SCANNING ELECTRON MICROSCOPE OBJECTIVE LENS SYSTEM AND METHOD FOR SPECIMEN OBSERVATION
20210110994 · 2021-04-15
Inventors
Cpc classification
H01J37/244
ELECTRICITY
H01J2237/2449
ELECTRICITY
H01J2237/24495
ELECTRICITY
International classification
Abstract
A scanning electron microscope objective lens system is disclosed, which includes: a magnetic lens, a deflection device, a deflection control electrode, specimen to be observed, and a detection device; in which, The opening of the pole piece of the magnetic lens faces to the specimen; the deflection device is located in the magnetic lens, which includes at least one sub-deflector; the deflection control electrode is located between the detection device and the specimen, and the deflection control electrode is used to change the direction of the primary electron beam and the signal electrons generating from the specimen; the detection device comprises the first sub-detector for detecting the back-scattered electrons and the second sub-detector for detecting the second electrons. A specimen detection method is also disclosed.
Claims
1. A scanning electron microscope objective lens system, comprising: a magnetic lens, a deflection device, a deflection control electrode, a specimen to be observed and a detection device, wherein, an opening of a pole piece of the magnetic lens faces to the specimen; the deflection device is arranged in the magnetic lens, which contains at least one sub-deflector; the deflection control electrode is located between the detection device and the specimen, and is arranged to change a direction of a primary electron beam impinging on the specimen and change a direction of signal electrons generated, at the specimen, due to the impinging; and the detection device comprises a first sub-detector for detecting back-scattered electrons among the signal electrons and a second sub-detector for detecting secondary electrons among the signal electrons.
2. The scanning electron microscope objective lens system according to claim 1, wherein the deflection control electrode includes: a first central hole and a plurality of deflection control sub-electrodes; and the plurality of deflection control sub-electrodes are deployed around the first central hole.
3. The scanning electron microscope objective lens system according to claim 2, wherein the first sub-detector comprises a second central hole, a diameter of the second central hole is smaller than that of the first central hole.
4. The scanning electron microscope objective lens system according to claim 1, wherein the first sub-detector includes at least one first sub-detection component; and each of the first sub-detection components is arranged to acquire a signal corresponding to signal electrons of a respective zone and send the signal to an external image processing device to image the signal electrons of the respective zone.
5. The scanning electron microscope objective lens system according to claim 3, wherein the diameter of the second central hole is of an order of millimeters.
6. The scanning electron microscope objective lens system according to claim 1, wherein the specimen to be observed is located on a specimen stage; and a second voltage of the specimen stage is V2, and the first sub-detector, the deflection control electrode, and the specimen stage make up a retarding electrostatic lens field.
7. The scanning electron microscope objective lens system according to claim 1, wherein the system further includes a high voltage tube, and a central axis of the high voltage tube coincides with that of the magnetic lens.
8. The scanning electron microscope objective lens system according to claim 7, wherein the sub-deflectors are magnetic deflectors.
9. The scanning electron microscope objective lens system according to claim 6, wherein, the second voltage of the specimen stage is V2, where V2 is no less than −30 kilovolts (kV) and no more than 5 kV; a voltage of the first sub-detector is 0 volt (V), the deflection control electrode is applied to a third voltage and a fourth voltage; the third voltage V3 is constant, where V3 is no less than V2 and no more than 0; and the fourth voltage V4 is an alternating voltage.
10. The scanning electron microscope objective lens system according to claim 7, wherein a voltage of the specimen to be observed is 0V, the deflection control electrode is applied to a third voltage and a fourth voltage; a voltage of the first sub-detector is V5, 5 kV≤V5≤30 kV; a third voltage V3 is constant, where V3 is no less than 0 and no more than V5; a fourth voltage V4 is an alternating voltage.
11. A specimen detection method, applied to a scanning electron microscope objective lens system, wherein a first sub-detector for receiving back-scattered electrons, a deflection control electrode, and a specimen to be observed in the scanning electron microscope objective lens system form a retarding electrostatic lens field, the retarding electrostatic lens field overlaps with a magnetic field produced by a magnetic lens in the scanning electron microscope objective lens system at a zone near the specimen, to form a compound objective retarding immersion lens field; the method comprises: making a primary electron beam to pass through the compound objective retarding immersion lens field, controlling a deflection device in the scanning electron microscope objective lens system and the deflection control electrode to deflect the primary electron beam, wherein after the deflection, the primary electron beam impinges on the specimen to produce signal electrons; controlling a voltage of the deflection control electrode, such that the signal electrons are received by the first sub-detector and a second sub-detector in the scanning electron microscope system.
12. The method according to claim 11, further comprising: controlling the voltage of the deflection device and the deflection control electrode, to couple a deflection field formed by the deflection device and the deflection control electrode to the compound objective retarding immersion lens field, and achieve shifting objective retarding receiving lens field scanning of the specimen or swing objective retarding receiving lens field scanning of the specimen.
13. The method according to claim 12, wherein in case the deflection device includes a plurality of sub-deflectors, wherein controlling the voltage of the deflection device and the deflection control electrode, to couple the deflection field to the compound objective retarding immersion lens field includes: controlling the voltage of the sub-detector nearest to the specimen among the plurality of sub-detectors, and controlling the voltage of the deflection control electrode, to couple the deflection field produced by the sub-deflector nearest to the specimen and the deflection control electrode with the compound objective retarding immersion lens field.
14. The method according to claim 11, wherein the sub-detector includes at least one sub-detector component, the method further comprises: acquiring, by each of the first sub-detection components, a signal corresponding to signal electrons of a respective zone, and sending the signal to an external image processing device to image the signal electrons of the respective zone.
15. The method according to claim 11, wherein the specimen is located at the specimen stage; a second voltage of the specimen stage is V2, the first sub-detector, the deflection control electrode, and the specimen stage make up a retarding electrostatic lens field.
16. The method according to claim 11, wherein the system further includes a high voltage tube, a central axis of the high voltage tube coincides with that of the magnetic lens.
17. The method according to claim 15, wherein the deflection control electrode is applied to a third voltage and a fourth voltage, and the fourth voltage is an alternating voltage; a voltage of the specimen stage is set to be V2, where V2 is no less than −30 kilovolts (kV) and no more than 5 kV; a voltage of the first sub-detector is set to be 0 volt (V), and the third voltage V3 is set to be a constant, where V3 is no less than V2 and no more than 0.
18. The method according to claim 16, wherein the deflection control electrode is applied to a third voltage and a fourth voltage, and the fourth voltage is an alternating voltage; a voltage V2 of the specimen stage is set to be 0; a voltage of the first sub-detector is set to be V5, where V5 is no less than 5 kV and no more than 30 kV, and the third voltage V3 is set to be a constant, where V3 is no less than 0 and no more than V5.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION
[0042] The details are described as follows with reference to the figures and several embodiments. It should be understood that the specific embodiments described herein are merely used to explain the disclosure, and are not intended to limit the disclosure.
[0043] Before the disclosure is further described in detail, the terms involved in the embodiments of the disclosure are described. The terms involved in the embodiments of the disclosure are applicable to the following explanations.
[0044] 1) Space charge effect. This is a phenomenon that in the electronic optical system the Coulomb forces between the electrons make the electron beam “expansion” and lead to increasing of the aberration of the electron beam imaging system. Especially when the electron beam forms a crossover beam spot, the density of the electron beam is very high in the crossover beam spot, and the distance between the electrons is small. Due to that the Coulomb's force is inversely proportional to the square of the distance between the electrons, a larger Coulomb force will cause the beam spot of the electron beam to expand.
[0045] 2) The primary electron beam. The electron beam generated by the electron source is referred to as the primary electron beam before reaching the specimen.
[0046] 3) Signal electrons. The electrons emitted from the specimen when the primary electron beam impinges on the specimen are referred to as the signal electrons, including: secondary electrons (SEs) and backscattered electrons (BSEs).
[0047] 4) Optical axis. It is the central axis of the electron beam.
[0048] 5) Large field (or large field scanning). The area of the specimen that is covered by the primary electron beam scanning is called the scanning field or field of view (FOV); therefore, large field usually refers to a scanning field whose area is large, in terms of the scanning electron microscope, when the side length of the field area reaches several hundreds of micrometers, the field can be called a large field.
Embodiment 1
[0049] The embodiment 1 of the disclosure provides a scanning electron microscope objective lens system. As shown in
[0050] In the embodiment 1 of the present disclosure, the magnetic lens 101 is a current-driven immersion magnetic lens, the opening of the annular polepiece faces to the specimen 107; the position of the optical axis of the magnetic lens 101 with the maximum magnetic field intensity is near to the specimen, so as to form a magnetic immersion lens.
[0051] In the embodiment 1 of the present disclosure, the deflection device 102 is located in the magnetic lens 101; the deflection device 102 includes at least one sub-deflector.
[0052] When the deflection device 102 includes multiple sub-deflectors, these sub-deflectors can be made up of pure electrostatic deflectors, or pure magnetic deflectors, or a combination of electrostatic and magnetic deflectors.
[0053] When the multiple sub-deflectors of the deflection device 102 are a combination of electrostatic and magnetic deflectors, there is no limit to the number of the two kinds of deflectors. For example, when the deflection device 102 includes four sub-deflectors, in an embodiment, there is one electrostatic deflector and three magnetic deflectors; in another embodiment, there are two electrostatic deflectors and two magnetic deflectors; in yet another embodiment, there are three electrostatic deflectors and one magnetic deflector; in yet another embodiment, there are four magnetic deflectors and no electrostatic deflector; and in yet another embodiment, there are four electrostatic deflectors and no magnetic deflector.
[0054] In the embodiment 1 of the present disclosure, the deflector device 102 is cylindrical, when the deflection device 102 includes multiple sub-deflectors, the sub-deflectors are deployed in the magnetic lens from top to bottom along the axis of the magnetic lens 101. When the multiple sub-deflectors are a combination of electrostatic and magnetic deflectors, there is no limit to the position of anyone of the deflectors. For example, when the deflection device 102 includes four sub-deflectors, in an embodiment, the types of the sub-deflectors from top to bottom along the axis of magnetic lens are respectively: electrostatic deflector, electrostatic deflector, magnetic deflector, and magnetic deflector; in another embodiment the types of the sub-deflectors from top to bottom along the axis of magnetic lens are respectively: electrostatic deflector, magnetic deflector, electrostatic deflector, and magnetic deflector; in yet another embodiment, the types of the sub-deflectors from top to bottom along the axis of magnetic lens are respectively: magnetic deflector, magnetic deflector, electrostatic deflector, and electrostatic deflector. Of course, there are some other combinations for the types and positon of the multiple deflectors, which we will not describe in detail here.
[0055] In the embodiment 1 of the present disclosure, the deflection-control electrode 103 is made of nonmagnetic and electrically conductive material, and it is located under the magnetic lens 101, and above the specimen 107.
[0056] In the embodiment 1 of the present disclosure, the deflection-control electrode 103 includes: a first central hole and multiple deflection control sub-electrodes; the multiple deflection control sub-electrodes are centered at the first central hole and deployed around the first central hole. Therefore, the deflection-control electrode is in the form of several petals.
[0057] For example, the deflection-control electrode is in the form of eight petals, a diagram of which is shown in
[0058] For example, the deflection control electrode is in the form of twelve petals, a diagram of which is shown in
[0059] In the embodiment 1 of the present disclosure, the first sub-detector 104 can be a backscattered electrons detector, the second sub-detector 105 can be a central detector. Here, the first sub-detector 104 and the second sub-detector 105 can be semiconductor detectors, avalanche detectors, or detectors made up of scintillator and optical guide tube, and the detectors are in the shape of circular disk with a central hole.
[0060] In the embodiment 1 of the present disclosure, the first sub-detector 104 has a second central hole, the diameter of the second central hole is smaller than that of the first central hole in the deflection-control electrode 103. In a preferred embodiment, the diameter of the second central hole in the first detector 104 is of an order of millimeters, as an example the diameter of the second central hole is less than 5 millimeters.
[0061] In the embodiment 1 of the present disclosure, the first detector device 104 includes at least one sub-detection component, each of the first sub-detection components is arranged to acquire a signal corresponding to signal electrons of a respective zone and send the signal to an external image processing device to image the signal electrons of the respective zone. The first sub-detector 104 is made of semiconductor material, when the first sub-detector 104 includes multiple first sub-detection components, these components are centered at the second central hole and deployed around the second central hole; and the multiple components are electrically insulated from each other. Each of the first sub-detection components is arranged to receive the signal electrons of a respective zone. Based on the structure of the first sub-detector 104, the detection area of the first sub-detector 104 is divided into multiple sub-detection zones according to the multiple sub-detection components.
[0062] In an embodiment, a diagram of the structure and detection zone of the first detector 104 is shown in
[0063] In another embodiment, a diagram of another structure and detection zone of the first detector 104 is shown in
[0064] In another embodiment, a diagram of another structure and detection zone of the first detector 104 is shown in
[0065] In the embodiment 1 of the present disclosure, a voltage is applied to the magnetic lens 101 by a power supply system, i.e., the power supply system powers the exciting coil of the magnetic lens 101, so that the magnetic lens 101 generates a stable magnetic field. The first sub-detector 104, the deflection-control electrode 103 and the specimen 107 are supplied voltages by the power supply system, the specimen 107 is located on a specimen stage, and the specimen 107 is supplied a voltage via the specimen stage by the power supply system.
[0066] In an embodiment of the present disclosure, the voltage of the first detector 104 is 0V, the range of the voltage V2 applied to the specimen 107 is where V2 is no less than −30 kilovolts (kV) and no more than 5 kV; wherein, the voltage of the deflection control electrode 103 includes a constant voltage V3 and a variable voltage V4, and V2≤V3≤0.
[0067] By controlling the electric potentials of the first detector 104, the deflection-control electrode 103 and the specimen 107, the first detector 104, the deflection-control electrode 103 and the specimen 107 together form a retarding electrostatic lens field, the electric potential distribution of the retarding electrostatic lens field on the optical axis is shown by 108 U(z) in
[0068] The retarding electrostatic lens field and the objective immersion lens field generated by the magnetic lens 101 together make up a compound retarding receiving immersion lens field; the compound retarding receiving immersion lens field mainly includes three functions; firstly, focusing the primary electron beam impinging on the specimen 107; secondly, decelerating the primary electron beam so as to impinge on the specimen with a low landing energy to reduce the charge effect on the non-conductive specimen; thirdly, accelerating the signal electrons (backscattered electrons and secondary electrons) to improve the efficiencies of the first sub-detector 104 and the second sub-detector 105 on collecting the signal electrons.
[0069] The compound retarding receiving immersion lens field is coupled with the scanning field generated by the deflection device 102 and the deflection control electrode 103, to achieve a swing objective retarding receiving immersion lens (SORRIL) scanning method or a moving objective retarding receiving immersion lens (MORRIL) scanning method. With the above two scanning methods, both the off-axis aberration and the deflection aberration are reduced, and therefore high resolution imaging of an order of hundreds of micrometers can be achieved.
Embodiment 2
[0070] The embodiment 2 of the disclosure provides another scanning electron microscope objective lens system, which is similar to that in embodiment 1. The main differences are shown in
[0071] In embodiment 2 of the disclosure, the deflection device 102 includes: sub-deflector 102a and sub-deflector 102d.
[0072] In embodiment 2 of the present disclosure, power supply system 106 is used to power the scanning electron microscope objective lens system. The voltage of the electron source is represented by V1, the range of V1 is: −30 kV≤V1≤−5 kV; the anode 202, the second sub-detector 105 and the first detector 104 are grounded, i.e., their voltages are zero; the range of the voltage V2 applied to the specimen 107 is where V2 is no less than −30 kilovolts (kV) and no more than 5 kV; the voltage of the deflection control electrode 103 includes a constant voltage V3 and a variable voltage V4, and V2≤V3≤0.
Embodiment 3
[0073] The embodiment 3 of the disclosure provides another scanning electron microscope objective lens system, which is similar to that in embodiment 2. The main differences shown in
Embodiment 4
[0074] The embodiment 4 of the disclosure provides another scanning electron microscope objective lens system, which is similar to that in embodiment 2. The main differences are shown in
[0075] In this embodiment of the disclosure, the deflection device includes: a sub-deflector 302a, and a sub-deflector 302d; and both the sub-deflector 302a and the sub-deflector 302d are magnetic deflectors.
[0076] In this embodiment of the disclosure, the scanning electron microscope objective lens system is powered by a power supply system 106. The voltage of the electron source 201 is represented by V1, the range of V1 is: −15 kV≤V1≤0 kV; the voltages of the anode 302a, the second sub-detector 105 and the first sub-detector 104 are all represented by V5, and the range of V5 is: 5 kV≤V5≤30 kV; the specimen to be observed is grounded, that is the voltage is zero; the voltage of the deflection control electrode includes a constant voltage V3 and a variable voltage V4, 0≤V3≤V5.
Embodiment 5
[0077] The embodiment 5 of the disclosure provides another scanning electron microscope objective lens system, which is similar to that in embodiment 4. The main differences shown in
Embodiment 6
[0078] Based on the scanning electron microscope objective lens system described in embodiment 1 to embodiment 5, embodiment 6 of the disclosure provides a specimen detection method, the method shown in
[0079] Step S101, the primary electron beam goes through the compound retarding receiving immersion lens field, and is deflected by the deflection device and the deflection control electrode, and finally impinges on the specimen surface to generate the signal electrons.
[0080] In an embodiment of the disclosure, in the scanning electron microscope objective lens system, the first sub-detector, the deflection-control electrode and the specimen together generate an electrostatic retarding lens field, this electrostatic retarding lens field overlaps with the magnetic lens field near the specimen to form a compound retarding receiving immersion lens field 405.
[0081] For example, the deflection device includes 402a and 402d, as shown in
[0082] In an embodiment of the disclosure shown in
[0083] In another embodiment of the disclosure shown in
[0084] In another example, the deflection device includes four sub-deflectors 402a, 402b, 402c and 402d, as shown in
[0085] In an embodiment of the disclosure shown in
[0086] In another embodiment of the disclosure shown in
[0087] It is to be noted that, compared to the deflection device with two sub-deflectors, the large field scanning method using the deflection device with four sub-deflectors is performed as follows: firstly deflecting the primary electron beam to a starting position of a sub-zone (for example a sub-zone 507b at the top left corner of 507) under a deflection field formed by the sub-deflectors 402a and 402d and the deflection control electrode 103, and then performing fast scanning of this sub-zone with the sub-deflectors 402b and 402c, and secondly moving to a starting position of a next sub-zone under a deflection field formed by the sub-deflectors 402a and 402d and the deflection control electrode 103, and then performing fast scanning of this sub-zone with sub-deflectors 402b and 402c, and then performing fast scanning of this sub-zone with the sub-deflectors 402b and 402c, and so forth, a large scanning field 507 is finally formed.
[0088] Step S102, by controlling the voltages of the deflection control electrode, the signal electrons are received by the first sub-detector and the second sub-detector.
[0089] In this embodiment of the disclosure, the voltage of the specimen is set to V2, 0≤V2≤−5 kV, the voltage of the first sub-detector is set to 0V, and the third voltage V3 is set to a constant value, V2≤V3≤0.
[0090] In another embodiment, the voltage of the specimen V2 is set to zero, the voltage of the first sub-detector is set to V5, where V5 is no less than 5 kV and no more than 30 kV, and the third voltage V3 is set to a constant value, 0≤V3≤V5.
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[0093] In conclusion, by adjusting the voltage of the deflection-control electrode, the signal electrons generated from both the center and the edge of the large scanning field can be received and detected with high efficiency.
[0094] What are described above are merely embodiments of the disclosure, and not intended to limit the scope of protection of the disclosure. One of ordinary skill in the art will readily recognize that there would be variations to the embodiments and those variations would be within the spirit and scope of the present disclosure. Therefore, the protection scope of the present disclosure should be subject to the protection scope of the claims.
INDUSTRIAL APPLICABILITY
[0095] With the scanning electron microscope objective lens system, as well as the large field of view scanning method according to the disclosure, the off-axis and deflection aberration is reduced, and therefore the high resolution at the edge of the large scanning field can be achieved. Since the BSE detector is designed with several sub-detection zones, the signal electrons emitted with different orientations or different angles are detected separately, with which images with different information can be achieved at the same time. With the flexibility of the deflection control electrode potential control, the deflection control electrode can act as both a deflector and an electrostatic lens electrode, so that the collection efficiency of the electron signals generated at the whole large scanning field is improved.