THERMALLY MODIFIED WOOD PRODUCT AND A PROCESS FOR PRODUCING SAID PRODUCT

Abstract

The present invention relates to a process for preparing a modified wood product. More specifically, the invention relates to a method of performing thermal modification, wherein the thermally modified wood is suitable for load bearing use. The present invention also relates to a modified wood product produced using said process.

Claims

1. Thermally modified solid wood which is suitable for load bearing purposes.

2. Thermally modified solid wood according to claim 1, having a characteristic bending strength of at least 18 N/mm.sup.2.

3. Thermally modified solid wood according to claim 2, wherein the bending strength is measured according to EN408:2010.

4. Thermally modified solid wood according to claim 1, which is suitable for load bearing purposes above ground.

5. Thermally modified solid wood according to claim 4, wherein the suitability for use above ground is defined in accordance with Use Class 3.1 as described in the European standard EN335:2013.

6. Thermally modified solid wood according to claim 1, wherein said wood is pine wood or spruce wood.

7. Process for preparing thermally modified solid wood, wherein wood is dried to an average moisture content of less than 5% at an average wood temperature of less than 100 C., followed by an increase in wood temperature to above 140 C.

8. Process according to claim 7, wherein the wood is dried to an average moisture content of less than 5% at an average wood temperature of less than 100 C., followed by an increase in wood temperature to above 160 C. at atmospheric pressure, wherein the wood is maintained at a temperature above 160 C. for at least one hour, followed by cooling to ambient temperature.

9. Process according to claim 8, wherein the wood is dried to an average moisture content of less than 5% at an average wood temperature of less than 100 C., followed by an increase in wood temperature to a temperature above 160 C. and below 250 C. at atmospheric pressure, wherein the wood is maintained at a temperature above 160 C. and below 250 C. for at least one hour, followed by cooling to ambient temperature.

10. Process according to claim 7, wherein the wood is dried to an average moisture content of less than 5% at an average wood temperature of less than 100 C., followed by an increase in wood temperature to above 120 C. at a pressure higher than atmospheric pressure, wherein the wood is maintained at a temperature above 120 C. for at least one hour, followed by cooling to ambient temperature.

11. Process according to claim 7, wherein the drying is performed at an absolute pressure below 1013 mBar.

12. Process according to claim 7, wherein the drying is performed at an absolute pressure above 1013 mBar.

13. Process according to claim 7, wherein the drying is performed at an absolute pressure of approximately 1013 mBar.

14. Thermally modified solid wood obtainable by the process according to claim 7.

Description

BRIEF DESCRIPTION OF THE FIGURES

[0029] FIG. 1. Normal schedule for treatment of Thermowood D.

[0030] FIG. 2. Special treatment schedule according to the present invention. Wood is pre dried at low temperature.

[0031] FIG. 3. Stiffness and bending strength determined according to EN 408 of untreated planks, planks treated according to normal Thermowood D schedule, and planks treated according to a special schedule based on the invention.

DETAILED DESCRIPTION

[0032] The bending strength of wood, such as the thermally modified wood according to the present invention, can be measured using methods known in the art. In particular, the bending strength of dimensional lumber can be measured according to EN408 Timber structuresStructural timber and glued laminated timberDetermination of some physical and mechanical properties. Results from tests according to EN 408 are used to determine characteristic values according to European standard EN 384 Structural timberDetermination of characteristic values of mechanical properties and density. Requirements for different strength classes are defined in European standard EN 338 Structural timberStrength classes. All of which are standards recognized by a person skilled in the art.

[0033] Thermal modification according to the present invention can be done on pre dried wood as well as green, unseasoned, wood. The initial moisture content of the wood used in the process according to the present invention is typically at least 10%. In one embodiment of the present invention, the moisture content is from 10% to 20%. In a further embodiment, the moisture content is from 11% to 15%, such as from 12% to 14%. In a further embodiment, the moisture content is about 12%. In one embodiment, the moisture content is close to the fiber saturation point. The moisture content as well as the fiber saturation point of wood can be determined using methods known in the art.

[0034] The time required for the drying step depends on the properties of the wood used, but is generally in the range of from 5 hours to 96 hours for softwood.

[0035] During the thermal modification step, the wood is heated at a temperature of from 160 C. to 250 C. at atmospheric pressure or at a temperature of from 120 C. to 250 C. at a pressure higher than atmospheric pressure.

[0036] In one embodiment of the present invention, the wood may be densified during or after the thermal modification step. The densification may be done by applying pressure to the wood. The densification may be done at a pressure of 1-3 kg/cm.sup.2 and the maximum compression should be about 10% of the thickness of the wood.

[0037] For densification, it is preferred to apply both pressure and heat, since this combination will improve the densification of the wood. The densification may be done off-line, on-line or in-line, i.e. in-line with the process according to the invention. If off-line densification is used, it is possible to use a hot press after the thermal modification step. If in-line densification is used it is possible to use roller or plate based systems. The densification can be done during the thermal modification step or after the thermal modification step.

[0038] By densifying the wood, the surface of the wood will become more set, i.e. the fibers on the surface have less tendency to react with moisture and retain its original form. This also leads to reduced tendency of fiber loosening on the surface of the wood. The surface density and thus also the hardness of the wood will also be improved.

[0039] The produced thermally modified wood can also be used for load bearing purposes.

[0040] The term solid wood as used herein is defined as a solid wood component of any kind of wood species, including finger jointed as well as laminated products.

[0041] The produced thermally modified wood product can be used for the production of many different products, such as cladding, decking, window and door profiles, light poles, jetties, joinery, furniture etc.

EXAMPLES

Thermal Treatment of the Material

[0042] Saw falling 45145 mm Norway spruce planks were heat treated according to a standard Thermowood D schedule and according to a special schedule according to the present invention. Both schedules used a 3 h plateau phase at temperature of 212 C. One set of planks from the same batch was kept untreated to be used as reference material.

Standard Thermowood Treatment

[0043] The standard Thermowood D schedule was designed as shown in FIG. 1. The 77 h schedule comprises of initial heating to 100 C., drying phase at increased temperature up to 130 C., heating to plateau temperature, 3 h treatment at 212 C., cooling, and conditioning.

[0044] The climate at the end of HT-drying phase at 130 C. dry bulb temperature and 99 C. wet bulb temperature corresponds to Equilibrium Moisture Content (EMC)=1% to 2.5%.

Special Treatment According to the Present Invention

[0045] The special treatment schedule is based on the idea to reduce or eliminate hydrolysis of the material by drying it to very low MC at low temperature. Drying is done at 90 C. dry bulb temperature with wet bulb temperature gradually reduced to 50 C., corresponding to EMC 2.5%.

[0046] The low temperature drying phase in the test was 52.5 h, followed by a 28 h HT-drying phase before temperature was increased up to 212 C. FIG. 2 shows the trend curves from the special treatment.

Results from Bending Tests

[0047] The results from the bending strength tests are summarized in Table 1. Critical values for approval for load bearing use are marked with bold text.

TABLE-US-00001 TABLE 1 Summary of test results from EN 408 bending tests Thermowood Normal according to Untreated Thermowood present Tested property Unit reference D invention Bending strength N/mm.sup.2 45.2 32.5 36.9 4-points edgewise Strength standard N/mm.sup.2 9.6 10.7 12.2 deviation Characteristic N/mm.sup.2 28.0 15.2 19.6 bending strength Number of planks n 22 77 75 tested Stiffness N/mm.sup.2 9.8 10.1 10.6 Global E-modulus E-mod standard N/mm.sup.2 1.8 1.8 1.9 deviation Number of planks n 22 71 73 tested

[0048] The test results show that strength values can be further improved by pre-sorting of the raw material prior to treatment. Table 2 shows strength values obtained after removal of planks with low local initial stiffness determined mechanically by a Metriguard longitudinal machine stress rating equipment:

TABLE-US-00002 TABLE 2 Test results from EN 408 bending tests with low stiffness planks removed. Normal Improved Untreated Thermowood Thermowood Tested property Unit reference D D Bending strength N/mm.sup.2 49.0 34.4 39.0 4-points edgewise Strength standard N/mm.sup.2 9.6 10.7 11.8 deviation Characteristic N/mm.sup.2 38.9 16.8 21.0 bending strength Number of planks n 16 30 32 tested Stiffness N/mm.sup.2 10.6 10.8 11.7 Global E-modulus E-mod standard N/mm.sup.2 1.1 1.8 1.8 deviation Number of planks n 16 27 32 tested

[0049] Removal of the planks with the lowest local stiffness gave a slight increase of the bending strength values.

[0050] However, the stress grading was done by mechanical bending flatwise, and the bending tests were made edgewise. By using more advanced stress grading procedures a larger increase of characteristic strength values is expected.

[0051] The improvement in bending strength is illustrated by the diagram in FIG. 3.

[0052] In view of the above detailed description of the present invention, other modifications and variations will become apparent to those skilled in the art. However, it should be apparent that such other modifications and variations may be effected without departing from the spirit and scope of the invention.