Ferromagnetic resonance (FMR) electrical testing apparatus for spintronic devices
10761154 ยท 2020-09-01
Assignee
Inventors
- Guenole Jan (San Jose, CA, US)
- Son Le (Gilroy, CA, US)
- Luc Thomas (San Jose, CA, US)
- Santiago Serrano (San Jose, CA, US)
Cpc classification
G01R33/24
PHYSICS
G01N24/00
PHYSICS
International classification
G01R33/24
PHYSICS
G01N24/00
PHYSICS
Abstract
A scanning ferromagnetic resonance (FMR) measurement system is disclosed with a radio frequency (RF) probe and one or two magnetic poles mounted on a holder plate and enable a perpendicular-to-plane or in-plane magnetic field, respectively, at test locations. While the RF probe tip contacts a magnetic film on a whole wafer under test (WUT), a plurality of microwave frequencies (f.sub.R) is sequentially transmitted through the probe tip. Simultaneously, a magnetic field (H.sub.R) is applied to the contacted region thereby causing a FMR condition in the magnetic film for each pair of (H.sub.R, f.sub.R) values. RF output signals are transmitted through or reflected from the magnetic film to a RF diode and converted to voltage signals which a controller uses to determine effective anisotropy field, linewidth, damping coefficient, and/or inhomogeneous broadening for a sub-mm area. The WUT is moved to preprogrammed locations to enable multiple FMR measurements at each test location.
Claims
1. A method of performing a ferromagnetic resonance (FMR) measurement on a whole wafer under test (WUT) having a magnetic film or a plurality of magnetic devices formed thereon, comprising: providing a wafer chuck or stage on which the WUT is held, and having a first link to a controller; providing a RF probe having a probe tip comprised of at least one signal pathway that is configured to contact a test surface which is comprised of the magnetic film or plurality of magnetic devices; applying a sequence of RF input signals from a RF generator that has a second link to the controller, each RF input signal passes through the RF probe tip and comprises a different microwave frequency that is sequentially transmitted to a first location on the test surface; applying a magnetic field from at least one magnetic pole simultaneously with each different microwave frequency to establish a FMR condition in the test surface thereby resulting in a RF output signal for each pair of an applied microwave frequency value and an applied magnetic field value; and transmitting a sequence of RF output signals from the RF probe tip to a RF diode that is configured to convert each RF output signal to a voltage signal and to send each voltage signal to the controller, the controller determines one or more properties in the magnetic film or plurality of magnetic devices.
2. The method of claim 1 wherein the RF probe and magnetic pole piece are mounted on a holder plate in an electrical probe station.
3. The method of claim 1 wherein the RF generator, RF probe tip, and RF diode are configured in a transmission mode whereby each of the RF input signals passes through a first signal pathway in the RF probe to the test surface, and each of the RF output signals is transmitted from the test surface through a second signal pathway in the RF probe to the RF diode.
4. The method of claim 1 wherein the RF generator, RF probe tip, and RF diode are configured in a reflectance mode whereby each of the RF input signals passes through a first signal pathway in the RF probe to the test surface, and each of the RF output signals is transmitted from the test surface through the first signal pathway to the RF diode.
5. The method of claim 4 wherein the RF input signal passes through a directional coupler between the RF generator and RF probe, and the RF output signal also passes through the directional coupler before reaching the RF diode.
6. The method of claim 1 further comprised of performing a FMR measurement at a plurality of different locations on the test surface in a scanning mode while the magnetic pole and RF probe are stationary, wherein the WUT and a wafer chuck on which the WUT is held are moved from the first location to one of the different locations by a sequence that comprises: separating the RF probe tip and test surface using a vertical movement of the wafer chuck; performing a lateral movement of the wafer chuck such that the RF probe tip and magnetic pole piece are aligned above one of the different locations; and performing a vertical movement of the wafer chuck such that the RF probe tip contacts the test surface at the one of the different locations.
7. The method of claim 1 wherein applying the magnetic field comprises sweeping through a range of magnetic fields from a minimum magnetic field value to a maximum magnetic field value.
8. The method of claim 1 wherein a single magnetic pole is aligned above the RF probe tip and applies the magnetic field in a perpendicular-to-plane direction to the test surface.
9. The method of claim 8 wherein the magnitude of the applied magnetic field is up to 3 Tesla, and the different microwave frequencies are in a range of about 1 to 100 GHz.
10. The method of claim 1 wherein two magnetic poles are positioned on opposite sides of the RF probe tip such that the magnetic field is applied in an in-plane direction at the test surface during the FMR measurement.
11. The method of claim 10 wherein the magnitude of the applied magnetic field is up to 3 Tesla, and the different microwave frequencies are in a range of about 0.01 to 100 GHz.
12. The method of claim 1 wherein the voltage signal from the RF diode is converted from an analog to digital form with an analog-to-digital converter that is between the RF diode and the controller.
13. A method comprising: positioning a probe proximate a first surface of a magnetic film; applying a sequence of RF input signals to the first surface through probe, wherein each RF input signal comprises a different microwave frequency that is sequentially transmitted to the first surface; applying a magnetic field from at least one magnetic pole with each different microwave frequency to establish a ferromagnetic resonance (FMR) condition in the first surface thereby resulting in a RF output signal for each pair of an applied microwave frequency value and an applied magnetic field value; transmitting a sequence of RF output signals from the probe to a RF diode that is configured to convert each RF output signal to a voltage signal and to send each voltage signal to a controller; and determining one or more properties in the magnetic film based on the RF output signals wherein the determining of the one or more properties in the magnetic film based on the RF output signals includes the controller determining the one or more properties in the magnetic film based on each voltage signal sent to the controller.
14. The method of claim 13, wherein the positioning of the probe proximate the first surface of the magnetic film includes positioning the probe directly on the first surface of the magnetic film.
15. The method of claim 13 wherein the applying of the magnetic field includes sweeping through a range of magnetic fields from a minimum magnetic field value to a maximum magnetic field value.
16. The method of claim 13 wherein the at least one magnetic pole is a single magnetic pole that is aligned above the RF probe and applies the magnetic field in a perpendicular-to-plane direction to the first surface.
17. The method of claim 13, wherein the magnitude of the applied magnetic field is up to 3 Tesla, and the different microwave frequencies are in a range of about 1 GHz to about 100 GHz.
18. The method of claim 13, wherein the at least one magnetic pole is two magnetic poles that are positioned on opposite sides of the RF probe such that the magnetic field is applied in an in-plane direction at the test surface during the FMR measurement.
19. The method of claim 13, wherein the magnetic film is part of a wafer under test.
20. The method of claim 13, wherein the positioning of the probe proximate the first surface of the magnetic film includes retaining the probe in a stationary position and moving the magnetic film relative to the probe.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION
(15) The present disclosure is a scanning FMR system that is designed to measure magnetic properties including H.sub.K and for magnetic structures that may be substantially smaller than 1 mm in diameter. Multiple test sites across a whole wafer are sequentially measured with either a RF transmission mode or a RF reflectance mode. X-axis and y-axis coordinates on the wafer under test (WUT) are in a plane that is aligned parallel to and above the plane of the wafer chuck. The present disclosure also encompasses a FMR test method for measuring magnetic properties of one or more magnetic films on unpatterned wafers or in device structures. The terms RE and microwave may be used interchangeably.
(16) In related U.S. patent application Ser. No. 15/463,074, we disclosed a FMR measurement system that relies on a waveguide transmission line (WGTL) that is attached to RF input and RF output connectors and is capable of taking measurements at a plurality of sites on a whole wafer. However, the WGTL is generally custom designed and requires the positioning of the WGTL as close as possible to the WUT to improve the coupling and magnetic field at the device level. Furthermore, the area probed in the measurement is quite large (mm to cm diameter) compared with sub-micron dimensions in the device structures. Now, we have discovered an improved scanning FMR measurement system that may be entirely constructed from commercially available components, and enables magnetic properties to be monitored and measured in smaller structures that may be substantially less than 1 mm in diameter.
(17) Referring to
(18) A magnetic field in magnetic assembly 30 (comprised of at least one magnetic field source) is produced by power input from the power generator 31 when instructed to do so by the controller through link 42a. In preferred embodiments, a magnetic field is applied to a predetermined (x.sub.n, y.sub.n) coordinate on the WUT while a RF signal pathway in the RF probe 40 on mounting bracket 46 contacts a top surface 22t of the magnetic film at the (x.sub.n, y.sub.n) coordinate. As a result of simultaneously applying a microwave frequency (RF input signal) from the RF probe, and a magnetic field of up to 3 Tesla from a pole tip (shown in
(19) The RF detector may be a power diode 44 hereinafter referred to as a RF diode, which detects a RF output signal transmitted from the magnetic film and that exits the RF probe through a second signal pathway and second RF connector (not shown). Each RF output signal corresponds to a RF power loss caused by the FMR condition where a certain amount of microwave power is absorbed and excites the magnetic film to a resonance state. Each FMR measurement may comprise a plurality of RF input signals each corresponding to a different RF frequency. After the FMR measurement is performed at the (x.sub.n, y.sub.n) coordinate, the wafer chuck 20 and WUT 22 are lowered 51d via a signal from the controller 11 through link 42d to reestablish a gap distance below the RF probe. Subsequently, the wafer chuck and WUT are moved to another predetermined (x.sub.n, y.sub.n) coordinate, and then the wafer chuck is raised 51u to enable the RF probe to contact magnetic film top surface 22t for another FMR measurement.
(20) The controller 11 has an electrical connection 42b to a RF generator 48 that provides a plurality of microwave frequencies through link 42c to a first RF connector (not shown) on RF probe 40. In some embodiments, the RF generator produces a first microwave frequency (f1) in the range of 1 to 20 GHz. However, the present disclosure anticipates inserting a frequency multiplier module (not shown) between the RF generator and RF probe that adjusts f1 to a second RF frequency (f2) where f2>f1. For example, when f1=20 GHz, the frequency multiplier module may be an active frequency doubler that adjusts f1 to f2 where f2=40 GHz. According to the first embodiment, RF frequencies below 1 GHz are not practical for the purpose of inducing a FMR condition in the magnetic film.
(21) In a preferred operating mode for a FMR measurement, the applied magnetic field is varied (swept from a minimum to a maximum value) at a constant microwave frequency. The FMR measurement is preferably repeated by sweeping the magnetic field successively through each of a plurality of different microwave frequencies. The RF diode converts the power output from the RF probe to a voltage signal that is transmitted through an output cable 45 to the controller. Thereafter, the controller calculates H.sub.k and , and in some cases and inhomogeneous broadening (L.sub.0), based on each pair of applied magnetic field value and applied microwave frequency used to establish a FMR condition, and on voltage output data from the RF diode for each (x.sub.n, y.sub.n) coordinate used in the FMR measurement sequence.
(22) The present disclosure encompasses designs other than the one illustrated in
(23) Referring to
(24) In
(25) Referring to
(26) Referring to
(27) Referring to
(28) In the exemplary embodiment, controller 11 has a link 42b to a commercial RF generator 48 with capability to generate a range of frequencies mentioned previously. The RF generator is connected by link 42c to a frequency multiplier module 47 such as an active frequency doubler, which in turn is connected through RF input cable 17a to RF input connector 15a on RF probe 40. RF probe end 40e contacts magnetic film 22f during a FMR measurement when a magnetic field from at least one magnetic pole tip (not shown), and a RF frequency from a first signal pathway (40s in
(29) During intervals when no FMR measurements are being performed, the RF probe tip including end 40e is a gap distance>0 from the top surface 22t of the magnetic film 22f on WUT 22. As indicated previously, when the scanning FMR measurement system is programmed to perform a plurality of FMR measurements at a certain (x.sub.n, y.sub.n) coordinate, the wafer chuck is raised so that the RF probe end contacts the magnetic film until the FMR measurements are completed. For the single pole embodiment (
(30) During a FMR measurement when a magnetic field is applied to an area around an (x.sub.n, y.sub.n) coordinate on the magnetic film contacted by the RF probe end 40e, a portion of the microwave power supplied by the RF input signal is absorbed by the magnetic film 22f during a FMR condition so that the RF output signal carried through RF output cable 17b and through a RF power diode has reduced power compared with the RF input signal. The RF power diode may be a Schottky diode, or another commercial RF diode, and converts the RF output signal for each (H.sub.R, f.sub.R) pair to a voltage measurement that is relayed to the controller. In other words, the intensity of the applied magnetic field (H.sub.R) may be varied for a given RF frequency (f.sub.R), or a plurality of RF frequencies may be applied with a constant magnetic field during each FMR measurement at an (x.sub.n, y.sub.n) coordinate. Preferably, the applied magnetic field is swept from a minimum to a maximum value at a constant microwave frequency (F1), and then the FMR measurement is repeated by sweeping the magnetic field successively with each of a plurality of different microwave frequencies (F2, F3, . . . Fn). Once a plurality of FMR measurements is taken at a first (x.sub.n, y.sub.n) coordinate, the wafer chuck and WUT are lowered and stepped to a second (x.sub.n, y.sub.n) coordinate for a second set of FMR measurements. Thus, the scanning FMR measurement method described herein comprises taking multiple FMR measurements at a plurality of preprogrammed (x.sub.n, y.sub.n) coordinates, and is managed by the controller 11.
(31) According to a second embodiment shown in
(32) A portion of the microwave power supplied by the RF input signal is absorbed by the magnetic film 22f proximate to a (x.sub.n, y.sub.n) coordinate contacted by the RF probe end. In this case, the RF output signal is carried through the signal pathway 40s used for the input signal and through RF input connector 15a back to directional coupler 60 where the RF signal is routed through RF output cable 17c to Schottky diode 44 or another RF diode, and ADC 49 before reaching controller 11. In alternative embodiments, a power divider or a bias tee may be used instead of the directional coupler as appreciated by those skilled in the art.
(33) As described earlier with respect to the transmission mode, the intensity of the applied magnetic field (H.sub.R) at the (x.sub.n, y.sub.n) coordinate may be swept from a minimum to a maximum value for each in a series of frequencies F1, F2, and so forth up to Fn. Alternatively, the RF frequency may be swept from a minimum to a maximum value for each applied magnetic field in a series of increasing magnitudes from H1, H2, and so forth up to Hn. Once a plurality of FMR measurements is taken at a first (x.sub.n, y.sub.n) coordinate, the wafer chuck and WUT are lowered and stepped to a second (x.sub.n, y.sub.n) coordinate for a second series of FMR measurements. Thus, the scanning FMR measurement method of the second embodiment that is based on a RF reflectance mode comprises taking multiple FMR measurements at a plurality of preprogrammed (x.sub.n, y.sub.n) coordinates on a magnetic film 22f. The Schottky diode 44 or another commercial RF diode, converts the RF output signal for each (H.sub.R, f.sub.R) pair to a voltage measurement that is relayed to the controller through ADC 49.
(34) The controller uses the FMR measurement data and one or more of equations (1)-(3) described previously to determine Hk, , and in some cases and inhomogeneous broadening (L.sub.0) at each (x.sub.n, y.sub.n) coordinate on the magnetic film. As indicated earlier, the term magnetic film may refer to a stack of layers in an unpatterned film, or in a plurality of devices having sub-millimeter or even sub-micron dimensions along the x-axis and y-axis directions. In all cases, there should be a conductive pathway through the magnetic film to enable a RF frequency (with an applied magnetic field) to induce a FMR condition in the magnetic film.
(35) Referring to
(36) In
(37) Referring to
(38) As a result of the simultaneous application of microwave frequency F1 and the variable magnetic field, the magnetic film achieves a FMR condition and absorbs a portion of the microwave power that depends on the magnetic properties of the magnetic film, the magnitude of F1, and the applied magnetic field (H.sub.R) that induced the ferromagnetic resonance state in the film. Accordingly, in step 112, the RF power diode detects a reduced power value in the RF output signal compared with the value specified by the controller in the RF input signal from step 111.
(39) In step 113, the RF power diode converts the RF output signal to a voltage measurement that is transmitted to the controller (through an ADC in the exemplary embodiments in
(40) Step 114 comprises a repetition of steps 111-113 except the RF input signal has a second frequency F2 that is applied to the magnetic film at the previously selected (x.sub.n, y.sub.n) coordinate after F1 is applied. In some embodiments, steps 111-113 are repeated a plurality of times at each (x.sub.n, y.sub.n) coordinate used for the FMR measurement method. In other words, a third frequency F3 that differs from F1 and F2 may be applied during an interval of time after F2, and so forth up to an nth frequency Fn after F3 is applied. Note that the applied magnetic field is preferably swept between a minimum and a maximum value for each frequency F1 up to Fn. Thus, a FMR condition occurs with each applied frequency and with a certain magnetic field value, and each FMR condition has a unique microwave absorbance that is translated into a corresponding voltage signal by the RF power diode. In an alternative embodiment, the applied magnetic field is held constant at a first value H1 while the microwave frequencies are varied (swept) from F1 up to Fn to establish a FMR condition. Thereafter, a second magnetic field H2 that is different from H1 may be applied while the microwave frequencies are varied through a range of values. The scanning FMR measurement method may be repeated by sweeping through a range of RF frequencies with a different magnetic field up to a maximum Hn value.
(41) Referring to step 115, the controller commands the wafer chuck and overlying magnetic film to move to a different (x.sub.n, y.sub.n) coordinate such as from (x.sub.1, y.sub.1) to (x.sub.2, y.sub.2). The movement comprises a first step of disengaging the RF probe tip from the first (x.sub.n, y.sub.n) coordinate with a downward movement of the wafer chuck and WUT (movement 51d in
(42) Thereafter, steps 111-114 are repeated to complete a FMR measurement at the second (x.sub.n, y.sub.n) coordinate. Note that each (x.sub.n, y.sub.n) coordinate may comprise a contact area of less than a square micron up to a plurality of square millimeters depending on the size of the signal probes 40s selected, and each (x.sub.n, y.sub.n) coordinate may be a center point in the area contacted by the RF probe tip.
(43) Depending on the diameter of the WUT that may be 6, 8, or 12, for example, and the number of different (x.sub.n, y.sub.n) coordinates desired for FMR measurements, step 116 indicates that steps 111-115 may be repeated a plurality of times to yield a plurality of FMR measurements involving n different (x.sub.n, y.sub.n) coordinates each with a plurality of (H.sub.R, f.sub.R) pairs where f.sub.R is one of F1 up to Fn, and H.sub.R may be varied from a minimum H1 value to a maximum Hn value. At step 117, a decision is made whether or not all of the pre-selected (x.sub.n, y.sub.n) coordinates on the magnetic film have been tested. If no, another FMR measurement is taken at a different (x.sub.n, y.sub.n) coordinate. If yes, step 118 indicates the scanning FMR measurement method is complete.
(44) As mentioned earlier, the controller is capable of determining magnetic properties in the magnetic film at each measurement location corresponding to a different (x.sub.n, y.sub.n) coordinate. Each FMR measurement yields one or more pairs (frequency, field) also referred to as (H.sub.R, f.sub.R) pairs in equation (1) corresponding to each FMR condition. The controller uses FMR measurement data and one or more of equations (1)-(3) described previously to determine Hk, , and in some cases and inhomogeneous broadening (L.sub.0).
(45) Using the transmission mode embodiment described earlier, we performed FMR measurements on full (unpatterned) film structures.
(46) All components required for assembling a scanning FMR measurement system for either the transmission mode or reflectance mode embodiments described herein are commercially available. The cross-sectional area of the device structures, or the area of unpatterned magnetic films that may be tested with a scanning FMR measurement scheme of the present disclosure are substantially smaller than in the prior art. Moreover, the magnetic assembly described previously enables a more uniform magnetic film to be applied thereby yielding more reliable FMR measurements than conventional methods.
(47) While this disclosure has been particularly shown and described with reference to the preferred embodiment thereof, it will be understood by those skilled in the art that various changes in form and details may be made without departing from the spirit and scope of this disclosure.