METHODS AND SYSTEMS FOR CRYSTALLIZING TACKY MATERIALS USING A TUMBLER
20200298449 ยท 2020-09-24
Inventors
Cpc classification
B01F29/401
PERFORMING OPERATIONS; TRANSPORTING
B29B9/16
PERFORMING OPERATIONS; TRANSPORTING
B01F35/93
PERFORMING OPERATIONS; TRANSPORTING
B29B9/12
PERFORMING OPERATIONS; TRANSPORTING
B01F29/40
PERFORMING OPERATIONS; TRANSPORTING
B01F35/2216
PERFORMING OPERATIONS; TRANSPORTING
International classification
B29B9/16
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A tumbler crystallizer for crystallizing pelleted, tacky, polymeric materials includes a housing for rotatably supporting a removable paneled drum on rollers. The removable panels may be made of a transparent, heat-insulating material. The drum receives a flow of hot pellets through an inlet chute, and a tumbling action of the drum and internal agitators keeps the pellets in motion relative to each other to prevent agglomeration until they reach a desired level of crystallinity and are no longer tacky. Baffle plates are provided at intervals along the length of the drum to slow the flow of pellets therethrough to increase residence time. Damper plates are provided near the exit end of the drum to aid in building a bed of pellets within the drum, and also to control residence time of the pellets within the drum.
Claims
1. A crystallizer tumbler device, comprising: a housing comprising: a rotatable drum comprising panels, a tumbling bed, a first thermocouple, the first thermocouple placed at an inlet of the rotatable drum to measure a first temperature of pellets flowing into the rotatable drum; a tilting device configured to adjust an angle of the housing relative to a horizontal plane; one or more connectors attached to one end of the housing and configured to rotate relative to one or more pivot points when the tilting device tilts the rotatable drum; one or more agitators configured to agitate pellets and prevent agglomerations within the rotatable drum as the drum rotates; and one or more damper plates arranged near the outlet of the rotatable drum configured to provide a partial impediment to a flow of pellets out of the rotatable drum.
2. The tumbler device of claim 1, wherein the panels comprise at least one transparent material selected from the group consisting of polycarbonate, glass, acrylic, ceramic, and combinations thereof.
3. The tumbler device of claim 1, wherein the panels are insulative panels configured to prevent heat loss from within the rotating drum.
4. The tumbler device of claim 1, further comprising a conduit connecting a pellet inlet chute to the rotatable drum, wherein the conduit is configured to house a powder feeder, the power feeder is configured to introduce a material for coating pellets to reduce agglomeration.
5. The tumbler device of claim 1, further comprising a second thermocouple, the second thermocouple placed at an outlet of the rotatable drum configured to measure a second temperature of pellets flowing out of the rotatable drum.
6. The tumbler device of claim 5, further comprising a controller coupled to the first thermocouple, the second thermocouple, and the tilting device, the controller comprising one or more processors configured to direct the tilting device to adjust the angle of the housing relative to a horizontal plane in response to determining that the first temperature exceeding a first threshold, the second temperature exceeding a second threshold, a temperature difference level between the first temperature and the second temperature exceeding a temperature difference threshold, or a combination thereof.
7. The tumbler device of claim 6, wherein a third thermocouple is placed inside the rotatable drum and is configured to monitor a third temperature of an air within the rotating drum, and wherein the controller is coupled to the third thermocouple and the one or more processors of the controller are further configured to direct the tilting device to adjust the angle of the housing relative to a horizontal plane in response to the third temperature exceeding a third threshold.
8. The tumbler device of claim 1, wherein the one or more agitators has a trapezoidal cross-section or L-shaped cross section.
9. The tumbler device of claim 1, wherein the tilting device is configured to lift up to five degrees or let down up to five degrees one end of the rotatable drum.
10. The tumbler device of claim 1, further comprising: an air tube partially disposed within the rotatable drum, the air tube configured to direct a heated gas received from a blower section to the rotatable drum through one or more apertures.
11. The tumbler device of claim 1, further comprising a vertically mounted deflector plate near the drum inlet and configured to prevent pellets flowing into the rotatable drum from prematurely bouncing and/or splashing towards the outlet of the rotatable drum.
12. The tumbler device of claim 1, wherein at least one damper plate of the one or more damper plates is configured to adjust to create an opening between two adjacent damper plates of the one or more damper plates for the flow of pellets to flow.
13. The tumbler device of claim 6, further comprising a motor rotatably coupled to the rotatable drum, wherein the one or more processors of the controller are further configured to change the rotation speed or rotational direction of the rotatable drum.
14. The tumbler device of claim 1, wherein the first and second thermocouples are attached to adjustable support arms that allows the first and second thermocouples to be adjusted into or out of the tumbling bed of pellets.
15. The tumbler device of claim 1, wherein baffle plates are placed circumferentially around the interior of the drum, and spaced longitudinally along the drum, the baffle plates configured to slow the flow of pellets from the inlet to the outlet of the drum.
16. The tumbler device of claim 15, wherein the baffle plates are arranged at an angle to the flow of pellets such that the angled baffle plates push back the pellets impeding their flow towards the outlet of the rotating drum.
17. A method of crystallizing pellets in a rotating drum crystallizer, the method comprising: providing pellets into the rotating drum of the crystallizer; determining a residence time of the pellets needed within the drum necessary to effect a desired level of crystallinity of the pellets; rotating the drum containing the pellets; adjusting the tilt angle of the drum so as to achieve the desired residence time of the pellets; and directing the flow of pellets out through an opening of the drum.
18. A method of crystallizing pellets in a crystallizer, the method comprising: providing pellets into a drum of the crystallizer; measuring, via a first thermocouple, a first temperature of the pellets after entering the drum; rotating the drum containing the pellets; tilting the drum to a predetermined angle to change a flow of the pellets within the drum based on the first temperature differing from a first predetermined temperature threshold; and directing the flow of pellets out an opening of the drum.
19. The method of claim 18, further comprising measuring a second temperature of the pellets before exiting the drum, wherein tilting the drum is based on whether the first temperature differs from the first predetermined temperature threshold, whether the second temperature differs from a second predetermined temperature threshold, whether a temperature difference between the first temperature and the second temperature differs from a predetermined temperature difference threshold, or a combination thereof.
20. The method of claim 19, further comprising: directing a flow of heated air from an air tube at least partially disposed within the drum through the drum; and changing a flow rate and/or temperature of the air based on the second temperature.
21. A method of crystallizing pellets in a crystallizer having a rotating drum, the method comprising: providing pellets into the rotating drum of the crystallizer; measuring, via a first thermocouple, a first temperature of the pellets entering the drum; rotating the drum containing the pellets; initiating a flow of heated air from an air tube at least partially disposed within the drum through the drum based on the first measured pellet temperature being below a temperature necessary to achieve crystallization; and directing the flow of pellets to exit through an opening of the drum.
22. The method of claim 21, further comprising: measuring, via a second thermocouple, a second temperature of the pellets exiting the drum; changing a flow rate and/or temperature of the heated air based on the second temperature.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0020] The above and other objects, features, and advantages of the present disclosure will become apparent from the following description of preferred embodiments given in conjunction with the accompanying drawings, in which:
[0021]
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DETAILED DESCRIPTION
[0031] The various embodiments of the presently disclosed subject matter are described with specificity to meet statutory requirements. However, the description itself is not intended to limit the scope of this patent. Rather, it has been contemplated that the claimed subject matter might also be embodied in other ways, to include different steps or elements similar to the ones described in this document, in conjunction with other present or future technologies.
[0032] It should also be noted that, as used in the specification and the appended claims, the singular forms a, an and the include plural references unless the context clearly dictates otherwise. References to a composition containing a constituent is intended to include other constituents in addition to the one named. Also, in describing the preferred embodiments, terminology will be resorted to for the sake of clarity. It is intended that each term contemplates its broadest meaning as understood by those skilled in the art and includes all technical equivalents which operate in a similar manner to accomplish a similar purpose.
[0033] The terms crystallizer, crystallization, crystalline, crystallized and crystallizable used herein are all used in connection with a process associated with partial alignment of a polymer's molecular chains. The degree of crystallinity, as estimated by different analytical methods, typically ranges from below 10% to above 80%, thus crystallized polymers are often called semi-crystalline. Throughout the following description, any reference to the above crystalline terms refers to semi-crystalline material, which may be of any degree of crystallinity.
[0034] The term pellet used herein, for example, can include, and be interchangeable with, micropellets or particulates. Such pellets/micropellets/particulates can take on a variety of shapes and are typified by regular or irregular shaped discrete particles without limitation to their dimensions, including flakes, stars, spheres, cylindrical pellets, lenticular or disc-shaped pellets, chopped fibers, rubber crumb pellets, and/or other shapes. They can also be round, square, rectangular, triangular, pentagonal, hexagonal or otherwise geometric in cross-section, star-shaped or other decorative designs, and can be the same or different when viewed in a second cross-section perpendicularly to the first. It shall also be understood that the pellets do not have to be solid pieces but may include particles defining openings or hollow shapes. Additionally, the pellets may include expanding agents, foaming agents, or volatiles, which may be partially or wholly expanded to produce low (or lower) bulk density particles.
[0035] Herein, the use of terms such as having, has, including, or includes are open-ended and are intended to have the same meaning as terms such as comprising or comprises and not preclude the presence of other structure, material, or acts. Similarly, though the use of terms such as can or may is intended to be open-ended and to reflect that structure, material, or acts are not necessary, the failure to use such terms is not intended to reflect that structure, material, or acts are essential. To the extent that structure, material, or acts are presently considered to be essential, they are identified as such.
[0036] It is also to be understood that the mention of one or more method steps does not preclude the presence of additional method steps or intervening method steps between those steps expressly identified. Moreover, although the term step may be used herein to connote different aspects of methods employed, the term should not be interpreted as implying any particular order among or between various steps herein disclosed unless and except when the order of individual steps is explicitly required. The components described hereinafter as making up various elements of the invention are intended to be illustrative and not restrictive. Many suitable components that would perform the same or similar functions as the components described herein are intended to be embraced within the scope of the invention. Such other components not described herein can include, but are not limited to, for example, similar components that are developed after development of the presently disclosed subject matter.
[0037] To facilitate an understanding of the principles and features of the invention, various illustrative embodiments are explained below. In particular, the presently disclosed subject matter is described in the context of being a crystallizer tumbler.
[0038]
[0039] Shown in more detail in
[0040] The base 22 may be constructed from a metal, wood, or hard plastic, and be configured to withstand the force of the drum's 60 rotation and weight and support the remainder of the housing 20 and the doors 30. For example, in some embodiments, the base 22 may be a stainless steel, such as 304 stainless steel, which allows for easy welding. In other embodiments, the base 22 may be a carbon steel. In further embodiments, the base 22 may be an aluminum, advantageously reducing its weight. The base 22 may vary in shape. For example, in some embodiments, the base 22 may be rectangular and include four I-beams or other beams, which may be attached to one another by means known in the art (e.g., welding, bolts, clamps, etc.). The base 22 may take on dimensions as needed to fit other components of the crystallizer tumbler 10, particularly the drum 60.
[0041] Extending vertically from the base 22, the faceplates 23, 24, 25 may contain the inner components (e.g., the drum 60, the blower section 70, etc.) of the crystallizer tumbler 10. The inlet faceplate 23 may extend vertically from the inlet end of the base 22 (i.e., the end of the tumbler 10 having the pellet inlet chute 40), and be configured to support the pellet inlet chute 40 as it extends through the inlet faceplate 23 to attach to the drum 60. The inlet faceplate 23 may be further configured with a floating seal 21 to prevent the pellets from exiting the drum back through the inlet faceplate 23. Details of the inlet construction, in accordance with some embodiments, may be found in the aforementioned U.S. Pat. No. 9,782,705.
[0042] The outlet faceplate 24 may extend vertically from the base 22 at the outlet end of the drum 60 (i.e., opposite the pellet inlet chute 40) and be configured to support the blower section 70 as it extends through the outlet faceplate 24 and inside of the drum 60. The outlet faceplate 24 may also be configured to prevent the flow of pellets beyond the outlet faceplate 24. In some embodiments, the outlet faceplate 24 may include a floating seal 21, or a similar device to prevent pellets from escaping the drum 60 through a gap between the outlet faceplate 24 and the air tube 73 (
[0043] The faceplates 23, 24, 25 may be constructed from a metal, wood, or hard plastic, and be configured to withstand the force of the drum's 60 rotation and weight and support the doors 30. For example, in some embodiments, the faceplates 23, 24, 25 may be constructed from stainless steel, carbon steel, or aluminum. In some embodiments, the faceplates 23, 24, 25 may have similar dimensions. For example, in one embodiment, the faceplates 23, 24, 25 may each be pentagonal having square bottom portion and a triangular top portion. In other embodiments, the faceplates 23, 24, 25 may be sized and shaped to contain the drum 60 and other inner components within the tumbler 10. The upper member 26 may be constructed from a metal, wood, or hard plastic, and be configured to horizontally support the top of the faceplates 23, 24, 25. For example, the upper member 26 may be constructed from stainless steel, carbon steel, or aluminum. In some embodiments, the upper member 26 may form an isosceles trapezoid that has a wider bottom face than the top face, as shown in
[0044] In one embodiment, the connectors 28 may be positioned on opposing sides of the inlet end of the tumbler 10. In other embodiments, however, the connectors 28 may be positioned on the outlet end of the tumbler 10 if the tilt mechanism 80 is switched to the inlet end of the tumbler 10. In some embodiments, the connectors 28 may form a pivot connection between the housing 20 and the frame 50, as shown in
[0045] In other embodiments, the tumbler 10 may not include a frame 50. Instead, the base 22 may be suspended from an above point via cables, ropes, beams, etc. For example, in one embodiment, the inlet and outlet ends of the tumbler 10 may be suspended above the ground surface via a cable. It is contemplated that the tumbler 10 may be configured such that its height off of the ground surface is adjustable, either via the cables or an adjustable height feature of the frame 50.
[0046] In some embodiments, the static dissipation brush 29 may be housed on the back side of the inlet faceplate 23 facing the drum 60, as shown in
[0047] As shown in
[0048] Once the doors 30 are closed and the crystallizer tumbler 10 is ready for operation, the pellet inlet chute 40 may be configured to receive and direct a flow of pellets into the drum 60 of the crystallizer tumbler 10. In some embodiments, as shown in
[0049] In some embodiments, the funnel 42 may be conically shaped and constructed from a metal, wood, or hard plastic. For example, in one embodiment, the funnel 42 may be rolled sheet metal. The funnel 42 may have a lower opening with a diameter about the same as that of the conduit 44, and a larger, upper opening for collecting the pellets. In other embodiments, the pellet inlet chute 40 may not include a funnel 42 as the conduit 44 may be directly attached to an outlet of an upstream component.
[0050] The conduit 44 may be a hollow cylindrical, rectangular, or other cross-sectional shaped conduit configured to transport the pellets into the drum 60, as shown in
[0051] As the material to be crystallized, e.g. pellets, leaves conduit 44 and enters into drum 60, the material tends to bounce off the interior surfaces of the drum and may bounce downstream in the drum prematurely, resulting in an uneven crystallization of the pellet bed. To aid in prevention of this premature downstream flow, deflector plate 200, shown in
[0052] Supporting the housing 20 off of the ground surface, the frame 50 is shown in
[0053] The cross members 54 may, in some embodiments, extend proximate a horizontal axis and connect one or more of the vertical members 52 to one another. The cross members 54 may be shaped as needed to structurally support the tumbler 10. In some embodiments, the cross members 54 may be rectangular and straight such that they are configured to attach to other components of the frame 50 at right angles. In other embodiments, the cross members 54 may be cylindrical and/or curved to provide clearance for other components. In further embodiments, the cross members 54 may be hollow to decrease their weight. In other embodiments, the cross members 54 may be solid or filled with a material to weight the frame 50 to prevent the tumbler 10 from moving despite its vibrations from the rotating drum 60.
[0054] In some embodiments, the corner support members 56 may connect the corners formed by at least some of the vertical members 52 and the horizontal members 58. The corner support members 56 may be triangular and configured to structurally support the frame 50 by keeping the vertical members 52 upright. It is also contemplated that the corner support members 56 may support other joints in the frame 50, including joints between the vertical members 52 and the cross members 54.
[0055] In other embodiments, the horizontal members 58 may extend proximate a horizontal axis and connect the top of the vertical members 52 to one another. The horizontal members 58 may be configured to receive the housing 20 such that the housing 20 fits snugly on top of the horizontal members 58. In some embodiments, the horizontal members may be configured to pivotally attach to the housing 20 via the connectors 28. In some embodiments, the horizontal member 58 may be a solid single surface that covers the bottom of the housing 20. The surface of the horizontal members 58 may include a rough surface to grip the housing 20 and prevent the housing 20 from sliding as the drum 60 rotates. In other embodiments, the horizontal members 58 may surround the perimeter of the housing 20. The horizontal members 58 may be hollow in some embodiments to reduce their weight, and solid in other embodiments for strength.
[0056] Shown in greater detail in
[0057] The knobs 64 and connectors 67 may have mating elements (e.g., other connectors or holes) for attaching the panels 62 onto the frame members 106. To secure the alignment of the panels 62, the panel frame 65 may include holes configured to fit around the connectors 67. In some embodiments, the panels 62 may snap onto the connectors 67.
[0058] In other embodiments, the knobs 64 may be positioned to slidably receive one or more edges of the panel 62 (or several panels 62). After sliding the edge of the panel 62 under the knob 64, an opposing edge of the panel 62 may be fastened to the drum 60 via the connector(s) 67. In this embodiment, the required number of connectors 67 may be limited by the use of the knobs 64. Further, the knobs 64 and connectors 67 may be configured to screw in, clip, latch and/or snap on such that an operator can quickly connect or remove the panel 62 without the use of tools. In other embodiments, the panels 62 may be bolted, welded, hinged and latched, clamped, and/or sealed to the drum 60. Additionally, seals or gaskets may be used at the connection points to help contain pellets and micropellets within the drum 60.
[0059] On the inside of the drum 60, as shown in
[0060] In some embodiments, the agitators 61 and/or other components within the tumbler 10 may be treated with various coatings, as desired. For example, in one embodiment, the agitators 61 may be treated with a wear resistant coating to help improve their durability. In other embodiments, inlet chute 44 and other non-rotating parts, as well as any rotating parts of drum 60, may be coated with non-stick coatings to prevent the tacky, non-crystallized material from sticking thereto. It is contemplated that any coatings or surfaces treatments may be used, including those described in U.S. Pat. No. 8,080,196, which is incorporated by reference herein.
[0061] The hand bars 69 may be U-shaped and extend outwardly from the exterior of the drum 60, as shown in
[0062] As shown in
[0063] Shown in detail in
[0064] In some embodiments, the stop ring 100 may have a hole configured to allow the air tube 73 to pass through it, as shown in
[0065] In between the ring 68 and the stop ring 100, the openings 102 may be configured to allow pellets to pass into the pellet outlet chute 90. In some embodiments, the openings 102, as defined by the space between the frame members 106, may be sized and shaped to allow all of the pellets to pass. In other embodiments, the openings 102 may be sized or shaped to limit the flow of the pellets to a rate or volume desired for a downstream process (e.g., bagging).
[0066] Downstream of the stop ring 100, the openings 104 may be defined by the space between the frame members 106. In some embodiments, the pellets are prevented from passing to this section of the drum 60, and accordingly, the panels 62 are not useful in this section.
[0067] In some embodiments, the frame members 106 may extend horizontally along the entire length of the drum 60 and connect the drum wheels 66 to one another. The frame members 106 may serve as a structural support for other components, such as the panels 62, the knobs 64, and the connectors 67, to connect to. In some embodiments, the frame members 106 may define the size and shape of the openings 102 and 104, as shown in
[0068] Partially disposed within the drum 60, as shown in
[0069] On the back end of the tumbler 10, the tilting mechanism 80 may be connected to the frame 50 and the housing 20 and configured to change the angle of the drum 60 relative to the horizontal to control the residence time of the pellets. In some embodiments, the tilting mechanism 80 may be a jack configured to lift or let down one end of the tumbler 10. As shown in
[0070] The motor 140, partially shown in
[0071] Extending from the motor 140, a driveshaft (not shown) may include one or more rollers 152 connected via a shaft 154, as shown in
[0072] Using the tumbler 10 as a crystallizer may be advantageous over using other crystallizers and crystallizing methods, which may be too rough and damage the pellets, such as a TorusDisc, or ineffective at sufficiently preventing agglomeration of materials that are tacky while crystallizing, such as a Vibra type vibrating conveyor. This may be particularly important when the pellets are both a tacky and brittle material prior to their crystallization. In one embodiment, as an example, the crystallizer tumbler 10 may be configured to maintain a pellet residence time of 15 minutes with a continuous flow rate of 5,000 lbs. per hour, achieving a 40% or better crystallization, while minimizing pellet fracture and fines production, and preventing agglomeration of the material. Residence time and/or flow rate may be varied by adjusting the inclination angle of the drum 60, the diameter of the drum, or the drum length, drum rotation speed, and/or pellet outlet damper plate design, depending on need.
[0073] In order to build up a bed of pellets within drum 60, to aid in controlling the residence time of the pellets within the drum, and to aid in sealing in hot air within the drum, adjustable damper plates 190,
[0074] In order to determine the necessary residence time to achieve the desired degree of crystallization, testing may be done with the desired material. To this end, freshly cut pellets with still intact internal heat may be collected and stored in an insulated container and the crystallinity may be determined at different time intervals until the time needed to achieve the desired crystallinity is determined. Alternatively, one may search for data sheets for the specific material which may give the crystallinity data as a function of time and temperature. Such information may be available and found on the internet for a variety of polymeric materials. Other sources of such information may be available, such as polymer textbooks or technical journals of polymer science. Once the required residence time is known, the tilt angle of the drum may be adjusted, either manually or automatically by a controller, so as to achieve the desired residence time of the pellets.
[0075] Other means may be provided to aid for increasing the residence time of the pellets as they flow from the inlet end of the drum towards the outlet end. To this end, as best shown in
[0076] After the pellets reach the pellet outlet chute 90, they may be directed to the pellet outlet 132 and delivered to a downstream device (e.g., another tumbler used as a second crystallizer, a coater, a bagging assembly, a conveying system, a pellet classifier, etc.). To prevent the pellets from undesirably exiting the drum 60 before reaching the pellet outlet 132, the ridges 92, seen in
[0077] During operation of the crystallizer tumbler 10, the drum 60 may be configured to rotate along its longitudinal axis in a clockwise and/or counter-clockwise direction. The motor 140 may rotate the driveshaft 154 and its rollers 152, which in turn cause the drum wheels 66 to rotate. In some embodiments, the drum 60 may be configured to rotate in a single direction (e.g., clockwise or counter-clockwise). In other embodiments the drum 60 may be configured to rotate in multiple directions, either randomly or in accordance with a predetermined pattern. Additionally, in other embodiments, the rotation speed of the drum 60 may vary based on a number of factors (e.g., the direction of rotation, air/gas flow rate within the tube 70, the material of the pellets, the speed of crystallization, the desired residence time, the desired pellet flow rate) or be fixed. For example, the rotation speed of the drum 60 may be fixed based on preset settings of the motor 140, or a variable frequency drive may allow infinitely variable adjustments in the drum rotation speed.
[0078] It is contemplated that one or more indicators or controllers (not shown), which may be computerized controllers having one or more processors, may automatically control operation of one or more components within the tumbler 10. For example, as shown in
[0079] The controller may also automatically control the opening and closing of the doors 30 based on an operation mode of the tumbler 10. For example, the controller may direct the doors 30 to close when the motor 140 begins to rotate the drum 60. The controller may direct the doors to open, for example, when the motor 140 is not rotating the drum 60.
[0080] The controller may be in communication with other sensors to improve operation of the tumbler 10. For example, in some embodiments, one or more flow sensors may measure the pellet inlet flow and/or outlet flow entering or exiting the tumbler 10. The controller may control features of the tumbler 10 to achieve a more consistent pellet flow exiting the tumbler 10. Further, the controller may detect blockages within the tumbler 10 disrupting pellet flow and shut down operation of one or more of the features of the tumbler 10. In other embodiments, the controller may send an alert to an operator (e.g., to a display in communication with the controller or to an operator's mobile phone, computer, or other device via a wireless or wired communication) upon detecting a blockage within the tumbler 10. In other embodiments, the flow sensors may measure the amount of pellets exiting the tumbler 10, which the controller may then provide to the operator (e.g., via the display). In further embodiments, the controller may be in communication with flow sensors at the pellet inlet chute 40 and the pellet outlet conduit 130, and may be configured to compare the measured flow of pellets at each point. When the difference between the measured flow of pellets at the inlet and outlet exceeds a predetermined threshold, the controller may shut down operation of the tumbler 10 or alert the operator to a clog or leak. In this manner, the controller may help the operator identify and remove clogs of pellets while they are small, thereby minimizing wasted product and lost machine time.
[0081] In other embodiments, the controller may be in communication with one or more static electricity sensors configured to measure the level of static electricity built up at certain points on the tumbler 10. In this manner, the controller may determine whether the static dissipation brush 29 or other static dissipation device is sufficient to dissipate the static electricity accrued by the tumbler 10, and serve as a safety mechanism to prevent the operator from undesired shocks. When the controller receives a signal from these sensors that the level of static electricity exceeds a predetermined threshold, the controller may respond by shutting down operation of the tumbler 10 and/or alerting the operator.
[0082] It is contemplated that, in conjunction with various sensors, the controller may configure the tumbler 10 for one or more modes of operation. In some embodiments, the controller may store the modes of operation on memory, and allow the operator to select a desired mode of operation via the display or another device in communication with the controller. The modes of operation may be directed to different pellet materials, sizes, or shapes, and flow rate. For example, tacky pellets may be handled with higher rotation rates than tacky and brittle materials.
[0083] Of course, it is contemplated that, in place of an automated controller, an operator may perform the same functions by reading the various signals from a digital or analog display and vary the conditions of the crystallizer tumbler accordingly.
[0084] In an exemplary method of operation, crystallizer tumbler 10 may be operated to crystallize a polymer in the following manner. A crystallizable material is first pelletized using an underwater pelletizer system such as one manufactured by Gala Industries and described in U.S. Pat. No. 9,032,641. In this pelletizer system, pellets quickly are transferred from a cutting chamber to a centrifugal dryer by means of a water system and an air injection system within the water system. This air injection system, developed by Gala Industries and termed CPT Process, causes the pellets to reach the dryer in a very short time so that the pellets retain the majority of the internal heat imparted to them through the extrusion process. In this way, the pellets exit the dryer and are transferred to the crystallizer tumbler with enough remaining internal heat to cause crystallization of the pellets, and the insulated nature of the tumbler drum will help prevent the loss of this retained heat throughout the residence time of the pellets. For materials for which use of the crystallizer tumbler is indicated, the pelleted material will remain in a tacky state until a certain desired level of crystallinity is achieved. In order to prevent agglomeration while the crystallization process takes place, the crystallizer tumbler will gently tumble the material and retain the material within the drum for a residence time needed to complete sufficient crystallization until the pellets are no longer tacky. This residence time is controlled by the inclination of the tumbler drum, the tumbler drum rotation speed, agitator design and quantity, location, number and design of the baffle plates, and the design and adjustment of the damper plates. Incoming pellet temperature and outgoing pellet temperature are monitored using the immersed thermocouples and other temperature sensors, to assure maintenance of sufficient heat to achieve crystallization. The gentle tumbling action of the pellets provided with the crystallizer tumbler of the present invention provides an improvement in preventing agglomeration over vibrating conveyor type crystallizers, provides an improvement in preventing fines generation and pellet fracture over torus disc type crystallizers, while not requiring any additional input of energy to heat the pellets. Further, the tumbler type crystallizer may have a lower power consumption to maintain the motion of the pellets than other crystallizing devices. In this manner, as explained in the various embodiments described herein, the tumbler crystallizer 10 provides an improvement over vibrating conveyor, torus disc, or stirring paddle type crystallizers for tacky materials.
[0085] While the present disclosure has been described in connection with a plurality of exemplary aspects, as illustrated in the various figures and discussed above, it is understood that other similar aspects can be used or modifications and additions can be made to the described aspects for performing the same function of the present disclosure without deviating therefrom. For example, in various aspects of the disclosure, methods and compositions were described according to aspects of the presently disclosed subject matter. However, other equivalent methods or composition to these described aspects are also contemplated by the teachings herein. Therefore, the present disclosure should not be limited to any single aspect, but rather construed in breadth and scope in accordance with the appended claims.