped with the membrane 5, then the specimen 10 is instantly placed into a triaxial confining pressure chamber, a 10 kPa confining pressure is applied to press the liquid latex 4 into voids of particles on the surface of the specimen until the voids are full of the liquid latex, and the specimen 10 stands for 5 h under the 10 kPa confining pressure to cure the liquid latex 4.
[0071] (5) Specimen Loading
[0072] The confining pressure is released; the specimen 10 wrapped with the membrane 5 is taken out, and the outer diameter d.sub.2 of the specimen 10 is measured with the slide caliper, wherein d.sub.2 is equal to the sum of d.sub.0, d.sub.1 and the thickness of the cured liquid latex 4. The influence of the thickness of the membrane having the liquid latex 4 cured thereon on the triaxial test is evaluated by calculation according to the following formula:
M=d.sub.2/d.sub.1.
[0073] If M is less than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon will not exert an additional constraint force on the specimen, and the prepared specimen will be loaded in terms of Standard for Soil Test Method (GB/T50123-1999) for the triaxial test; or, if M is greater than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon may exert an additional constraint force on the specimen, which will increase the intensity of the specimen; and in this case, specimen preparation and loading need to be carried out again according to Step (1)-Step (4) until M is less than 1.01, and then the triaxial shear test will be carried out.
[0074] M obtained by the specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock according to the invention is 1.007.
[0075] The triaxial shear test is carried out in terms of Standard for Soil Test Method (GB/T50123-1999), a TSZ30-2.0 bench triaxial instrument produced by Nanjing Soil Instrument Co., Ltd. is used as test equipment, and the specific steps of the test are the same as those in Example 1.
Comparative Test 1:
[0076] Due to the fact that the curing time of the liquid latex 4 has a great influence on the triaxial specimen preparation method, which will indirectly influence the accuracy of test results, and that the thickness of the liquid latex 5 smeared in the membrane 5 in Step (3) in Example 1 and Example 2 also has a great influence on the test results, this comparative test adopts a test material and condition the same as those in Example 2 and a different curing time and thickness of the liquid latex 4.
[0077] As shown in
[0078] (1) Specimen Cutting
[0079] A soil column with sizes a bit larger than the sizes (diameter 38.0 mm, height 80.0 mm) of a triaxial specimen is obtained; the soil column is cut with a soil cutter at first until the height of the specimen reaches 82.0 mm; then, the side face of the specimen is cut with a wire saw until the specimen is cut into a cylinder with a diameter of 40.0 mm; and finally, the specimen is cut with the wire saw until the height of the specimen reaches 80.0 mm, so that a cylindrical specimen 10 with standard sizes is obtained, as shown in
[0080] (2) Pit Filling
[0081] Wet first filter paper 1a and wet second filter paper 1b are pasted on the upper surface and the lower surface of the specimen 10 respectively; then the first filter paper 1a, the specimen 10 and the second filter paper 1b are sequentially placed on a horizontal test stand; a liquid latex 4 to be filled in pits in the surface of the specimen is scrapped with a small blade, and the liquid latex 4 adopted in Example 1 is No.C1204 produced by Woodland Scenics and is filled in pits between the clay particles 2 and the sand particles 3; after that, the liquid latex 4 is carefully leveled with the soil cutter to make the specimen 10 as smooth as possible; when all the pits are filled with the liquid latex 4, the first filter paper 1a, the specimen 10 and the second filter paper 1b are placed in a moisture preservation vat and stand for 3 h until the liquid latex 4 is cured, and the cylindrical specimen 10 obtained after pit filing is shown in
[0082] (3) Surface Smoothing
[0083] As shown in
[0084] (4) Specimen Shaping
[0085] The plastic suction bulb 8, the first rubber band 9a, the second rubber band 9b and the membrane tube 6 are removed sequentially, a porous stone is placed in each of upper and lower portions of the specimen 10 wrapped with the membrane 5, then the specimen 10 is instantly placed into a triaxial confining pressure chamber, a 10 kPa confining pressure is applied to press the liquid latex 4 into voids of particles on the surface of the specimen until the voids are full of the liquid latex, and the specimen 10 stands for 5 h under the 10 kPa confining pressure to cure the liquid latex 4.
[0086] (5) Specimen Loading
[0087] The confining pressure is released; the specimen 10 wrapped with the membrane 5 is taken out, and the outer diameter d.sub.2 of the specimen 10 is measured with the slide caliper, wherein d.sub.2 is equal to the sum of d.sub.0, d.sub.1 and the thickness of the cured liquid latex 4. The influence of the thickness of the membrane having the liquid latex 4 cured thereon on the triaxial test is evaluated by calculation according to the following formula:
M=d.sub.2/d.sub.1.
[0088] If M is less than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon will not exert an additional constraint force on the specimen, and the prepared specimen will be loaded in terms of Standard for Soil Test Method (GB/T50123-1999) for the triaxial test; or, if M is greater than 1.01, it will be regarded that the thickness of the membrane having the liquid latex 4 cured thereon may exert an additional constraint force on the specimen, which will increase the intensity of the specimen; and in this case, specimen preparation and loading need to be carried out again according to Step (1)-Step (4) until M is less than 1.01, and then the triaxial shear test will be carried out.
[0089] M obtained by the specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock according to the invention is 1.006.
[0090] The triaxial shear test is carried out in terms of Standard for Soil Test Method (GB/T50123-1999), a TSZ30-2.0 bench triaxial instrument produced by Nanjing Soil Instrument Co., Ltd. is used as test equipment, and the specific steps of the test are the same as those in Example 1 and Example 2.
Comparative Test 2:
[0091] The test material in Example 1 is adopted: highly-weathered granite in Xiamen containing 15.0 wt % of gravel particles, 50.0 wt % of sand particles and 35.0 wt % of clay particles; the specimen is a standard triaxial specimen (with a diameter of 50.0 mm and a height of 100.0 mm) and undisturbed, the thickness d.sub.0 of a membrane adopted is 0.3 mm, and a confining pressure for consolidation is 500 kPa.
[0092] To compare the advantages and disadvantages of the technical solution of the invention and existing specimen preparation methods for weakening an membrane penetration effect on an undisturbed specimen, the specimen preparation method put forward in the literature (Lu, Xiaoping et al., “Study on the influence of End Restraints on Triaxial Specimens of Coarse-grained Soil,” Chinese Journal of Geotechnical Engineering, 2017, 39 (Supplement 1): 236-240) fills a specimen with a stainless steel sheet or a copper sheet in the specimen preparation process and comprises the following steps: a specimen cap is lubricated by placing a polished stainless steel sheet or copper sheet with a hole in the middle (for draining) at two ends of the specimen and placing a latex membrane (0.4 mm thick) with one side coated with lubricating oil (silicon grease) between the stainless steel sheet or the copper sheet and the specimen, wherein the periphery of the latex membrane is cut in the radial direction and the side coated with the lubricating oil is attached to the stainless steel sheet; and the specimen loading method put forward by Lu Xiaoping adopts a triaxial test process and steps completely the same as those in Example 1.
[0093] As shown in
[0094] In addition, according to triaxial test results obtained in Example 1 and Example 2 of the specimen preparation method for eliminating a membrane penetration effect on a highly-weathered rock (
[0095] The technical solution of the invention can effectively eliminate disadvantageous influences of a membrane penetration effect on a highly-weathered rock, such that an obtained triaxial shear test result is true, reliable and precise. The method is featured by non-toxic test materials, low costs, feasible steps, simple operations, and a short test period. The technical solution can avoid the problem of test failures caused when protruding quartz particles on the surface of a specimen penetrate through a membrane under high pressure.
[0096] The above examples are merely preferred ones of the invention, and are not intended to limit the invention. Any simple modifications, changes and equivalent structural transformations made to the above examples based on the principle of the invention should also fall within the protection scope of the technical solution of the invention.