Compliant hermetic seal system for flat glass panel assembly

Abstract

A hermetically-sealed enclosure including at least two wall elements of substantially congruent shapes, and a spacer system that defines an interior space between the wall elements. The enclosure also includes a bridge element that has one or more flexible metal foil layers extending between adjacent, respective edges of the wall elements to isolate the interior space from a surrounding environment. The bridge element is substantially free of step discontinuities in total thickness along the intended weld path, and the bridge element is bonded to each of the wall elements via an ultrasonic weld to form a continuous bond line.

Claims

1. A hermetically-sealed enclosure comprising: at least two wall elements of substantially congruent shapes; a spacer system defining an interior space between the wall elements; and a bridge element including one or more flexible metal foil layers extending between adjacent, respective edges of the wall elements to isolate the interior space from a surrounding environment, wherein the bridge element is substantially free of step discontinuities in total thickness along the intended weld path, and wherein the bridge element is bonded to each of the wall elements via an ultrasonic weld to form a continuous bond line.

2. The enclosure of claim 1, wherein the wall elements include glass.

3. The enclosure of claim 1, wherein the bridge element includes a first foil layer and a second foil layer that is thicker than the first foil layer.

4. The enclosure of claim 3, wherein the first foil layer is defined by two pieces of foil having a butt joint, and wherein the second foil layer overlays the butt joint.

5. The enclosure of claim 1, wherein each foil layer is fabricated from a single sheet of foil.

6. The enclosure of claim 1, wherein at least one foil layer includes separate pieces of foil that are hermetically bonded at a joint between the separate pieces of foil, and wherein the joint crosses the bond line.

7. The enclosure of claim 1, wherein the bridge element is bonded via an ultrasonic weld that forms a plurality of bond lines, and wherein at least part of at least one bond line is defined by a plurality of ultrasonic weld segments overlapping at or near their adjacent ends.

8. The enclosure of claim 1, wherein the bridge element is bonded via an ultrasonic weld that forms a plurality of bond lines, wherein at least part of at least one bond line has first and second ultrasonic weld segments that are adjacent and substantially parallel to each other, and wherein the second ultrasonic weld segment overlaps the first ultrasonic weld segment.

9. The enclosure of claim 1, wherein at least one bond line is made to a coated surface of a wall element without removal of the coating from the bond line region.

10. The enclosure of claim 1, wherein at least one bond line is made to a coated surface of a wall element, and wherein the coating has been removed in the region of the bond line by chemical edge deletion.

11. A method for manufacturing a hermetically-sealed enclosure, the method comprising: assembling first and second wall elements of substantially congruent shapes together and separating the two wall elements from each other to form a space; extending a bridge element between adjacent, respective edges of the wall elements, the bridge element including one or more layers of flexible metal foil, and the bridge element being substantially free of step discontinuities in total thickness; bonding the bridge element to the first wall element by ultrasonic welding to form a continuous bond on the first wall element; and bonding the bridge element to the second wall element by ultrasonic welding to form a continuous bond on the second wall element.

12. The method of claim 11, further comprising bonding first and second foil layers to at least one of the first wall element and the second wall element.

13. The method of claim 12, wherein each of the first and second layers is fabricated from a single sheet of foil.

14. The method of claim 12, wherein the first foil layer is defined by two pieces of foil having a butt joint, and wherein the second foil layer overlays the butt joint.

15. The enclosure of claim 11, wherein at least one foil layer includes separate pieces of foil that are hermetically bonded at a joint between the separate pieces of foil, and wherein at least one of the joints crosses the bond line.

16. The method of claim 11, wherein at least one layer of the bridge element includes separate pieces that are hermetically bonded at joints, and wherein at least one of the joints crosses a bond line formed by bonding the bridge element to the first wall element, or a bond line formed by bonding the bridge element to the second wall element.

17. The method of claim 11, further comprising forming a plurality of ultrasonic weld segments that overlap at least one of the bonds at or near their adjacent ends.

18. The method of claim 11, wherein at least one bond formed by the bonding steps is made to a coated surface of a wall element without removal of the coating from the weld path region.

19. The method of claim 11, wherein at least one bond formed by the bonding steps is made to a coated surface of a wall element, and wherein the coating has been removed in the region of the weld path by chemical edge deletion.

20. An insulated glazing unit comprising: a first flat panel element; a second flat panel element, the first and second flat panel elements having congruent shapes; and a plurality of spacers disposed between the first flat panel element and the second flat panel element to space the first flat panel element from the second flat panel element; and a bridge element including one or more flexible metal foil layers extending between adjacent, respective edges of first and second flat panel elements to isolate the interior space from a surrounding environment, wherein the bridge element is substantially free of step discontinuities in total thickness along the intended weld path, and wherein the bridge element is bonded to each of the wall elements via an ultrasonic weld to form a continuous bond line.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

(1) FIG. 1a is an elevation view of a portion of an exemplary enclosure having spaced apart wall elements and illustrating a foil bridge corner seal.

(2) FIG. 1b is a partial section view of the exemplary enclosure of FIG. 1a.

(3) FIG. 2a is an elevation view of a portion of an exemplary enclosure having a joint-less single- or multi-layer foil bridge corner seal.

(4) FIG. 2b is partial section view of a portion of the enclosure of FIG. 2a, illustrating a joint-less single- or multi-layer foil bridge corner seal.

(5) FIG. 3a is an elevation view of a portion of an exemplary enclosure having a joint-less single- or multi-layer foil bridge, dish-drawn seal.

(6) FIG. 3b is a section view of a portion of the exemplary enclosure of FIG. 3a, illustrating a joint-less single- or multi-layer foil bridge, dish-drawn seal.

(7) FIG. 4 illustrates an exemplary cold welding process for attaching a multi-layer foil to a wall element.

(8) FIG. 5a illustrates an exemplary cold welding process for attaching a two-layer foil splice joint.

(9) FIG. 5b is an enlarged view of the process of FIG. 5a, illustrating the two layer foil splice joint having a butt joint in one layer.

(10) FIG. 6a is an elevation view of a multi-layer foil bridge corner seal using overlapping straight line welds to effect a continuous hermetic seal at the corner.

(11) FIG. 6b is a partial section view of the multi-layer foil bridge corner seal of FIG. 6a, illustrating a two-layer splice joint and using overlapping straight line welds to effect the continuous hermetic seal at the corner.

(12) FIG. 7a is an elevation view of a multi-layer foil bridge corner seal having a two-layer splice joint and using a weld following a 90 degree arc to effect a continuous hermetic seal at the corner.

(13) FIG. 7b is a partial section view of the mu multi-layer foil bridge corner seal of FIG. 7a, illustrating a two-layer splice joint and using the weld following a 90 degree arc to effect a continuous hermetic seal at the corner.

(14) FIG. 8a is an elevation view of a portion of an exemplary enclosure including one aluminum foil layer in a single strip with a right angle fold and a second layer of foil to create welded hermetic seals that cross the paths of subsequent closed-loop welds.

(15) FIG. 8b a partial section view of the enclosure of FIG. 8a, illustrating the aluminum foil layer in a single strip with a right angle fold and a second layer of foil to create welded hermetic seals which cross the paths of subsequent closed-loop welds.

(16) FIG. 9a is a perspective view of a two-layer foil bridge system using only a single thin foil layer as the flexible portion of the edge seal.

(17) FIG. 9b illustrates a partial section view of the two-layer foil bridge system of FIG. 9a.

(18) FIG. 10 is a partial section view of an exemplary enclosure including a foil bridge system that has protection for the foil bridge.

(19) FIG. 11a is an elevation view of an exemplary enclosure including warm-edge, dual-pane insulating glass and the bridge seal according to any of the previous figures.

(20) FIG. 11b is a partial section view of one edge of the insulating glass during manufacture of the seal.

(21) FIG. 11c is a partial section view of one edge of the insulating glass after completion of manufacture of the seal.

(22) FIG. 12 is a schematic view of a chemical edge deletion process for removing low-emissivity coating from glass.

(23) FIG. 13 is a partial section view of an exemplary enclosure including a foil bridge system that has protection for the foil bridge.

(24) It should be understood that the invention is not limited in its application to the details of construction and the arrangements of the components set forth in the following description or illustrated in the above-described drawings. Before any embodiments of the invention are explained in detail, it is to be understood that the invention is not limited in its application to the details of construction and the arrangement of components set forth in the following description or illustrated in the following drawings. The invention is capable of other embodiments and of being practiced or of being carried out in various ways.

DETAILED DESCRIPTION

(25) As used herein, the terms insulated glazing unit and glass panel assembly are synonymous and denote a window glazing assembly formed from one or more glass members or glass elements (referred to as glass panes for purposes of description) that are at least partially transparent to electromagnetic radiation, that are substantially parallel along their planar faces, and that are substantially congruent shapes with surrounding edges sealed to form an interior space between the glass panes. These terms also encompass flat panel assemblies that have at least one element including glass and another element that can include glass, ceramic, aluminum, stainless steel, or other material. The interior space can be at least partially filled with a gas that is less conductive and, in some constructions, more viscous than air, or evacuated (e.g., by drawing a vacuum).

(26) Pane refers to a glass element intended for use as a wall element in a flat hermetically-sealed enclosure assembly.

(27) Differential pane movement refers to the relative pane movement between two adjacent glass panes that occurs when the temperature of one pane changes relative to the temperature of the other pane. It may also refer to the relative pane movement that occurs under mechanical influence or other influence (e.g., impact during handling or use).

(28) Hermetic refers to a seal that allows helium leakage rates of no more than about 10.sup.8 to 10.sup.9 standard cubic centimeters/second (scc/sec) per foot of seal length.

(29) Highly-hermetic refers to a seal that allows helium leakage rates of no more than about 10.sup.9 scc/sec, and preferably no more than about 10.sup.11 scc/sec, and most preferably no more than about 10.sup.12 scc/sec per foot of seal length.

(30) The terms flexible and compliant refer to a structure having a resilient nature, and the ability to accommodate movement.

(31) The term non-compliant refers to a structure having a rigid or brittle nature, in contrast with flexible or compliant.

(32) The term highly-malleable refers to an object or material having a yield stress no greater than 10,000 psi (e.g., no greater than 5,500 psi).

(33) The term cold weld refers to a weld that is produced by a bonding process (e.g., ultrasonic welding) that does not require the bulk glass temperature or the bulk foil temperature to be substantially above room temperature at the onset of the welding process.

(34) The term sonotrode refers to a vibrating tool tip that transmits translational motion to the assembly of substrates to be welded by an ultrasonic welder.

(35) The term anvil refers to the surface upon which rests the assembly to be welded by an ultrasonic welder and that resists translational movement of the bottom of the assembly.

(36) The term inboard, with respect to a weld line location, refers to a location on the side of the weld line that is closest to the centroid of a glass pane being welded.

(37) The phrase substantially free of step continuities in total thickness, with respect to the flexible seal, refers to limiting total thickness variation to no more than about 0.001 inches.

(38) FIGS. 1a and 1b show a portion of an exemplary insulated glazing unit including two flat panel elements 1, 2 that are spaced apart by spacers 3 (FIG. 1b) made of an incompressible or substantially incompressible material (e.g., composite, plastic, glass, metal, etc.). Each spacer 3 is relatively small in size (e.g., approximately 100 microns in diameter by 1000 microns long). When the glazing unit is viewed from a distance, the small size of the spacers 3 makes the spacers 3 visually unobtrusive (i.e. substantially invisible under most lighting and background conditions). In some constructions, the spacers 3 can be replaced by a portion of one or both flat panel elements 1, 2. That is, one or both flat panel elements 1, 2 can be formed as a dished

(39) The insulated glazing unit also includes an edge seal 4 that is formed by a joint-less single- or multi-layer foil bridge corner seal. As illustrated in FIGS. 1a, 1b, 2a, and 2b, the edge seal 4 can be applied to a glazing unit that has the same-sized first and second flat panel elements 1, 2 (FIGS. 1a and 1b), or that has different-sized first and second flat panel elements 1, 2 (FIGS. 2a, 2b). In both exemplary glazing units, the edge seal 4 includes one or more sheets of foil (e.g., aluminum) that is sized to be approximately as large as the larger glass pane to provide an edge seal 4 that provides a compliant seal without joints. Excess foil, such as that covering the intended viewing area of window glazing units, can be cut away after seal manufacture and recycled. The use of pane-size foil sheets allows for inspection of the assembly (e.g., to check for leaks) during the manufacturing process before the excess foil is cut away and before the foil protruding from the assembly is welded to the second flat panel element 2.

(40) FIGS. 3a and 3b illustrate a joint-less single- or multi-layer foil bridge corner seal 4 that is formed from dish-drawn foil. In this construction, the foil seal 4 has been drawn into a dished shape with edge flanges offset from each other. The depth of the offset is about the same as the thickness of the second flat panel element 2 to allow a cold weld to be made to the exterior surface of the element 2, which is oriented to face outside the enclosure assembly.

(41) FIG. 4 illustrates an exemplary cold welding process for welding multi-layer foil 4 to the first flat panel element 1. In this construction, a thin foil 36 is placed in contact with the first flat panel element 1, and a thicker foil 35 is placed in contact with the thin foil 36. A sonotrode 37 of an ultrasonic seam welder (not shown) is used to weld the two foil layers 35, 36 to each other and to the glass surface in a single operation to produce a hermetic seal between two-layer foil 4 and the flat panel element 1.

(42) FIGS. 5a and 5b illustrate an exemplary two-layer foil seal 4 that has a butt weld 40 connecting or joining a butt joint 42 in the foil layer 36. Two pieces of foil 36 (first foil) are arranged on an anvil 38 to form the butt joint 42, and another piece of foil 35 (second foil) is arranged over the joint 42 to splice the two pieces of foil 36. The sonotrode 37 can be used to make the spliced butt weld 40.

(43) FIGS. 6a and 6b illustrate an exemplary jointed multi-layer foil bridge corner seal 4 including the flexible spliced butt weld 40 illustrated and described with regard to FIGS. 5a and 5b. With reference to FIGS. 6a and 6b, one side of the foil strip 4 is bonded to the gap-side of the first flat panel element 1 (e.g., the gap-side surface can be provided without a coating). The other side of the foil strip 4 is bonded to the second flat panel element 2, which can optionally include a low-emissivity coating 14. As illustrated, overlapping welds 40 are used at the corners to effect a continuous hermetic seal.

(44) FIGS. 7a and 7b illustrate an exemplary foil bridge corner seal or strip 4 that has flexible spliced butt welds 40 that extend between each two-layer foil strip 4 and a two-layer foil triangle 39. The resulting foil strip assembly is bonded by a seam weld 5 to the gap-side of the uncoated flat panel element 1, and by another seam weld 5 to the second flat panel element 2 with the optional low-emissivity coating 14 without removing the coating 14. As illustrated in FIG. 7a, the seam welds 5 follow a circular 90 degree arc at each corner to connect each corresponding pair of straight sections of welds to effect a continuous hermetic seal.

(45) FIGS. 8a and 8b illustrate an exemplary assembly including a right-angle fold in a layer of foil (e.g., foil 36) and an overlaying second, thicker layer of foil (e.g., foil 35). A seam weld 43 is made to hermetically seal across the welds 5 along one or both edges of the folded foil.

(46) FIGS. 9a and 9b illustrate a two-layer foil bridge system including a single thin foil layer that acts as the flexible portion of the edge seal 4 to reduce heat transfer from the warm pane edge to the cold pane edge (i.e., the foil seal functions as a warm edge seal). A foil strip assembly including a wide strip of thin foil 35 serves as the bridge element. Two narrow strips of foil 36 (e.g., thicker than the foil 35) overlay each long edge of the bridge element 35. The two-layer edges are bonded by seam welds 5 to their respective flat panel elements 1, 2. In the corners of panes 1 and 2, a crisscross weld may be used to form a closed loop seal (e.g., see FIGS. 1a, 1b), although a seam weld 5 that follows a circular 90 degree arc at each corner (e.g., see FIGS. 2a, 2b) can connect each corresponding pair of straight sections of welds 5 to effect a continuous closed loop hermetic seal. Substantial contact between foil strip 36 and the flat panel element 1, which could result in additional heat loss, is prevented by using the spacers 3, which maintain a larger gap between the elements 1, 2 than the nominal total thickness of the foil stack or bridge formed by the foils 35, 36.

(47) FIG. 10 illustrates an exemplary glazing unit with structure that can protect the edge foil bridge from inadvertent damage (e.g., during handling). The exemplary unit includes the foil bridge system described and illustrated with regard to FIGS. 9a and 9b, and a guard strip 10 that is mounted on the exposed portion of the weld 5 using adhesive 11. The guard strip 10 can be continuous at the corners or assembled with joints. The joints and the gap between the guard strip 10 and the edge of the second flat panel element 2 can be filled with a sealant 15.

(48) FIGS. 11a, 11b, and 11c illustrate a glazing unit including warm-edge dual-pane insulated glass that has been hermetically sealed. FIG. 11b illustrates one edge of the glazing unit during manufacture of the seal 4, whereas FIG. 11c illustrates the edge after completion of manufacture of the seal. The first and second flat panel elements 1, 2 are held parallel and prevented from touching each other by a desiccant-filled insulating spacer 12 that is bonded to each respective flat panel elements 1, 2 by an adhesive strip 11. Hermetic welds 5 of aluminum foil 4 are applied to flat panel elements 1, 2 using the sonotrode 37. A sealant 13 (e.g., having a low permeability to gas) fills the perimeter space between flat panel elements 1, 2.

(49) FIG. 12 illustrates an exemplary chemical edge deletion process for removing the low-emissivity coating 14 from the first flat panel element 1 to leave behind a smooth surface for ultrasonic welding. The process uses a suitable liquid chemical 17 that produces a reaction resulting in a dissolved coating 16 on the portion of the element 1 that is in contact with the chemical 17. The portion of coating that is dissolved can be controlled by the adjusting the level 19 of the liquid chemical 17 in the container 18.

EXAMPLES

Example 1

(50) A square piece of aluminum window screen is cut to 9 inches by 9 inches and mounted with common centers on a clean, untempered 10 inch by 10 inch pane of soda lime glass such that the squares nearly have a common center. Two layers of 1100 series aluminum foil, one 2 mil layer and one 1 mil layer, were placed together such that they could be shear-cut simultaneously to a square shape of 12 inches12 inches.

(51) This two-layer foil assembly was mounted on top of the window screen, with common center so as to produce an equal amount of foil overhang at each pane edge. An annular region of the glass pane, covered only by foil but not screen, was available for accommodating a weld line. This stacked assembly was mounted onto the table (serving as the anvil) of a 100 watt ultrasonic seam welder of custom design.

(52) A single continuous weld line was made to weld the foil to the lateral glass surface adjacent the edges of the pane, using a straight line weld path except at the corners where the weld path was curved, following a circular 90 degree arc. The end of the weld line overlapped its start to form a closed loop. Inboard of the first closed-loop weld line, a second closed-loop weld line was made, parallel and partially overlapping the first, thereby forming a single weld of greater width than the first.

(53) This assembly was evacuated through an 8 mm diameter hole drilled through the glass pane. The window screen prevented the layered aluminum foil sheet assembly from contacting the glass pane except for the annular area between the edge of the windows screen and the inside edge of the double weld. After holding vacuum overnight, a pressure of less than 1 mTorr was measured by spinning rotor gauge on the pumped connection. No leaks greater that 2E.sup.10 scc/sec per foot of seal length were found using the helium spray method on a Vacuum Instruments Corporation MS-40 helium leak detector.

Example 2

(54) From the tested assembly produced in Example 1, the foil and window screen was removed from the area inboard of the closed-loop weld, leaving only a continuous, joint-free stripe of two-layer foil welded to the outer edge of the 10 inch square pane. A clean 12 inch by 12 inch soda lime glass pane with sputtered low-emissivity coating on one side was populated on its coated surface with metal spacers about 125 microns thick on a 20 mm20 mm grid pattern, according to a co-pending patent application. The 10 inch square glass-and-foil assembly was laid atop the spacers of the 12 inch square glass pane, with the foil trapped between the two panes, such that the two glass panes had a common center, and producing an equal amount of foil overhang at each pane edge. An annular region of the larger glass pane was available for accommodating a weld. This stacked assembly was bonded together into an enclosure using the equipment and technique described in Example 1.

(55) A single continuous weld line was made to weld the foil to the lateral glass surface adjacent the edge of the 12 inch square pane, using a straight line weld path except at the corners where the weld path was curved, following a circular 90 degree arc. The end of the weld line overlapped its start to form a closed loop. Inboard of the first closed-loop weld line, a second closed-loop weld line was made, parallel and partially overlapping the first, thereby forming a single weld of greater width than the first.

(56) This two pane assembly was evacuated through an 8 mm diameter hole drilled through the smaller glass pane. The spacers prevented the smaller glass pane from contacting the larger glass pane. A vacuum of less than 1 mTorr was drawn, as measured by spinning rotor gauge on the pumped connection. No leaks greater that 2E.sup.10 scc/sec per foot of seal length were found using the helium spray method on a Vacuum Instruments Corporation MS-40 helium leak detector.

Example 3

(57) With reference to FIG. 13, a highly hermetic seal is formed around a rectangular neutron detector enclosure of 1 meter by 1 meter by 1 centimeter. The enclosure is intended to be filled with argon gas and a sensing apparatus. The enclosure includes two parallel glass panes 1, 2 seal and a glass edge spacer 41. A coating-free clear soda lime glass pane 1 meter1 meter inch is used for glass pane 1, while a coating-free clear soda lime glass pane 0.975 meters0.975 meters is used for glass pane 2. Four glass edge spacers 41 (e.g., 0.965 meters long and having a cross-section of 1 cm1 cm) are rigidly and hermetically bonded to pane 2, each adjacent one edge of pane 2, using solder glass 42. The corner joints between the four glass spacers 42 are likewise filed with solder glass to form highly hermetic seals upon heating to 450 C.

(58) After cooling, excess solder glass at these corner joints, intentionally protruding above the spacer 41 surfaces intended for the weld path, is ground off so the surface of the remaining solder glass 42 is flush with the spacer surface intended for the weld, and is polished to an acceptable finish for ultrasonic welding, that is, a finish comparable to that of the lateral surfaces of the float glass panes 1, 2. Four single-layer aluminum foil strips (e.g., each 13 mm wide and 25 microns thick and 1 meter long) are arranged using accurately-cut butt joints, ultrasonically welded, to form a continuous loop without substantial thickness discontinuities along the surface of glass spacer 41 opposite pane 2 so that only the inner portion of each foil strip is in contact with each corresponding spacer 41 and the outer portion is cantilevered off the outside edge of each spacer 41.

(59) After appropriate fixturing to maintain alignment, a single continuous weld line is made to weld the foil to the lateral glass surface adjacent the edge of glass pane 2, using a straight line weld path except at the corners where the weld path was curved, following a circular 90 degree arc according to the present invention. With continued reference to FIG. 13, the assembled glass pane 2 and the spacer 41 are mounted onto glass pane 1 using a set of rolling rod spacers 3 installed to separate the glass spacer 41 from glass pane 1 to provide a small gap for differential thermal movement of either pane. After appropriate fixturing to maintain alignment, a single continuous weld line is made to weld the foil to the lateral glass surface adjacent the edge of glass pane 1, using a straight line weld path except at the corners where the weld path was curved, following a circular 90 degree arc. The end of the weld line overlaps its start to form a closed loop. Inboard of the first closed-loop weld line, a second closed-loop weld line is made, parallel and partially overlapping the first, thereby forming a single weld of greater width than the first. This two-pane assembly is then placed in a low vacuum chamber and evacuated through an 8 mm diameter hole drilled through the smaller glass pane. The chamber is then backfilled with argon gas.

(60) It is understood that the invention may embody other specific forms, or incorporate combinations of the embodiments described herein, without departing from the spirit or characteristics the invention. While specific embodiments have been illustrated and described, other modifications may be made without significantly departing from the spirit of the invention.

(61) Various features of the invention are set forth in the following claims.