Liquid-crystalline medium

Abstract

Compounds of the formula I ##STR00001## in which R.sup.1 is alkyl or alkoxy in which CH.sub.2 groups are optionally replaced, and X.sup.1 is alkyl OCF.sub.3, CF.sub.3, CHF.sub.2, OCF.sub.2CF.sub.3, CCF.sub.2CHFCF.sub.3, OCFCF.sub.2, OCHCF.sub.2 or F, a liquid-crystalline medium containing a compound of formula I, and use thereof in electro-optical liquid-crystal displays, in particular in TN, STN, TN-TFT, OCB, IPS, PS-IPS, FFS, HB-FFS or PS-FFS-, positive VA displays and in shutter spectacles for 3D effects and LC lenses.

Claims

1. Shutter spectacles having 3D effects, LC lenses or positive VA displays containing in said shutter spectacles, LC lenses or positive VA displays, a nematic liquid-crystalline medium, comprising in said nematic liquid-crystalline medium: one or more compounds of formula I, ##STR00434## in which R.sup.1 denotes a straight-chain alkyl radical having 3 to 5 C atoms, and X.sup.1 denotes CF.sub.3; and further comprising: one or more compounds of formulae II and/or III, ##STR00435## in which A denotes 1,4-phenylene or trans-1,4-cyclohexylene, a denotes 0 or 1, R.sup.3 denotes alkenyl having 2 to 9 C atoms, and R.sup.4 denotes an alkyl radical having 1 to 15 C atoms, wherein at least one CH.sub.2 group is replaced by CHCH, and optionally one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00436## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, or C.sub.1-15 alkyl in which one or more CH.sub.2 group is replaced, independently of one another, by ##STR00437## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen; or one or more compounds of formulae X and/or XI, ##STR00438## in which ##STR00439## each, independently of one another, denote ##STR00440## R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00441## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, and Y.sup.1-4 each, independently of one another, denote H or F; or one or more compounds of formulae D1, D2, D3, D4 or D5, ##STR00442## in which R.sup.0, X.sup.0 and Y.sup.1-Y.sup.2 independently have one of the meanings as defined above; or one or more compounds of formulae Y-1, Y-2, Y-3 or Y-4, ##STR00443## in which R.sup.2A denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00444## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, L.sup.1 and L.sup.2 each, independently of one another, denote F, Cl, CF.sub.3 or CHF.sub.2, Z.sup.2 and Z.sup.2 each, independently of one another, denote a single bond, CH.sub.2CH.sub.2, CHCH, CF.sub.2O, OCF.sub.2, CH.sub.2O, OCH.sub.2, COO, OCO, C.sub.2F.sub.4, CFCF or CHCHCH.sub.2O, p denotes 0, 1 or 2, q denotes 0 or 1, (O)C.sub.vH.sub.2v+1 denotes OC.sub.vH.sub.2v+1 or C.sub.vH.sub.2v+1, and v denotes 1 to 6; or one or more compounds of formulae CR, PH-1, PH-2, or BS, ##STR00445## in which R.sup.B1, R.sup.B2, R.sup.CR1, R.sup.CR2, R.sup.1 and R.sup.2 each, independently of one another, denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00446## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, and c denotes 0, 1 or 2.

2. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises one or more compounds of formulae II and/or III.

3. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 2, wherein the liquid crystalline medium comprises one or more compounds of the following formulae, ##STR00447## ##STR00448## in which R.sup.3a and R.sup.4a each, independently of one another, denote H, CH.sub.3, C.sub.2H.sub.5 or C.sub.3H.sub.7, and alkyl denotes a straight-chain alkyl group having 1 to 8 C atoms.

4. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more compounds of formulae IV to VIII, ##STR00449## in which R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00450## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, Y.sup.1-6 each, independently of one another, denote H or F, Z.sup.0 denotes C.sub.2H.sub.4, (CH.sub.2).sub.4, CHCH, CFCF, C.sub.2F.sub.4, CH.sub.2CF.sub.2, CF.sub.2CH.sub.2, CH.sub.2O, OCH.sub.2, COO, CF.sub.2O or OCF.sub.2, in the formulae V and VI also a single bond, and r denotes 0 or 1.

5. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 4, wherein the liquid crystalline medium comprises one or more compounds of formula V which is selected from compounds of the formulae Va to Vj, ##STR00451## ##STR00452##

6. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 4, wherein the liquid crystalline medium comprises one or more compounds of formula VI which are selected from compounds of the formulae VI-1a to VI-1d, ##STR00453##

7. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 4, wherein the liquid crystalline medium comprises one or more compounds of formula VI which are selected from compounds of the formulae VI-2a to VI-2f, ##STR00454##

8. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 4, wherein the liquid crystalline medium comprises one or more compounds of formulae X and/or XI.

9. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more compounds of formula XII, ##STR00455## in which R.sup.1 and R.sup.2 each, independently of one another, denote C.sub.1-9-alkyl, C.sub.2-9-alkenyl, C.sub.1-9-alkoxy, C.sub.1-9-oxaalkyl, C.sub.1-9-fluoroalkyl or C.sub.2-9-alkenyloxy.

10. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 4, wherein the liquid crystalline medium additionally comprises one or more compounds of formulae XIII to XVI, ##STR00456## in which R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00457## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, and Y.sup.1-2 each, independently of one another, denote H or F.

11. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more compounds of formulae ##STR00458##

12. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises one or more compounds of formulae D1, D2, D3, D4 or D5.

13. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises one or more compounds of formulae Y-1, Y-2, Y-3 or Y-4.

14. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises one or more compounds of formulae BC, CR, PH-1, PH-2, BF or BS.

15. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises 1-30% by weight of compounds of the formula I.

16. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more UV stabilizers and/or antioxidants.

17. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more polymerizable compounds.

18. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein in the liquid crystalline medium R1 is propyl.

19. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the medium has a rotational viscosity, .sub.1, of <120 mPa.Math.s.

20. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium comprises one or more compounds of formulae X and/or XI.

21. The shutter spectacles having 3D effects, LC lenses or positive VA displays according to claim 1, wherein the liquid crystalline medium additionally comprises one or more compounds of formulae XIII to XVI, ##STR00459## in which R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00460## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, and Y.sup.1-2 each, independently of one another, denote H or F.

22. Shutter spectacles having 3D effects, LC lenses or positive VA displays, comprising in said shutter spectacles, LC lenses or positive VA displays a nematic liquid-crystalline medium, comprising in said nematic liquid-crystalline medium: one or more compounds of formula I, ##STR00461## in which R.sup.1 denotes a straight-chain alkyl radical having 3 to 5 C atoms, and X.sup.1 denotes CF.sub.3; and further comprising: one or more compounds of formulae II and/or III, ##STR00462## in which A denotes 1,4-phenylene or trans-1,4-cyclohexylene, a denotes 0 or 1, R.sup.3 denotes alkenyl having 2 to 9 C atoms, and R.sup.4 denotes an alkyl radical having 1 to 15 C atoms, wherein at least one CH.sub.2 group is replaced by CHCH, and optionally one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00463## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, or C.sub.1-15 alkyl in which one or more CH.sub.2 group is replaced, independently of one another, by ##STR00464## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen; or one or more compounds of formulae X and/or XI, ##STR00465## in which ##STR00466## each, independently of one another, denote ##STR00467## R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00468## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, and Y.sup.1-4 each, independently of one another, denote H or F; or one or more compounds of formulae D1, D2, D3, D4 or D5, ##STR00469## in which R.sup.0, X.sup.0 and Y.sup.1-Y.sup.2 independently have one of the meanings as defined above; or one or more compounds of formulae Y-1, Y-2, Y-3 or Y-4, ##STR00470## in which R.sup.2A denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00471## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, L.sup.1 and L.sup.2 each, independently of one another, denote F, Cl, CF.sub.3 or CHF.sub.2, Z.sup.2 and Z.sup.2 each, independently of one another, denote a single bond, CH.sub.2CH.sub.2, CHCH, CF.sub.2O, OCF.sub.2, CH.sub.2O, OCH.sub.2, COO, OCO, C.sub.2F.sub.4, CFCF or CHCHCH.sub.2O, p denotes 0, 1 or 2, q denotes 0 or 1, (O)C.sub.vH.sub.2v+1 denotes OC.sub.vH.sub.2v+1 or C.sub.vH.sub.2v+1, and v denotes 1 to 6; or one or more compounds of formula BS ##STR00472## in which R.sup.1 and R.sup.2 each, independently of one another, denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00473## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, and c denotes 0, 1 or 2.

23. Shutter spectacles having 3D effects, LC lenses or positive VA displays, comprising in said shutter spectacles, LC lenses or positive VA displays, a nematic liquid-crystalline medium, comprising in said nematic liquid-crystalline medium: one or more compounds of formula CLP-n-T, ##STR00474## in which n is 3, and further comprising: one or more compounds of formulae II and/or III, ##STR00475## in which A denotes 1,4-phenylene or trans-1,4-cyclohexylene, a denotes 0 or 1, R.sup.3 denotes alkenyl having 2 to 9 C atoms, and R.sup.4 denotes an alkyl radical having 1 to 15 C atoms, wherein at least one CH.sub.2 group is replaced by CHCH, and optionally one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00476## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, or C.sub.1-15 alkyl in which one or more CH.sub.2 group is replaced, independently of one another, by ##STR00477## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen; or one or more compounds of formulae X and/or XI, ##STR00478## in which ##STR00479## each, independently of one another, denote ##STR00480## R.sup.0 denotes an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00481## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, cycloalkyl with 3 to 6 C atoms, X.sup.0 denotes F, Cl, a mono- or polyfluorinated alkyl or alkoxy radical having 1 to 6 C atoms, a mono- or polyfluorinated alkenyl or alkenyloxy radical having 2 to 6 C atoms, and Y.sup.1-4 each, independently of one another, denote H or F; or one or more compounds of formulae D1, D2, D3, D4 or D5, ##STR00482## in which R.sup.0, X.sup.0 and Y.sup.1-Y.sup.2 independently have one of the meanings as defined above; or one or more compounds of formulae Y-1, Y-2, Y-3 or Y-4, ##STR00483## in which R.sup.2A denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00484## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, L.sup.1 and L.sup.2 each, independently of one another, denote F, Cl, CF.sub.3, or CHF.sub.2, Z.sup.2 and Z.sup.2 each, independently of one another, denote a single bond, CH.sub.2CH.sub.2, CHCH, CF.sub.2O, OCF.sub.2, CH.sub.2O, OCH.sub.2, COO, OCO, C.sub.2F.sub.4, CFCF or CHCHCH.sub.2O, p denotes 0, 1 or 2, q denotes 0 or 1, (O)C.sub.vH.sub.2v+1 denotes OC.sub.vH.sub.2v+1 or C.sub.vH.sub.2v+1, and v denotes 1 to 6; or one or more compounds of formula BS ##STR00485## in which R.sup.1 and R.sup.2 each, independently of one another, denotes H, an alkyl or alkoxy radical having 1 to 15 C atoms, where, in addition, one or more CH.sub.2 groups in these radicals may each be replaced, independently of one another, by ##STR00486## in such a way that O atoms are not linked directly to one another, and in which, in addition, one or more H atoms may be replaced by halogen, and c denotes 0, 1 or 2.

Description

EXAMPLES

(1) m.p. denotes melting point, cl.p.=clearing point. Furthermore, C=crystalline state, N=nematic phase, S=smectic phase and I=isotropic phase. The data between these symbols represent the transition temperatures. Furthermore, V.sub.o denotes threshold voltage, capacitive [V] at 20 C. n denotes the optical anisotropy measured at 20 C. and 589 nm denotes the dielectric anisotropy at 20 C. and 1 kHz cp. denotes clearing point [ C.] K.sub.1 denotes elastic constant, splay deformation at 20 C., [pN] K.sub.3 denotes elastic constant, bend deformation at 20 C., [pN] .sub.1 denotes rotational viscosity measured at 20 C. [mPa.Math.s], determined by the transient current method in a electric field LTS denotes low-temperature stability (nematic phase), determined in glass vials.

Mixture Examples

(2) The electro-optical data are measured in a TN cell at the 1st minimum (i.e. at a d.Math.n value of 0.5 m) at 20 C., unless expressly indicated otherwise. The optical data are measured at 20 C., unless expressly indicated otherwise. All physical properties are determined in accordance with Merck Liquid Crystals, Physical Properties of Liquid Crystals Status November 1997, Merck KGaA, Germany, and apply for a temperature of 20 C., unless explicitly indicated otherwise.

Example M1

(3) TABLE-US-00009 CC-3-V 51.50% Clearing point [ C.]: 74 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1175 CCP-V-1 5.50% [1 kHz, 20 C.]: 2.2 CLP-3-T 4.50% .sub.|| [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.50% .sub.1 [mPa .Math. s, 20 C.]: 45 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 14.1 PGU-2-F 4.00% K.sub.3 [pN, 20 C.]: 13.7 PGUQU-3-F 3.00% LTS [bulk, 20 C.]: >1000 h PP-1-2V1 6.00% PPGU-3-F 1.00%

Example M2

(4) TABLE-US-00010 CC-3-V 51.50% Clearing point [ C.]: 73.5 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1174 CCP-V-1 6.00% [1 kHz, 20 C.]: 2.2 CLP-3-T 3.50% .sub.|| [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.50% .sub.1 [mPa .Math. s, 20 C.]: 44 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 13.9 PGU-2-F 4.50% K.sub.3 [pN, 20 C.]: 13.6 PGUQU-3-F 3.00% LTS [bulk, 20 C.]: >1000 h PP-1-2V1 6.00% PPGU-3-F 1.00%

Example M3

(5) TABLE-US-00011 CC-3-V 53.00% Clearing point [ C.]: 73.5 CC-3-V1 3.00% n [589 nm, 20 C.]: 0.1170 CCP-V-1 7.00% [1 kHz, 20 C.]: 2.2 CLP-3-T 3.00% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.50% .sub.1 [mPa .Math. s, 20 C.]: 43 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 13.7 PGU-2-F 5.00% K.sub.3 [pN, 20 C.]: 13.5 PGUQU-3-F 3.00% PP-1-2V1 5.50% PPGU-3-F 1.00%

Example M4

(6) TABLE-US-00012 CC-3-V 51.50% Clearing point [ C.]: 74 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1182 CCP-V-1 5.00% [1 kHz, 20 C.]: 2.2 CLP-3-T 4.50% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 45 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 14.2 PGU-2-F 4.00% K.sub.3 [pN, 20 C.]: 13.7 PGUQU-3-F 3.00% PP-1-2V1 6.00% PPGU-3-F 1.00%

Example M5

(7) TABLE-US-00013 CC-3-V 26.00% Clearing point [ C.]: 105 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1192 CC-3-2V1 9.00% [1 kHz, 20 C.]: 5.2 CCP-V-1 11.00% .sub. [1 kHz, 20 C.]: 8.0 CCP-V2-1 8.00% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 5.50% .sub.1 [mPa .Math. s, 20 C.]: 86 PGP-2-3 2.50% K.sub.1 [pN, 20 C.]: 19.6 PGP-2-2V 10.00% K.sub.3 [pN, 20 C.]: 19.2 APUQU-3-F 6.50% PGUQU-3-F 2.50% PGUQU-4-F 6.00% CPGU-3-OT 3.00%

Example M6

(8) TABLE-US-00014 CC-3-V 28.00% Clearing point [ C.]: 102 CC-3-V1 9.00% n [589 nm, 20 C.]: 0.1184 CC-3-2V1 9.00% [1 kHz, 20 C.]: 5.2 CCP-V-1 12.00% .sub. [1 kHz, 20 C.]: 8.0 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 6.00% .sub.1 [mPa .Math. s, 20 C.]: 83 PGP-2-3 2.50% K.sub.1 [pN, 20 C.]: 19.0 PGP-2-2V 10.00% K.sub.3 [pN, 20 C.]: 18.7 APUQU-3-F 6.00% LTS [bulk, 20 C.]: >1000 h PGUQU-3-F 3.50% PGUQU-4-F 6.00% CPGU-3-OT 2.00%

Example M7

(9) TABLE-US-00015 CC-3-V 28.00% Clearing point [ C.]: 101 CC-3-V1 9.50% n [589 nm, 20 C.]: 0.1176 CC-3-2V1 9.00% [1 kHz, 20 C.]: 5.2 CCP-V-1 12.00% .sub. [1 kHz, 20 C.]: 8.0 CCP-V2-1 5.50% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 6.50% .sub.1 [mPa .Math. s, 20 C.]: 81 PGP-2V 12.50% K.sub.1 [pN, 20 C.]: 18.7 APUQU-3-F 5.50% K.sub.3 [pN, 20 C.]: 18.5 PGUQU-3-F 4.00% PGUQU-4-F 6.50% CPGU-3-OT 1.00%

Example M8

(10) TABLE-US-00016 CC-3-V 28.00% Clearing point [ C.]: 100 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1181 CC-3-2V1 8.50% [1 kHz, 20 C.]: 5.2 CCP-V-1 12.00% .sub. [1 kHz, 20 C.]: 8.0 CCP-V2-1 5.50% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 6.50% .sub.1 [mPa .Math. s, 20 C.]: 80 PGP-2-2V 13.00% K.sub.1 [pN, 20 C.]: 18.6 APUQU-3-F 5.50% K.sub.3 [pN, 20 C.]: 18.6 PGUQU-3-F 5.00% PGUQU-4-F 6.00%

Example M9

(11) TABLE-US-00017 CC-3-V 28.00% Clearing point [ C.]: 100.5 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1184 CC-3-2V1 9.00% [1 kHz, 20 C.]: 5.2 CCP-V-1 11.50% .sub. [1 kHz, 20 C.]: 8.0 CCP-V2-1 4.50% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 7.50% .sub.1 [mPa .Math. s, 20 C.]: 81 PGP-2-2V 13.00% K.sub.1 [pN, 20 C.]: 19.1 APUQU-3-F 5.50% K.sub.3 [pN, 20 C.]: 18.7 PGUQU-3-F 4.00% PGUQU-4-F 6.00% CPGU-3-OT 1.00%

Example M10

(12) TABLE-US-00018 APUQU-2-F 6.00% Clearing point [ C.]: 80 APUQU-3-F 4.00% n [589 nm, 20 C.]: 0.1009 CC-3-V 41.00% [1 kHz, 20 C.]: 9.5 CC-3-V1 10.50% .sub. [1 kHz, 20 C.]: 12.7 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 3.2 CCP-3OCF.sub.3 4.50% .sub.1 [mPa .Math. s, 20 C.]: 69 CCP-V-1 6.00% K.sub.1 [pN, 20 C.]: 13.5 PGUQU-3-F 6.00% K.sub.3 [pN, 20 C.]: 15.8 PGUQU-4-F 6.00% PGUQU-5-F 6.00% PUQU-3-F 3.00%

Example M11

(13) TABLE-US-00019 APUQU-2-F 6.00% Clearing point [ C.]: 79.5 APUQU-3-F 4.00% n [589 nm, 20 C.]: 0.1006 CC-3-V 44.00% [1 kHz, 20 C.]: 9.4 CC-3-V1 6.50% .sub. [1 kHz, 20 C.]: 12.6 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 3.2 CCP-3OCF.sub.3 4.50% .sub.1 [mPa .Math. s, 20 C.]: 68 CCP-V-1 7.00% K.sub.1 [pN, 20 C.]: 13.2 PGUQU-3-F 6.00% K.sub.3 [pN, 20 C.]: 15.4 PGUQU-4-F 6.00% PGUQU-5-F 6.00% PUQU-3-F 3.00%

Example M12

(14) TABLE-US-00020 APUQU-2-F 7.00% Clearing point [ C.]: 83.5 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1014 CC-3-V 42.00% [1 kHz, 20 C.]: 9.5 CC-3-V1 9.00% .sub. [1 kHz, 20 C.]: 12.7 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 3.2 CCP-3OCF.sub.3 5.00% .sub.1 [mPa .Math. s, 20 C.]: 72 CCP-V-1 7.00% K.sub.1 [pN, 20 C.]: 13.8 PGUQU-3-F 7.00% K.sub.3 [pN, 20 C.]: 16.0 PGUQU-4-F 6.00% PGUQU-5-F 6.00%

Example M13

(15) TABLE-US-00021 APUQU-2-F 6.00% Clearing point [ C.]: 83.5 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1014 CC-3-V 40.50% [1 kHz, 20 C.]: 9.5 CC-3-V1 8.00% .sub. [1 kHz, 20 C.]: 12.6 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 3.2 CCP-3OCF.sub.3 5.00% .sub.1 [mPa .Math. s, 20 C.]: 73 CCP-V-1 9.00% K.sub.1 [pN, 20 C.]: 13.8 PGUQU-3-F 6.00% K.sub.3 [pN, 20 C.]: 16.0 PGUQU-4-F 6.00% PGUQU-5-F 5.00% PUQU-3-F 2.50%

Example M14

(16) TABLE-US-00022 APUQU-2-F 7.00% Clearing point [ C.]: 83.5 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1019 CC-3-V 42.00% [1 kHz, 20 C.]: 9.5 CC-3-V1 9.00% .sub. [1 kHz, 20 C.]: 12.7 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 3.2 CCP-3OCF3 5.00% .sub.1 [mPa .Math. s, 20 C.]: 72 CCP-V-1 6.50% K.sub.1 [pN, 20 C.]: 14.0 PGUQU-3-F 7.00% K.sub.3 [pN, 20 C.]: 15.7 PGUQU-4-F 6.00% PGUQU-5-F 5.50%

Example M15

(17) TABLE-US-00023 CC-3-V 28.50% Clearing point [ C.]: 94 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1057 CC-3-2V1 6.00% [1 kHz, 20 C.]: 17.6 CCP-V-1 6.00% .sub. [1 kHz, 20 C.]: 21.5 CLP-3-T 5.50% .sub. [1 kHz, 20 C.]: 3.9 APUQU-2-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 111 APUQU-3-F 9.00% K.sub.1 [pN, 20 C.]: 16.0 PGUQU-3-F 3.50% K.sub.3 [pN, 20 C.]: 16.7 CDUQU-3-F 7.50% DPGU-4-F 6.00% DGUQU-4-F 8.00% DGUQU-2-F 3.00% PGU-4-T 1.00%

Example M16

(18) TABLE-US-00024 CC-3-V 29.00% Clearing point [ C.]: 94.5 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1040 CC-3-2V1 6.00% [1 kHz, 20 C.]: 17.2 CCP-V-1 6.00% .sub. [1 kHz, 20 C.]: 21.1 CLP-3-T 5.50% .sub. [1 kHz, 20 C.]: 3.9 APUQU-2-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 108 APUQU-3-F 9.00% K.sub.1 [pN, 20 C.]: 15.9 PGUQU-3-F 3.50% K.sub.3 [pN, 20 C.]: 16.9 CDUQU-3-F 8.00% DPGU-4-F 6.00% DGUQU-4-F 8.00% DGUQU-2-F 3.00%

Example M17

(19) TABLE-US-00025 CC-3-V 29.00% Clearing point [ C.]: 93.5 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1040 CC-3-2V1 6.00% [1 kHz, 20 C.]: 17.1 CCP-V-1 5.00% .sub. [1 kHz, 20 C.]: 20.9 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 3.8 APUQU-2-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 110 APUQU-3-F 9.00% K.sub.1 [pN, 20 C.]: 16.2 PGUQU-3-F 4.00% K.sub.3 [pN, 20 C.]: 16.6 CDUQU-3-F 8.00% DPGU-4-F 5.00% DGUQU-4-F 8.00% DGUQU-2-F 3.00%

Example M18

(20) TABLE-US-00026 CC-3-V 50.00% Clearing point [ C.]: 77.5 CC-3-V1 2.00% n [589 nm, 20 C.]: 0.1172 CLP-3-OT 7.50% [1 kHz, 20 C.]: 2.3 CLP-3-T 11.00% .sub. [1 kHz, 20 C.]: 4.8 PGP-1-2V 2.00% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 16.00% .sub.1 [mPa .Math. s, 20 C.]: 48 PGP-3-2V 1.00% K.sub.1 [pN, 20 C.]: 17.3 PGU-2-F 2.50% K.sub.3 [pN, 20 C.]: 14.4 PP-1-2V1 8.00%

Example M19

(21) TABLE-US-00027 CC-3-V 51.50% Clearing point [ C.]: 75 CC-3-V1 4.00% n [589 nm, 20 C.]: 0.1175 CLP-3-OT 6.00% [1 kHz, 20 C.]: 2.3 CLP-3-T 7.00% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 2.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 17.00% .sub.1 [mPa .Math. s, 20 C.]: 46 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 15.6 PGU-2-F 5.50% K.sub.3 [pN, 20 C.]: 13.6 PP-1-2V1 5.00%

Example M20

(22) TABLE-US-00028 CC-3-V 53.50% Clearing point [ C.]: 75 CC-3-V1 3.50% n [589 nm, 20 C.]: 0.1188 CLP-3-OT 7.00% [1 kHz, 20 C.]: 2.3 CLP-3-T 3.00% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 2.50% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.00% .sub.1 [mPa .Math. s, 20 C.]: 44 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 14.5 PGU-2-F 5.00% K.sub.3 [pN, 20 C.]: 13.8 PGUQU-3-F 3.00% PP-1-2V1 5.50% PPGU-3-F 1.00%

Example M21

(23) TABLE-US-00029 CC-3-V 28.50% Clearing point [ C.]: 98.5 CC-3-V1 10.00% n [589 nm, 20 C.]: 0.1183 CC-3-2V1 10.00% [1 kHz, 20 C.]: 5.2 CLP-V-1 11.50% .sub. [1 kHz, 20 C.]: 7.9 CCP-V-1 7.50% .sub. [1 kHz, 20 C.]: 2.7 CLP-3-T 7.00% .sub.1 [mPa .Math. s, 20 C.]: 77 PGP-2-2V 8.00% K.sub.1 [pN, 20 C.]: 19.6 PGU-2-F 4.00% K.sub.3 [pN, 20 C.]: 18.2 PGUQU-3-F 6.00% PGUQU-4-F 6.00% CPGU-3-OT 1.50%

Example M22

(24) TABLE-US-00030 CC-3-V 28.50% Clearing point [ C.]: 98 CC-3-V1 11.00% n [589 nm, 20 C.]: 0.1179 CC-3-2V1 9.00% [1 kHz, 20 C.]: 5.1 CLP-V-1 11.50% .sub. [1 kHz, 20 C.]: 7.9 CCP-V-1 8.00% .sub. [1 kHz, 20 C.]: 2.8 CLP-3-T 7.00% .sub.1 [mPa .Math. s, 20 C.]: 76 PGP-2-2V 7.50% K.sub.1 [pN, 20 C.]: 19.3 PGU-2-F 4.50% K.sub.3 [pN, 20 C.]: 18.4 PGUQU-3-F 6.00% PGUQU-4-F 6.00% CPGU-3-OT 1.00%

Example M23

(25) TABLE-US-00031 CC-3-V 33.00% Clearing point [ C.]: 92 CC-3-V1 7.00% n [589 nm, 20 C.]: 0.1042 CC-3-2V1 4.00% [1 kHz, 20 C.]: 16.7 CLP-V-1 8.00% .sub. [1 kHz, 20 C.]: 20.5 CLP-3-T 5.50% .sub. [1 kHz, 20 C.]: 3.8 APUQU-2-F 9.00% .sub.1 [mPa .Math. s, 20 C.]: 105 APUQU-3-F 9.00% K.sub.1 [pN, 20 C.]: 15.8 PGUQU-3-F 3.50% K.sub.3 [pN, 20 C.]: 16.4 CDUQU-3-F 8.00% DPGU-4-F 2.00% DGUQU-4-F 8.00% DGUQU-2-F 3.00%

Example M24

(26) TABLE-US-00032 APUQU-2-F 9.50% Clearing point [ C.]: 85 APUQU-3-F 7.50% n [589 nm, 20 C.]: 0.1035 CC-3-V 46.00% [1 kHz, 20 C.]: 9.6 CC-3-V1 6.00% .sub. [1 kHz, 20 C.]: 12.8 CLP-3-T 3.00% .sub. [1 kHz, 20 C.]: 3.2 CLP-V-1 10.00% .sub.1 [mPa .Math. s, 20 C.]: 70 CCP-V-1 3.00% K.sub.1 [pN, 20 C.]: 14.0 PGUQU-3-F 8.00% K.sub.3 [pN, 20 C.]: 15.6 PGUQU-4-F 7.00%

Example M25

(27) TABLE-US-00033 APUQU-2-F 9.00% Clearing point [ C.]: 84 APUQU-3-F 7.50% n [589 nm, 20 C.]: 0.1013 CC-3-V 42.50% [1 kHz, 20 C.]: 9.4 CC-3-V1 11.00% .sub. [1 kHz, 20 C.]: 12.6 CCP-V-1 6.50% .sub. [1 kHz, 20 C.]: 3.2 CLP-3-T 4.00% .sub.1 [mPa .Math. s, 20 C.]: 70 CLP-V-1 4.50% K.sub.1 [pN, 20 C.]: 13.9 PGUQU-3-F 8.00% K.sub.3 [pN, 20 C.]: 16.0 PGUQU-4-F 5.00% PGUQU-5-F 2.00%

Example M26

(28) TABLE-US-00034 CC-3-V 51.50% Clearing point [ C.]: 74 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1174 CCP-V-1 5.00% [1 kHz, 20 C.]: 2.2 CLP-3-OT 4.50% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.50% .sub.1 [mPa .Math. s, 20 C.]: 44 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 13.7 PGU-2-F 4.00% K.sub.3 [pN 20 C.]: 13.6 PGUQU-3-F 3.50% LTS [bulk, 20 C.]: >1000 h PP-1-2V1 6.00% PPGU-3-F 1.00%

Example M26a

(29) Liquid-crystalline mixture M26 is additionally stabilized with 300 ppm of the compound of the formula ST-2

(30) 300 ppm of

(31) ##STR00417##

Example M27

(32) TABLE-US-00035 CC-3-V 51.50% Clearing point [ C.]: 73.5 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1174 CCP-V-1 6.00% [1 kHz, 20 C.]: 2.2 CLP-3-T 3.50% .sub. [1 kHz, 20 C.]: 4.9 PGP-1-2V 3.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 14.50% .sub.1 [mPa .Math. s, 20 C.]: 44 PGP-3-2V 2.00% K.sub.1 [pN, 20 C.]: 13.9 PGU-2-F 4.50% K.sub.3 [pN, 20 C.]: 13.6 PGUQU-3-F 3.00% LTS [bulk, 20 C.]: >1000 h PP-1-2V1 6.00% PPGU-3-F 1.00%

Example M27a

(33) Liquid-crystalline mixture M27 is additionally stabilized with 300 ppm of the compound of the formula ST-2

(34) 300 ppm of

(35) ##STR00418##

Example M28

(36) TABLE-US-00036 CC-3-V 48.00% Clearing point [ C.]: 88 CCP-V-1 12.00% n [589 nm, 20 C.]: 0.1154 CCP-V2-1 5.00% [1 kHz, 20 C.]: 3.5 PP-1-2V1 1.00% .sub. [1 kHz, 20 C.]: 6.3 PGP-1-2V 5.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 7.50% .sub.1 [mPa .Math. s, 20 C.]: 59 PGP-3-2V 4.00% K.sub.1 [pN, 20 C.]: 15.0 CLP-3-T 5.00% K.sub.3 [pN, 20 C.]: 15.7 PGUQU-4-F 5.50% LTS [bulk, 20 C.]: >1000 h APUQU-3-F 4.00% PGU-2-F 3.00%

Example M28a

(37) Liquid-crystalline mixture M28 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and 1000 ppm of the compound of the formula ST-2

(38) 400 ppm of

(39) ##STR00419##

(40) and

(41) 1000 ppm of

Example M29

(42) TABLE-US-00037 CC-3-V 49.50% Clearing point [ C.]: 89.5 CCP-V-1 5.00% n [589 nm, 20 C.]: 0.1172 CLP-V-1 8.50% [1 kHz, 20 C.]: 3.5 PP-1-2V1 1.00% .sub. [1 kHz, 20 C.]: 6.3 PGP-1-2V 5.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 8.00% .sub.1 [mPa .Math. s, 20 C.]: 57 PGP-3-2V 4.50% K.sub.1 [pN, 20 C.]: 15.2 CCP-30CF.sub.3 6.50% K.sub.3 [pN, 20 C.]: 15.8 PGUQU-4-F 5.00% PGUQU-5-F 2.50% APUQU-3-F 4.50%

Example M29a

(43) Liquid-crystalline mixture M29 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and 1000 ppm of the compound of the formula ST-2

(44) 400 ppm of

(45) ##STR00420##

(46) and

(47) 1000 ppm of

Example M30

(48) TABLE-US-00038 CC-3-V 52.00% Clearing point [ C.]: 85.5 CLP-V-1 11.50% n [589 nm, 20 C.]: 0.1187 PP-1-2V1 3.00% [1 kHz, 20 C.]: 3.5 PGP-1-2V 5.00% .sub. [1 kHz, 20 C.]: 6.2 PGP-2-2V 8.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-3-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 56 CLP-3-T 7.00% K.sub.1 [pN, 20 C.]: 16.2 PGUQU-4-F 5.00% K.sub.3 [pN, 20 C.]: 15.4 PGUQU-5-F 2.50% LTS [bulk, 20 C.]: >1000 h APUQU-3-F 3.00%

Example M30a

(49) Liquid-crystalline mixture M30 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and 1000 ppm of the compound of the formula ST-2

(50) 400 ppm of

(51) ##STR00421##

(52) and

(53) 1000 ppm of

Example M31

(54) TABLE-US-00039 CC-3-V 51.50% Clearing point [ C.]: 85.5 CLP-V-1 11.50% n [589 nm, 20 C.]: 0.1175 PP-1-2V1 3.00% [1 kHz, 20 C.]: 4.1 PGP-1-2V 5.00% .sub. [1 kHz, 20 C.]: 6.8 PGP-2-2V 6.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-3-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 58 CLP-3-T 7.00% K.sub.1 [pN, 20 C.]: 16.0 PGUQU-4-F 5.00% K.sub.3 [pN, 20 C.]: 15.5 PGUQU-5-F 5.00% LTS [bulk, 20 C.]: >1000 h APUQU-3-F 3.00%

Example M31a

(55) Liquid-crystalline mixture M31 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and 1000 ppm of the compound of the formula ST-2

(56) 400 ppm of

(57) ##STR00422##

(58) and

(59) 1000 ppm of

Example M32

(60) TABLE-US-00040 CC-3-V 41.00% Clearing point [ C.]: 81 B-5O-OT 4.50% n [589 nm, 20 C.]: 0.1060 B-2O-O5 6.00% [1 kHz, 20 C.]: 4.6 CCP-V-1 15.50% .sub. [1 kHz, 20 C.]: 9.0 CLP-V-1 6.00% .sub. [1 kHz, 20 C.]: 4.4 PGP-2-2V 2.00% .sub.1 [mPa .Math. s, 20 C.]: 64 CCP-30CF.sub.3 7.50% K.sub.1 [pN, 20 C.]: 14.5 PUQU-3-F 3.00% K.sub.3 [pN, 20 C.]: 13.9 PGU-3-F 5.00% V.sub.0 [V, 20 C.]: 1.88 DGUQU-4-F 5.00% DPGU-4-F 4.50%

Example M33

(61) TABLE-US-00041 CC-3-V 42.00% Clearing point [ C.]: 80.5 B-5O-OT 4.50% n [589 nm, 20 C.]: 0.1047 B-2O-O5 6.00% [1 kHz, 20 C.]: 4.5 CCP-V-1 15.50% .sub. [1 kHz, 20 C.]: 8.9 CCP-V2-1 8.00% .sub. [1 kHz, 20 C.]: 4.4 PGP-2-2V 2.00% .sub.1 [mPa .Math. s, 20 C.]: 66 CLP-3-T 4.50% K.sub.1 [pN, 20 C.]: 14.4 PUQU-3-F 3.00% K.sub.3 [pN, 20 C.]: 14.0 PGU-3-F 5.00% V.sub.0 [V, 20 C.]: 1.89 DGUQU-4-F 5.00% DPGU-4-F 4.50%

Example M34

(62) TABLE-US-00042 CC-3-V 33.00% CC-3-V1 5.00% B-2O-O5 4.00% B(S)-2O-O4 3.00% B(S)-2O-O5 4.00% CLP-3-T 3.00% CCP-3OCF.sub.3 3.00% CCP-V-1 13.00% CCP-V2-1 6.00% CCVC-3-V 5.00% PUQU-3-F 6.00% CPGP-5-2 4.00% APUQU-2-F 2.50% APUQU-3-F 2.00% CDUQU-3-F 2.50% DGUQU-4-F 2.00% DPGU-4-F 1.50% PPGU-3-F 0.50%

Example M35

(63) TABLE-US-00043 CC-3-V 30.00% CC-3-V1 5.00% B-2O-O5 4.00% B(S)-2O-O4 6.00% B(S)-2O-O5 6.00% CLP-3-T 3.00% CCP-30CF.sub.3 5.00% CCP-V-1 13.00% CCP-V2-1 1.50% CCVC-3-V 5.00% PUQU-3-F 6.00% CPGP-5-2 4.00% APUQU-2-F 2.50% APUQU-3-F 2.50% CDUQU-3-F 2.50% DGUQU-4-F 2.00% DPGU-4-F 1.50% PPGU-3-F 0.50%

Example M36

(64) TABLE-US-00044 CC-3-V 34.00% CC-3-V1 7.50% B-2O-O5 4.00% B(S)-2O-O4 3.00% B(S)-2O-O5 4.00% CCP-3OCF.sub.3 5.00% CLP-3-T 5.00% CCP-V-1 13.00% PUQU-3-F 4.00% APUQU-2-F 5.00% APUQU-3-F 4.00% CDUQU-3-F 3.50% DGUQU-4-F 3.00% DPGU-4-F 2.00% PPGU-3-F 0.50% CPGP-5-2 2.50%

Example M37

(65) TABLE-US-00045 CC-3-V 31.50% CC-3-V1 7.50% B-2O-O5 4.00% B(S)-2O-O4 6.00% B(S)-2O-O5 6.00% CCP-3OCF.sub.3 5.00% CLP-3-T 5.00% CCP-V-1 9.50% PUQU-3-F 4.00% APUQU-2-F 4.00% APUQU-3-F 4.50% CDUQU-3-F 5.00% DGUQU-4-F 3.00% DPGU-4-F 2.00% PPGU-3-F 0.50% CPGP-5-2 2.50%

Example M38

(66) TABLE-US-00046 Y-4O-O4 10.50% CC-3-V 25.00% CCP-3OCF.sub.3 5.00% CLP-3-T 5.00% CCP-V-1 14.00% CCP-V2-1 4.50% PGP-2-2V 6.50% DGUQU-4-F 5.00% DPGU-4-F 5.00% APUQU-2-F 7.00% APUQU-3-F 8.00% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M39

(67) TABLE-US-00047 Y-4O-O4 10.50% CC-3-V 22.00% B(S)-2O-O4 3.00% B(S)-2O-O5 4.00% CCP-3OCF.sub.3 5.00% CLP-3-T 5.00% CCP-V-1 13.00% CCP-V2-1 6.00% DGUQU-4-F 5.00% DPGU-4-F 5.00% APUQU-2-F 7.00% APUQU-3-F 7.00% CDUQU-3-F 3.00% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M40

(68) TABLE-US-00048 CC-3-V 49.00% Clearing point [ C.]: 80.5 CC-3-V1 12.00% n [589 nm, 20 C.]: 0.0930 CCP-V-1 10.00% [1 kHz, 20 C.]: 2.7 CLP-V-1 7.00% .sub. [1 kHz, 20 C.]: 5.3 PGP-2-2V 5.50% .sub. [1 kHz, 20 C.]: 2.6 CLP-3-T 4.00% .sub.1 [mPa .Math. s, 20 C.]: 48 PGUQU-3-F 3.00% K.sub.1 [pN, 20 C.]: 14.9 APUQU-2-F 6.00% K.sub.3 [pN, 20 C.]: 16.0 PP-1-2V1 3.00% PPGU-3-F 0.50%

(69) Liquid-crystalline mixture M40 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and various concentrations of the compound of the formula ST-2 or ST-3:

(70) ##STR00423##

(71) TABLE-US-00049 Mixture ST-1 ST-2 ST-3 Example M40a 400 ppm Example M40b 400 ppm 100 ppm Example M40c 400 ppm 500 ppm Example M40d 400 ppm 1000 ppm Example M40e 400 ppm 100 ppm Example M40f 400 ppm 500 ppm Example M40g 400 ppm 1000 ppm

Example M41

(72) TABLE-US-00050 CC-3-V 42.50% B-2O-O5 3.50% B(S)-2O-O4 4.00% B(S)-2O-O5 4.00% CCP-3OCF.sub.3 5.00% CLP-3-T 5.00% CCP-V-1 1.50% DGUQU-4-F 5.00% DPGU-4-F 4.00% APUQU-2-F 7.00% APUQU-3-F 7.00% CDUQU-3-F 2.00% PGUQU-3-F 4.00% PGUQU-4-F 5.00% PPGU-3-F 0.50%

Example M42

(73) TABLE-US-00051 CC-3-V 43.00% Clearing point [ C.]: 80 B-5O-OT 5.00% n [589 nm, 20 C.]: 0.1048 B-2O-O5 5.50% [1 kHz, 20 C.]: 4.6 CCP-V-1 15.00% .sub. [1 kHz, 20 C.]: 9.0 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 4.4 PGP-2-2V 2.50% K.sub.1 [pN, 20 C.]: 14.3 CLP-3-T 6.00% K.sub.3 [pN, 20 C.]: 13.9 PGU-3-F 7.00% V.sub.0 [V, 20 C.]: 1.88 DGUQU-4-F 5.50% DPGU-4-F 4.50%

Example M43

(74) TABLE-US-00052 APUQU-2-F 4.00% APUQU-3-F 5.50% B-2O-O5 4.00% CC-3-V 22.00% CC-3-V1 4.00% CCP-3-1 4.00% CCP-30CF.sub.3 8.00% CCP-V-1 6.50% CDUQU-3-F 4.50% DGUQU-4-F 5.00% DPGU-4-F 3.00% PGUQU-3-F 3.00% PPGU-3-F 0.50% PY-3-O2 9.50% Y-4O-O4 5.00% CCY-3-O2 4.50% CLP-3-T 5.00% PGP-2-2V 2.00%

Example M44

(75) TABLE-US-00053 APUQU-2-F 4.00% APUQU-3-F 5.00% B-2O-O5 3.50% CC-3-V 33.00% PP-2-2V1 2.00% B(S)-2O-O4 4.00% CC-3-V1 4.00% CLP-3-T 5.00% B(S)-2O-O5 4.00% CCP-30CF.sub.3 8.00% CCP-V-1 5.00% CDUQU-3-F 4.00% DGUQU-4-F 5.00% DPGU-4-F 3.00% PGUQU-3-F 3.00% PGUQU-4-F 3.00% PPGU-3-F 1.50% Y-4O-O4 3.00%

Example M45

(76) TABLE-US-00054 APUQU-2-F 4.00% APUQU-3-F 5.00% B-2O-O5 3.50% CC-3-V 33.00% PP-1-2V1 2.00% B(S)-2O-O4 4.00% CC-3-V1 4.00% CLP-3-T 5.00% B(S)-2O-O5 4.00% CCP-30CF.sub.3 8.00% CCP-V-1 5.00% CDUQU-3-F 4.00% DGUQU-4-F 5.00% DPGU-4-F 3.00% PGUQU-3-F 3.00% PGUQU-4-F 3.00% PPGU-3-F 1.50% Y-4O-O4 3.00%

Example M46

(77) TABLE-US-00055 Y-4O-O4 10.50% Clearing point [ C.]: 81 CC-3-V 25.00% n [589 nm, 20 C.]: 0.1141 CCP-30CF.sub.3 6.00% [1 kHz, 20 C.]: 10.6 CLP-3-T 3.50% .sub. [1 kHz, 20 C.]: 15.7 CCP-V-1 14.00% .sub. [1 kHz, 20 C.]: 5.1 CCP-V2-1 4.50% .sub.1 [mPa .Math. s, 20 C.]: 87 PGP-2-2V 6.00% K.sub.1 [pN, 20 C.]: 13.3 DGUQU-4-F 6.00% K.sub.3 [pN, 20 C.]: 12.8 DPGU-4-F 5.00% V.sub.0 [V, 20 C.]: 1.17 APUQU-2-F 7.00% APUQU-3-F 8.00% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M47

(78) TABLE-US-00056 Y-4O-O4 5.00% Clearing point [ C.]: 81 CC-3-V 21.50% n [589 nm, 20 C.]: 0.1120 CC-3-V1 4.00% [1 kHz, 20 C.]: 7.9 B-2O-O5 4.00% .sub.|| [1 kHz, 20 C.]: 14.0 PY-3-O2 9.50% .sub. [1 kHz, 20 C.]: 6.2 CCP-30CF.sub.3 6.00% .sub.1 [mPa .Math. s, 20 C.]: 99 CCP-V-1 14.00% K.sub.1 [pN, 20 C.]: 14.3 CCP-V2-1 1.50% K.sub.3 [pN, 20 C.]: 13.9 CLP-3-T 4.00% V.sub.0 [V, 20 C.]: 1.42 CCY-3-O2 4.50% APUQU-2-F 4.00% APUQU-3-F 5.00% CDUQU-3-F 4.00% DGUQU-4-F 5.00% DPGU-4-F 3.50% PGUQU-3-F 4.00% PPGU-3-F 0.50%

Example M48

(79) TABLE-US-00057 Y-4O-O4 7.00% CC-3-V 28.00% B-2O-O5 4.00% B(S)-2O-O4 3.50% B(S)-2O-O5 4.00% CCP-30CF.sub.3 6.50% CCP-V-1 15.00% PGP-2-2V 4.00% CLP-3-T 4.00% APUQU-2-F 5.00% APUQU-3-F 6.50% CDUQU-3-F 4.50% DGUQU-4-F 5.00% DPGU-4-F 3.50% PPGU-3-F 0.50%

Example M49

(80) TABLE-US-00058 Y-4O-O4 10.50% CC-3-V 24.00% CCP-30CF.sub.3 6.00% CLP-3-T 4.00% CCP-V-1 13.00% CCP-V2-1 5.00% PGP-2-2V 7.00% DGUQU-4-F 5.00% DPGU-4-F 3.50% APUQU-2-F 6.50% APUQU-3-F 7.50% CDUQU-3-F 3.50% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M50

(81) TABLE-US-00059 CC-3-V 48.00% Clearing point [ C.]: 79.5 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0930 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.7 CCP-V2-1 6.00% .sub.|| [1 kHz, 20 C.]: 5.3 CLP-3-T 5.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 5.00% .sub.1 [mPa .Math. s, 20 C.]: 49 PGUQU-3-F 4.00% K.sub.1 [pN, 20 C.]: 14.7 APUQU-2-F 4.50% K.sub.3 [pN, 20 C.]: 16.3 PP-1-2V1 5.00% PPGU-3-F 0.50%

(82) Liquid-crystalline mixture M50 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and various concentrations of the compounds of the formula ST-2 or ST-3:

(83) TABLE-US-00060 Mixture ST-1 ST-2 ST-3 Example M50a 400 ppm Example M50b 400 ppm 100 ppm Example M50c 400 ppm 500 ppm Example M50d 400 ppm 1000 ppm Example M50e 400 ppm 100 ppm Example M50f 400 ppm 500 ppm Example M50g 400 ppm 1000 ppm

Example M51

(84) TABLE-US-00061 CC-3-V 48.00% Clearing point [ C.]: 80.5 CC-3-V1 12.00% n [589 nm, 20 C.]: 0.0937 CCP-V-1 11.50% [1 kHz, 20 C.]: 2.7 CLP-V-1 9.00% .sub.|| [1 kHz, 20 C.]: 5.3 PGP-2-2V 4.50% .sub. [1 kHz, 20 C.]: 2.6 PGUQU-3-F 3.00% .sub. [mPa .Math. s, 20 C.]: 49 APUQU-2-F 7.50% K.sub.1 [pN, 20 C.]: 14.4 PP-1-2V1 4.00% K.sub.3 [pN, 20 C.]: 16.0 PPGU-3-F 0.50%

(85) Liquid-crystalline mixture M51 is additionally stabilized with 400 ppm of the compound of the formula ST-1 and various concentrations of the compounds of the formula ST-2 or ST-3:

(86) TABLE-US-00062 Mixture ST-1 ST-2 ST-3 Example M51a 400 ppm Example M51b 400 ppm 100 ppm Example M51c 400 ppm 500 ppm Example M51d 400 ppm 1000 ppm Example M51e 400 ppm 100 ppm Example M51f 400 ppm 500 ppm Example M51g 400 ppm 1000 ppm

Example M52

(87) TABLE-US-00063 CC-3-V 48.50% Clearing point [ C.]: 79.0 CC-3-V1 12.00% n [589 nm, 20 C.]: 0.0939 CCP-V-1 10.50% [1 kHz, 20 C.]: 2.9 PGP-2-2V 3.50% .sub.|| [1 kHz, 20 C.]: 5.4 PGUQU-3-F 5.00% .sub. [1 kHz, 20 C.]: 2.6 APUQU-2-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 48 PP-1-2V1 5.00% K.sub.1 [pN, 20 C.]: 14.1 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 15.8 CLP-V-1 9.00%

Example M53

(88) TABLE-US-00064 CC-3-V 48.00% Clearing point [ C.]: 80.6 CC-3-V1 12.00% n [589 nm, 20 C.]: 0.0930 CCP-V-1 11.50% [1 kHz, 20 C.]: 2.7 PGP-2-2V 4.50% .sub.| [1 kHz, 20 C.]: 6.3 PGUQU-3-F 3.00% .sub. [1 kHz, 20 C.]: 2.6 APUQU-2-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 49 PP-1-2V1 4.00% K.sub.1 [pN, 20 C.]: 15.0 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 17.1 CLP-3-T 4.00% CLP-V-1 6.50

Example M54

(89) TABLE-US-00065 CC-3-V 48.00% Clearing point [ C.]: 80.0 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0956 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.7 PGP-2-2V 5.00% .sub.|| [1 kHz, 20 C.]: 5.3 PGUQU-3-F 4.00% .sub. [1 kHz, 20 C.]: 2.6 APUQU-2-F 4.50% .sub.1 [mPa .Math. s, 20 C.]: 49 PP-1-2V1 5.00% K.sub.1 [pN, 20 C.]: 15.0 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 16.3 CLP-3-T 5.50% CLP-V-1 6.00

Example M55

(90) TABLE-US-00066 PGUQU-3-F 3.00% Clearing point [ C.]: 70.2 PPGU-3-F 0.50% n [589 nm, 20 C.]: 0.1345 PGP-1-2V 7.00% [1 kHz, 20 C.]: 5.3 PGP-2-2V 11.00% .sub.|| [1 kHz, 20 C.]: 8.3 PGU-3-F 6.50% .sub. [1 kHz, 20 C.]: 3.0 PUQU-3-F 10.00% .sub.1 [mPa .Math. s, 20 C.]: 55 CC-3-V 34.00% K.sub.1 [pN, 20 C.]: 15.7 PP-1-2V1 10.00% K.sub.3 [pN, 20 C.]: 13.3 CLP-3-T 6.00% V.sub.0 [V, 20 C.]: 1.81 CCP-V-1 2.00% CC-3-V1 6.00% CC-3-2V1 4.00%

(91) Liquid-crystalline mixture M55 is additionally stabilized with 0.05% of the compound of the formula ST-1

(92) ##STR00424##

Example M56

(93) TABLE-US-00067 PGUQU-3-F 1.50% Clearing point [ C.]: 63.1 PPGU-3-F 0.50% n [589 nm, 20 C.]: 0.1337 PGP-1-2V 6.50% [1 kHz, 20 C.]: 5.1 PGP-2-2V 10.50% .sub.|| [1 kHz, 20 C.]: 8.1 PGU-3-F 7.50% .sub. [1 kHz, 20 C.]: 3.0 PUQU-3-F 10.00% .sub.1 [mPa .Math. s, 20 C.]: 49 CC-3-V 42.00% K.sub.1 [pN, 20 C.]: 14.6 PP-1-2V1 14.00% K.sub.3 [pN, 20 C.]: 11.8 CLP-3-T 7.50% V.sub.0 [V, 20 C.]: 1.78

(94) Liquid-crystalline mixture M56 is additionally stabilized with 0.05% of the compound of the formula ST-1

(95) ##STR00425##

Example M57

(96) TABLE-US-00068 APUQU-2-F 2.00% Clearing point [ C.]: 104 DGUQU-4-F 4.00% n [589 nm, 20 C.]: 0.0949 DPGU-4-F 2.00% [1 kHz, 20 C.]: 4.5 CCG-V-F 17.00% .sub.|| [1 kHz, 20 C.]: 7.4 CCP-30CF3 4.00% .sub. [1 kHz, 20 C.]: 2.9 CCP-50CF3 3.00% .sub.1 [mPa .Math. s, 20 C.]: 84 CCP-V-1 10.00% K.sub.1 [pN, 20 C.]: 16.0 CCP-V2-1 4.00% K.sub.3 [pN, 20 C.]: 20.2 CCQU-3-F 5.50% V.sub.0 [V, 20 C.]: 1.98 CCVC-3-V 5.00% CLP-3-T 3.00% PGP-2-2V 3.00% CC-3-2V1 4.00% CC-3-V 23.50% CC-3-V1 5.50% PP-1-2V1 4.50%

Example M58

(97) TABLE-US-00069 DGUQU-4-F 1.50% Clearing point [ C.]: 79.5 CCG-V-F 6.00% n [589 nm, 20 C.]: 0.1051 CCQU-2-F 3.50% [1 kHz, 20 C.]: 4.5 CCVC-3-V 6.50% .sub.|| [1 kHz, 20 C.]: 7.9 CDU-2-F 13.00% .sub. [1 kHz, 20 C.]: 3.4 CLP-3-T 4.00% .sub.1 [mPa .Math. s, 20 C.]: 61 PGP-1-2V 12.00% K.sub.1 [pN, 20 C.]: 13.4 PGP-2-2V 4.00% K.sub.3 [pN, 20 C.]: 13.3 PGU-2-F 4.00% V.sub.0 [V, 20 C.]: 1.80 CC-3-V 31.50% CCH-34 4.00% PCH-302 10.00%

Example M59

(98) TABLE-US-00070 CC-3-2V1 3.50% Clearing point [ C.]: 74.8 CC-3-V 49.00% n [589 nm, 20 C.]: 0.1189 CC-3-V1 4.00% [1 kHz, 20 C.]: 3.1 CLP-3-T 6.50% .sub.| [1 kHz, 20 C.]: 5.9 PGP-1-2V 6.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 12.00% .sub.1 [mPa .Math. s, 20 C.]: 45 PGP-3-2V 4.00% K.sub.1 [pN, 20 C.]: 13.6 PGU-2-F 5.00% K.sub.3 [pN, 20 C.]: 13.1 PGUQU-3-F 3.00% V.sub.0 [V, 20 C.]: 2.20 PP-1-2V1 3.00% PPGU-3-F 1.00% PUQU-3-F 3.00%

(99) Liquid-crystalline mixture M59 is additionally stabilized with 0.04% of the compound of the formula ST-1

(100) ##STR00426##

Example M60

(101) TABLE-US-00071 APUQU-2-F 6.00% Clearing point [ C.]: 90.6 APUQU-3-F 7.00% n [589 nm, 20 C.]: 0.1155 CC-3-V 27.50% [1 kHz, 20 C.]: 10.4 CC-3-V1 8.00% .sub.|| [1 kHz, 20 C.]: 13.9 CCP-V-1 9.00% .sub. [1 kHz, 20 C.]: 3.5 CCP-V2-1 6.50% .sub.1 [mPa .Math. s, 20 C.]: 73 CDUQU-3-F 8.50% K.sub.1 [pN, 20 C.]: 13.9 CLP-3-T 3.00% K.sub.3 [pN, 20 C.]: 15.5 PGP-1-2V 5.00% V.sub.0 [V, 20 C.]: 1.22 PGP-2-2V 5.00% PGUQU-3-F 1.00% PPGU-3-F 1.00% PUQU-3-F 12.50%

(102) Liquid-crystalline mixture M60 is additionally stabilized with 0.04% of the compound of the formula ST-1

(103) ##STR00427##

Example M61

(104) TABLE-US-00072 APUQU-2-F 6.00% Clearing point [ C.]: 90.4 APUQU-3-F 7.00% n [589 nm, 20 C.]: 0.1179 CC-3-V 28.00% [1 kHz, 20 C.]: 10.9 CC-3-V1 8.00% .sub.|| [1 kHz, 20 C.]: CCP-V-1 9.00% .sub. [1 kHz, 20 C.]: CCP-V2-1 5.50% .sub.1 [mPa .Math. s, 20 C.]: 91 CDUQU-3-F 8.00% K.sub.1 [pN, 20 C.]: 14.7 CLP-3-T 4.00% K.sub.3 [pN, 20 C.]: 16.4 PGP-1-2V 5.00% V.sub.0 [V, 20 C.]: 1.23 PGP-2-2V 5.00% PQUQU-3-F 1.50% PPGU-3-F 1.00% PUQU-3-F 12.00%

(105) Liquid-crystalline mixture M61 is additionally stabilized with 0.04% of the compound of the formula ST-1

(106) ##STR00428##

Example M62

(107) TABLE-US-00073 CC-3-V 47.50% Clearing point [ C.]: 74.8 CC-3-V1 7.50% n [589 nm, 20 C.]: 0.1192 CLP-3-T 7.00% [1 kHz, 20 C.]: 4.7 CPGU-3-OT 2.00% .sub.| [1 kHz, 20 C.]: 7.6 PGP-2-2V 16.00% .sub. [1 kHz, 20 C.]: 2.9 PGU-2-F 11.00% .sub.1 [mPa .Math. s, 20 C.]: 45 PGUQU-3-F 6.00% K.sub.1 [pN, 20 C.]: 13.3 PP-1-2V1 2.00% K.sub.3 [pN, 20 C.]: 12.6 PPGU-3-F 1.00% V.sub.0 [V, 20 C.]: 1.78

(108) Liquid-crystalline mixture M62 is additionally stabilized with 0.04% of the compound of the formula ST-1

(109) ##STR00429##

Example M63

(110) TABLE-US-00074 CC-3-2V1 7.00% Clearing point [ C.]: 70.0 CC-3-V 46.00% n [589 nm, 20 C.]: 0.1185 CC-3-V1 3.00% [1 kHz, 20 C.]: 3.0 CLP-3-T 5.00% .sub.|| [1 kHz, 20 C.]: 5.7 PGP-1-2V 7.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 11.00% .sub.1 [mPa .Math. s, 20 C.]: 45 PGP-3-2V 2.50% K.sub.1 [pN, 20 C.]: 13.2 PGU-2-F 5.50% K.sub.3 [pN, 20 C.]: 12.8 PP-1-2V1 6.00% V.sub.0 [V, 20 C.]: 2.21 PPGU-3-F 1.00% PUQU-3-F 6.00%

(111) Liquid-crystalline mixture M63 is additionally stabilized with 0.04% of the compound of the formula ST-1

(112) ##STR00430##

Example M64

(113) TABLE-US-00075 APUQU-2-F 6.00% Clearing point [ C.]: 80.0 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1129 PGUQU-3-F 2.00% [1 kHz, 20 C.]: 3.9 PPGU-3-F 0.50% .sub.|| [1 kHz, 20 C.]: 6.7 CCP-V-1 2.50% .sub. [1 kHz, 20 C.]: 2.8 PGP-1-2V 4.00% .sub.1 [mPa .Math. s, 20 C.]: 52 PGP-2-2V 16.50% K.sub.1 [pN, 20 C.]: 14.1 CC-3-V 52.00% K.sub.3 [pN, 20 C.]: 14.1 CC-3-V1 6.50% V.sub.0 [V, 20 C.]: 2.03 CLP-3-T 5.00%

Example M65

(114) TABLE-US-00076 APUQU-2-F 5.00% Clearing point [ C.]: 80.0 PGUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1131 PPGU-3-F 0.50% [1 kHz, 20 C.]: 3.5 CCP-V-1 8.50% .sub.|| [1 kHz, 20 C.]: 6.2 PGP-2-2V 16.50% .sub. [1 kHz, 20 C.]: 2.7 PP-1-2V1 4.00% .sub.1 [mPa .Math. s, 20 C.]: 51 CC-3-V 48.00% K.sub.1 [pN, 20 C.]: 14.6 CC-3-V1 6.50% K.sub.3 [pN, 20 C.]: 14.7 CLP-3-T 5.00% V.sub.0 [V, 20 C.]: 2.17

Example M66

(115) TABLE-US-00077 APUQU-2-F 4.00% Clearing point [ C.]: 76.0 PGUQU-3-F 3.00% n [589 nm, 20 C.]: 0.1176 PPGU-3-F 0.50% [1 kHz, 20 C.]: 2.4 CCP-V-1 4.00% .sub.|| [1 kHz, 20 C.]: 5.1 PGP-1-2V 6.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 15.50% .sub.1 [mPa .Math. s, 20 C.]: 48 PP-1-2V1 6.00% K.sub.1 [pN, 20 C.]: 14.3 CC-3-V 52.00% K.sub.3 [pN, 20 C.]: 14.6 CC-3-V1 4.50% CLP-3-T 4.50%

Example M67

(116) TABLE-US-00078 APUQU-2-F 7.00% Clearing point [ C.]: 76.0 PGUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1173 PPGU-3-F 0.50% [1 kHz, 20 C.]: 4.0 CCP-V-1 1.00% .sub.|| [1 kHz, 20 C.]: 6.8 PGP-1-2V 4.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 51 PP-1-2V1 4.50% K.sub.1 [pN, 20 C.]: 14.5 CC-3-V 50.00% K.sub.3 [pN, 20 C.]: 14.6 CC-3-V1 5.00% CC-3-2V1 2.00% CLP-3-T 5.00%

Example M68

(117) TABLE-US-00079 APUQU-2-F 3.00% Clearing point [ C.]: 76.5 PGUQU-3-F 2.00% n [589 nm, 20 C.]: 0.1177 PPGU-3-F 0.50% [1 kHz, 20 C.]: 2.5 CLP-V-1 7.00% .sub.|| [1 kHz, 20 C.]: 5.1 PGP-1-2V 2.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 14.00% .sub.1 [mPa .Math. s, 20 C.]: 51 PP-1-2V1 7.00% K.sub.1 [pN, 20 C.]: 15.4 CC-3-V 49.00% K.sub.3 [pN, 20 C.]: 14.4 CC-3-V1 6.00% CLP-3-T 4.50% PUQU-3-F 2.00% PGP-3-2V 2.50%

Example M69

(118) TABLE-US-00080 CC-3-2V1 1.00% Clearing point [ C.]: 77.5 CC-3-V 50.00% n [589 nm, 20 C.]: 0.1169 CC-3-V1 2.00% [1 kHz, 20 C.]: 4.2 CCP-V-1 2.00% .sub.|| [1 kHz, 20 C.]: 7.0 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 2.8 CLP-V-1 6.50% .sub.1 [mPa .Math. s, 20 C.]: 51 PGP-2-2V 12.50% K.sub.1 [pN, 20 C.]: 15.0 PP-1-2V1 6.00% K.sub.3 [pN, 20 C.]: 13.9 PGU-4-T 3.50% PGUQU-3-F 5.00% PGUQU-4-F 5.00% PPGU-3-F 0.50%

Example M70

(119) TABLE-US-00081 APUQU-2-F 3.00% Clearing point [ C.]: 75.0 CC-3-V 49.50% n [589 nm, 20 C.]: 0.1186 CC-3-V1 6.00% [1 kHz, 20 C.]: 2.3 CLP-1V2-1 5.50% .sub.|| [1 kHz, 20 C.]: 5.0 CLP-3-T 4.00% .sub. [1 kHz, 20 C.]: 2.6 PGP-1-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PGP-2-2V 13.00% K.sub.1 [pN, 20 C.]: 15.2 PGP-3-2V 2.50% K.sub.3 [pN, 20 C.]: 15.1 PGUQU-3-F 2.00% PP-1-2V1 9.00% PPGU-3-F 0.50% PUQU-3-F 2.00%

Example M71

(120) TABLE-US-00082 APUQU-2-F 3.00% Clearing point [ C.]: 76.5 CC-3-V 49.50% n [589 nm, 20 C.]: 0.1178 CC-3-V1 6.00% [1 kHz, 20 C.]: 2.4 CLP-1V-1 6.00% .sub.|| [1 kHz, 20 C.]: 5.0 CLP-3-T 4.50% .sub. [1 kHz, 20 C.]: 2.7 PGP-1-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PGP-2-2V 13.00% K.sub.1 [pN, 20 C.]: 15.2 PGP-3-2V 2.50% K.sub.3 [pN, 20 C.]: 15.1 PGUQU-3-F 2.00% PP-1-2V1 8.00% PPGU-3-F 0.50% PUQU-3-F 2.00%

Example M72

(121) TABLE-US-00083 APUQU-2-F 3.00% CC-3-V 49.50% CC-3-V1 6.00% CLP-V2-1 6.00% CLP-3-T 4.50% PGP-1-2V 3.00% PGP-2-2V 13.00% PGP-3-2V 2.50% PGUQU-3-F 2.00% PP-1-2V1 8.00% PPGU-3-F 0.50% PUQU-3-F 2.00%

Example M73

(122) TABLE-US-00084 CC-3-V 46.00% Clearing point [ C.]: 76.0 CC-3-V1 6.00% n [589 nm, 20 C.]: 0.1180 CCP-V-1 1.50% [1 kHz, 20 C.]: 2.9 PGP-2-2V 12.00% .sub.|| [1 kHz, 20 C.]: 6.8 PGP-3-2V 2.50% .sub. [1 kHz, 20 C.]: 3.9 PGU-2-F 6.50% .sub.1 [mPa .Math. s, 20 C.]: 54 PGUQU-3-F 5.00% K.sub.1 [pN, 20 C.]: 15.0 CLP-3-T 5.00% K.sub.3 [pN, 20 C.]: 13.4 B(S)-2O-O4 3.50% B(S)-2O-O5 3.50% CC-3-2V1 1.00% DGUQU-4-F 1.50% CY-3-O2 2.50% CLP-V-1 3.50%

Example M74

(123) TABLE-US-00085 CC-3-V 44.00% Clearing point [ C.]: 85.00 CC-3-V1 6.00% n [589 nm, 20 C.]: 0.1178 CC-3-2V1 4.00% [1 kHz, 20 C.]: 3.2 CCP-V-1 1.50% .sub.|| [1 kHz, 20 C.]: 6.9 PGP-2-2V 10.50% .sub. [1 kHz, 20 C.]: 3.7 PGP-3-2V 5.00% .sub.1 [mPa .Math. s, 20 C.]: 62 DGUQU-4-F 4.50% K.sub.1 [pN, 20 C.]: 16.7 PGUQU-3-F 6.50% K.sub.3 [pN, 20 C.]: 15.5 CLP-3-T 5.00% B(S)-2O-O4 4.00% B(S)-2O-O5 3.50% CLP-V-1 5.50%

Example M75

(124) TABLE-US-00086 CC-3-V 44.00% Clearing point [ C.]: 80.0 CC-3-V1 6.00% n [589 nm, 20 C.]: 0.1186 CC-3-2V1 5.00% [1 kHz, 20 C.]: 3.0 PGP-2-2V 10.50% .sub. [1 kHz, 20 C.]: 6.9 PGP-3-2V 4.00% .sub. [1 kHz, 20 C.]: 3.8 DGUQU-4-F 2.50% .sub.1 [mPa .Math. s, 20 C.]: 60 PGUQU-3-F 6.50% K.sub.1 [pN, 20 C.]: 16.2 CLP-3-T 5.00% K.sub.3 [pN, 20 C.]: 14.9 B(S)-2O-O4 4.00% B(S)-2O-O5 3.50% CLP-V-1 4.50% PGU-2-F 3.00% PY-3-O2 1.50%

Example M76

(125) TABLE-US-00087 Y-4O-O4 7.00% CC-3-V 28.00% B-2O-O5 4.00% B(S)-2O-O4 3.50% B(S)-2O-O5 4.00% CCP-30CF.sub.3 6.50% CCP-V-1 15.00% PGP-2-2V 4.00% CLP-1V2-T 4.00% APUQU-2-F 5.00% APUQU-3-F 6.50% CDUQU-3-F 4.50% DGUQU-4-F 5.00% DPGU-4-F 3.50% PPGU-3-F 0.50%

Example M77

(126) TABLE-US-00088 Y-4O-O4 10.50% CC-3-V 24.00% CCP-30CF.sub.3 6.00% CLP-V2-T 4.00% CCP-V-1 13.00% CCP-V2-1 5.00% PGP-2-2V 7.00% DGUQU-4-F 5.00% DPGU-4-F 3.50% APUQU-2-F 6.50% APUQU-3-F 7.50% CDUQU-3-F 3.50% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M78

(127) TABLE-US-00089 CC-3-V 49.50% CCP-V-1 5.00% CLP-1V2-1 8.50% PP-1-2V1 1.00% PGP-1-2V 5.00% PGP-2-2V 8.00% PGP-3-2V 4.50% CCP-30CF.sub.3 6.50% PGUQU-C4-F 5.00% PGUQU-C5-F 2.50% APUQU-C3-F 4.50%

Example M79

(128) TABLE-US-00090 Y-4O-O4 10.50% CC-3-V 24.00% CCP-30CF.sub.3 6.00% CLP-V2-1 4.00% CCP-V-1 13.00% CCP-V2-1 5.00% PGP-2-2V 7.00% DGUQU-4-F 5.00% DPGU-4-F 3.50% APUQU-2-F 6.50% APUQU-3-F 7.50% CDUQU-3-F 3.50% PGUQU-4-F 4.00% PPGU-3-F 0.50%

Example M80

(129) TABLE-US-00091 CC-3-V 48.00% Clearing point [ C.]: 79.0 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0932 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.6 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 5.2 PGP-2-2V 5.00% .sub. [1 kHz, 20 C.]: 2.6 PGUQU-3-F 4.00% .sub.1 [mPa .Math. s, 20 C.]: 49 APUQU-2-F 4.50% K.sub.1 [pN, 20 C.]: 14.3 PP-1-2V1 5.00% K.sub.3 [pN, 20 C.]: 15.9 PPGU-3-F 0.50% CLP-V-T 5.50%

Example M81

(130) TABLE-US-00092 CC-3-V 48.00% Clearing point [ C.]: 79.0 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0930 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.5 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 5.0 PGP-2-2V 5.00% .sub. [1 kHz, 20 C.]: 2.5 PGUQU-3-F 4.00% .sub.1 [mPa .Math. s, 20 C.]: 48 APUQU-2-F 4.50% K.sub.1 [pN, 20 C.]: 13.9 PP-1-2V1 5.00% K.sub.3 [pN, 20 C.]: 15.9 PPGU-3-F 0.50% CLP-V-OT 5.50%

Example M82

(131) TABLE-US-00093 APUQU-2-F 6.00% Clearing point [ C.]: 80.0 DGUQU-4-F 5.50% n [589 nm, 20 C.]: 0.0983 DPGU-4-F 4.00% [1 kHz, 20 C.]: 5.9 PGUQU-3-F 3.50% .sub. [1 kHz, 20 C.]: 8.9 PPGU-3-F 0.50% .sub. [1 kHz, 20 C.]: 3.0 CC-3-2V1 9.00% .sub.1 [mPa .Math. s, 20 C.]: 58 CC-3-V 48.50% K.sub.1 [pN, 20 C.]: 14.7 CC-3-V1 7.00% K.sub.3 [pN, 20 C.]: 15.2 CLP-3-T 4.00% CLP-1V2-OT 3.00% PGP-2-2V 9.00%

Example M83

(132) TABLE-US-00094 APUQU-2-F 6.00% Clearing point [ C.]: 79.0 DGUQU-4-F 5.50% n [589 nm, 20 C.]: 0.0987 DPGU-4-F 4.00% [1 kHz, 20 C.]: 5.9 PGUQU-3-F 4.00% .sub. [1 kHz, 20 C.]: 8.8 PPGU-3-F 0.50% .sub. [1 kHz, 20 C.]: 2.9 CC-3-2V1 6.00% .sub.1 [mPa .Math. s, 20 C.]: 58 CC-3-V 49.00% K.sub.1 [pN, 20 C.]: 14.1 CC-3-V1 9.00% K.sub.3 [pN, 20 C.]: 15.3 CLP-1V2-OT 7.00% LTS bulk [20 C.]: >1000 h PGP-2-2V 8.00% PP-1-2V1 1.00%

Example M84

(133) TABLE-US-00095 APUQU-3-F 1.00% Clearing point [ C.]: 75.5 PPGU-3-F 0.50% n [589 nm, 20 C.]: 0.0987 CCP-V-1 12.00% [1 kHz, 20 C.]: 2.3 PGP-2-3 6.00% .sub. [1 kHz, 20 C.]: 4.9 PGP-2-4 7.00% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-5 2.00% .sub.1 [mPa .Math. s, 20 C.]: 52 PUQU-3-F 7.00% K.sub.1 [pN, 20 C.]: 14.2 CC-3-2V1 3.00% K.sub.3 [pN, 20 C.]: 14.8 CC-3-V 46.50% CC-3-V1 10.00% CLP-1V2-T 5.00%

Example M85

(134) TABLE-US-00096 CC-3-V 48.00% Clearing point [ C.]: 80.5 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0938 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.7 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 5.2 CLP-1V2-T 5.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 5.00% .sub.1 [mPa .Math. s, 20 C.]: 54 PGUQU-3-F 4.00% K.sub.1 [pN, 20 C.]: 15.0 APUQU-2-F 4.50% K.sub.3 [pN, 20 C.]: 17.0 PP-1-2V1 5.00% LTS bulk [20 C.]: >1000 h PPGU-3-F 0.50%

Example M86

(135) TABLE-US-00097 CC-3-V 48.00% CC-3-V1 10.50% CCP-V-1 11.00% CLP-V-1 6.00% CLP-1V2-T 5.50% PGP-2-2V 5.00% PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 5.00% PPGU-3-F 0.50%

Example M87

(136) TABLE-US-00098 CC-3-V 48.00% Clearing point [ C.]: 80.5 CC-3-V1 10.50% n [589 nm, 20 C.]: 0.0941 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.7 CCP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 5.3 CLP-1V-T 5.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 5.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PGUQU-3-F 4.00% K.sub.1 [pN, 20 C.]: 14.7 APUQU-2-F 4.50% K.sub.3 [pN, 20 C.]: 16.8 PP-1-2V1 5.00% PPGU-3-F 0.50%

Example M88

(137) TABLE-US-00099 APUQU-2-F 4.00% Clearing point [ C.]: 76.0 PGUQU-3-F 3.00% n [589 nm, 20 C.]: 0.1180 PPGU-3-F 0.50% [1 kHz, 20 C.]: 2.4 CCP-V-1 4.00% .sub. [1 kHz, 20 C.]: 5.1 PGP-1-2V 6.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 15.50% .sub.1 [mPa .Math. s, 20 C.]: 48 PP-1-2V1 6.00% K.sub.1 [pN, 20 C.]: 14.4 CC-3-V 52.00% K.sub.3 [pN, 20 C.]: 14.4 CC-3-V1 4.50% CLP-1V-T 4.50%

Example M89

(138) TABLE-US-00100 APUQU-2-F 7.00% Clearing point [ C.]: 76.5 PGUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1184 PPGU-3-F 0.50% [1 kHz, 20 C.]: 4.0 CCP-V-1 1.00% .sub. [1 kHz, 20 C.]: 6.8 PGP-1-2V 4.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 52 PP-1-2V1 4.50% K.sub.1 [pN, 20 C.]: 14.5 CC-3-V 50.00% K.sub.3 [pN, 20 C.]: 14.3 CC-3-V1 5.00% CC-3-2V1 2.00% CLP-1V-T 5.00%

Example M90

(139) TABLE-US-00101 CC-3-V 49.00% Clearing point [ C.]: 79.5 CC-3-V1 12.00% n [589 nm, 20 C.]: 0.0938 CCP-V-1 11.00% [1 kHz, 20 C.]: 2.7 CLP-1V-1 8.00% .sub. [1 kHz, 20 C.]: 5.3 PGP-2-2V 3.00% .sub. [1 kHz, 20 C.]: 2.6 PGUQU-3-F 3.50% .sub.1 [mPa .Math. s, 20 C.]: 49 APUQU-2-F 7.00% K.sub.1 [pN, 20 C.]: 14.6 PP-1-2V1 6.00% K.sub.3 [pN, 20 C.]: 16.9 PPGU-3-F 0.50%

Example M91

(140) TABLE-US-00102 CC-3-V 49.00% Clearing point [ C.]: 81.0 CC-3-V1 10.00% [1 kHz, 20 C.]: 2.7 CCP-V-1 8.00% .sub. [1 kHz, 20 C.]: 5.3 CLP-V-1 7.50% .sub. [1 kHz, 20 C.]: 2.5 CLP-1V-1 3.50% .sub.1 [mPa .Math. s, 20 C.]: 50 CLP-3-T 5.50% K.sub.1 [pN, 20 C.]: 15.6 PGP-2-2V 2.00% K.sub.3 [pN, 20 C.]: 17.1 PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 5.50% PPGU-3-F 0.50%

Example M92

(141) TABLE-US-00103 CC-3-V 49.00% Clearing point [ C.]: 81.0 CC-3-V1 10.50% [1 kHz, 20 C.]: 2.7 CCP-V-1 10.00% .sub. [1 kHz, 20 C.]: 5.3 CLP-V2-1 5.00% .sub. [1 kHz, 20 C.]: 2.6 CLP-1V-1 3.50% .sub.1 [mPa .Math. s, 20 C.]: 50 CLP-3-T 5.50% K.sub.1 [pN, 20 C.]: 15.5 PGP-2-2V 2.00% K.sub.3 [pN, 20 C.]: 17.2 PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 5.50% PPGU-3-F 0.50%

Example M93

(142) TABLE-US-00104 APUQU-3-F 1.00% Clearing point [ C.]: 76.5 PPGU-3-F 0.50% n [589 nm, 20 C.]: 0.0995 CCP-V-1 5.00% [1 kHz, 20 C.]: 2.3 CLP-1V-1 9.00% .sub. [1 kHz, 20 C.]: 4.9 PGP-2-3 6.00% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-4 7.00% .sub.1 [mPa .Math. s, 20 C.]: 53 PUQU-3-F 9.00% K.sub.1 [pN, 20 C.]: 14.6 CC-3-2V1 6.50% K.sub.3 [pN, 20 C.]: 15.4 CC-3-V 46.00% CC-3-V1 10.00%

Example M94

(143) TABLE-US-00105 APUQU-3-F 1.50% PPGU-3-F 0.50% CLP-V-1 10.00% CLP-1V-1 5.00% PGP-2-3 5.00% PGP-2-4 7.00% PUQU-3-F 8.50% CC-3-2V1 6.50% CC-3-V 47.00% CC-3-V1 9.00%

Example M95

(144) TABLE-US-00106 CC-3-V 49.50% CC-3-V1 10.00% CCP-V-1 10.00% CLP-1V-1 6.00% CLP-1V2-T 5.50% PGP-2-2V 4.00% PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 6.00% PPGU-3-F 0.50%

Example M96

(145) TABLE-US-00107 APUQU-2-F 3.00% Clearing point [ C.]: 75.5 CC-3-V 49.50% n [589 nm, 20 C.]: 0.1132 CC-3-V1 8.50% [1 kHz, 20 C.]: 2.5 CLP-1V-1 6.00% .sub. [1 kHz, 20 C.]: 5.1 CLP-3-T 4.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 14.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PGP-3-2V 2.50% K.sub.1 [pN, 20 C.]: 15.1 PGUQU-3-F 2.50% K.sub.3 [pN, 20 C.]: 15.0 PP-1-2V1 7.00% PPGU-3-F 0.50% PUQU-3-F 2.00

Example M97

(146) TABLE-US-00108 APUQU-2-F 7.50% Clearing point [ C.]: 76.0 CC-3-V 50.00% n [589 nm, 20 C.]: 0.1091 CC-3-V1 9.50% [1 kHz, 20 C.]: 2.5 CLP-1V-1 6.00% .sub. [1 kHz, 20 C.]: 5.1 CLP-3-T 4.50% .sub. [1 kHz, 20 C.]: 2.6 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PP-1-2V1 7.00% K.sub.1 [pN, 20 C.]: 15.2 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 15.0

Example M98

(147) TABLE-US-00109 APUQU-2-F 7.50% Clearing point [ C.]: 76.5 CC-3-V 52.00% n [589 nm, 20 C.]: 0.1062 CC-3-V1 7.50% [1 kHz, 20 C.]: 2.5 CCP-V-1 2.00% .sub. [1 kHz, 20 C.]: 5.1 CLP-1V-1 6.00% .sub. [1 kHz, 20 C.]: 2.6 CLP-3-T 4.50% .sub.1 [mPa .Math. s, 20 C.]: 50 PGP-2-2V 14.00% PP-1-2V1 6.00% PPGU-3-F 0.50%

Example M99

(148) TABLE-US-00110 CC-3-V 46.00% CC-3-V1 7.00% CLP-1V-1 8.00% CLP-3-T 7.00% PGP-1-2V 2.00% PGP-2-2V 14.50% PP-1-2V1 9.00% PPGU-3-F 0.50% PUQU-3-F 4.50% PGUQU-3-F 1.50%

Example M100

(149) TABLE-US-00111 APUQU-2-F 7.50% Clearing point [ C.]: 81.5 DGUQU-4-F 5.00% n [589 nm, 20 C.]: 0.0989 DPGU-4-F 4.50% [1 kHz, 20 C.]: 6.1 PGUQU-3-F 3.00% .sub. [1 kHz, 20 C.]: 9.1 PPGU-3-F 0.50% .sub. [1 kHz, 20 C.]: 3.0 CLP-1V-1 3.50% .sub.1 [mPa .Math. s, 20 C.]: 58 CC-3-2V1 5.00% K.sub.1 [pN, 20 C.]: 14.8 CC-3-V 50.00% K.sub.3 [pN, 20 C.]: 15.2 CC-3-V1 8.00% CLP-3-T 5.00% PGP-2-2V 8.00%

Example M101

(150) TABLE-US-00112 CC-3-V 48.00% CC-3-V1 10.50% CCP-V-1 11.00% CLP-V-1 6.00% CLP-1V2-T 2.50% CLP-3-T 3.00% PGP-2-2V 5.00% PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 5.00% PPGU-3-F 0.50%

Example M102

(151) TABLE-US-00113 CC-3-V 49.50% CC-3-V1 10.00% CCP-V-1 10.00% CLP-1V-1 6.00% CLP-1V2-T 5.50% PGP-2-2V 4.00% PGUQU-3-F 4.00% APUQU-2-F 4.50% PP-1-2V1 6.00% PPGU-3-F 0.50%

Example M103

(152) TABLE-US-00114 APUQU-2-F 4.00% Clearing point [ C.]: 76.5 PGUQU-3-F 3.00% n [589 nm, 20 C.]: 0.1182 PPGU-3-F 0.50% [1 kHz, 20 C.]: 2.4 CCP-V-1 4.00% .sub. [1 kHz, 20 C.]: 5.1 PGP-1-2V 6.00% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 15.50% .sub.1 [mPa .Math. s, 20 C.]: 50 PP-1-2V1 6.00% K.sub.1 [pN, 20 C.]: 14.4 CC-3-V 52.00% K.sub.3 [pN, 20 C.]: 14.6 CC-3-V1 4.50% CLP-1V2-T 4.50%

Example M104

(153) TABLE-US-00115 APUQU-2-F 7.00% Clearing point [ C.]: 77 PGUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1179 PPGU-3-F 0.50% [1 kHz, 20 C.]: 4.0 CCP-V-1 1.00% .sub. [1 kHz, 20 C.]: 6.8 PGP-1-2V 4.00% .sub. [1 kHz, 20 C.]: 2.8 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 53 PP-1-2V1 4.50% K.sub.1 [pN, 20 C.]: 14.4 CC-3-V 50.00% K.sub.3 [pN, 20 C.]: 14.8 CC-3-V1 5.00% CC-3-2V1 2.00% CLP-1V2-T 5.00%

Example M105

(154) TABLE-US-00116 APUQU-2-F 5.50% Clearing point [ C.]: 81 DGUQU-4-F 5.50% n [589 nm, 20 C.]: 0.0982 DPGU-4-F 5.00% [1 kHz, 20 C.]: 6.1 PGUQU-3-F 3.00% .sub. [1 kHz, 20 C.]: 9.0 PPGU-3-F 0.50% .sub. [1 kHz, 20 C.]: 3.0 CCP-V-1 1.00% .sub.1 [mPa .Math. s, 20 C.]: 60 CC-3-2V1 9.00% K.sub.1 [pN, 20 C.]: 15.3 CC-3-V 48.00% K.sub.3 [pN, 20 C.]: 15.5 CC-3-V1 7.00% CLP-3-T 4.00% CLP-1V-T 3.00% PGP-2-2V 8.50%

Example M106

(155) TABLE-US-00117 CC-3-V 50.00% Clearing point [ C.]: 83 CC-3-V1 11.50% n [589 nm, 20 C.]: 0.0943 CLP-V-1 11.00% [1 kHz, 20 C.]: 2.7 CLP-1-V1 6.00% .sub. [1 kHz, 20 C.]: 5.2 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 2.5 PGP-2-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 53 PGUQU-3-F 3.00% K.sub.1 [pN, 20 C.]: 16.6 APUQU-3-F 5.00% K.sub.3 [pN, 20 C.]: 17.3 PP-1-2V1 4.00% PPGU-3-F 0.50%

Example M107

(156) TABLE-US-00118 CC-3-V 51.50% Clearing point [ C.]: 82 CC-3-V1 11.50% n [589 nm, 20 C.]: 0.0923 CLP-1V-1 9.00% [1 kHz, 20 C.]: 2.7 CLP-V2-1 6.50% .sub. [1 kHz, 20 C.]: 5.2 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 2.5 PGP-2-2V 2.00% .sub.1 [mPa .Math. s, 20 C.]: 54 PGUQU-3-F 3.00% K.sub.1 [pN, 20 C.]: 16.5 APUQU-2-F 5.00% K.sub.3 [pN, 20 C.]: 18.0 PP-1-2V1 5.00% PPGU-3-F 0.50%

Example M108

(157) TABLE-US-00119 CC-3-V 50.00% Clearing point [ C.]: 81 CC-3-V1 11.50% n [589 nm, 20 C.]: 0.0956 CLP-1V-1 11.00% [1 kHz, 20 C.]: 2.7 CLP-V2-1 6.00% .sub. [1 kHz, 20 C.]: 5.2 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 2.5 PGP-2-2V 1.00% .sub.1 [mPa .Math. s, 20 C.]: 51 PGUQU-3-F 3.00% K.sub.1 [pN, 20 C.]: 16.4 APUQU-2-F 5.00% K.sub.3 [pN, 20 C.]: 17.3 PP-1-2V1 6.00% PPGU-3-F 0.50%

Example M109

(158) TABLE-US-00120 CC-3-V 51.50% CC-3-V1 11.50% CLP-1V-1 8.00% CLP-V2-1 6.00% CLP-3-T 6.50% PGP-2-2V 2.00% PGUQU-3-F 3.00% APUQU-2-F 5.00% PP-1-2V1 6.00% PPGU-3-F 0.50%

Example M110

(159) TABLE-US-00121 CC-3-2V1 1.00% Clearing point [ C.]: 77.5 CC-3-V 50.00% n [589 nm, 20 C.]: 0.1175 CC-3-V1 2.00% [1 kHz, 20 C.]: 4.2 CCP-V-1 2.00% .sub. [1 kHz, 20 C.]: 7.0 CLP-3-T 6.00% .sub. [1 kHz, 20 C.]: 2.7 CLP-1V-1 6.50% .sub.1 [mPa .Math. s, 20 C.]: 54 PGP-2-2V 11.50% K.sub.1 [pN, 20 C.]: 16.6 PP-1-2V1 7.00% K.sub.3 [pN, 20 C.]: 14.9 PGU-4-T 3.50% PGUQU-3-F 5.00% PGUQU-4-F 5.00% PPGU-3-F 0.50%

Example M111

(160) TABLE-US-00122 APUQU-2-F 3.00% Clearing point [ C.]: 76.5 CC-3-V 49.50% n [589 nm, 20 C.]: 0.1178 CC-3-V1 6.00% [1 kHz, 20 C.]: 2.4 CLP-1V-1 6.00% .sub. [1 kHz, 20 C.]: 5.0 CLP-3-T 4.50% .sub. [1 kHz, 20 C.]: 2.7 PGP-1-2V 3.00% .sub.1 [mPa .Math. s, 20 C.]: 50 PGP-2-2V 13.00% K.sub.1 [pN, 20 C.]: 15.2 PGP-3-2V 2.50% K.sub.3 [pN, 20 C.]: 15.1 PGUQU-3-F 2.00% PP-1-2V1 8.00% PPGU-3-F 0.50% PUQU-3-F 2.00%

Example M112

(161) TABLE-US-00123 APUQU-2-F 2.00% Clearing point [ C.]: 75 PGUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1171 PPGU-3-F 0.50% [1 kHz, 20 C.]: 2.4 CCP-V-1 2.50% .sub. [1 kHz, 20 C.]: 5.0 LPP-3-2 3.50% .sub. [1 kHz, 20 C.]: 2.7 PGP-2-2V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 46 PP-1-2V1 9.00% K.sub.1 [pN, 20 C.]: 15.3 CC-3-V 51.00% K.sub.3 [pN, 20 C.]: 14.3 CC-3-V1 5.00% CLP-3-T 4.50% CLP-1V-1 2.00%

Example M113

(162) TABLE-US-00124 CC-3-V 46.00% Clearing point [ C.]: 77.5 CC-3-V1 6.00% n [589 nm, 20 C.]: 0.1196 CLP-1V-1 1.50% [1 kHz, 20 C.]: 2.9 PGP-2-2V 11.00% .sub. [1 kHz, 20 C.]: 6.8 PGP-3-2V 2.00% .sub. [1 kHz, 20 C.]: 3.9 PGU-2-F 6.50% .sub.1 [mPa .Math. s, 20 C.]: 57 PGUQU-3-F 5.00% K.sub.1 [pN, 20 C.]: 15.6 CLP-3-T 5.00% K.sub.3 [pN, 20 C.]: 14.2 B(S)-2O-O4 3.50% B(S)-2O-O5 3.50% CC-3-2V1 1.00% DGUQU-4-F 1.50% PY-3-O2 2.50% CLP-1-V1 5.00%

Example M114

(163) TABLE-US-00125 APUQU-2-F 4.50% PGUQU-3-F 4.00% PPGU-3-F 0.50% CLP-1V-1 6.00% PGP-1-2V 2.50% PGP-2-2V 16.50% PP-1-2V1 7.50% CC-3-V 52.50% CC-3-V1 6.00%

Example M115

(164) TABLE-US-00126 CC-3-V 47.50% Clearing point [ C.]: 79.5 CC-3-V1 5.50% n [589 nm, 20 C.]: 0.1178 PGP-2-2V 12.00% [1 kHz, 20 C.]: 2.9 PGP-3-2V 2.50% .sub. [1 kHz, 20 C.]: 6.6 PGU-2-F 5.50% .sub. [1 kHz, 20 C.]: 3.8 PGUQU-3-F 2.00% .sub.1 [mPa .Math. s, 20 C.]: 58 CLP-3-T 5.00% K.sub.1 [pN, 20 C.]: 15.8 B(S)-2O-O4 3.50% K.sub.3 [pN, 20 C.]: 14.7 B(S)-2O-O5 3.50% CC-3-2V1 2.50% DGUQU-4-F 3.00% CLP-1V-1 4.50% PGIY-2-O4 1.50% APUQU-2-F 1.50%

Example M116

(165) TABLE-US-00127 CC-3-V 47.50% Clearing point [ C.]: 81.5 CC-3-V1 2.00% n [589 nm, 20 C.]: 0.1195 PGP-2-2V 12.00% [1 kHz, 20 C.]: 2.9 PGP-3-2V 1.00% .sub. [1 kHz, 20 C.]: 6.7 PGU-2-F 7.50% .sub. [1 kHz, 20 C.]: 3.8 PGUQU-3-F 1.00% CLP-3-T 5.00% B(S)-2O-O4 3.50% B(S)-2O-O5 3.50% CC-3-2V1 3.00% DGUQU-4-F 3.00% CLP-1V-1 4.00% PGIY-2-O4 1.00% APUQU-2-F 1.00% CLP-V-1 5.00%

Example M117

(166) TABLE-US-00128 APUQU-2-F 6.00% Clearing point [ C.]: 80 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1129 PGUQU-3-F 2.00% [1 kHz, 20 C.]: 3.9 PPGU-3-F 0.50% .sub. [1 kHz, 20 C.]: 6.7 CCP-V-1 2.50% .sub. [1 kHz, 20 C.]: 2.8 PGP-1-2V 4.00% .sub.1 [mPa .Math. s, 20 C.]: 52 PGP-2-2V 16.50% K.sub.1 [pN, 20 C.]: 14.1 CC-3-V 52.00% K.sub.3 [pN, 20 C.]: 14.1 CC-3-V1 6.50% V.sub.0 [V, 20 C.]: 2.03 CLP-3-T 5.00%

(167) Liquid-crystalline mixture M117 is additionally stabilized with 0.05% of the compound of the formula ST-1

(168) ##STR00431##

Example M118

(169) TABLE-US-00129 APUQU-2-F 5.00% Clearing point [ C.]: 80 PGUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1131 PPGU-3-F 0.50% [1 kHz, 20 C.]: 3.5 CCP-V-1 8.50% .sub. [1 kHz, 20 C.]: 6.2 PGP-2-2V 16.50% .sub. [1 kHz, 20 C.]: 2.7 PP-1-2V1 4.00% .sub.1 [mPa .Math. s, 20 C.]: 51 CC-3-V 48.00% K.sub.1 [pN, 20 C.]: 14.6 CC-3-V1 6.50% K.sub.3 [pN, 20 C.]: 14.7 CLP-3-T 5.00% V.sub.0 [V, 20 C.]: 2.17

(170) Liquid-crystalline mixture M118 is additionally stabilized with 0.05% of the compound of the formula ST-1

(171) ##STR00432##

Example M119

(172) TABLE-US-00130 APUQU-2-F 2.50% Clearing point [ C.]: 85 CC-3-2V1 5.00% n [589 nm, 20 C.]: 0.1093 CC-3-V 24.50% [1 kHz, 20 C.]: 8.6 CC-3-V1 5.00% .sub. [1 kHz, 20 C.]: 10.6 CCP-3OCF.sub.3 3.00% .sub. [1 kHz, 20 C.]: 2.0 CCP-V-1 9.00% .sub.1 [mPa .Math. s, 20 C.]: 94 CCP-V2-1 8.00% K.sub.1 [pN, 20 C.]: 14.9 CLP-3-T 7.00% K.sub.3 [pN, 20 C.]: 14.6 CPGP-4-3 2.00% V.sub.0 [V, 20 C.]: 1.39 DGUQU-4-F 5.00% DPGU-4-F 5.50% PGP-2-2V 2.00% PGUQU-3-F 6.00% PGUQU-4-F 6.00% PPGU-3-F 0.50% Y-4O-O4 9.00%

(173) Liquid-crystalline mixture M119 is additionally stabilized with 0.04% of the compound of the formula ST-1 and with 0.02% of the compound of the formula ST-3

(174) ##STR00433##

(175) The preceding examples can be repeated with similar success by substituting the generically or specifically described reactants and/or operating conditions of this invention for those used in the preceding examples.

(176) From the foregoing description, one skilled in the art can easily ascertain the essential characteristics of this invention and, without departing from the spirit and scope thereof, can make various changes and modifications of the invention to adapt it to various usages and conditions.