Packing element for heat and mass transfer

Abstract

Packing element for heat and/or mass transfer, including a plurality of circumferentially spaced panel shaped wall members, each wall member extending radially outward from an inner end extending along a central axis of the packing element to an outer edge opposite to the inner end and at least part of the outer edge extending along a surface of revolution having the central axis as an axis of revolution.

Claims

1. Packing element (i) for heat and/or mass transfer, comprising a plurality of circumferentially spaced panel shaped wall members (2), each wall member (2) extending radially outward from an inner end (2a) extending along a central axis (3) of the packing element (i) to an outer edge (2b) opposite to the inner end (2a) and at least part of the outer edge (2b) extending along a surface of revolution (5) having the central axis (3) as an axis of revolution, the outer edge (2b) of at least one wall member (2) has at least one recess (7), the recess (7) being formed as a slot starting at the outer edge (2b) and extending radially inward from the outer edge (2b) of the wall member (2).

2. Packing element according to claim 1, wherein the surface of revolution (5) is a cylindrical, spherical or ellipsoidal surface.

3. Packing element according to claim 1, wherein the number of wall members (2) comprises 2, 3, 4, 5 or more wall members (2).

4. Packing element according to claim 1, wherein the wall members (2) are disposed at equal circumferential angular distances.

5. Packing element according to claim 1, wherein at least one wall member (2) is helically formed, at least part of the outer edge (2b) extending along a helical line (4) on the surface of revolution (5) and being disposed at an angle (6) of at least 1 relative to the central axis (3).

6. Packing element according to claim 1, wherein the outer edge (2b) of at least one wall member (2) has a plurality of recesses (7), projections (7a) being formed between two adjacent recesses (7), a surface area of a projection (7a) being between 20% and 250% of a surface area of an adjacent recess (7).

7. Packing element according to claim 1, wherein a radial depth (d) of at least one recess (7) is at least 5% of a radial extension of the wall member (2) adjacent to the recess (7).

8. Packing element according to claim 1, wherein the packing element is made of metal, of glass, of ceramics, of plastics, or of a composite comprising at least one of these materials.

9. Packing element according to claim 1, wherein a circumferential thickness (8) of the wall members (2) is between 0.1% and 25%, of a maximum radial or longitudinal dimension of the wall members (2).

10. Packing element according to claim 1, wherein the packing element (i) is formed in one piece, or is assembled from several parts.

11. Reactor column for heat and/or mass transfer, comprising a large number of packing elements (i) according to claim 1.

12. Packing element according to claim 6, wherein a radial depth (d) of at least one recess (7) is at least 5% of a radial extension of the wall member (2) adjacent to the recess (7).

Description

BRIEF DESCRIPTION OF THE DRAWINGS

(1) In the drawings:

(2) FIG. 1 shows a lateral view of a first embodiment of a packing element according to the invention,

(3) FIG. 2 shows a lateral view of another embodiment of a packing element according to the invention,

(4) FIG. 3 shows a top view of another embodiment of a packing element according to the invention,

(5) FIG. 4 shows a lateral view of the embodiment according to FIG. 3,

(6) FIG. 5 shows a lateral view of an embodiment similar to FIG. 1

(7) FIG. 6 shows a lateral view of the embodiment of FIG. 5, and

(8) FIG. 7 shows a pilot plant using packing elements according to the invention.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS

(9) The invention is now more particularly described with reference to the embodiments illustrated in the drawings.

(10) Referring to FIGS. 1 to 6 of the drawing, different embodiments of an inventive packing element 1 are illustrated. In particular, FIG. 3 and FIG. 4 clearly show the spatial structure of the nozzle or packing element 1 according to the invention, which is made up by four panel shaped wall members 2, each wall member 2 extending radially outward from an inner end 2a extending along a central axis 3 of the packing element 1.

(11) Each wall member 2 is circumferentially spaced from two adjacent wall members 2 and extends from the central axis 3 in a radial direction to an outer edge 2b opposite to the central axis 3.

(12) Each wall member 2 is screw-like or helically formed and can be thought as being deformed from an initially planar member by bringing the outer edge 2b into an orientation along a helical line 4 on a surface of revolution 5 disposed around and defined by the central axis 3. In this way, each wall member undergoes, starting at the central axis 3, a progressive helical or screw-like form until the outer edge 2b is reached.

(13) The mentioned surface of revolution 5 containing the outer edges 2b of the wall members 2 may be a cylindrical surface having the central axis 3 as an axis of revolution 5. In an alternative, the surface of revolution 5 can be spherical where the central axis 3 forms a diameter of a spherical surface, or an ellipsoidal surface where the central axis 3 runs along the semi-major axis of the ellipsoidal surface.

(14) In the embodiments shown, the outer edge 2b extends along a helical line 4 which is inclined relative to the central axis at an angle 6 of about 30.

(15) The wall members 2 are shown to have a number of recesses 7 starting at the outer edge 2b of the wall members 2, the recesses 7 being formed as rectangular slots extending radially inward from the outer edge 2b of each wall member 2.

(16) In a particular example, the packing element 1 can have a diameter D between 10 mm and 200 mm, in particular between 50 mm and 100 mm and preferably 75 mm. The packing element 1 can have an axial length or height H in the direction of the central axis 3 between 10 mm and 200 mm, in particular between 50 mm and 100 mm and preferably 75 mm. The wall members 2 can have a thickness 8 between 1 mm and 10 mm, preferably between 3 mm and 6 mm and most preferably between 4 mm and 5 mm. The recesses or slots 7 can have a radial depth d of between 10 mm and 30 mm, preferably 20 mm, in the case of a diameter of 75 mm, and an axial extension h, along the central axis 3, of between 10 mm and 30 mm, preferably 20 mm, in the case of a length of 75 mm.

(17) Tests of screw-shaped packing elements 1 according to the invention were carried out on an experimental titanium installation (FIG. 7) for air desorption and absorption of iodine from drilling waters, its diameter being 470 mm and height 5,200 mm under a layer height (bulk) of packing elements of 3,200 mm. Studies in hydrodynamics and kinetics of the process of air desorption of iodine from the drilling waters were carried out at the loads to packed column by air4,800-6,600 m.sup.3/m.sup.2/hour; by drilling water48.64 mm.sup.3/m.sup.2/hour.

(18) The experimental-industrial pilot plant of FIG. 7 is for air desorption and absorption of iodine from drilling waters and comprises a desorber 10, packing elements (bulk) 1, air blower 11, water pump 12, absorber 13, sorbent tank 14, sorbent circulation pump 15, sulfurase anhydride container 16 and sulfuric acid tank 17.

(19) The studies were carried out when the columns were operated with submerged and partially submerged packing elements, under various hydrodynamic modes (including the emulsified one). The results of studies in hydrodynamics and kinetics of the process of air desorption of iodine from drilling waters demonstrate the high efficiency of the screw-shaped packing element, which allows the column operating in emulsified mode or close to it, at a packing layer height of 3.2 m, to achieve the degree of iodine desorption 95%, whereas while using other types of packing elements at the iodine desorption stage (including a 2-way screw-shaped packing element) at a layer height of 12 m, the degree of iodine desorption is only 90%.

(20) The packing element for mass exchangers according to the invention can be made up in a form of a screw having a shape close to a cylinder and can have four slots with a total area of 20 cm.sup.2 on each of the four wall members of the screw surface vertically, which, compared to a previously known screw packing element, can significantly increase the mass transfer efficiency due to increased turbulization and uniform distribution of the liquid and gas phases in the desorption and absorption columns. It allows to reduce the hydraulic resistance of a screw-shaped packing element by 15-20% and due to its high operating efficiency, in a mode close to the phase inversion mode, reduce 1.5-2.0 times the height of industrial titanium installations for air desorption and absorption of iodine, which will significantly reduce the capital costs to manufacture them.

REFERENCE SIGNS

(21) 1 packing element 2 wall member 2a inner end 2b outer edge 3 central axis 4 helical line 5 surface of revolution 6 angle 7 recess 7a projection 8 thickness D diameter H length d radial depth h axial extension