Scanning probe microscope
10712363 ยท 2020-07-14
Assignee
Inventors
- Masayuki Iwasa (Tokyo, JP)
- Yoshiteru Shikakura (Tokyo, JP)
- Shinya Kudo (Toyko, JP)
- Toshihiro Ueno (Toyko, JP)
Cpc classification
International classification
Abstract
Provided is a scanning probe microscope with which measurement data and a distribution image of differential data of the measurement data can be displayed selectively or together, an edge enhancement image can be obtained, and user convenience is improved. A scanning probe microscope (200) includes: a distribution image calculator (40a) configured to calculate a one-dimensional or two-dimensional first distribution image (201) of measurement data, and a one-dimensional or two-dimensional second distribution image (202) of differential data of adjacent data elements of the measurement data; and a display controller (40b) configured to instruct the distribution image calculator to calculate at least one of the first distribution image or the second distribution image, and to display the calculated distribution image on a predetermined display.
Claims
1. A scanning probe microscope, comprising: a cantilever including a probe to be brought into contact with or closer to a surface of a sample; and a displacement detector configured to detect a signal indicating a displacement of the cantilever, the scanning probe microscope being configured to acquire measurement data obtained when a predetermined physical quantity between the cantilever and the surface of the sample is kept constant based on the signal, and when the probe is scanned relatively along the surface of the sample, the scanning probe microscope further comprising: a distribution image calculator configured to calculate a one-dimensional or two-dimensional first distribution image of the measurement data, and a one-dimensional or two-dimensional second distribution image of differential data of adjacent data elements of the measurement data; and a display controller configured to instruct the distribution image calculator to calculate at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image, and to display, on a predetermined display, the calculated at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image, wherein the display controller is configured to display, when displaying both of the one-dimensional or two-dimensional first distribution image and the one-dimensional or two-dimensional second distribution image, the measurement data and the differential data at the same position at the same time.
2. A scanning probe microscope according to claim 1, further comprising a calculation direction specification module configured to specify a data calculation direction, in which the one-dimensional or two-dimensional first distribution image and the one-dimensional or two-dimensional second distribution image are to be calculated, wherein the distribution image calculator is configured to calculate, along the data calculation direction specified by the calculation direction specification module, a distribution image to be displayed on the predetermined display, of the one-dimensional or two-dimensional first distribution image and the one-dimensional or two-dimensional second distribution image.
3. A scanning probe microscope according to claim 1, further comprising a subtraction order specification module configured to specify a subtraction order for a difference of adjacent data elements, in which the one-dimensional or two-dimensional second distribution image is to be calculated, wherein the distribution image calculator is configured to calculate the one- dimensional or two-dimensional second distribution image in the subtraction order specified by the subtraction order specification module.
4. A scanning probe microscope comprising: a cantilever including a probe to be brought into contact with or closer to a surface of a sample; and a displacement detector configured to detect a signal indicating a displacement of the cantilever, the scanning probe microscope being configured to acquire measurement data obtained when a predetermined physical quantity between the cantilever and the surface of the sample is kept constant based on the signal, and when the probe is scanned relatively along the surface of the sample, the scanning probe microscope further comprising: a distribution image calculator configured to calculate a one-dimensional or two-dimensional first distribution image of the measurement data, and a one-dimensional or two-dimensional second distribution image of differential data of adjacent data elements of the measurement data; a display controller configured to instruct the distribution image calculator to calculate at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image, and to display, on a predetermined display, the calculated at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image; and a calculation direction specification module configured to specify a data calculation direction, in which the one-dimensional or two-dimensional first distribution image and the one-dimensional or two-dimensional second distribution image are to be calculated, wherein the distribution image calculator is configured to calculate, along the data calculation direction specified by the calculation direction specification module, a distribution image to be displayed on the predetermined display, of the one-dimensional or two-dimensional first distribution image and the one-dimensional or two-dimensional second distribution image, the display controller is configured to display the one-dimensional or two-dimensional second distribution image sequentially for each element of the differential data along one of a scanning direction and the data calculation direction, and wherein the distribution image calculator is configured to calculate, when at least one of the data calculation direction or the subtraction order is specified by at least one of the calculation direction specification module or the subtraction order specification module during display of the one-dimensional or two-dimensional second distribution image, the one-dimensional or two-dimensional second distribution image based on the specified at least one of the data calculation direction or the subtraction order.
5. A scanning probe microscope according to claim 4, wherein the distribution image calculator is configured to recalculate the one- dimensional or two-dimensional second distribution image of the measurement data before the specification based on the specified at least one of the data calculation direction or the subtraction order, and wherein the display controller is configured to display both of the recalculated one-dimensional or two-dimensional second distribution image and the one-dimensional or two- dimensional second distribution image after the specification.
6. A scanning probe microscope according to claim 1, wherein the display controller is configured to display at least one of the measurement data or the differential data line by line in one of a scanning direction and the data calculation direction.
7. A scanning probe microscope, comprising: a cantilever including a probe to be brought into contact with or closer to a surface of a sample; and a displacement detector configured to detect a signal indicating a displacement of the cantilever, the scanning probe microscope being configured to acquire measurement data obtained when a predetermined physical quantity between the cantilever and the surface of the sample is kept constant based on the signal, and when the probe is scanned relatively along the surface of the sample, the scanning probe microscope further comprising: a distribution image calculator configured to calculate a one-dimensional or two-dimensional first distribution image of the measurement data, and a one-dimensional or two-dimensional second distribution image of differential data of adjacent data elements of the measurement data; a display controller configured to instruct the distribution image calculator to calculate at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image, and to display, on a predetermined display, the calculated at least one of the one-dimensional or two-dimensional first distribution image or the one-dimensional or two-dimensional second distribution image; and a subtraction order specification module configured to specify a subtraction order for a difference of adjacent data elements, in which the one-dimensional or two-dimensional second distribution image is to be calculated, wherein the distribution image calculator is configured to calculate the one-dimensional or two-dimensional second distribution image in the subtraction order specified by the subtraction order specification module, the display controller is configured to display the one-dimensional or two- dimensional second distribution image sequentially for each element of the differential data along one of a scanning direction and the data calculation direction, and the distribution image calculator is configured to calculate, when at least one of the data calculation direction or the subtraction order is specified by at least one of the calculation direction specification module or the subtraction order specification module during display of the one-dimensional or two-dimensional second distribution image, the one-dimensional or two-dimensional second distribution image based on the specified at least one of the data calculation direction or the subtraction order.
8. A scanning probe microscope according to claim 7, wherein the distribution image calculator is configured to recalculate the one-dimensional or two-dimensional second distribution image of the measurement data before the specification based on the specified at least one of the data calculation direction or the subtraction order, and wherein the display controller is configured to display both of the recalculated one-dimensional or two-dimensional second distribution image and the one-dimensional or two- dimensional second distribution image after the specification.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1)
(2)
(3)
(4)
(5)
(6)
(7)
(8)
(9)
(10)
(11)
(12)
(13)
DESCRIPTION OF THE EMBODIMENTS
(14) Now, embodiments of the present invention are described with reference to the drawings.
(15)
(16) In
(17) The probe microscope controller 24 includes a frequency vibration characteristics detection mechanism 7.
(18) The computer 40 includes a control board configured to control operation of the scanning probe microscope 200, a central processing unit (CPU), a ROM, a RAM, a hard disk drive, or other such storage, an interface, an operation device, and other such components. Moreover, a monitor (display) 41 and a keyboard 42 are connected to the computer 40.
(19) The scanning probe microscope 200 is a sample scanning system in which the cantilever 1 is fixed to scan the sample 300 side.
(20) The probe microscope controller 24 includes a Z control circuit 20, which is to be described later, the frequency vibration characteristics detection mechanism 7, the excitation power supply 21, an XYZ output amplifier 22, and a coarse movement control circuit 23. The probe microscope controller 24 is connected to the computer 40 and is capable of high-speed data communication. The computer 40 is configured to control operation conditions of the circuits in the probe microscope controller 24, and read and control measured data to achieve measurement of a surface shape and other physical properties of the surface, for example.
(21) The probe microscope controller 24 is configured to amplify measurement data as appropriate, and acquire a sample surface shape and a physical quantity obtained by interaction between the cantilever and the sample.
(22) A bias supply circuit 29 is configured to directly apply a bias voltage to the sample stage 10, and is used also in a Kelvin probe force microscope (KFM) configured to measure a surface potential between the probe 99 and the sample 300, for example.
(23) The computer 40 corresponds to the distribution image calculator, the display controller, the calculation direction specification module, and the subtraction order specification module in the appended claims.
(24) A coarse movement mechanism 12 is configured to roughly move an actuator 11 and the sample stage 10 above the actuator 11 three-dimensionally, and its operation is controlled by the coarse movement control circuit 23.
(25) The actuator (scanner) 11 is configured to move (finely move) the sample stage 10 (and the sample 300) three-dimensionally, and is a cylinder including two (biaxial) piezoelectric elements 11a and 11b configured to scan the sample stage 10 in x and y directions (in the plane of the sample 300), respectively, and a piezoelectric element 11c configured to scan the sample stage 10 in a z (height) direction. A piezoelectric element is an element in which crystals are deformed when applied with an electric field, and when the crystals are forcedly deformed by an external force, an electric field is generated. As the piezoelectric element, lead zirconate titanate (PZT), which is a type of ceramics, can be generally used, but a shape and an operation method of the coarse movement mechanism 12 are not limited thereto.
(26) The piezoelectric elements 11a to 11c are connected to the XYZ output amplifier 22, and predetermined control signals (voltages) are output from the XYZ output amplifier 22 to drive the piezoelectric elements 11a and 11b in the x and y directions, respectively, and drive the piezoelectric element 11c in the z direction. An electric signal output to the piezoelectric element 11c is detected in the probe microscope controller 24, and is read as the above-mentioned measurement data.
(27) The sample 300 is placed on the sample stage 10, and the sample 300 is arranged to be opposed to the probe 99.
(28) The cantilever 1 is in contact with a side surface of a cantilever tip portion 8 to form the structure of a cantilever spring. The cantilever tip portion 8 is pressed to a slope block 2 by a cantilever tip portion holder 9, and the slope block 2 is fixed to the vibrator portion 3. Then, the vibrator portion 3 is vibrated with an electric signal from the excitation power supply 21 to vibrate the cantilever 1 and the probe 99 at the tip end of the cantilever 1. Methods of vibrating the cantilever include a piezoelectric element, an electric field and a magnetic field, irradiation with light, and passing of an electric current, for example.
(29) The vibrator portion 3 is fixed to a housing 13. The housing 13 has, in a portion directly above the cantilever 1, an opening for allowing light reflected by a dichroic mirror 31 and the light further reflected by a back surface of the cantilever 1 to pass therethrough.
(30) Then, laser light enters the dichroic mirror 31 from a laser light source 30 to irradiate the back surface of the cantilever 1, and the laser light reflected by the cantilever 1 is reflected by a mirror 32, and is detected by the displacement detector 5. The displacement detector 5 is a quadrant photo detector, for example, and a vertical displacement amount (in the z direction) of the cantilever 1 is detected, by the displacement detector 5, as a change in optical path (incident position) of the laser reflected by the cantilever 1. In other words, a vibration amplitude of the cantilever 1 corresponds to an amplitude of an electric signal of the displacement detector 5.
(31) The electric signal of the displacement detector 5 passes through a preamplifier 50 to be amplified in amplitude as appropriate, and is converted into a DC level signal corresponding to a magnitude of the amplitude by the AC-DC conversion mechanism 6.
(32) The DC level signal of the AC-DC conversion mechanism 6 is input to the Z control circuit 20. The Z control circuit 20 transmits a control signal to a Z signal portion of the XYZ output amplifier 22 so as to match a target amplitude of the probe 99 in a DFM measurement mode, and the Z signal portion outputs a control signal (voltage) for driving the piezoelectric element 11c in the z direction. In other words, a displacement of the cantilever 1 caused by atomic force that acts between the sample 300 and the probe 99 is detected by the above-mentioned mechanism, and the piezoelectric element 11c is displaced so that the vibration amplitude of the probe 99 (cantilever 1) becomes the target amplitude to control force with which the probe 99 and the sample 300 are brought into contact with each other. Then, under this state, the piezoelectric elements 11a and 11b are displaced in the x and y directions by the XYZ output amplifier 22 to scan the sample 300 to map a shape and a physical property value of a surface of the sample 300.
(33) Moreover, the DC level signal from the AC-DC conversion mechanism 6 is input to the frequency vibration characteristics detection mechanism 7 of the probe microscope controller 24. Further, the electric signal from the excitation power supply 21 is also input to the frequency vibration characteristics detection mechanism 7. The frequency vibration characteristics detection mechanism 7 processes a predetermined frequency vibration characteristics signal calculated based on the inputs from the AC-DC conversion mechanism 6 and the excitation power supply 21 to acquire, for example, sin, cos, and amplitude signals by lock-in detection, and transmit the signals to the computer 40.
(34) Then, the probe microscope operates as follows. With respect to a displacement in the xy plane of the sample stage 10, on the computer 40, (i) a three-dimensional shape image is displayed based on displacement of the height of the sample stage 10, (ii) a phase image is displayed based on a phase value in a resonance state, (iii) an error signal image is displayed based on a difference of the vibration amplitude from the target value, and (iv) a multifunction measurement image is displayed based on the physical property value between the probe and the sample, to thereby perform analysis and processing.
(35) Next, referring to
(36) As illustrated in
(37) Moreover, the distribution image calculator 40a calculates the first distribution image and the second distribution image in a calculation direction in accordance with an instruction from a calculation direction specification module 40c. Similarly, the distribution image calculator 40a calculates the second distribution image in a subtraction order in accordance with an instruction from a subtraction order specification module 40d.
(38) The instructions from the calculation direction specification module 40c and the subtraction order specification module 40d are issued by the user through the keyboard 42.
(39) Then, the display controller 40b displays the distribution image calculated by the distribution image calculator 40a on the monitor 41.
(40) Next, a processing flow in the computer 40 is described.
(41) In
(42) After determination processing in Step S110 to be described later, the distribution image calculator 40a calculates the specified distribution image line by line (Step S102).
(43) The display controller 40b displays the calculated distribution image line by line on the monitor 41 (Step S104).
(44) In this case, unless specified in Step S110 to be described later, in Step S102 and Step S104, the calculation direction and the subtraction order, which are to be described later, have default values (for example, the calculation direction is the same as a scanning direction). Moreover, when the calculation direction is the same as the scanning direction, one line corresponds to one scan line.
(45)
(46) The first distribution image 201, which is a shape image, includes a large hill M1 and a small hill M2, and with coloration adapted for highness and lowness of the large asperities on two dimensions, there are problems such as the small hill M2 having low contrast and becoming hard to see.
(47) To address those problems, through calculating and displaying the second distribution image 202 formed of the differential data of the adjacent measurement data elements, even when the large hill M1 and the small hill M2 are included in the same image, for example, a clear image 202 in which edges are enhanced to distinguish the hills M1 and M2 is obtained.
(48) In particular, when the first distribution image 201 and the second distribution image 202 are displayed on one monitor 41, as compared to the case in which one of the distribution images is displayed, the first distribution image 201 as the original image (for example, a shape image) and the second distribution image 202 consisting of the differential data can be compared on one screen, and hence more useful information can be obtained.
(49) In particular, of the first distribution image 201 and the second distribution image 202, when the measurement data and the differential data at the same position are displayed at the same time, a difference between the distribution images can be compared at the same position, and even more useful information can be obtained.
(50) The expression same position as used herein may correspond to one pixel of the measurement data, for example, but with the display being generally performed for each scan line or other such line, one particular line of the measurement data and data of one line of the differential data based on the measurement data of the particular one line may be regarded as the same position.
(51) Moreover, when the expression at the same time is used, in a case where one pixel of the measurement data is displayed sequentially, one pixel of the measurement data and one pixel of the differential data of pixels before and after the one pixel of the measurement data are displayed in association with each other at the same time. It should be noted, however, that with the display being generally performed for each scan line or other such line, one particular line of the measurement data and data of one line of the differential data may be displayed at the same time.
(52) Moreover, without departing from the above-mentioned spirit, another unit of data may be displayed at the same position or at the same time (for example, two lines may be displayed at the same time as one unit).
(53) Incidentally, as illustrated in
(54) To address this problem, when a calculation direction S2, in which the first distribution image and the second distribution image are calculated, is set to a vertical direction crossing the cross, for example, instead of the same direction as the scanning direction S1, it can be ensured that a second distribution image 202y contain useful information as illustrated in
(55) The processing of
(56) First, the distribution image calculator 40a determines, after Step S100 and before S102, whether a data calculation direction and/or a subtraction order has been specified (Step S110). The subtraction order is described later.
(57) In this case, the calculation direction can be specified, for example, when the user inputs a calculation direction through the keyboard 42, and the calculation direction specification module 40c sets the calculation direction in the distribution image calculator 40a.
(58) When the determination is Yes in Step S110, the processing proceeds to Step S112, and when the determination is No, the processing proceeds to Step S102.
(59) In Step S112, the distribution image calculator 40a calculates, of the first distribution image and the second distribution image, the distribution image (in this example, both of the first distribution image and the second distribution image) displayed on the display line by line along the specified calculation direction.
(60) Subsequently, when the determination is No in Step S114, the processing proceeds to Step S104, in which the distribution image calculated in the specified calculation direction is displayed.
(61) In
(62) When a direction in which the measurement data elements a1, a2, and a3 are lined is the scanning direction S1, there are a large number of calculation directions different from the scanning direction S1, which are not limited as long as the individual measurement data elements are connected in line in the direction, and include, in addition to the calculation direction S2 orthogonal to the scanning direction S1, a calculation direction S31, which is a bisector of an angle (in this example, 90) formed by the calculation directions S1 and S2, a calculation direction S32 between the calculation directions S1 and S31, and a calculation direction S33 between the calculation directions S2 and S31, for example.
(63) Moreover, in the case of the calculation direction S31, for example, one line includes all data elements on individual lines parallel to the calculation direction S31, and in
(64) Incidentally, there are cases in which the user sees the second distribution image 202 of
(65) In this case, as illustrated in
(66) To address this problem, as illustrated in
(67) In
(68) The processing in
(69) First, the distribution image calculator 40a determines, after Step S112, whether to recalculate the second distribution image before the specification of the calculation direction (Step S114).
(70) In this case, whether to recalculate the second distribution image can be determined when, for example, the user inputs a request for the recalculation through the keyboard 42, and the distribution image calculator 40a acquires the request. Alternatively, setting may be made to perform the recalculation by default.
(71) When the determination is Yes in Step S114, the processing proceeds to Step S116, in which it is determined whether a flag to be described later is set. In Step S116, when the determination is Yes, the processing proceeds to Step S104, and when the determination is No, the processing proceeds to Step S118.
(72) In Step S118, the distribution image calculator 40a recalculates the second distribution image in the specified calculation direction based on the measurement data before the specification, and sets a flag indicating that the second distribution image has been recalculated.
(73) Next, in Step S120, the display controller 40b displays the second distribution image recalculated in Step S118 and the second distribution image after the specification of the calculation direction together on the monitor 41.
(74) Subsequently to Step S120 or Step S104, in Step S130, the distribution image calculator 40a determines whether the measurement data has ended. The processing is ended when the determination is Yes, and the processing returns to Step S110 and is repeated when the determination is No.
(75) When the second distribution image is recalculated in the first Step S114, after the flag is set in S118, the second distribution image recalculated in Step S120 and the second distribution image after the specification of the calculation direction are displayed together. Next, in the second and subsequent Steps S114, with the flag indicating that the second distribution image has already been recalculated being set, the determination is No, and the processing proceeds to Step S104 without performing further recalculation.
(76) In other words, in
(77) Next, referring to
(78) As illustrated in
(79) Therefore, when the second distribution image 202 is hard to see in the lines D1 to D3 in
(80) The adjacent data elements from which the difference D is determined are not limited to such a data sequence along the horizontal axis of
(81) Differences of
(82) The processing in which the distribution image calculator 40a recalculates the second distribution image in the subtraction order specified by the subtraction order specification module 40d is similar to Step S110 to Step S120 (
(83) Moreover, as illustrated in
(84) In
(85) In
(86) Meanwhile, in
(87) The same applies to
(88) It can be seen that highness/lowness (lightness/darkness) is inverted between the differences +D and D, and that highness/lowness (lightness/darkness) is similarly inverted between the differences +D and D. Therefore, when the second distribution image is obtained by taking predetermined differences as required, more information can be acquired.
(89) In
(90) The present invention is not limited to the above-mentioned embodiment.
(91) For example, in the above-mentioned embodiment, the case in which the measurement data is the shape data has been described, but the measurement data may be another physical quantity that can be measured by a scanning probe microscope. Moreover, in the above-mentioned embodiment, the DFM measurement mode has been described, but the present invention may be applied to a contact mode, for example. For example, the present invention may be applied when a friction image is measured in the contact mode.
(92) Further, the present invention may also be applied to a lever scanning system in which the cantilever side of the scanning probe microscope is scanned for measurement.