Stirrer producing intermittent jet flow

Abstract

The problem of providing a stirrer capable of more effectively shearing a fluid to be treated is addressed, by using the action of an intermittent jet stream. A stirrer is provided with a rotor having a blade and a screen, which are relatively rotated such that the fluid to be treated is discharged from the inside of the screen to the outside as an intermittent jet stream through a slit in the screen, the stirrer satisfying condition 1 and condition 2. (Condition 1) the relationship among the width b in the rotating direction of a tip part of the blade, the width s in the circumferential direction of the slit, and the width t in the circumferential direction of the screen member is b2s+t. (Condition 2) the relationship between the width b in the rotating direction of the tip part of the blade and the maximum inner diameter c of the screen is b0.1c.

Claims

1. A stirrer comprising: a supporting tube; a hollow housing supported by the supporting tube, the hollow housing including a sucking chamber and a sucking port, wherein the hollow housing is configured to suck a fluid to be processed into the sucking chamber via the sucking port then to introduce it to a stirring chamber via a comparting wall; a rotating rotor provided with a plurality of blades and accommodated in the stirring chamber; and a screen arranged around the rotor, wherein the screen is tapered towards a central axis of the supporting tube and is arranged around the rotor; wherein: the rotor and the screen are provided within the hollow housing, each blade includes an edge portion at an outermost circumferential surface thereof, the screen comprises a plurality of slits in a circumferential direction thereof and a screen member located between the slits that are located in a neighborhood to each other, a clearance from the edge portion of each blade to the screen is a constant value, the edge portion of each blade and each slit have a matching region where they are in the same position and overlapped with each other in a longitudinal direction of the respective slit, of the rotor and the screen, at least the rotor is rotated so as to relatively rotate the rotor and the screen thereby ejecting a fluid to be processed in the stirring chamber from inside the screen to outside thereof through the slits as an intermittent jet flow, and the stirrer satisfies following condition 1 and condition 2: (Condition 1) in the matching region, a relationship among a width (b) of the edge portion of each blade in a rotational direction, a width (s) of the respective slit in a circumferential direction, and a width (t) of the screen member in a circumferential direction is shown by b2s+t, and (Condition 2) in the matching region, a relationship between the width (b) of the edge portion of each blade in a rotational direction and a maximum inner diameter (c) of the screen is shown by b0.1c.

2. The stirrer according to claim 1, wherein the width of the slits in a circumferential direction is in a range of 0.2 to 4.0 mm.

3. The stirrer according to claim 1, wherein diameters of each blade and the screen become shorter as each blade and the screen are more apart in an axial direction from an introduction port to introduce the fluid to be processed from the sucking chamber into the screen.

4. The stirrer according to claim 1, wherein: the plurality of the slits have an identical width in the circumferential direction and are formed with an identical interval in the circumferential direction, and the screen does not rotate.

5. The stirrer according to claim 1, wherein a total sum of a cross section area of the plurality of blades in a plane perpendicular to a rotation axis of the rotor is smaller than a cross section area of a space inside the screen.

6. The stirrer according to claim 1, wherein the comparting wall is provided between the sucking port and the plurality of blades, and wherein the comparting wall extends towards the rotor.

7. The stirrer according to claim 1, wherein the sucking port is tapered away from the central axis of the supporting tube.

8. The stirrer according to claim 1, wherein the clearance is between an inner wall of the screen and the edge portion of each blade and is in the range of 0.2 to 4.0 mm, and wherein a fluid to be processed is ejected, as the intermittent jet flow, from inside the screen to outside thereof through the slits located in a front side of the rotational direction of each blade and the fluid to be processed is sucked through the slits located in a back side of the rotational direction of each blade, the stirrer being configured to generate a period between ejection from the slits located in the front side of the rotational direction of each blade and suction from the slits located in the back side of the rotational direction of each blade, where the fluid to be processed becomes static by setting the clearance.

9. A stirrer comprising: a supporting tube; a hollow housing supported by the supporting tube, the hollow housing including a sucking chamber and a sucking port, wherein the hollow housing is configured to suck a fluid to be processed into the sucking chamber via the sucking port then to introduce it to a stirring chamber via a comparting wall; a rotating rotor provided with a plurality of blades and accommodated in the stirring chamber; and a screen arranged around the rotor, wherein the screen is tapered towards a central axis of the supporting tube and is arranged around the rotor; wherein: the rotor and the screen are provided within the hollow housing, each blade includes an edge portion at an outermost circumferential surface thereof, the screen comprises a plurality of slits in a circumferential direction thereof and a screen member located between the slits that are located in a neighborhood to each other, the edge portion of each blade and each slit have a matching region where they are in the same position and overlapped with each other in a longitudinal direction of the respective slit, the rotor is rotated and the screen is rotated in an opposite direction to the rotor thereby ejecting a fluid to be processed in the stirring chamber from inside the screen to outside thereof through the slits as an intermittent jet flow, and the stirrer satisfies following condition 1 and condition 2: (Condition 1) in the matching region, a relationship among a width (b) of the edge portion of each blade in a rotational direction, a width (s) of the respective slit in a circumferential direction, and a width (t) of the screen member in a circumferential direction is shown by b2s+t, and (Condition 2) in the matching region, a relationship between the width (b) of the edge portion of each blade in a rotational direction and a maximum inner diameter (c) of the screen is shown by b0.1c.

10. The stirrer according to claim 9, wherein the width of the slits in a circumferential direction is in a range of 0.2 to 4.0 mm.

11. The stirrer according to claim 9, wherein diameters of each blade and the screen become shorter as each blade and the screen are more apart in an axial direction from an introduction port to introduce the fluid to be processed from the sucking chamber into the screen.

12. The stirrer according to claim 9, wherein: the supporting tube includes a stirring blade located on an outer circumferential surface thereof, the plurality of the slits have an identical width in the circumferential direction and are formed with an identical interval in the circumferential direction.

13. The stirrer according to claim 9, wherein a total sum of a cross section area of the plurality of blades in a plane perpendicular to a rotation axis of the rotor is smaller than a cross section area of a space inside the screen.

14. The stirrer according to claim 9, wherein the comparting wall is provided between the sucking port and the plurality of blades, and wherein the comparting wall extends towards the rotor.

15. The stirrer according to claim 9, wherein the sucking port is tapered away from the central axis of the supporting tube.

16. The stirrer according to claim 9, wherein a clearance between an inner wall of the screen and the edge portion of each blade is in the range of 0.2 to 4.0 mm, and wherein a fluid to be processed is ejected, as the intermittent jet flow, from inside the screen to outside thereof through the slits located in a front side of the rotational direction of each blade and the fluid to be processed is sucked through the slits located in a back side of the rotational direction of each blade, the stirrer being configured to generate a period between ejection from the slits located in the front side of the rotational direction of each blade and suction from the slits located in the back side of the rotational direction of each blade, where the fluid to be processed becomes static by setting the clearance.

Description

(1) FIG. 1 This is the front view showing the state how the stirrer of the present invention is used.

(2) FIG. 2 This is the enlarged vertical sectional view of the essential part of the said stirrer.

(3) FIG. 3 This is the front view showing the state how the stirrer of other embodiment of the present invention is used.

(4) FIG. 4 This is the front view showing the state how the stirrer of still other embodiment of the present invention is used.

(5) FIG. 5 This is the front view showing the state how the stirrer of still other embodiment of the present invention is used.

(6) FIG. 6 (A) is an enlarged view of the essential part of the stirrer according to the embodiment applied with the present invention; (B) is an enlarged view of the essential part showing this action; (C) is an enlarged view of the essential part of the stirrer according to a conventional example; and (D) is an enlarged view of the essential part showing this action.

(7) FIG. 7 This is the sectional view of the essential part of the said stirrer according to the embodiment in which the present invention is applied.

(8) FIG. 8 This is the explanatory drawing of the experimental apparatus according to Examples and Comparative Examples of the present invention.

(9) FIG. 9 This is the graph showing the experimental result of Examples 1A and Comparative Example 1A.

(10) FIG. 10 This is the graph showing the experimental result of Examples 1B and Comparative Example 1B.

(11) FIG. 11 This is the graph showing the experimental result of Example 2.

BEST MODES FOR CARRYING OUT THE INVENTION

(12) Hereunder, the first embodiment of the present invention will be explained based on the drawings.

(13) Firstly, with referring to FIG. 1 and FIG. 2, the basic structure of one example of the stirrer according to the present invention will be explained.

(14) The stirrer according to this embodiment comprises the processing member 1 disposed in the fluid that will be subjected to the processing treatment such as emulsification, dispersion, and mixing and the rotor 2 disposed in the processing member 1.

(15) The processing member 1 is a hollow housing, which is supported by the supporting tube 3 and is arranged either in the accommodating vessel 4 in which the fluid to be processed is accommodated or in the flow path of the fluid to be processed. In this embodiment, it is shown that the processing member 1 is arranged in the front end of the supporting tube 3 and is inserted from the upper side of the accommodating vessel 4 into the lower side therein; however this is not always the case, so that execution of the embodiment may also be possible in such away that the processing member 1 may be supported by the supporting tube 3 so as to be projected from the bottom of the accommodating vessel 4 toward the upper direction thereof, as shown in FIG. 3.

(16) The processing member 1 comprises the sucking chamber 6 having the sucking port 5 through which the fluid to be processed is sucked into inside the chamber from the outside thereof, and the stirring chamber 7 that is connected through to the sucking chamber 6. The circumference of the stirring chamber 7 is stipulated by the screen 9 that has plural slits 8.

(17) Meanwhile, in this specification, explanation will be made as to the screen 9 which is constituted by the slit 18, i.e., a space portion, and the screen member 19, i.e., an actual member located between the slits 18. Therefore, the screen 9 means the entirety including the slit 18 formed in plural screen members 19; and thus, the screen member 19 means each of actually existing members between the neighboring slits 18.

(18) Between the sucking chamber 6 and the stirring chamber 7 is comparted by the comparting wall 10, and these compartments are connected through via the introduction opening 11 that is arranged in the comparting wall 10. However, the sucking chamber 6 and the comparting wall 10 are not essential; and thus, for example, the entirety of the upper part of the stirring chamber 7 may be the introduction opening without arranging the sucking chamber 6 whereby introducing the fluid to be processed in the accommodating vessel 4 directly into the stirring chamber 7, or alternatively the sucking chamber 6 and the stirring chamber 7 may form a configuration of one space in which these chambers are not comparted by the comparting wall 10.

(19) The rotor 2 is a rotating body having plural blades 12 in the circumferential direction; and this rotates with keeping a very narrow clearance between the blades 12 and the screen 9. As to the mechanism to rotate the rotor 2, various rotation drive mechanisms may be used; and in this embodiment, the rotor 2 is arranged in the front end of the rotation axis 13, and this is accommodated in the stirring chamber 7 so as to be able to rotate. In more detail, the rotation axis 13 is inserted through the supporting tube 3 so as to go through the sucking chamber 6 and the opening 11 of the comparting wall 10 until the stirring chamber 7, and is provided with the rotor 2 in its front end (in the drawing, the lower end). The rear end of the rotation axis 13 is connected to the rotation drive mechanism such as the motor 14. The motor 14 is preferably subjected to the control of the control system such as the numerical control or a computer.

(20) In this stirrer, during the time when the rotating blades 12 are passing the inner wall of the screen member 19 by rotation of the rotor 2, a shear force is applied to the fluid to be processed that is present between the blades and the wall whereby executing emulsification, dispersion, or mixing. At the same time with this, by rotation of the rotor 2, the kinetic energy is given to the fluid to be processed thereby accelerating the fluid to be processed while it is passing through the slits 18; and as a result, the fluid to be processed is discharged to outside the stirring chamber 7 while forming the intermittent jet flow. By this intermittent jet flow, the liquid-liquid shear force is also generated in the velocity interface whereby executing emulsification, dispersion, or mixing.

(21) The screen 9 has a form of cylinder having a circular cross section. It is preferable that the screen 9 is made such that the diameter thereof becomes shorter as moving more apart from the introduction port 11 (in example of FIG. 2, as going downward), like a conical surface shape, for example.

(22) If the diameter is made constant in the axial direction, the discharged amount from the slits 18 is larger in the part near to the introduction opening 11 (in FIG. 2, in the upper part), whereas the discharged amount is smaller in the part apart far from the opening (in FIG. 2, in the lower part). As a result, there is a risk of generating the uncontrollable cavitation which may cause a mechanical malfunction.

(23) The slits 18 that are extended linearly to the direction of the rotation axis 13 (vertical direction in the example of the drawing) are shown; however, they may be extended spirally or with a curve. The shape of the slits 18 is not necessarily a narrow and long space; they may be in the shape of polygonal, circular, ellipse, or the like. In addition, although the slits 18 are formed in plural with the same intervals in the circumferential direction; however, they may be formed with putting off in the intervals, and besides, the slits 18 having plural shapes and sizes may not be excluded.

(24) The slit 18 may be configured so as to have the lead angle variously changed. As illustrated in the drawing, the slit 18 may be configured so as to be linearly extended upward and downward with the lead angle of 90 between the plane perpendicular to the rotation axis 13 and the extending direction of the slit 18; or alternatively, the slit may be configured so as to be a spiral form having a prescribed lead angle, or so as to be extended upward and downward with a curve.

(25) The blades 12 of the rotor 2 may be extended radially and linearly from the center of the rotor 2 with a constant width in the traverse sectional view (the cross section perpendicular to the axial direction of the rotation axis 13); or alternatively, they may become gradually wider in their sizes or may be warped as they are extending toward the outside.

(26) Also, these blades 12 may have the lead angle of the edge portion 21 thereof arbitrarily changed. For example, the blade may be configured so as to be linearly extended upward and downward with the lead angle of 90 between the plane perpendicular to the rotation axis 13 and the extending direction of the edge portion 21; or alternatively, the blade may be configured so as to be a spiral form having a prescribed lead angle, or so as to be extended upward and downward with a curve.

(27) The shape of these individual constituent members have a matching region where the edge portion of the blade 12 and the slit 18 are in the same position and overlapped with each other in the longitudinal direction of the slit 18. By rotation of the rotor 2, shearing of the fluid to be processed can be generated between the blade 12 and the screen member 19 in this matching region, and also, with rotation of the blade 12, a kinetic energy can be given to the fluid to be processed that goes through the slit 18 so as to generate the intermittent jet flow.

(28) The clearance between the screen 9 and the blades 12 may be arbitrarily changed so far as the shear force and the jet flow as mentioned above can be generated; however, usually the clearance is preferably in the range of about 0.2 to 4.0 mm.

(29) Also, in the case that, as shown in FIG. 2, the screen 9 having a tapered shape as a whole is used, this clearance can be readily controlled by making at least any one of the stirring chamber 7 and the rotor 2 movable in the axial direction.

(30) With regard to other structure of the stirrer, the stirrers shown in FIG. 4 and FIG. 5 may also be employed.

(31) In the example of FIG. 4, in order to make the entirety of the fluid to be processed in the accommodating vessel 4 uniform by stirring, a separate stirring equipment is installed in the accommodating vessel 4. Specifically, the stirring blade 15 to stir the entirety inside the accommodating vessel 4 may be installed such that it may rotate integrally with the stirring chamber 7. In this case, both the stirring blade 15 and the stirring chamber 7 including the screen 9 are rotated together. During this time, the directions of the rotations of the stirring blade 15 and of the stirring chamber 7 may be either as same as the direction of the rotation of the rotor 2 or opposite to it. That is, because rotation of the stirring chamber 7 including the screen 9 becomes slower relative to rotation of the rotor 2 (specifically the circumferential velocity of rotation of the screen is in the range of about 0.02 to 0.5 m/sec), this does not substantially influence the shear force and the jet flow.

(32) In the example shown in FIG. 5, the stirring chamber 7 is made rotatable to the supporting tube 3, and the rotation axis of the second motor 20 is connected to the front end of the stirring chamber 7, so that the screen 9 is made rotatable at high rotation speed. The screen 9 is rotated in the direction opposite to the rotational direction of the rotor 2 disposed inside the stirring chamber 7. By so doing, the relative rotation velocity of the screen 9 to the rotor 2 is increased.

(33) In the stirrer described above, the present invention is applied as follows. In the stirrer according to the present invention, the liquid-liquid shear force is generated in the velocity interface by the intermittent jet flow, and with this, processing of emulsification, dispersion, or mixing is conducted. At this time, in the stirrer according to the embodiment of the present invention, the rotor 2 and the screen 9, for example, as shown in FIG. 6(A), FIG. 6(B), and FIG. 7, may be used. In the rotor 2 and screen 9 of this example, in the matching region (namely, the edge portion 21 of the blade 12 and the slit 18 of the screen 9 are in the same position and overlapped with each other in the longitudinal direction of the slit 18) in which the shear action in the screen 9 can be expressed, the condition 1 and the condition 2 shown below are satisfied.

(34) (Condition 1)

(35) The relationship among the width (b) of the edge portion 21 of the blade 12 in a rotational direction, the width (s) of the slit 18 in a circumferential direction, and the width (t) of the screen member 19 in a circumferential direction satisfies the condition b2s+t. In other words, the width of the edge portion 21 of the blade 12 in the rotor 2 in the rotational direction is set larger than the distance between both edges of the neighboring two slits 18.

(36) (Condition 2)

(37) The relationship between the width (b) of the edge portion 21 of the blade 12 in a rotational direction and the maximum inner diameter (c) of the screen 9 satisfies the condition b0.1c. In other words, the ratio of the edge portion 21 of the blade 12 to the maximum inner diameter of the screen 9 is set so as to be larger than a prescribed value.

(38) As mentioned above, the stirrer according to the presently applied invention satisfies both the condition 1 and the condition 2 in the matching region. With regard to the position of the rotation axis of the rotor 2 in the axial direction, any position may be allowed so far as it is in the matching region; however, it is preferable that both the condition 1 and the condition 2 are satisfied at least in the position where the position of the rotation axis 13 in the axial direction is the maximum inner diameter of the screen 9.

(39) It was found that when the rotor 2 and the screen 9 satisfy these two conditions, this stirrer can increase the liquid-liquid shear force in the velocity interface, so that the stirrer is very effective in realization of very fine dispersion and emulsification such as nano-level dispersion and emulsification. On the basis of this finding, the present invention could be completed.

(40) Explanation with regard to the action of the intermittent jet flow will be made with comparing to the conventional example shown in FIG. 6(C) and FIG. 6(D). Firstly, as mentioned before, the intermittent jet flow is generated by rotation of the blade 12. To explain this more specifically, the pressure of the fluid to be processed increases in the front side of the rotational direction of the blade 12. With this, the fluid to be processed is ejected as the intermittent jet flow from the slit 18 that is located in the front side of the blade 12. On the other hand, in the back side in the rotational direction of the blade 12, the pressure of the fluid to be processed decreases, so that the fluid to be processed is sucked from the slit 18 that is located in the back side of the blade. As a result of it, outside the screen 9, the forward flow and the backward flow (ejection flow and suction flow) are generated in the fluid to be processed; and thus, due to the relative difference in the velocities in the interface of the both flows, the liquid-liquid shear force is generated among the fluids to be processed.

(41) In the conventional example shown in FIG. 6(C) and FIG. 6(D), because the width of the edge portion 21 of the blade 12 was narrow, it was difficult for the fluid to be processed to follow the change of the state between ejection and suction; and as a result, the relative difference in the velocities in the interface of the forward flow and the backward flow (ejection flow and suction flow) of the fluid to be processed was in a state of comparatively small, so that the shear force thereof was small, too.

(42) On the other hand, in the embodiment of the present invention shown in FIG. 6(A) and FIG. 6(B), the width of the edge portion 21 of the blade 12 is wide, so that a period during which the fluid to be processed stays static between ejection and suction is generated. Because of this, the fluid to be processed can follow very well to the change of opening and closing of the slit 18 due to the blade 12, so that the relative difference in the velocities of the forward flow and the backward flow (ejection flow and suction flow) of the fluid to be processed in the interface thereof increases; and as a result, the shear force generated between the fluids to be processed can be increased. The conditions to favorably realize this are the condition 1 and the condition 2.

(43) (With Regard to the Matching Region)

(44) The edge portion 21 of the blade 12 and the slit 18 have at least the matching region in which they are in the same position and overlapped with each other in the longitudinal direction of the slit 18. Usually, the length of the blade 12 is set longer than the length of the slit 18, and thus, the entire length of the slit 18 is in the same position, where the blade 12 overlaps with the slit 18 with each other; however, the embodiment that the length of the blade 12 is shorter than the length of the slit 18 may also be allowed. In the present invention, when the relationship between the blade 12 and the slit 18 is stipulated, this refers to the relationship in the matching region unless explained otherwise.

(45) (With Regard to the Screen)

(46) As mentioned before, the embodiment wherein the screen 9 has the diameter thereof changed, like a tapered shape, etc., may also be allowed. In the present invention, in the case that the inner diameter is changed, the maximum inner diameter refers to the maximum diameter of the screen 9 in the matching region unless explained otherwise.

(47) (With Regard to the Slit and the Screen Member)

(48) The slit 18 may be extended parallel in the axial direction of the rotation axis of the rotor 2, or may be those having an angle to the axial direction, such as the one extended spirally. In any cases, in the present invention, the width (s) of the slit 18 in the circumferential direction refers to the length in the circumferential direction of the screen 9 (in other words, the direction perpendicular to the axial direction of the rotation axis of the rotor 2) in the matching region unless explained otherwise. In the axial direction of the rotation axis of the rotor 2, any position may be allowed so far as it is in the matching region; however, it is preferable that at least the position of the rotation axis 13 in the axial direction is the position of the maximum inner diameter of the screen 9. The width (s) of the slit 18 in the circumferential direction is preferably in the range of 0.2 to 4.0 mm, while more preferably in the range of 0.5 to 2.0 mm; however, this may be changed arbitrarily so far as the intermittent jet flow is generated.

(49) The width (t) of the screen member 19 in the circumferential direction (in other words, the distance between the slits 18 that are located in a neighborhood to each other in the circumferential direction) may be arbitrarily changed; however, the width thereof is preferably 0.1 to 10 times, while more preferably about 0.5 to 2 times, as much as the width (s) of the slit 18 in the circumferential direction. If the width (t) of the screen member 19 in the circumferential direction is too wide, the number of the shearing decreases thereby leading to decrease in the throughput, while if the said width is too narrow, it may lead to substantially the same situation as the situation that the slits 18 are continuous, or it can cause significant decrease in a mechanical strength thereof.

(50) (With Regard to the Rotor)

(51) As mentioned before, the rotor 2 is a rotating body having plural blades 12. By making the edge portion 21 of the blade 12 satisfy the condition 1 and the condition 2 in the matching region, the action effect of the present invention can be expressed. Meanwhile, if the width of the edge portion 21 of the blade 12 is made too wide, the space volume between the blade 12 and the blade 12 becomes too small, so that it can cause a problem such as a unnecessarily decrease in the throughput. Considering this aspect, though different depending on the inner diameter of the screen 9, in rotor 2, in the region defined by the outer circumferential surface of the rotation axis 13 and the inner circumferential surface of the screen 9, it is preferable to set the total sum of the cross section area of the blades 12 in the plane perpendicular to the rotation axis 13 be smaller than the cross section area of the space inside the screen 9. As described before, in the matching region, when the total sum of the cross section area of the blades 12 in the plane perpendicular to the rotation axis 13 is represented by Y in the following specific formulas 1 and 2, and similarly, when in the matching region, the cross section area of the space inside the screen 9 in the plane perpendicular to the rotation axis 13 is represented by Z in the following specific formulas 1 and 2, it is preferable that Y and Z satisfy the specific formula 2. X in the specific formula 1 represents, in the matching region, the cross section area perpendicular to the rotation axis in the region defined by the outer circumferential surface of the rotation axis 13 and the inner circumferential surface of the screen 9.
XY=Z(Specific Formula 1)
Y<Z(Specific Formula 2)

(52) It is preferable that, of plural cross sections in the matching region, at least one cross section satisfy the specific formula 2, while more preferably all the cross sections satisfy the specific formula 2. And, as shown in FIG. 2, when the screen 9 whose diameter becomes gradually shorter as moving more apart from the introduction port 11 (in example of FIG. 2, as going downward) is used, and also the position of the plane in the axial direction perpendicular to the rotation axis 13 is the position of the maximum inner diameter of the screen 9 in the matching region, Y/Z is preferably in the range of 0.2 or more to less than 1, more preferably in the range of 0.34 to 0.6 (both ends inclusive), while still more preferably in the range of 0.34 to 0.5 (both ends inclusive). Y/Z can be calculated on the basis of the diameter of the rotation axis 13, the diameter of the blade 12, the width of the blade 12 in the rotational direction, the inner diameter of the screen 9, and so forth.

(53) (Preferable Use Conditions)

(54) The numerical conditions of the screen 9, the slit 18, and the rotor 2, which can apply the condition 1 and the condition 2 of the present invention and are considered to be suitable for mass production by the today's technology, are as follows.

(55) Maximum inner diameter of the screen 9: 30 to 500 mm (however, maximum diameter in the matching region)

(56) Rotation number of the screen 9: 15 to 390 rotations/second

(57) Number of the slit 18: 20 to 500

(58) Maximum outer diameter of the rotor 2: 30 to 500 mm

(59) Rotation number of the rotor 2: 15 to 390 rotations/second

(60) As a matter of course, these numerical conditions show one example; and as the technologies such as rotation control, etc., advances in future, the present invention does not preclude to employ the conditions other than the above conditions.

EXAMPLES

(61) Hereunder, the present invention will be explained further specifically by showing Examples. However, the present invention is not limited to the following Examples.

Example 1 and Comparative Example 1

(62) As Example 1 (namely, Example 1A and Example 1B) and Comparative Example 1 (namely, Comparative Example 1A and Comparative Example 1B), two kinds of the fluid to be processed were processed for testing (Example 1A/Comparative Example 1A, and Example 1B/Comparative Example 1B) by using the stirrer according to the first embodiment of the present invention (FIG. 1 and FIG. 2).

(63) In Example 1A/Comparative Example 1A in which pigment was subjected to the dispersion processing, copper phthalocyanine/sodium dodecylsulfate/pure water=2/0.2/97.8 (weight ratio) was used as the fluid to be processed.

(64) In Example 1B/Comparative Example 1B in which resins were subjected to the emulsification processing, methyl methacrylate monomer/Aqualon KH-10/pure water=10/1/89 (weight ratio) was used as the fluid to be processed. However, Aqualon KH-10 is a surfactant manufactured by DKS Co., Ltd.

(65) By using a pump in the test equipment shown in FIG. 8, the fluid to be processed of the preliminary mixture stored in the outside vessel (1-L tall beaker equipped with a stirrer) was introduced into the processing vessel (350 cc) having the stirrer, and the processing vessel was completely filled with the liquid; and the fluid to be processed was introduced into the processing vessel by means of the pump, whereby ejecting the fluid to be processed from the ejection port to carry out the processing to refine the particles with ejecting the fluid from the screen by rotating the rotor of the stirrer at the rotation speed of 20000 rpm while circulating the fluid between the processing vessel and the outside vessel under the condition shown in Table 1. Meanwhile, in all examples, the screen was not rotated.

(66) The width of the slit and the width of the screen member shown in Table 1 are the width of the slit and the width of the screen member at the position where the plane perpendicular to the rotation axis 13 in the axial direction is the maximum inner diameter of the screen 9 in the matching region.
In Example 1, both the condition 1 and the condition 2 were satisfied; on the contrary, in Comparative Example 1, neither the Condition 1 nor the Condition 2 was satisfied.

Example 1

(67)
3.6>20.8+1.19=2.79(Condition 1)
3.6>0.130.4=3.04(Condition 2)

Comparative Example 1

(68)
2.4<20.8+1.19=2.79(Condition 1)
2.4<0.130.4=3.04(Condition 2)

(69) With regard to Example 1 and Comparative Example 1, particle diameters (D50 and D90) of the particle as well as coefficient of variation (C. V.) of the particle diameter measured at several time points till the maximum processing time of 45 minutes are shown in FIG. 9 and FIG. 10. The coefficient of variation of the particle diameter is an indicator to show the evenness of the obtained particles; and this coefficient can be obtained from the average particle diameter (D50) in the particle diameter distribution of the particle and the standard deviation with the formula: Coefficient of Variation (C. V.) (%)=Standard DeviationAverage Particle Diameter (D50)100. When the value of this coefficient of variation becomes smaller, distribution of the particle diameter of the obtained particles becomes narrower, namely, the particles become higher in its evenness.

(70) From FIG. 9 and FIG. 10, it becomes clear that in Example 1, the particle diameter and the coefficient of variation of the particle diameter decrease more significantly with elapse of the processing time as compared with Comparative Example 1.

Example 2

(71) Next, even when the rotor and the screen having larger diameter than those of Example 1 were used in Example 2, it was confirmed whether or not the particle diameter significantly decreases with elapse of the processing time. The processing conditions are shown in Table 1, and the test results are shown in FIG. 11, respectively. The processing equipment was substantially the same as those of Example 1, except that the whole equipment was made larger in accordance with the throughput (outer vessel: 300-L tank equipped with a stirrer, processing vessel: 8.5 L). With regard to the fluid to be processed, dextrin was used as the component to be refined, and a plant oil was used as the dispersion medium.

(72) In Example 2, too, as can be clearly seen in Table 1, both the condition 1 and the condition 2 were satisfied.

Example 2

(73)
11.3>21.1+1.90=4.10(Condition 1)
11.3>0.195.4=9.54(Condition 2)

(74) From FIG. 11, it becomes clear that in Example 2, too, the particle diameters (D50 and D90) are significantly decreased with elapse of the processing time.

(75) TABLE-US-00001 TABLE 01 Comparative Comparative Example 1A Example 1A Example 1B Example 1B Example 2 Screen nominal 30 30 30 30 95 diameter Maximum inner 30.4 30.4 30.4 30.4 95.4 diameter of the screen (at a part having slits) (mm) width of a slit (mm) 0.8 0.8 0.8 0.8 0.8 number of slits 48 48 48 48 100 lead angle of a slit 90 90 90 90 90 () Width of a screen 1.19 1.19 1.19 1.19 1.90 member (distance between neighboring screen) (mm) number of blades 4 6 4 6 4 width of a blade tip 3.6 2.4 3.6 2.4 11.3 (mm) blade rotation number 20000 20000 20000 20000 5700 (rpm) lead angle of a blade 90 90 90 90 90 () fluid to be processed copper copper copper copper component to be phthalocyanine/sodium phthalocyanine/sodium phthalocyanine/sodium phthalocyanine/sodium refined:dextrin dodecylsulfate/pure dodecylsulfate/pure dodecylsulfate/pure dodecylsulfate/pure dispersion water = water = water = water = medium:plant oil 2/0.2/97.8 2/0.2/97.8 2/0.2/97.8 2/0.2/97.8 (weight ratio) (weight ratio) (weight ratio) (weight ratio) throughput (Kg) 2.0 2.0 2.0 2.0 126.5 circulating amount 3.1 3.1 6.0 6.0 17 (L/min.) processing duration 45 45 45 45 390 (min.) processing 19 to 22 (room 19 to 22 (room 15 to 18 (room 15 to 18 (room 10 to 24 (room temperature ( C.) temperature) temperature) temperature) temperature) temperature)

REFERENCE NUMERALS

(76) 1. Processing member

(77) 2. Rotor

(78) 3. Supporting tube

(79) 4. Accommodating vessel

(80) 5. Sucking port

(81) 6. Sucking chamber

(82) 7. Stirring chamber

(83) 9. Screen

(84) 10. Comparting wall

(85) 11. Opening

(86) 12. Blade

(87) 13. Rotation axis

(88) 14. Motor

(89) 15. Stirring blade

(90) 18. Slit

(91) 19. Screen member

(92) 20. Second motor

(93) 21. Edge portion