PIEZOELECTRIC MICROELECTROMECHANICAL RESONATOR DEVICE AND CORRESPONDING MANUFACTURING PROCESS
20210099154 ยท 2021-04-01
Inventors
- Federico VERCESI (Milano, IT)
- Lorenzo Corso (Ruginello, IT)
- Giorgio Allegato (Monza, IT)
- Gabriele GATTERE (Castronno, IT)
Cpc classification
H03H2003/027
ELECTRICITY
B81B7/0038
PERFORMING OPERATIONS; TRANSPORTING
B81C2203/0118
PERFORMING OPERATIONS; TRANSPORTING
H03H9/171
ELECTRICITY
H03H2003/022
ELECTRICITY
B81C1/00285
PERFORMING OPERATIONS; TRANSPORTING
H03H3/02
ELECTRICITY
International classification
B81B7/00
PERFORMING OPERATIONS; TRANSPORTING
B81C1/00
PERFORMING OPERATIONS; TRANSPORTING
H03H3/02
ELECTRICITY
Abstract
A microelectromechanical resonator device has: a main body, with a first surface and a second surface, opposite to one another along a vertical axis, and made of a first layer and a second layer, arranged on the first layer; a cap, having a respective first surface and a respective second surface, opposite to one another along the vertical axis, and coupled to the main body by bonding elements; and a piezoelectric resonator structure formed by: a mobile element, constituted by a resonator portion of the first layer, suspended in cantilever fashion with respect to an internal cavity provided in the second layer and moreover, on the opposite side, with respect to a housing cavity provided in the cap; a region of piezoelectric material, arranged on the mobile element on the first surface of the main body; and a top electrode, arranged on the region of piezoelectric material, the mobile element constituting a bottom electrode of the piezoelectric resonator structure.
Claims
1. A micro-electro-mechanical system resonator device, comprising: a main body having a first layer with a first surface and a second layer with a second surface opposite to the first surface along an axis, the second layer having an internal cavity facing the first layer along the axis, the first layer including a mobile element overlapping the internal cavity and suspended in a cantilever fashion relative to the internal cavity; a bonding element; a cap having first surface and a second surface opposite to one another along the axis, and the first surface of the cap bonded to the first surface of the main body by the bonding element, the cap including a housing cavity overlapping the internal cavity, the mobile element suspended in the cantilever fashion relative to the housing cavity; and a piezoelectric resonator structure including: the mobile element, configured as a bottom electrode; a piezoelectric region of a piezoelectric material, arranged on said mobile element at the first surface of the main body; and a top electrode arranged on the piezoelectric region.
2. The device according to claim 1, wherein said first layer is a structural substrate of doped monocrystalline silicon; and wherein said second layer is an epitaxial layer grown from said structural substrate.
3. The device according to claim 1, comprising: a first contact element and a second contact element arranged on said second layer at the second surface of the main body; and a first interconnection element and a second interconnection element that electrically couple the top and bottom electrodes of said piezoelectric resonator structure to said first and second contact elements, respectively, said first and second interconnection elements extending throughout a thickness of said main body along said axis.
4. The device according to claim 3, further comprising insulation regions extending through said main body along said axis, wherein said first and second interconnection elements each includes a stack of a first interconnection portion of said second layer and a second interconnection portion of said first layer; and said first and second interconnection elements are electrically insulated from one another by the insulation regions.
5. The device according to claim 4, wherein said insulation regions comprise: insulation trenches in said first layer, the insulation trenches filled with a dielectric material, and insulation openings in said second layer that overlap the dielectric material that fills in the insulation trenches along said axis.
6. The device according to claim 4, further comprising at least one path of conductive material arranged on the first surface of said main body and electrically coupling said first interconnection element to said top electrode of the piezoelectric resonator structure.
7. The device according to claim 1, wherein said bonding element is a dielectric material laterally separated from the mobile element, the first surface of said main body being spaced apart from the first surface of said cap by said bonding element.
8. The device according to claim 1, further comprising a getter region within said housing cavity, arranged on a wall of said housing cavity facing said mobile element.
9. The device according to claim 1, comprising a wafer-level package, wherein said second surface of the main body and said second surface of the cap constitute outer surfaces in contact with an external environment.
10. A process, comprising: forming a main body having a first surface of a first layer, a second surface of a second layer opposite to the first surface along an axis, and a piezoelectric resonator structure on the first surface, the second layer having an internal cavity facing the first layer along the axis, the piezoelectric resonator structure including: a resonator portion of the first layer overlapping the internal cavity and suspended in a cantilever fashion relative to the internal cavity, a piezoelectric region of a piezoelectric material on said resonator portion at the first surface of the main body, and an electrode on the piezoelectric region; forming a cap having a first surface and a second surface opposite to one another along the axis, the first surface of the cap including a housing cavity; bonding the first surface of the cap to the first surface of the main body by a bonding element, the mobile element overlapping the housing cavity and suspended in a cantilever fashion relative to the housing cavity.
11. The process according to claim 10, wherein the forming the main body comprises: receiving a silicon-on-insulator wafer including said first layer of doped monocrystalline silicon, a supporting substrate, and a dielectric layer between said first layer and said supporting substrate; forming a definition trench throughout a thickness of the first layer along the axis, the trench laterally surrounding said resonator portion of the first layer; forming a surface dielectric layer over the first layer and within said definition trench; forming a sacrificial portion of the surface dielectric layer on said resonator portion by patterning said surface dielectric layer, the sacrificial portion having a side extension laterally beyond said resonator portion; forming said second layer by growing epitaxial silicon over said first layer and coating said sacrificial portion; releasing the resonator portion of said first layer by removing the dielectric material within said definition trench; and forming said internal cavity in said second layer by removing the sacrificial portion.
12. The process according to claim 11, wherein the forming the main body further comprises: bonding a handling wafer to the silicon-on-insulator wafer; flipping said silicon-on-insulator wafer by using said handling wafer; and exposing a working surface of said first layer by completely removing said supporting substrate and removing said dielectric layer.
13. The process according to claim 12, further comprising: forming a layer of piezoelectric material above said working surface of said first layer; and forming said piezoelectric region above said mobile element by patterning said layer of piezoelectric material.
14. The process according to claim 11, further comprising: forming insulation trenches throughout a thickness of said first layer, laterally with respect to said definition trench, the insulation trenches defining between them a first bottom interconnection portion and a second bottom interconnection portion of said first layer, wherein said forming the surface dielectric layer fills said insulation trenches; forming a first contact element and a second contact element on said second layer at positions vertically overlapping said first and second bottom interconnection portions of said first layer, respectively; and forming a first top interconnection portion and a second top interconnection portion of said second layer that overlap said first bottom interconnection portion and said second bottom interconnection portion, respectively, by forming insulation openings through said second layer.
15. The process according to claim 14, further comprising forming at least one path of conductive material above the first surface of said main body, and coupling said first bottom interconnection portion to said electrode of said piezoelectric resonator structure.
16. The process according to claim 10, wherein the forming the cap comprises: providing a cap wafer; forming said housing cavity within a first surface of said cap wafer; and wherein the bonding comprises bonding said cap wafer onto said first layer through said bonding element of a dielectric material, said resonator portion facing said housing cavity, said bonding element being laterally spaced away with respect to the resonator portion, and the cap wafer being spaced away from said first layer by a distance in the axis.
17. The process according to claim 16, further comprising forming a getter region on a wall of said housing cavity facing the mobile element, the getter region defining a level of vacuum within said housing cavity.
18. The process according to claim 16, further comprising thinning the second surface of said cap wafer to a thickness along the vertical axis.
19. A structure, comprising: a first body having a piezoelectric resonator structure suspended over a first cavity embedded in the first body along a first direction, the first cavity having a dimension in a second direction that contains a dimension of the piezoelectric resonator structure in the second direction, the second direction traverse to the first direction, the piezoelectric resonator structure including a first electrode, a second electrode and a piezoelectric layer positioned between the first electrode and the second electrode in the first direction; a second body having a second cavity overlapping the piezoelectric resonator structure in the first direction, the second cavity having a dimension in the second direction that contains the dimension of the piezoelectric resonator structure in the second direction; and a bonding layer between the first body and the second body in the first direction.
20. The structure of claim 19, wherein the piezoelectric layer protrudes toward the second cavity beyond a surface of the first body that faces the second body in the first direction.
Description
BRIEF DESCRIPTION OF THE SEVERAL VIEWS OF THE DRAWINGS
[0013] For a better understanding of the present disclosure, preferred embodiments thereof are now described, purely by way of non-limiting example, with reference to the attached drawings, wherein:
[0014]
[0015]
[0016]
DETAILED DESCRIPTION
[0017]
[0018] The MEMS resonator 1 comprises a mass 2, coupled to which is an arm (or beam) 3, with main longitudinal extension, which extends in cantilever fashion in a suspended way from the same mass 2.
[0019] The MEMS resonator 1 further comprises a first electrode and a second electrode 4, 5, arranged facing and parallel to the arm 3, on opposite sides thereof.
[0020] During operation, application of an appropriate biasing voltage between the first electrode 4 (acting as driving electrode) and the arm 3 causes a resonance movement of the same arm 3 at the mechanical resonance frequency.
[0021] The consequent approach to, or moving away from, the second electrode 5 (acting as sensing electrode) causes a variation of the capacitive coupling, which enables generation of an associated electrical signal, also at the resonance frequency, by an electronic circuit associated to the MEMS resonator 1 (not illustrated herein).
[0022] The present Applicant has found that the MEMS resonator 1 of a capacitive type described previously is affected by some problems that do not enable full exploitation of the advantages thereof.
[0023] In some embodiments, the distance (or gap, designated by g in
[0024] Moreover, the device 1 uses an actuation of a non-linear type and, consequently, a dedicated electronic circuit, and is therefore not able to constitute a direct replacement of traditional quartz resonators, which operate on the basis of the piezoelectric effect.
[0025] MEMS resonator devices of a piezoelectric type, e.g., operating on the basis of the piezoelectric effect, can overcome some of the aforesaid problems. In such solutions, a mobile element is driven in resonance by application of an appropriate electrical biasing to a region of piezoelectric material coupled to the same mobile element. The piezoelectric solutions may be advantageous as compared to capacitive solutions, given that, being based upon the piezoelectric effect, like traditional quartz solutions, they can be associated to pre-existent electronic circuits (therefore enabling direct replacement of traditional quartz resonators).
[0026] With reference to
[0027] The manufacturing process envisages providing a SOI wafer 10, having a front surface 10a and a rear surface 10b, which extend in a horizontal plane xy defined by a first horizontal axis x and a second horizontal axis y and are opposite to one another along a vertical axis z, and comprising: a structural substrate 11, defining the aforesaid front surface 10a and made of monocrystalline silicon doped so as to be electrically conductive. As will be described herein in detail, in this structural substrate 11, the bottom electrode of a piezoelectric resonator structure will be provided; a supporting substrate 12, defining the aforesaid rear surface 10b; and a dielectric layer 13, for example, of silicon oxide, interposed between the aforesaid structural substrate 11 and supporting substrate 12. As shown in the aforesaid
[0028] As illustrated in
[0029] The surface dielectric layer 16 is then subjected to chemical etching (using an appropriate photolithographic mask, not illustrated herein) so as to define: a sacrificial portion 16a, set in an area located above the resonator portion 11a of the structural substrate 11 (and having a side extension, in the horizontal plane xy, greater than that of the resonator portion 11a); and insulation portions 16b, which are arranged laterally with respect to the sacrificial portion 16a (along the aforesaid first horizontal axis x) and define between them openings 17, in a position vertically corresponding to the aforesaid first and second bottom interconnection portions 11b, 11c of the structural substrate 11.
[0030] As illustrated in
[0031] As illustrated in the same
[0032] The epitaxial silicon layer 18 is then subjected to etching from a corresponding top surface 18a, which is not in contact with the structural substrate 11, to form, laterally with respect to the aforesaid first and second contact pads 19a, 19b, insulation openings 20, which define between them a first top interconnection portion 21a and a second top interconnection portion 21b of the epitaxial silicon layer 18 that constitute a prolongation along the vertical axis z of the first bottom interconnection portion 11b and of the second bottom interconnection portion 11c, respectively, of the structural substrate 11. The first top interconnection portion 21a and a second top interconnection portion 21b are to form, jointly therewith, interconnection elements of the piezoelectric resonator structure. The aforesaid insulation openings 20 thus provide electrical insulation between the aforesaid first and second top interconnection portions 21a, 21b of the epitaxial silicon layer 18.
[0033] As illustrated in
[0034] As illustrated in the same
[0035] As illustrated in
[0036] As illustrated in the same
[0037] On the aforesaid region of piezoelectric material 28 a layer of conductive material, in some embodiments a metal material, for example, molybdenum, is then deposited and defined so as to form a top electrode region 30 of what will be the piezoelectric resonator structure.
[0038] In the embodiment illustrated, definition of the aforesaid layer of piezoelectric material moreover leads to formation of a further piezoelectric region 31, arranged laterally with respect to the aforesaid region of piezoelectric material 28, above the residual portions 13a of the dielectric layer 13. In some embodiments, this further piezoelectric region 31 fills the second opening 26b arranged in a position vertically corresponding to the second contact pad 19b, whereas it leaves the first opening 26a arranged in a position vertically corresponding to the first contact pad 19a exposed and accessible.
[0039] Moreover, definition of the aforesaid layer of conductive material also leads to formation of a conductive path 32, which extends on the aforesaid further piezoelectric region 31 and in some embodiments into the aforesaid first opening 26a so as to come directly into contact with the underlying interconnection element of what will be the piezoelectric resonator structure (formed jointly by the first bottom interconnection portion 11b of the structural substrate 11 and the first top interconnection portion 21a of the epitaxial silicon layer 18), in electrical contact with the aforesaid first contact pad 19a.
[0040] In a way not illustrated in the cross-sectional view of
[0041] As illustrated in
[0042] It is noted that the aforesaid etching process does not, instead, lead to removal of the remaining dielectric regions, which are not in fact accessible from the top surface being processed, e.g., the surface of the structural substrate 11 opposite to the epitaxial silicon layer 18.
[0043] As illustrated in
[0044] The cap wafer 42 itself has, in a position vertically corresponding to the mobile element 40, a housing cavity 44.
[0045] In some embodiments, an appropriate level of vacuum may be defined within the aforesaid housing cavity 44, by formation, for example, by deposition, of a getter region 45 within the housing cavity 44, for example, on a corresponding wall facing the mobile element 40.
[0046] The top surface of the cap wafer 42, opposite to the surface 42a facing the SOI wafer 10, designated by 42b, may be subjected to thinning by removal of material and/or chemical etching so as to obtain a resulting desired thickness, e.g., along the vertical axis z.
[0047] As illustrated in
[0048] The aforesaid subsequent manufacturing steps envisage, in some embodiments, total removal of the handling wafer 24 and moreover total or partial removal of the adhesion layer 25; for instance, as in the example illustrated in the aforesaid
[0049] The manufacturing process then terminates with dicing of the SOI wafer 10 (and of the cap wafer 42), for definition of the resulting resonator device, which is illustrated in
[0050] The resonator device 50 therefore comprises a main body 52 (resulting from dicing of the aforesaid SOI wafer 10) having a first surface 52a and a second surface 52b, opposite to one another along the vertical axis z, and constituted by: the structural substrate 11, of doped monocrystalline silicon, which defines the aforesaid first surface 52a; and the epitaxial silicon layer 18, grown on the structural substrate 11, which defines the second surface 52b of the aforesaid main body 52.
[0051] The resonator device 50 further comprises a cap 54, resulting from dicing of the aforesaid cap wafer 42, having a respective first surface 54a and a respective second surface 54b, opposite to one another along the vertical axis z and bonded to the first surface 52a of the main body 52 through the bonding elements 43.
[0052] The resonator device 50 therefore has a package of the so-called wafer-level type, where the aforesaid second surface 52b of the main body 52 and the aforesaid second surface 54b of the cap 54 constitute outer surfaces in contact with an external environment (in a way not illustrated, a coating layer, for example, of epoxy resin, may be formed on the second surface 52b of the main body 52; alternatively, on the same second surface 52b part of the adhesion layer 25 may be present, in the case where it has been removed only in part during the manufacturing process).
[0053] In some embodiments, the resonator device 50 defines internally and integrally a piezoelectric resonator structure 60, comprising: the mobile element 40, formed by the resonator portion 11a of the structural substrate 11, appropriately coupled (in a manner not illustrated herein) to the aforesaid structural substrate 11 so as to be suspended in cantilever fashion, facing the internal cavity 39 formed in the epitaxial layer 18 and moreover, on the opposite side, the housing cavity 44, formed in the cap 54; and furthermore the region of piezoelectric material 28, arranged on the same mobile element 40 on the first surface 52a of the main body 52; and the top electrode 30, arranged on the region of piezoelectric material 28 (to form the so-called piezoelectric stack).
[0054] The piezoelectric resonator structure 60 further comprises the bottom electrode, of the same material as that of the mobile element 40 (monocrystalline silicon) and moreover a first interconnection element 62a and a second interconnection element 62b, which electrically connect the aforesaid top and bottom electrodes to the first and second contact pads 19a, 19b, which are arranged on the second surface 52b of the main body 52 (being in this way accessible from outside).
[0055] As mentioned previously, these interconnection elements 62a, 62b are electrically insulated from one another (due to the presence of the insulation trenches 15 filled with dielectric material and of the insulation openings 20, possibly filled with the material of the adhesion layer 25, in the case where it not has been removed completely or it has been formed in a localized manner and not within the insulation openings 20), and are formed by superimposition of the first and second top interconnection portions 21a, 21b, respectively, of the epitaxial silicon layer 18 and the first and second bottom interconnection portions 11b, 11c, respectively, of the structural substrate 11.
[0056] In some embodiments, the aforesaid first contact pad 19a enables electrical connection (for the purposes of biasing of the piezoelectric resonator structure 60 and of detection of an electrical signal at an appropriate oscillation frequency generated as a result of the corresponding movement at the resonance frequency) towards the top electrode 30, through the conductive path 32 formed on the first surface 52a of the main body 52; and the aforesaid second contact pad 19b enables electrical connection (once again for the purposes of biasing of the piezoelectric resonator structure 60 and of detection of the corresponding electrical signal at the oscillation frequency) to the bottom electrode (constituted, as has been mentioned, by the same mobile element 40).
[0057] The advantages of the present solution emerge clearly from the foregoing description.
[0058] In some embodiments, it is emphasized that the resonator device 50 has a low dependence on temperature of the corresponding oscillation frequency, thanks to the stability in temperature of the material used (doped monocrystalline silicon).
[0059] In addition, the resonator device 50 has small dimensions and in some embodiments a small thickness of the stack along the vertical axis z, thanks to the use of a wafer-level package and to the possibility of reduction of the thickness of the cap 54 (via the operation of thinning of the cap wafer 42, which exploits the temporary presence of the handling wafer 24).
[0060] Moreover advantageous, once again for the purposes of reduction of the dimensions, is the arrangement of the contact pads 19a, 19b on the outer surface of the epitaxial layer 18, which is grown directly on the structural substrate 11, with the interconnection elements 62a, 62b that connect the contact pads 19a, 19b to the top and bottom electrodes of the piezoelectric resonator structure 60, traversing the entire thickness of the same structural substrate 11 and the epitaxial silicon layer 18.
[0061] Bonding of the cap 54 to the main body 52, in some embodiments by glass-frit bonding, enables a hermetic packaging of the piezoelectric resonator structure 60 to be obtained (with the desired level of vacuum that can internally be obtained through the getter region 45).
[0062] Formation of the piezoelectric stack, obtained by stacking of the region of piezoelectric material 28 and of the top electrode region 30, advantageously enables adjustment and calibration of the electrical properties, for example, in terms of the frequency offset, of the piezoelectric resonator structure 60, via precise definition of the dimensions of the regions of material that are formed, the so-called trimming operations, which can involve, as an alternative or in addition, also the resonator portion 11a constituting the mobile element 40 of the piezoelectric resonator structure.
[0063] It is moreover underlined that, unlike known solutions that require complex and costly manufacturing steps, for example, starting from C-SOI substrates, the present disclosure allows to obtain the internal cavity 39, with respect to which the mobile element 40 is suspended in cantilever fashion, within a layer of epitaxial material, by etching of a sacrificial material on which the same epitaxial layer is previously grown, e.g., with standard semiconductor techniques, having low complexity and cost.
[0064] The resonator device 50 can advantageously replace traditional resonant quartz structures in pre-existing oscillator circuits, for example, for RTC applications, in some embodiments possibly constituting a direct replacement, e.g., using the same pins and contacts of pre-existing quartz resonators, exploiting in fact the same piezoelectric principle and therefore being altogether compatible with the associated electronic circuits.
[0065] In this regard, an electronic device 70 is illustrated schematically in
[0066] The clock circuit 72 comprises the MEMS resonator device 50, described previously, and an associated electronic reading circuit 73.
[0067] Finally, it is clear that modifications and variations may be made to what has been described and illustrated herein, without thereby departing from the scope of the present disclosure.
[0068] In some embodiments, it is underlined that the geometry, dimensions, and coupling with respect to the structural substrate 11 of the mobile element 40 of the piezoelectric resonator structure 60 may vary with respect to what has been illustrated previously.
[0069] Moreover, it is underlined that the resonator device 50 can advantageously be used in a wide range of further applications, other than the real-time clock application to which particular reference has been made previously, for example, in reference high-frequency oscillators (which are, for example, used for supplying an appropriate frequency reference for operations of demodulation in electronic circuits).
[0070] The various embodiments described above can be combined to provide further embodiments. Aspects of the embodiments can be modified, if necessary to employ concepts of the various patents, applications and publications to provide yet further embodiments. These and other changes can be made to the embodiments in light of the above-detailed description. In general, in the following claims, the terms used should not be construed to limit the claims to the specific embodiments disclosed in the specification and the claims, but should be construed to include all possible embodiments along with the full scope of equivalents to which such claims are entitled. Accordingly, the claims are not limited by the disclosure.