Electrically conductive, gas-sealed, aluminum-to-aluminum connection and methods of making same
10510520 ยท 2019-12-17
Assignee
Inventors
- Stephen Schwed (Bridgewater, NJ, US)
- Edward William Douglas (Mendham, NJ, US)
- Stephen Diego Pellegrino (Randolph, NJ, US)
- Christopher Rempel (Morristown, NJ, US)
Cpc classification
H01J47/005
ELECTRICITY
International classification
H01J47/00
ELECTRICITY
Abstract
Various configurations of electrically conductive, gas-sealed connections between two pieces of aluminum are described along with methods of making an electrically conductive, gas-sealed connection between two pieces of aluminum.
Claims
1. An electrically conductive, gas-sealed, aluminum-to-aluminum connection comprising: a first piece of aluminum; a second piece of aluminum; the first and second pieces of aluminum being electrically connected by galling between a first segment of the first piece of aluminum and a corresponding first segment of the second piece of aluminum, a high elongation polymer, located between a second segment of the first piece of aluminum and a corresponding second segment of the second piece of aluminum, such that the second segments are spaced apart from each other, with the high elongation polymer in between, the high elongation polymer having a thickness, measured normal to one of the second segments, that is greater than 76.2 micrometers; and wherein the combination of the first and second segments, and high elongation polymer, form a seal having a Helium gas leak rate of less than 110.sup.8 bar l/s, measured by a mass spectrometer leak detector.
2. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the thickness of the high elongation polymer is less than 500 micrometers.
3. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein at least one of the first segments includes at least one protrusion.
4. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the second segment of the first piece of aluminum is a terminal end surface.
5. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the second segment of the second piece of aluminum is a terminal end surface.
6. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the first segment of the first piece of aluminum is a terminal end surface.
7. The electrically conductive, gas-sealed, aluminum-to-aluminum connection of claim 1, wherein the first segment of the second piece of aluminum is a terminal end surface.
8. A method of making an electrically conductive, gas-sealed, connection, the method comprising: i) applying a curable high elongation polymer to at least one of two pieces of aluminum, each having a first segment and a second segment, wherein the first segments are correspondingly positioned relative to each other, and the second segments are correspondingly positioned relative to each other, the applying being performed such that the second segment of the at least one of the two pieces of aluminum contains the high elongation polymer and the first segments are substantially free of the high elongation polymer; and ii) causing a relative sliding motion between the first segments of the two pieces of aluminum to cause galling between the respective first segments, while the respective second segments remain spaced apart from each other, but in contact with the high elongation polymer such that, when the high elongation polymer is cured, a flexible seal will exist between the respective second segments, and the joined first and second segments will collectively form an electrically conductive, gas-sealed, connection between the first and second pieces of aluminum with a Helium gas leak rate of less than 110.sup.8 bar l/s.
9. The method of claim 8, wherein, during ii), the respective second segments remain spaced apart from each other by a spacing greater than 76.2 micrometers and less than 500 micrometers, measured normal to the two pieces of aluminum at corresponding locations of the second segments.
10. An electrically conductive, gas-sealed, aluminum-to-aluminum connection comprising: an aluminum tube having an open end; an aluminum end cap; the aluminum tube and aluminum end cap being electrically connected by galling between a first segment of the aluminum end cap and a corresponding first segment of the aluminum tube, and a high elongation polymer, located between a second segment of the aluminum tube and a corresponding second segment of the aluminum end cap, the second segments being spaced apart from each other such that the high elongation polymer has a thickness, measured normal to one of the second segments, that is greater than 76.2 micrometers; wherein the combination of the first and second segments, and high elongation polymer, form a seal having a Helium gas leak rate of less than 110.sup.8 bar l/s, measured by a mass spectrometer leak detector.
11. The connection of claim 10, wherein the spacing between the second segments is less than 500 micrometers when measured in a radial direction.
12. The connection of claim 10 wherein the first segments are located between the second segments and an interior volume defined by an interior wall of the aluminum tube.
13. The connection of claim 10, wherein the second segments are located between the first segments and an interior volume defined by an interior wall of the aluminum tube.
14. The connection of claim 10, wherein at least one of the first segments includes at least one protrusion.
15. The connection of claim 10, wherein at least one of the first segments is located on an interior wall of the aluminum tube.
16. The connection of claim 10, wherein at least one of the first segments is located on an exterior wall of the aluminum tube.
17. The connection of claim 10, wherein at least one of the second segments is located on an interior wall of the aluminum tube.
18. The connection of claim 10, wherein at least one of the second segments is located on an exterior wall of the aluminum tube.
19. The connection of claim 10, wherein the second segment of the aluminum tube includes a terminal end surface of the aluminum tube.
20. A method of sealing an aluminum tube to an aluminum end cap comprising: i) applying a curable high elongation polymer to at least one of an aluminum tube or an aluminum end cap, each having a first segment and a second segment, wherein, when assembled, the first segments are correspondingly positioned relative to each other, and the second segments are correspondingly positioned relative to each other, the applying being performed such that the second segment of the at least one of the aluminum tube or aluminum end cap contains the high elongation polymer and the first segments are substantially free of the high elongation polymer; and ii) causing a relative sliding motion between the first segments of the aluminum tube and aluminum end cap to cause galling between the respective first segments, while the respective second segments remain spaced apart from each other, but in contact with the high elongation polymer such that, when the high elongation polymer is cured, a flexible seal will exist between the respective second segments to form a gas-sealed, connection between the aluminum tube and aluminum end cap with a Helium gas leak rate of less than 110.sup.8 bar l/s, and the joined first segments form an electrically conductive path between the aluminum tube and aluminum end cap.
21. The method of claim 20 wherein, prior toi) the method further comprises: roughening at least one of: a) the second segment of the aluminum end cap, or b) the second segment of the aluminum tube.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) This disclosure is further described in the detailed description that follows, with reference to the drawings, wherein the same reference numerals refer to the same parts throughout the various views, in which:
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DETAILED DESCRIPTION
(30) U.S. patent application Ser. No. 15/971,894, U.S. Provisional Patent Application No. 62/667,309 and International Application No. PCT/US19/28585 are each incorporated herein by reference in their entirety.
(31) Our technical solution improves upon current technology and provides a solution to aforementioned problems.
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(34) As shown in
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(37) As shown, the aluminum end cap 104 of
(38) In addition, the aluminum end cap 106 includes a fill tube opening 404 that can be used to introduce the reactive gas into an assembled muon drift tube 100 and then sealed.
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(40) As noted above, the equipment and time involved in creation of those features 502, 504 add significant cost to the manufacture of muon drift tubes 100 and require significant expertise to ensure creation of a proper seal.
(41) What follows is a description of the components and method for construction of a muon drift tube that requires fewer parts, is simpler to manufacture, and does not require all the expensive and complex equipment needed to manufacture a muon drift tube as described in connection with
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(46) At this point, it should be understood that, as with the conventional end caps 104, 106, the fill tube opening 404 and fill tube 702 could be in either style cap 600, 700, the placement being one of design choice. In addition, it is to be further understood that an end cap as described herein can be constructed that is neither a male type nor a female type end cap.
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(48) Having shown the relevant components, various examples of our simplified approach to joining two pieces of aluminum in a way that is appropriate for constructing a muon drift tube and, more particularly, achieving the requisite gas seal that will ensure a Helium gas leak rate of less than 110.sup.8 bar l/s, between those two pieces of aluminum, for example, an aluminum tube and aluminum end cap, will now be discussed using different variant aluminum end cap configurations.
(49) As an initial matter, it is to be understood that, although a particular variant may be shown in connection with a male style, a female style or generic style end cap, unless otherwise expressly noted herein, each such connection variant could be used with any other style end cap in addition to, or as alternatives to, the ones described herein.
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(51) As shown in
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(53) In order to create an electrically conductive connection, relative motion between two closely spaced aluminum surfaces, under pressure and without lubrication, is used. As shown in the enlarged portion of
(54) Although specific dimensions in the foregoing paragraph are provided for purposes of explanation and understanding, the spacing needed to create the interference fit will be a straightforward function of lubricity and hardness of the tube and end cap materials, as well as the axial length of the intended interference fit and, in the case of the most common muon tube geometry, a round tube, the outer and/or inner diameter of the tube (depending upon which is used for the interference fit. In general, the fit should be close enough to allow for the relative sliding motion between the two aluminum components while concurrently being close enough to cause sufficient galling between them to create an electrical connection of minimal electrical resistivity appropriate for the intended use.
(55) As is also shown in the enlarged portion of
(56) In general, high elongation polymers suitable for use as described herein will typically have elongations in the 30% to 500% range, although higher elongations may be acceptable for some applications, with elongations in the 250% to 500% range being contemplated as more typical. Nevertheless, materials with elongations in the range of 100% to 250% can be used for some applications, as can, in some applications, materials with elongations in the 30% to 100% range.
(57) In general, the high elongation polymer to be used will be one that, at a minimum, can be exposed to, in the case of a sealed muon drift tube, the highest operating environment temperature (typically about 55 C.) for normal operational time periods without degradation and should, but need not always, also remain above its glass transition temperature (Tg) at least at the lowest typical operating temperature (typically about 40 C.).
(58) In addition, the high elongation polymer 1002 will typically be a two-part polymer, although the two part aspect is not required, that will be applied in precursor form either prior to interference fitting or after the interference fit is formed (the latter being subject to an appropriately selected gap size, high elongation polymer viscosity, and the ability to inject the selected high elongation polymer into the gap post-fitting) and, in either case, that will cure in situ. In the latter case, injecting the high elongation polymer may involve directly introducing it via the open end of the gap, if accessible, or injecting the high elongation polymer into the gap thorough one or more openings provided for that purpose and that will not provide a path for gas within the aluminum tube that bypasses the portion of the seal made up of the interference fit aluminum segments.
(59) Numerous suitable high elongation polymers can be used, depending upon the particular gap spacing. By way of representative, non-limiting, examples, some suitable high elongation polymers include: Epiclon EXA-4816 commercially available from Sun Chemical Corporation, 35 Waterview Boulevard, Parsippany, N.J. 07054, Max Cast AB commercially available from Polymer Composites Inc., 1871 S. Lake Place, Ontario, Calif. 91761, Epoxonic EX 2840 commercially available from Epoxonic GmbH, Reaktionsharzsysteme, Gewerbestrasse 16, 85652 Landsham/Pliening, Germany, Permabond Mont. 3809 commercially available from Permabond LLC, 14 Robinson St., Pottstown, Pa. 19464, MasterSil 157 commercially available from Master Bond Inc, 154 Hobart Street, Hackensack, N.J. 07601, TS-33D commercially available from Silicone Solutions, 338 Remington Rd. Cuyahoga Falls, Ohio 44224, 3M 551 commercially available from 3M Company, 3M Center, St. Paul, Minn. 55144, Loctite UK 3173 commercially available from Henkel Corp., 200 Elm Street, Stamford, Conn. 06902, EP21TPND commercially available from Master Bond Inc., 154 Hobart Street, Hackensack, N.J. 07601, PR-1440 commercially available from the PPG Aerospace unit of PPG Industries, Inc., 12780 San Fernando Road, Sylmar, Calif. 91342, and Viton-containing high elongation polymers such as THA-3000 commercially available from Thermodyn Corp., 3550 Silica Rd., Sylvania, Ohio 43500, and PLV-3145 commercially available from Pelseal Technologies, LLC, 3161 State Road, Ste. G, Bensalem, Pa. 19020.
(60) In general, the selection of the particular high elongation polymer will be a function of the gap spacing, in the axial and/or radial direction, between the corresponding second segments and the viscosity of the particular high elongation polymer. As a guide, a high elongation polymer viscosity in the vicinity of 3,000 centipoise (cP) would be appropriate for a spacing in the range of about 0.0762 mm (0.003) to 0.127 mm (0.005), whereas a high elongation polymer viscosity in the vicinity of 10,000 cP to 100,000 cP would be more appropriate for a spacing in the range of about 0.254 mm (0.01) to 0.382 mm (0.015). For a spacing of about 0.508 mm (0.02) high elongation polymer viscosities in the range of 100,000 cP to 10,000,000 cP can be used.
(61) Thus, it should now be generally understood that the connection formed by the segments 908A, 908B, 910A, 910B results in an overall electrically conductive, gas-sealed connection between the aluminum tube and aluminum end cap.
(62) Optionally, for some variants, one or both of the second segments (i.e., of the aluminum tube and/or aluminum end cap) may be surface roughened to promote better adherence of the high elongation polymer to the segments. The surface roughening can be created using any appropriate means, for example, any known mechanical means, such as abrasion or knurling, or any appropriate known chemical means, for example, as disclosed in U.S. Pat. No. 9,493,878, incorporated herein by reference, or any other approach that results in a roughened surface and that does not impede adherence of the selected high elongation polymer.
(63) Now, as shown in the segment configuration of
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(65) In addition, as represented in
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(68) As shown in
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(70) The variant of
(71) Advantageously, for some implementations employing the teachings of
(72) A further advantage arising from some implementations according to the teachings of
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(74) As shown in
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(77) As shown in
(78) Up until now, the foregoing variant examples have been described in connection with an aluminum end cap that interference fits inside of an aluminum tube. It should also be understood that implementations can be constructed that are the reverse, in that the connection aspects described in connection with the aluminum end cap, e.g., features like roughening, protrusion, high-elongation polymer placement, etc., could be present on the aluminum tube instead and the connection aspects described in connection with the aluminum tube could be present on the aluminum end cap instead. In addition, in some variants, the connection aspects, e.g., features like surface roughening, protrusion placement, high-elongation polymer placement, etc., could be on both the aluminum tube and aluminum end cap.
(79) Likewise, it should be understood that same approaches can be used for variants where an aluminum tube fits inside of an aluminum end cap, or an aluminum end cap surrounds an aluminum tube.
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(81) Likewise, where the outer circumferential surface 1704 of the groove 1702 forms all or part the interference fit with an aluminum tube, a) another portion of that surface 1704 can be the segment where the high elongation polymer will be located, and/or b) the inner circumferential surface 1706 of the groove 1702 can be all or part of the surface where high elongation polymer will be located.
(82) Conversely, where the inner circumferential surface 1706 of the groove 1702 forms all or part the interference fit with an aluminum tube, a) another portion of that surface 1706 can be the segment where the high elongation polymer will be located, and/or b) the outer circumferential surface 1704 of the groove 1702 can be all or part of the surface where high elongation polymer will be located.
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(88) In addition, as represented in
(89) Moreover, as can be seen in
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(92) As shown in
(93) In contrast, the aluminum end cap 2104 on the right side of the figure is coupled to the aluminum tube 906 such that the first segments 908A, 908B that are interference fit are on the exterior surface of the tube 906 and abut the larger diameter surface of the groove, whereas the second segments 910A, 910B are on the interior surface of the tube with the high elongation polymer 1002 located in between.
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(95) As shown in enlarged view alternative A of
(96) In contrast, with this variant configuration, the terminal end 2204 of the aluminum tube 906 forms the second segment 901B of the aluminum tube 906 and the second segment 910A of the aluminum end cap includes the deepest part of the groove 1702 along with the sections of the larger and smaller diameter surfaces of the groove 1702 that are beyond the terminal end 2204 of the aluminum tube 906, such that the high elongation polymer 1002 (indicated using diagonal hashing) will be located in between.
(97) Enlarged view alternative B of
(98) Enlarged view alternative C of
(99) As noted previously, configurations similar to
(100) Having described numerous variant components that can be used to make a muon drift tube that includes an electrically conductive, gas-sealed connection between an aluminum end cap and the aluminum tube, an example of method for making a muon drift tube according to the teachings herein will now be described.
(101) The method involves: i) threading an anode wire through an aluminum tube having a first end, a second end, and a longitudinal axis, such that the wire extends beyond both the first end and second end of the aluminum tube, ii) inserting a first end of the anode wire into a first electrode located within, but electrically isolated from, a first end cap; and iii) inserting a second end of the anode wire into a second electrode located within, but electrically isolated from, a second end cap.
(102) Steps i), ii) and iii) can occur in any order, provided that steps ii) and iii) cannot likely both occur prior to step i) for most implementations.
(103) The method then involves, in one variant approach, at some point, before, concurrent with, or following completion of, any one or more of steps i)-iii) but before coupling of the specific part to which the high elongation polymer will be applied, applying a high elongation polymer, as described herein (selected consistent with the gap in which it will be used) to a second segment of at least one of the first part of the first end cap, or a second segment of the first end of the aluminum tube, while ensuring that a first segment of both the first part of the first end cap and a first segment of the second end of the aluminum tube is substantially free of the high elongation polymer. This may be performed by applying the high elongation polymer to only select portions of the appropriate component(s) or by more broadly applying the high elongation polymer and then removing some of the applied high elongation polymer that need to be substantially free of the high elongation polymer, for example, to ensure a good electrically conductive connection can be formed. Note here that substantially free as used herein is intended to mean that there can be some minor residual high elongation polymer in the areas that are intended to be free of the high elongation polymer, resulting from the application process or that may occur during joining of components, the important aspect being that whatever high elongation polymer is present, it is not present in a sufficient amount or over a sufficient area such that the desired electrically conductive connection cannot or will not be formed. Alternatively, with the appropriately selected gap spacing and high elongation polymer, this step can be delayed until after the aluminum end cap and aluminum tube are joined.
(104) The method then involves, for the variants where the high elongation polymer is applied prior to joining: iv) coupling a first part of the first end cap to the first end of the aluminum tube and coupling a first part of the second end cap to the second end of the aluminum tube, (bearing in mind that application of the high elongation polymer must occur before the particular part is coupled in this step). This coupling of the first part of an end cap to an end of the aluminum tube comprises interference fitting the first part of the first end cap and the first end of the aluminum tube together such that galling will occur between the respective first segments and a flexible seal will be formed by the high elongation polymer located between the respective second segments, such that the first and second segments collectively form an electrically conductive, gas-sealed, connection between the first end cap and the aluminum tube.
(105) For variant approaches where the high elongation polymer is not applied prior to coupling a first part of the first end cap to the first end of the aluminum tube and/or coupling a first part of the second end cap to the second end of the aluminum tube, once the coupling of an end cap to an end of the aluminum tube is complete, at any time thereafter, but prior to insertion of the reactive gas, the high elongation polymer will be injected into the gap and cured to form the flexible seal.
(106) Next, the method involves, depending upon approach variant, either before or after creating the seal with the high elongation polymer, v) tensioning the anode wire such that the longitudinal axis of the aluminum tube and the anode wire are co-linear; and, finally vi) coupling portions of the tensioned anode wire, associated with the first and second ends of the tensioned anode wire, to the first and second electrodes.
(107) While this is just one simplified example of how to make a muon drift tube according to the teachings herein, any other method of making a muon drift tube, including conventional methods, that can be straightforwardly modified to be compatible with, and/or accommodate, the configuration variants described herein can be used.
(108) It is to be noted and understood that although certain geometries have been illustrated for the various tubes, end caps, grooves, protrusions, limiting features, etc., those were provided merely for purposes of illustration and understanding, and that numerous other variations and modifications of those aspects, by way of non-limiting example, rounded as opposed to squared corners or vice versa, different size, number or shaped protrusions, filleting, tapering, smooth or abrupt transitions, use of tube shapes other than round, etc. can be straightforwardly incorporated without departing from the teachings herein, the permutations and combinations of those variations being straightforwardly usable by one of ordinary skill in light of the teachings herein. Moreover, roughening can be used on the segments that form the interference fit connection, provided that the connection made does not have an undesirably high resistivity for the intended application.
(109) It is also to be noted and understood that, merely for purposes of illustration, in some figures and the associated description, the end cap connections to the tube are shown as using different variants at opposite ends. In reality, while the use of two different variants of end cap to tube connections could be used on different ends of a given tube to construct a muon drift tube, in practice, in many implementation cases, the same connection style will be used on both ends. Thus, it should be understood that the use of the same variant style of connection on both ends of the tube and different variant styles on opposite ends of the tube are all contemplated. Moreover, it is contemplated that, in some cases, a connection variant consistent with the teachings herein may be used on one end of a muon drift tube, while an opposite end may incorporate a conventional connection between the end cap and tube. Thus, the description herein should not be considered as requiring any particular muon drift tube to have more than one end cap-to-tube coupling constructed consistent with the teachings herein.
(110) Finally, while the foregoing description has focused specifically on joining an end cap to a tube, the same approaches can be used to join two aluminum tubes together using a sleeve coupling in place of the end cap where both electrical conductivity and a gas seal as described herein is desired, for example, to create a longer muon drift tube.
(111) Having described and illustrated the principles of this application by reference to one or more examples, it should be apparent that the embodiment(s) may be modified in arrangement and detail without departing from the principles disclosed herein and that it is intended that the application be construed as including all such modifications and variations insofar as they come within the spirit and scope of the subject matter disclosed.