Method and device for producing of high quality alcoholic beverages

Abstract

A method and device for producing high quality alcohol beverages, including liquor, cordial, tincture, whiskey, cognac, brandy, vodka, rum, gin, wine, cocktail, etc., is based on the action of hydrodynamic cavitation treatment of components of alcohol beverages. The fluid flow moves at a high rate through a multi-stage blending hydrodynamic device and multi-stage cavitation device to generate hydrodynamic cavitation features in the fluid flow. The cavitation features generate changes in the velocity, pressure, temperature, chemical composition and physical properties of the liquid. Hydrodynamic cavitation processing provides effective blending of components and homogenization of alcoholic beverage, improves its organoleptic qualities.

Claims

1. A system for producing an alcoholic beverage, comprising: a fluid tank; a pump fluidly connected to a processing outlet on the fluid tank; a hydrodynamic cavitation device fluidly connected to an outlet on the pump; wherein the hydrodynamic cavitation device comprises a plurality of cavitation stages; wherein each of the plurality of cavitation stages comprises a helical plate immediately followed by a cylinder body, wherein the helical plate consists of a single spiral element forming a spiral flow path and the cylinder body comprises in sequence a constriction nozzle, a central channel, and an expansion diffuser; and a fluid line fluidly connecting an outlet of the hydrodynamic cavitation device to the fluid tank.

2. The system of claim 1, wherein the helical plate has a length that satisfies the relationship 0.5H<=L<=3H, where H is a height of a step and L is the length of the swirling element.

3. The system of claim 2, wherein an angle of rotation of the helical plate is 180 degrees when L=0.5H and 1080 degrees when L=3H, having a proportional angle of rotation therebetween.

4. The system of claim 1, further comprising a plurality of inlet fluid tanks fluidly connected to the fluid tank, wherein each inlet fluid tank contains a fluid component of the alcoholic beverage.

5. The system of claim 4, further comprising a hydrodynamic blending device fluidly disposed between the plurality of inlet fluid tanks and the fluid tank, wherein the hydrodynamic blending device comprises a plurality of mixing stages, the number of mixing stages corresponding to one less than the number of inlet fluid tanks.

6. The system of claim 5, wherein each of the plurality of mixing stages comprises a swirling element forming a spiral flow path followed by a cylinder element forming a constricted-expanded flow path and having a side inlet channel in the cylinder element.

7. The system of claim 6, wherein one of the plurality of inlet fluid tanks is fluidly connected to a main inlet on the blending device and the remaining plurality of inlet fluid tanks are each fluidly connected to one of the plurality of mixing stages through the corresponding side inlet channel.

8. The system of claim 6, wherein the side inlet channel is oriented at an angle of intersection () relative to the cylinder element according to the relationship /2<=<=90 degrees, where is an angle of a conical surface in the cylinder element immediately before the constricted-expanded flow path.

9. The system of claim 6, wherein the blending device further comprises a cavitation stage disposed after the plurality of mixing stages.

10. The system of claim 7, further comprising a dosing pump and an individual cavitation device serially and fluidly disposed between each of the plurality of inlet fluid tanks and the blending device.

11. The system of claim 10, wherein the individual cavitation device comprises a plurality of cavitation stages having a swirling element forming a spiral flow path followed by a cavitation element forming a constricted-expanded flow path.

12. The system of claim 11, further comprising a bypass line selectively connecting the dosing pump directly to the blending device.

13. The system of claim 1, further comprising a filter element fluidly disposed between the hydrodynamic cavitation device and the fluid tank.

14. The system of claim 1, further comprising a filter element fluidly connected to a final outlet on the fluid tank.

15. The system of claim 1, further comprising a safety valve fluidly connecting the system pump directly to the fluid tank so as to selectively bypass the cavitation device.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

(1) The accompanying drawings illustrate the invention. In such drawings:

(2) FIG. 1 illustrates in a flow chart a preferred embodiment of the system for blending of alcoholic beverages;

(3) FIG. 2 is an isometric drawing of a preferred embodiment of the system for blending of alcoholic beverages.

(4) FIG. 3 illustrates a preferred embodiment of the multi-stage cavitation device;

(5) FIG. 4 illustrates a preferred embodiment of the multi-stage blending hydrodynamic device;

(6) FIG. 5 is a close-up view of an injection zone on the multi-stage blending hydrodynamic device in circle 41 of FIG. 4;

(7) FIG. 6 is a close-up view of an alternate embodiment of the injection zone on the multi-stage blending hydrodynamic device;

(8) FIG. 7 is a close-up view of a swirling zone on the multi-stage cavitation device in circle 31 of FIG. 3;

(9) FIG. 8 is a close-up view of an alternate embodiment of the swirling zone on the multi-stage cavitation device;

(10) FIG. 9 is a close-up view of another alternate embodiment of the swirling zone on the multi-stage blending hydrodynamic device.

(11) FIG. 10 illustrates in a flow chart another preferred embodiment of the system for blending of alcoholic beverages.

(12) FIG. 11 is an isometric drawing another preferred embodiment of the system for blending of alcoholic beverages.

(13) FIG. 12 is a computer modeling of flow lines through a preferred embodiment of the blending device according to the present invention.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS

(14) A principal diagram of a preferred system 10 for blending of alcohol beverages is depicted in FIG. 1. The blending system 10 is comprised of the several parts that more efficiently provide for the production and treatment of alcoholic beverages and removal of various contaminants therefrom by using filtration. The system 10 consists of inlet tanks 12 for alcohol beverage components, which tanks 12 are filled with the fluids to be blended. Liquid components of alcoholic beverages are fed from the tanks 12 through a separate dosing pump 14 for each tank 12. The use of separate dosing pumps 14 allow for readily mixing in a continuous flow state. Before mixing, the liquid components of alcoholic beverages from the tanks 12 may be processed in a set 20 of multiple cavitation devices 16one for each dosing pump 14.

(15) The dosing pumps 14 feed the fluids from the tanks 12 to the set of cavitation devices 20 for the cavitation treatment of the fluids (FIG. 1 and FIG. 2). The set of tanks 12, the set of dosing pumps 14 and the set 20 of cavitation devices 16 may comprise one, two, three, or more tanks 12, dosing pumps 14, and devices 16 as needed.

(16) As shown in FIG. 3, the multi-stage cavitation devices 16 preferably comprise several stages or regions 30 to generate cavitation in the fluid stream. A stage or region 30 for generating cavitation preferably consists of at least two elements for swirling and cavitating the fluid flow. The first such element is preferably a twisted plate 32 to form a single spiral element, i.e., a single planar element twisted along a longitudinal axis, to tighten and swirl the flow of liquid. The second such element is preferably a work piece in the form of a cylinder 34 with a central channel 35 having a constriction nozzle 35a and expansion diffuser 35b in the channel for inception of cavitation in the liquid. The constriction 35a and expansion 35b of the passage section of the fluid flow of the central channel 35 is preferably designed in the form of a Venturi tube. The cavitation stages 30 are installed in a housing 36. Feeding and discharge of the treated liquid is done through inlet 38 and the outlet 39 installed on the housing 36.

(17) In the multi-stage cavitation device 16 (FIG. 3), macro vortexes are generated in the fluid flow, by both the twisted plate 32 and cylinder 34, which are accompanied by local pressure decreases to the saturated vapor point of the fluid at the given temperature. When this happens, the proper conditions for the growth of cavitation nuclei in the cavitation bubbles are reached. The formed cavitation bubbles pulse and implode in downstream high-pressure zones.

(18) Blending of an alcoholic beverage is carried out in a multi-stage blending hydrodynamic device 18 that contains mixing zones for components 40 (FIG. 4). A region 40 for components blending may consist of elements such as a twisted plate 42 to form a single spiral element, i.e., a single planar element twisted along a longitudinal axis, to tighten the flow of liquid and a work piece in the form of a cylinder 44 with a central channel 45 having a constriction nozzle 45a and expansion diffuser 45b in the passage section of the fluid flow for inception of cavitation. The constriction 45a and expansion 45b of the passage section of the fluid flow of the central channel 45 is preferably designed in the form of Venturi tube. The blending stages 40 are installed in a housing 43. Feeding and discharge of the treated liquid is done through inlet 48 and the outlet 49 installed on the housing 43.

(19) The central channel 45 has a channel 47 for introducing the component into the main stream of the alcoholic beverage (FIG. 4). The channel 47 can be located both perpendicular to the channel 45 and at an angle to it (FIG. 5, FIG. 6). To supply the component to the channel 47, a branch pipe 46 is installed on the housing body 43, through which the component is fed into the device 18. The twisted plate 42 for swirling the flow ensures fluid flow along a spiral path. Consequently, in the central part of the flow in the channel 45, the pressure is significantly reduced compared to the flow along a straight path. This helps to reduce the hydraulic resistance when injecting the component into the main flow of the resulting alcoholic beverage.

(20) The location of the channel 47 at an angle to the central channel 45 will also help to reduce the hydraulic resistance when the component is injected into the main flow (FIG. 6). The angle of intersection a of the central axes of the central channel 45 and the channel 47 is recommended to be selected from the interval /290, where is the angle of the conical surface forming a constriction in the cylinder 44 immediately before the central channel 45. The upper limit of the angle is due to the fact that at a value greater than 90 degrees, the injected flow from the channel 47 will face the main flow in the channel 45, which greatly reduces the injection effect and increases the hydraulic resistance device. The lower limit of the angle is due to the value of the angle of narrowing of the flow , which forms the current lines in the initial portion of the liquid flow in the central channel 45. In addition, at an angle of less than half the angle , the conical surface of the confuser and the cylindrical surface of the channel 45 can intersect.

(21) At a high flow rate in channel 45, the flow of the injected component from channel 47 is sucked into it. If the flow velocity in channel 45 is sufficiently high, the component flow from the channel 47 to the channel 45 can be achieved without pumping. In this case, it is possible to exclude the supply of the component to the device 18 by the dosing pumps 14. Calculation of the parameters of the main and injected flow is carried out according to the known method of calculating injectors (Pullen, William Wade Fitzherbert. Injectors: the Theory, Construction and Working (Second ed.) London: The Technical Publishing Company Limited, 1900). The number of injection zones 40 is preferably one less than the number of mixing flows being supplied by the tanks 12. The main component of the produced alcoholic beverage is supplied to the inlet 48.

(22) The elements 32, 42 for creating swirling flows can be made either in the preferred form of a twisted plate (FIG. 7), or in the form of an auger (FIG. 8) or a screw (FIG. 9) in a single-pass or multi-pass version. The recommended length of the part for swirling the flow L can be chosen from the relation 0.5HL3H, where H is a screw step. If the length of the part for swirling the flow is L=0.5H, the angle of rotation of the helical surface of the element is preferably 180 degrees. This is sufficient to ensure a spiraling path of flow of fluid in the channel 45. If the length of the part for swirling the flow is L=3H, the angle of rotation of the helical surface of the element is preferably 1080 degrees. The swirling of the flow at an angle of more than 1080 degrees is impractical, since it significantly increases the hydraulic resistance of the section for swirling the flow.

(23) At the outlet of the device 18, a cavitation module 30 may be installed to generate vortices and cavitation for better mixing of the flow components. The cavitation module 30, as described above, may consist of elements such as a twisted plate 32 and a cylinder 34 with a central channel 35 having a constriction 35a and expansion 35b. The outlet 49 of the blending device 18 is connected to the inlet port of the main or system pump 22.

(24) The main hydrodynamic and cavitation treatment of the alcoholic beverage is carried out in a multi-stage cavitation device 16, which is connected to the outlet on the main or system pump 22 (FIG. 1, FIG. 2). The outlet pipe or return fluid line 39 of the multistage cavitation device 16 is connected to the finish or main fluid tank 24 for the processed alcohol beverage. Between the finish tank 24 and the cavitation device 16, a filter module 26 may be installed to remove impurities and contaminants from the alcoholic beverage. The filter module 26 may have a cartridge containing loose filter or adsorbent material, fibrous material, rigid or flexible porous tubes or membranes. For multiple treatments of an alcoholic beverage in the cavitation device 16, a processing outlet line 25 from the finish tank 24 can be recycled to the inlet of the main pump 22.

(25) The scheme of an alternate system for blending and improvement of the quality of alcohol beverages is shown in FIG. 10 and FIG. 11. This alternate embodiment of the system 50 for blending and improvement of the quality of alcohol beverages comprises the liquid measure tanks 52, which measuring or inlet tanks 52 are not shown in FIG. 11 for simplicity. The measuring tanks 52 are fluidly connected to main or storage tank 54. A system pump 56 is connected to the tank 54 for transfer of the liquid to be treated to multi-stage cavitation devices 58, similar to the cavitation device 16 described above. From the device 58, the alcoholic beverage passes through return line 59 where it re-enters tank 54. A filter cartridge 60 is connected to the outlet from the tank 54 to remove chemical impurities, as well as solid and colloidal particles from the liquid. The filter cartridge 60 may have a cartridge containing loose filter or adsorbent material, fibrous material, rigid or flexible porous tubes or membranes.

(26) The system 10 and the alternate version of the system 50 preferably has a safety valve 62 to control fluid flow in multiple processing modes, whether to dispense blended alcoholic beverage, or to rinse and drain washing water from the system. Although not shown in FIG. 1, the first embodiment of the system 10 may also include a safety valve 62 on the main pump 22 as described for the system 50. To control the fluid pressure at the outlet of the pump 56, a manometer 64 is provided. The operation of the devices 10 and 50 is controlled through an electronic control system 66 that is operationally connected to pump 56.

(27) Looking at FIG. 1, the inventive blending system 10 preferably functions as follows. The components of an alcoholic beverage, for example, water, ethyl alcohol, solutions of aromatic and flavor additives are poured into containers 12 in the proportions of the recipe. In accordance with the technology, the components can be separately treated in a multi-stage cavitation device 16. To this end, a separate component or several components are pumped through the device 16 by metering pumps 14. In a multi-stage cavitation device 16, the liquid component undergoes intensive hydrodynamic and cavitation treatment. If the technology for preparing an alcoholic beverage does not involve the hydrodynamic and cavitation treatment of one or more components, same can be fed to the blending device 18 along the bypass lines 28.

(28) When the treated fluid flows into the multi-stage cavitation device 16, it passes through the inlet 38 and successively passes through each cavitation generating stage 30 and then is discharged from the multi-stage cavitation device 16 through the outlet 39. At each stage 30, the liquid first flows around the helical plate 32 and then passes through the cylinder 34, having in sequence the constriction nozzle 35a, the central channel 35 and the expansion diffuser 35b. As the liquid flows relative to the surface of the helical plate 36, the liquid swirls. The swirling flow passes through the central channel 35 of the cylindrical body 34, entering the constriction nozzle 35a and exiting the expansion diffuser 35b, having the overall shape of a Venturi tube, in which cavitation is generated. The swirling flow passes through the central channel 37 at a higher velocity than a comparable flow with streamlines parallel to the central axis 37. The high flow velocity in the zone of the channel 35 with a minimum flow area or throat of the Venturi tube causes reduction in the flow pressure to the saturated vapor pressure and the formation of cavitation bubbles that pulsate and collapse when they enter the zone of increased pressure in the diffuser or at the outlet of the Venturi tube.

(29) The collapse of cavitation bubbles produces enough energy for the dissociation of water, alcohol and other molecules followed by the generation of protons, hydroxyl ions, hydroxyl radicals, peroxide and hydrogen molecules. Gas molecules present in these bubbles are excited and affected by multiple energy and charge exchange processes. Oxygen and hydrogen molecules participate in a number of reactions, including the formation of hydroperoxyl radicals.

(30) For blending an alcoholic beverage, its components are mixed in the device 18, the diagram of which is shown in FIG. 4. The flow of the bulk component is supplied to the inlet 48 of the device 18. As it passes through the swirling zone, the main flow passes into a spiraling motion as it flows around the part for swirling the flow, for example, in the form of a twisted plate 42 and then enters the constriction nozzle 45a, central channel 45, and expansion diffuser 45b of the cylinder 44. In the central channel 45, the flow is accelerated and the pressure in the flow decreases. Due to an injection effect, another component of the mixed alcoholic beverage is drawn by vacuum into the flow through the channel 47. The alcoholic beverage component can also be supplied from the channel 47 under pressure by the metering pump to the channel 45 through the channel 47. Due to the vortex flow of the main flow, and also due to the cavitation effect, the components of the alcoholic beverage are mixed.

(31) The mixture flow of the two components of the alcoholic beverage passes to the next mixing zone 40, where another component is mixed with this mixture. The number of mixing zones 40 should be smaller by one than the number of fluid components. The required number of components in a given volume is added to the flow of the mixture of alcoholic beverage.

(32) In order to prepare a homogeneous mixture of components, a cavitation module 30 for generating vortices and cavitation may be installed just before the outlet 49 of the device 18 for better mixing of the flow components. Components of the flow of alcoholic beverages are intensively mixed and processed in it due to vortex formation and cavitation.

(33) From the mixing device 18, the flow of the alcoholic beverage enters the main pump 22, and then under pressure it is fed to a multi-stage cavitation device 16. When the treated fluid flows into the multi-stage cavitation device 16, it passes through the inlet 38 and successively passes through each cavitation generating stage 30 and then be discharged from the multi-stage cavitation device 16 through the outlet 39. At each stage 30, the liquid first flows around the helical plate 32 and then passes through the cylinder 34, having in sequence the constriction nozzle 35a, central channel 35, and expansion diffuser 35b. As the liquid flows relative to the surface of the helical plate 32, the liquid swirls. The swirling flow passes through the central channel 35 of the cylindrical body 34, entering the constriction nozzle 35a and exiting the expansion diffuser 35b, having the overall shape of a Venturi tube, in which cavitation is generated. The swirling flow passes through the central channel 35 at a higher velocity than a comparable flow with streamlines parallel to the central axis 37. The high flow velocity in the zone of the channel 35 with a minimum flow area or throat of the Venturi tube causes reduction in the flow pressure to the saturated vapor pressure and the formation of cavitation bubbles that pulsate and collapse when they enter the zone of increased pressure in the diffuser or at the outlet of the Venturi tube.

(34) The collapse of cavitation bubbles produces enough energy for the dissociation of water, alcohol and other molecules followed by the generation of protons, hydroxyl ions, hydroxyl radicals, peroxide and hydrogen molecules. Gas molecules present in these bubbles are excited and affected by multiple energy and charge exchange processes. Oxygen and hydrogen molecules participate in a number of reactions, including the formation of hydroperoxyl radicals.

(35) Alcoholic beverages based on an aqueous solution of alcohol (vodka, brandy, whiskey, rum, gin and others), as well as food ethanol may contain impurities such as Acetaldehyde and/or Acetal, Benzene, Methanol, Fusel Oils, as Isobutyl, Isoamyl and active Amyl, Non Volatile Matter, Heavy Metals and others. The presence of these impurities in alcohol-containing beverages reduces their flavor and aroma qualities. Cavitation treatment of alcohol beverages and ethanol causes destruction of impurities, and decreases the concentration of Acetaldehyde, Acetal, Benzene, Methanol, Fusel Oils, precipitation of salts of heavy metals, thus helping to improve the organoleptic indicators of alcohol beverages.

(36) After the hydrodynamic cavitation treatment in the device 16, the flow of the alcoholic beverage can be directed to the finished product tank 24. The filtration module 26 provides filtration on the fluid. The filter module 26 can be installed in the form of a standard cartridge for quick replacement. In the design of the filter module 26, various materials and substances can be used for mechanical or sorption purification of liquids in the form of loose, fibrous materials, flexible or rigid tubes and membranes. The filter module 26 can work in a dead-end mode, where a contaminated fluid passes through a special pore-sized microfilter to separate suspended particles from the process liquid. In the filtration module 26, an alcohol beverage is purified to remove microparticles, solid particles, and colloid particles, whose dimensions are larger than the pores of the microfilter.

(37) From the tank 24, the alcoholic beverage is drained for transfer to the consumer. The alcoholic beverage can undergo additional treatment in the device 16, if necessary or in accordance with the technology. To this end, the beverage from the tank 24 may be supplied to the inlet of the pump 22. In this case, other flows are not supplied to the pump 22. From the pump 22, the beverage is fed for repeated or multiple treatment in the device 16. If necessary, one or more of the components may be re-added to the alcoholic beverage, wherein the beverage is re-supplied from the tank 24 to the inlet of the blending device 18. The necessary component(s) is(are) also supplied to the device 18 from the tank 12 through another metering pump 14. From the mixing device 18, the alcoholic beverage is supplied to the pump 22, and then is recycled in the device 16 and enters the tank 24.

(38) The scheme of the system for producing alcoholic beverages 50 is alternatively shown in FIG. 10. In the system 50, the liquid components of the alcoholic beverage are transferred from inlet tanks 52 into main tank 54. In the tank 54, a stirring device may be installed to premix the components. The initial mixture of components is fed to the system pump 56, from which it enters the multi-stage cavitation device 58, where homogenization, hydrodynamic and cavitation processing of the alcoholic beverage occur. From the device 58, the alcoholic beverage passes through return fluid line 59 where it re-enters the tank 54 again and may be processed multiple times, circulating in a closed loop from the tank 54 to the pump 56 and the device 58.

(39) The pump 56 has a safety valve 62 that operates at a pressure higher than the preset pressure. The valve 62 is connected to the tank 54 into which liquid can flow when the valve 62 is actuated. A pressure sensor is installed at the outlet of the pump 56, upon the signal from which the pump 56 can be stopped if the pressure exceeds a predetermined value.

(40) After repeated treatment of the alcoholic beverage in system 50, it is drained into tank 54, from which through filter 60 it can be discharged through the outlet.

(41) One or more components in the required volume can be re-added to an alcoholic beverage. To do this, the component is poured into the tank 54 while the pump 56 is running. With the circulation mixing in the system 50, the alcoholic beverage is homogenized and treated in the device 58 to the desired condition.

(42) FIG. 12 illustrates a computer modelling of flow lines through a preferred embodiment of the blending device 18 described herein. This modelling shows how the fluid flows through each mixing or blending stage 40 as well as, enters through the side channels 47. The dark areas are regions where the fluid flow rate is comparatively lower and generally correspond to the swirling elements 42. The light areas are regions where the fluid flow rate is comparatively higher and generally correspond to the central channels 45 and side inlets 47. Each of these areas of increased fluid flow rate also result in increased agitation and mixing of the fluid components.

(43) The choice of components for an alcoholic beverage can be carried out by the consumer in accordance with the recommended recipe and technology or the consumer can independently choose the components and their volumes.

Example 1

(44) The form of flow lines and mixing several components, calculated with the specialized software ANSYS for the blending device 18 (length 50 cm, diameter 4 cm, 3 mixing zones) which is similar to the apparatus in FIG. 4 is shown on FIG. 12. Flow moves from left to right. The central channel 45 of cylinder 44 and the central channel 35 of cylinder 34 have the Venturi tube profile in a longitudinal section (FIG. 4). The device 18 was operated at a flow rate of 10 gpm and an inlet pressure of 300 psi. The flow lines show that there is an intensive blending of the components. The presence of hydrodynamic cavitation determines the number of cavitation (C.sub.V) shown for each zone. Cavitation onsets after the hydrostatic pressure of the liquid has decreased to the saturated vapor pressure of the liquid or its components and is categorized by the cavitation number (C.sub.V). Cavitation ideally begins where (C.sub.V) equals 1, where a (C.sub.V) less than 1 indicates a high degree of cavitation. The example in FIG. 12 it is indicated for the water flow as the main component.

Example 2

(45) Purified water in the volume of 600 ml and ethyl alcohol (96%) in a volume of 400 ml were poured into the tank 54. A sample of an untreated mixture of alcoholic beverage of the vodka type was pumped through the device 58 for 10 minutes circulating in a closed loop. The pressure at the outlet of the pump was 300 psi, the flow was 10 GPM. After treatment, an alcoholic drink of the vodka type was drained from the tank 54 through a filter 60. Impurities were determined using FFAP column chromatography.

(46) Table 1 shows that the amount of chemical impurities in vodka decreased by an average of 16%. The harsh smell of vodka dissipated, and its taste became softer.

(47) TABLE-US-00001 TABLE 1 Concentration, milligram/liter Impurity Before treatment After treatment Acetaldehyde 1.0634 1.0122 Methyl acetate 0.912 0.840 Ethyl acetate 0.888 0.862 Isopropanol 1.096 1.055

(48) Although several embodiments have been described in detail for purposes of illustration, various modifications may be made without departing from the scope and spirit of the invention. Accordingly, the invention is not to be limited, except as by the appended claims.