Rayleigh scattering based distributed fiber sensors with optimized scattering coefficients
10663326 ยท 2020-05-26
Assignee
Inventors
Cpc classification
C03C2201/40
CHEMISTRY; METALLURGY
C03C2214/16
CHEMISTRY; METALLURGY
G02B6/02395
PHYSICS
C03B37/01433
CHEMISTRY; METALLURGY
C03C14/006
CHEMISTRY; METALLURGY
G01D5/3538
PHYSICS
C03B37/01838
CHEMISTRY; METALLURGY
G01D5/35361
PHYSICS
C03C3/06
CHEMISTRY; METALLURGY
C03B37/02718
CHEMISTRY; METALLURGY
International classification
C03C14/00
CHEMISTRY; METALLURGY
C03B37/014
CHEMISTRY; METALLURGY
C03C3/06
CHEMISTRY; METALLURGY
C03B37/025
CHEMISTRY; METALLURGY
C03B37/018
CHEMISTRY; METALLURGY
G01D5/353
PHYSICS
Abstract
A fiber sensor includes an optical fiber configured for operation at a wavelength from about 800 nm to about 1600 nm. The optical fiber includes a cladding that is defined by a fiber outer diameter and a core that is surrounded by the cladding. The core of the optical fiber has a Rayleigh scattering coefficient, .sub.s, that is controlled by controlling a concentration of one or more dopants in the core. The Rayleigh scattering coefficient is tuned to be within a predetermined range of an optimum Rayleigh scattering coefficient for a given total length, L, of the optical fiber. The predetermined range is from about 70% of the optimum .sub.s to about 130% of the optimum .sub.s.
Claims
1. A fiber sensor, comprising: an optical fiber configured for operation at a wavelength from about 800 nm to about 1600 nm, wherein the optical fiber comprises: a cladding that is defined by a fiber outer diameter; and a core that is surrounded by the cladding, wherein the core of the optical fiber has a Rayleigh scattering coefficient, .sub.s, that is tuned to be within a predetermined range of an optimum .sub.s for a given total length, L, of the optical fiber, wherein the optimum .sub.s value is given by:
2. The fiber sensor of claim 1, wherein the at least one dopant further comprises GeO.sub.2 at a concentration of at least about 20%.
3. The fiber sensor of claim 1, wherein the at least one dopant further comprises GeO.sub.2 at a concentration of at least about 30%.
4. The fiber sensor of claim 1, wherein the at least one dopant further comprises GeO.sub.2 at a concentration of at least about 40%.
5. The fiber sensor of claim 1, wherein the nanoparticles are doped into the core of the optical fiber at a concentration of at least 850/mm.sup.3.
6. The fiber sensor of claim 5, wherein the diameter of the nanoparticles is 100 nm.
7. The fiber sensor of claim 1, wherein the nanoparticles are doped into the core of the optical fiber at a concentration of at least 1880/mm.sup.3.
8. The fiber sensor of claim 7, wherein the diameter of the nanoparticles is 150 nm.
9. The fiber sensor of claim 1, wherein the nanoparticles are doped into the core of the optical fiber at a concentration of at least 1490/mm.sup.3.
10. The fiber sensor of claim 9, wherein the diameter of the nanoparticles is 175 nm.
11. The fiber sensor of claim 1, wherein the nanoparticles are doped into the core of the optical fiber at a concentration of at least 1350/mm.sup.3.
12. The fiber sensor of claim 11, wherein the diameter of the nanoparticles is 200 nm.
13. The fiber sensor of claim 1, wherein the optical fiber has a graded index profile.
14. The fiber sensor of claim 1, wherein the optical fiber has a step index profile.
15. The fiber sensor of claim 1, wherein the optical fiber has a total attenuation of 0.205 dB/km or less.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1)
(2)
(3)
(4)
(5)
(6)
(7)
DETAILED DESCRIPTION
(8) Reference will now be made in detail to the present preferred embodiments, examples of which are illustrated in the accompanying drawings. Whenever possible, the same reference numerals will be used throughout the drawings to refer to the same or like parts.
(9) An up-dopant is herein considered to be a dopant which has a propensity to raise the refractive index relative to pure undoped silica. A down-dopant is herein considered to be a dopant which has a propensity to lower the refractive index relative to pure undoped silica. Examples of up-dopants include GeO.sub.2, Al.sub.2O.sub.3, P.sub.2O.sub.5, TiO.sub.2, Cl, and Br. Further, the terms germania, Ge and GeO.sub.2 are used interchangeably herein and refer to GeO.sub.2. Examples of down-dopants include F and B. Further, the terms fluorine and F are used interchangeably to denote a fluorine dopant originating from a fluorine dopant precursor including, but not limited to, CF.sub.4, SiF.sub.4 and C.sub.2F.sub.6.
(10) Distributed fiber sensors and fiber sensor systems that employ optical fibers capable of transmitting optical signals with less signal loss and higher signal-to-noise ratios are outlined in exemplary fashion in the present disclosure. More particularly, this disclosure details distributed fiber sensors and sensor systems that employ fibers that rely on Rayleigh scattering mechanisms and are designed and controlled for predetermined sensing distances.
(11) As depicted in
(12) Referring to
(13) In a Rayleigh scattering based distributed sensing system, such as that shown in
P.sub.s=C.sub.slP.sub.0e.sup.2(.sup.
where P.sub.s is the power detected from Rayleigh scattering (e.g., the observed power 54), z is a location along the optical fiber 14 (e.g., the intermediate location 50), P.sub.0 is the launch power 46 into the optical fiber 14 at the first end 42 where the location is z=0, .sub.s is the Rayleigh scattering coefficient, .sub.0 is the loss coefficient due to factors other than Rayleigh scattering, and l is the pulse sensing segment that is related to the pulse width from the light source.
(14) The capture efficiency of an optical fiber, C, may be given by Equation (2a):
(15)
where NA is the numerical aperture of the core, n.sub.1 is the refractive index of the core, is a parameter that is dependent upon the type of core utilized in the fiber. For a multimode fiber with a step refractive index profile is typically about 0.38. For a multimode fiber with a graded refractive index profile is typically about 0.25. For a single mode optical fiber, the capture efficiency, C, may be rewritten as shown in Equation (2b):
(16)
where v.sub.g is the group velocity, n.sub.eff is the effective index, k.sub.0 is the wavenumber, and D.sub.MF is the mode field diameter.
(17) According to some embodiments, the condition under which the maximum Rayleigh scattering power is detected can be derived from Equation (1) and is given by Equation (3):
(18)
where L is the total length of the fiber and .sub.s has units of dB/km.
(19) Referring now to
(20) Table 1 below shows examples of Rayleigh scattering coefficients that provide an optimum backscatter power for various fiber sensor sensing lengths. Table 1 further includes ranges of sensing distances for 90% and 80% of the optimum backscattered power levels. As optimum backscatter values may not be necessary in some applications, the ranges of sensing distances that correspond to 90% and 80% of the optimum backscattered power levels may be used to aid in the selection of an appropriate Rayleigh scattering coefficient for a given application. While specific examples are set forth in Table 1 below, the present disclosure is not so limited.
(21) TABLE-US-00001 TABLE 1 90% of 80% of Optimum Optimum Optimum Rayleigh Power Power Power Scattering Fiber Core Properties Sensing Sensing Sensing Coefficient Nanoparticle Dopant Distance Distance Distance (dB/km) Dopant Diameter Concentration (km) (km) (km) 4.3 ZrO.sub.2 200 nm 1350/mm.sup.3 0.5 0.32-0.82 0.27-1.05 2.15 ZrO.sub.2 175 nm 1490/mm.sup.3 1 0.64-1.63 0.54-2.1 1.075 ZrO.sub.2 150 nm 1880/mm.sup.3 2 1.3-3.25 1.09-4.21 0.43 ZrO.sub.2 100 nm 850/mm.sup.3 5 3.2-8.2 2.7-10.5 0.35 GeO.sub.2 N/A 62.7% (w/w) 6 3.9-9.7 3.3-12.6 0.215 GeO.sub.2 N/A 24% (w/w) 10 6.4-16.3 5.4-21.sup. 0.143 Pure Silica N/A N/A 15 9.7-24.4 8.1-31.5 0.1075 Pure Silica N/A N/A 20 12.9-32.6 10.8-42
(22) The Rayleigh scattering coefficient of the optical fiber can be altered by various methods. These methods include, but are not limited to, changing the dopant used, changing the concentration of the dopant used, altering processing conditions for the optical fiber, utilizing more than one dopant (e.g., co-doping), increasing the cooling rate of the optical fiber during the drawing of the optical fiber in the manufacturing process, and combinations thereof. Suitable dopants include, but are not limited to, germanium, fluorine, aluminum, tantalum, and nanoparticles. For germanium-doped optical fibers, increasing the concentration of germanium in the core increases the Rayleigh scattering coefficient. For optical fibers with high Rayleigh scattering coefficients, the germanium concentration is preferably greater than about 20%. For optical fibers with high Rayleigh scattering coefficients, the germanium concentration is more preferably greater than about 30%. For optical fibers with high Rayleigh scattering coefficients, the germanium concentration is most preferably greater than about 40%.
(23) The type of dopant used may dictate at what point in the manufacturing process the dopant is added. For example, oxidizable dopants, such as germanium, are typically added to the process during the deposition of the soot layer. More specifically, in an outside vapor deposition (OVD) process, the dopant gas and oxygen may be flowed to a natural gas burner or hydrogen-oxygen burner. As the dopant gas flows through the burner the dopant gas reacts with oxygen under the heat of the burner by forming solid particles that are commonly referred to as soot. The soot may be alternatively referred to as a low-density glass. The soot is deposited onto a ceramic target to form a soot preform. The soot preform is dried with Cl.sub.2 gas at an elevated temperature (e.g., 1100 C.) in a consolidation furnace to remove water from the soot. Once dried, the soot preform is consolidated into transparent glass at a consolidation temperature (e.g., 1450 C.) while exposed to a Helium atmosphere. Non-oxidizable dopants, such as chlorine and fluorine, may be added during the consolidation step. More specifically, the non-oxidizable dopant may be flowed into the preform as a gas and as the soot is exposed to the heat provided by the furnace in the consolidation step the non-oxidizable dopant reacts with the soot and is incorporated into the glass structure formed by the consolidation of the soot.
(24) Dopants may be incorporated into the soot preform using processes other than the OVD process discussed above. For example, dopants may be incorporated into the preform by vapor axial deposition (VAD), modified chemical vapor deposition (MCVD), or plasma chemical vapor deposition (PCVD). In embodiments that utilize nanoparticles, the nanoparticles may be incorporated using a solution doping process. In the solution doping process, a soot preform is prepared, for example by the OVD process. Then the soot preform is submerged in a solution that contains the nanoparticles and the nanoparticles diffuse into the preform. Once the nanoparticles have diffused into the soot preform, the soot preform is dried and consolidated into a glass preform. An alternative approach to the solution doping process for incorporation of the nanoparticles into the soot preform is to utilize a soot pressing process. In the soot pressing process soot powders are mixed uniformly with nanoparticles. Then, the soot and nanoparticle mixture is placed into a cylindrical mod and pressed together under pressure to form a soot preform that is doped with nanoparticles. Next, the soot preform is dried and consolidated into a glass preform. Once the preform is completed, regardless of the process used to achieve the preform, the preform can be drawn into a fiber using a fiber drawing tower. As the fiber is drawn on the drawing tower, the Rayleigh scattering coefficient can be controlled further by altering the cooling rate during the fiber drawing process. The cooling rate can be used to further control the Rayleigh scattering coefficient because the Rayleigh scattering coefficient is proportional to the fictive temperature at which the glass structure is frozen or set during the drawing process. For example, a rapid cooling rate increases the fictive temperature and results in a proportional increase in the Rayleigh scattering coefficient.
(25) Referring to
(26) Referring now to
(27) As described in Equations 1-2b, the observed power is proportional to the Rayleigh scattering coefficient and the capture efficiency, C. The capture efficiency is inversely proportional to the square of the mode field diameter. As shown in
(28) Referring to
(29) The signal level of the OTDR traces is directly proportional to the Rayleigh scattering coefficient and inversely proportional to the square of the mode field diameter for the associated optical fiber. The slope of the OTDR traces is proportional to the total attenuation coefficient of the associated fiber. Fiber 5 has the smallest mode field diameter and highest Rayleigh scattering coefficient of Fibers 5-7. The OTDR trace of Fiber 5 shows the greatest Rayleigh backscattered signal level of Fibers 5-7. Fiber 6 has a larger mode field diameter and lower Rayleigh scattering coefficient compared with Fiber 5. Fiber 6 has a corresponding intermediate OTDR trace with a backscattered signal level lower than that of Fiber 5. Fiber 7 has the same mode field diameter as Fiber 6 and the lowest Rayleigh scattering coefficient of Fibers 5-7. The OTDR trace of Fiber 7 has the lowest backscattered signal level. The slope of the OTDR trace corresponds to the total attenuation of the associated fiber. In
(30) In embodiments of the foregoing aspects, the optical fiber may be a single mode fiber or a multimode fiber. The optical fiber may be configured for operation at or around wavelengths within a range from about 800 nm to about 1600 nm. It is contemplated that the optical fiber may be configured for operation at a wavelength or range of wavelengths that corresponds to a desired light source. For example, the optical fiber may be configured for operation at any wavelength that falls within the range of about 800 nm to about 1600 nm. The optical fiber may be configured for operation at any range of wavelengths that falls within the range of about 800 nm to about 1600 nm. For example, the optical fiber may be configured for operation in a wavelength range that is from about 825 nm to about 875 nm. The optical fiber may be configured for operation in a wavelength range that is from about 980 nm to about 1060 nm. The optical fiber may be configured for operation in a wavelength range that is from about 1275 nm to about 1325 nm. The optical fiber may be configured for operation in a wavelength range that is from about 1525 nm to about 1575 nm. The optical fiber may be configured for operation at a combination of wavelength ranges and/or wavelengths that fall within the range of about 800 nm to about 1600 nm.
(31) In some embodiments of the foregoing aspects, the core of the optical fiber has a Rayleigh scattering coefficient, .sub.s, that is tuned to be within a predetermined range of an optimum .sub.s value. The optimum .sub.s value is tuned for a given total length, L, of the optical fiber. The predetermined range of the optimum .sub.s value may be from about 70% of the optimum .sub.s value to about 130% of the optimum .sub.s value. The predetermined range of the optimum .sub.s value may be from about 75% of the optimum .sub.s value to about 125% of the optimum .sub.s value. The predetermined range of the optimum .sub.s value may be from about 80% of the optimum .sub.s value to about 120% of the optimum .sub.s value. The predetermined range of the optimum .sub.s value may be from about 85% of the optimum .sub.s value to about 115% of the optimum .sub.s value. The predetermined range of the optimum .sub.s value may be from about 90% of the optimum .sub.s value to about 110% of the optimum .sub.s value. The predetermined range of the optimum .sub.s value may be from about 95% of the optimum .sub.s value to about 105% of the optimum .sub.s value.
(32) In embodiments of the foregoing aspects, the optical fiber may be doped with a first dopant. The first dopant may be GeO.sub.2. The concentration of the first dopant may be at least about 10%. The concentration of the first dopant may be at least about 20%. The concentration of the first dopant may be at least about 30%. The concentration of the first dopant may be at least about 40%. The concentration of the first dopant may be at least about 50%. The concentration of the first dopant may be at least about 60%. The concentration of the first dopant may be at least about 70%. The concentration of the first dopant may be at least about 80%.
(33) The optical fibers may be additionally or alternatively doped with a second dopant. The second dopant may be nanoparticles for increasing the Rayleigh scattering coefficient. The optical fibers may be doped with nanoparticles in the silica core and a low index dopant in the cladding. The nanoparticles may have a diameter of less than 300 nm. The nanoparticles may have a diameter of less than 275 nm. The nanoparticles may have a diameter of less than 250 nm. The nanoparticles may have a diameter of less than 225 nm. The nanoparticles may have a diameter of less than 200 nm. The nanoparticles may have a diameter of less than 175 nm. The nanoparticles may have a diameter of less than 150 nm. The nanoparticles may have a diameter of less than 125 nm. The nanoparticles may have a diameter of less than 100 nm. The nanoparticles may have a diameter of less than 75 nm. The nanoparticles may have a diameter of less than 50 nm. The nanoparticles may have a diameter of less than 25 nm. The concentration of nanoparticles may be at least about 800/mm.sup.3. The concentration of nanoparticles may be at least about 850/mm.sup.3. The concentration of nanoparticles may be at least about 900/mm.sup.3. The concentration of nanoparticles may be at least about 950/mm.sup.3. The concentration of nanoparticles may be at least about 1000/mm.sup.3. The concentration of nanoparticles may be at least about 1050/mm.sup.3. The concentration of nanoparticles may be at least about 1100/mm.sup.3. The concentration of nanoparticles may be at least about 1150/mm.sup.3. The concentration of nanoparticles may be at least about 1200/mm.sup.3. The concentration of nanoparticles may be at least about 1250/mm.sup.3. The concentration of nanoparticles may be at least about 1300/mm.sup.3. The concentration of nanoparticles may be at least about 1350/mm.sup.3. The concentration of nanoparticles may be at least about 1400/mm.sup.3. The concentration of nanoparticles may be at least about 1450/mm.sup.3. The concentration of nanoparticles may be at least about 1500/mm.sup.3. The concentration of nanoparticles may be at least about 1550/mm.sup.3. The concentration of nanoparticles may be at least about 1600/mm.sup.3. The concentration of nanoparticles may be at least about 1650/mm.sup.3. The concentration of nanoparticles may be at least about 1700/mm.sup.3. The concentration of nanoparticles may be at least about 1750/mm.sup.3. The concentration of nanoparticles may be at least about 1800/mm.sup.3. The concentration of nanoparticles may be at least about 1850/mm.sup.3. The concentration of nanoparticles may be at least about 1900/mm.sup.3.
(34) In some embodiments it may be beneficial to utilize undoped optical fibers. For example, in applications that seek to utilize fiber sensors that are capable of sensing long distances, such as distances greater than 15 km, it may be beneficial to utilize an optical fiber that is pure silica as the fiber sensor.
(35) The optical fibers and fiber sensors disclosed herein may be formed by various processes. These processes include, but are not limited to, a chemical vapor deposition process, such as outside vapor deposition (OVD), vapor axial deposition (VAD), modified chemical vapor deposition (MCVD, plasma chemical vapor deposition (PCVD), or combinations thereof.
(36) It will be apparent to those skilled in the art that various modifications and variations can be made without departing from the spirit or scope of the claims.