METHOD FOR CONSTRUCTING OR ALTERING A MATTER- AND/OR HEAT-EXCHANGE DEVICE
20190301796 ยท 2019-10-03
Assignee
Inventors
- Patrice Cavagne (Le Perreux, FR)
- Benoit Davidian (Saint Maur des Fosses, FR)
- Bernard SAULNIER (La Garenne Colombes, FR)
Cpc classification
F25J2290/30
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F25J3/0489
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F25J2290/42
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F25J3/04945
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F25J3/0295
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
International classification
F25J3/04
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
Abstract
The invention relates to a method for constructing or altering a matter- and/or heat-exchange device, said mass- and/or heat-exchange device comprising an assembly of at least one first and one second stackable modular elements (A, B, C, D, E, F, G, H, I, J, K, L), in which the first element is secured over the second element or the second element is secured below the first element in a sealed manner, such that a fluid can flow from the body of the first element to the body of the second element and/or from the body of the second element to the body of the first element.
Claims
1-15. (canceled)
16. A method for construction or modification of a device for exchange of mass and/or of heat, wherein the device for exchange of mass and/or heat comprises: an assembly of at least one first stackable modular element and one second modular stackable element, wherein each of the first and second modular stackable elements comprise: a box that is parallelepipedal and has a length, a width and a height, the box having opposite horizontal upper and lower faces, two opposite vertical end faces and two opposite vertical lateral faces, the horizontal upper and lower faces of the box being defined by the length and the width of the box, the two vertical end faces of the box by the length and the height of the box and the two vertical lateral faces of the box by the width and the height of the box, wherein the box contains at least one layer of thermal insulation, the layer of thermal insulation covering at least the lateral faces and the vertical end faces of the box and surrounding at least one chamber of parallelepipedal volume inside the box, the at least one chamber having a length, a width and a height, the chamber having opposite horizontal upper and lower faces, the upper face and/or the lower face of the chamber being at least partially open, two opposite vertical end faces and two opposite vertical lateral faces, the upper and lower faces of the chamber being defined by the length and the width of the chamber, the two end faces of the chamber by the length and the height of the chamber and the two lateral faces of the chamber by the width and the height of the chamber, the chamber containing at least one body of material enabling the exchange of mass and/or of heat, the body being of parallelepipedal shape and filling at least a part of the chamber, wherein i) the layer of thermal insulation has a thickness less than one third of the width of the box, and ii) the first element having the at least one chamber featuring an opening on the lower face communicating with an opening in the lower face of the box and the second element having the at least one chamber featuring an opening on the upper face communicating with an opening in the upper face of the box to enable the transfer of fluid from the body of the first element to the body of the second element and/or from the second element to the body of the first element and in which the method includes the steps of: a) affixing the first element on top of the second element or affixing the second element underneath the first element in a sealed manner, so that a fluid can pass from the body of the first element to the body of the second element and/or from the body of the second element to the first element body, and/or b) unfastening the first element from the second element, on top of which the first element is affixed in a sealed manner, or unfastening the second element from the first element underneath which the second element is affixed in a sealed manner, so that a fluid can pass from the body of the first element to the body of the second element and/or from the second element to the body of the first element.
17. The method as claimed in claim 16, wherein the body of the first element and the body of the second element are both i) a body of adsorbent material, or ii) a stack of vertically oriented metal plates, the plates being separated by fins, or iii) a stack of vertically oriented corrugated plates, the corrugations being oriented at an angle to the horizontal between 10 and 80.
18. The method as claimed in claim 16, wherein the at least one body fills at least a part of the chamber inside the box of the first and/or the second element and i) another body enabling the exchange of mass and/or of heat fills another part, or even the rest, of the chamber or another chamber, and/or ii) at least one material transfer conduit passes through the other part, or even the rest of the chamber or another chamber, to enable the material to pass through the box, and/or iii) the other part, or even the rest of the chamber or the other chamber constitutes a means enabling the transfer of material through the box.
19. The method as claimed in claim 16, wherein the assembly constitutes at least a part of an adsorbent bed, a heat exchanger or a preferably cryogenic distillation device and in that i) the addition of the second element enables increasing of the capacity of the assembly and/or increasing the efficiency of the assembly, or ii) the removal of the second element enables reduction of the capacity of the assembly and/or reduction of the efficiency of the assembly and/or reduction of the volume of the assembly.
20. The method as claimed in claim 16, wherein the first and/or second element constitutes an element of a stack of at least two elements, each element of the stack comprising a parallelepipedal box having a length, a width and a height, the box having opposite horizontal upper and lower faces, two opposite vertical end faces and two opposite vertical lateral faces, the upper and lower faces of the box being defined by the length and the width of the box, the two end faces of the box by the length and the height of the box and the two lateral faces of the box by the width and the height of the box, most of the elements, or even each element, of the stack having the same width and/or the same length and/or the same height.
21. The method as claimed in claim 16, wherein the layer of insulation further covers the upper and lower faces.
22. The method as claimed in claim 16, wherein the first element is added into the stack of elements above the second element and below another element.
23. The method as claimed in claim 16, wherein the first element is removed and the first element is replaced by another element having the same body type i), ii) or iii) as described in claim 17 as the first body, but having a greater capacity and/or better efficiency and/or less defective operation than that of the first element.
24. The method as claimed in claim 16, wherein the first element is removed and the first element is replaced by an element of parallelepipedal shape having the same length and the same width as the first element but not containing a body of same type as the first body.
25. The method as claimed in claim 24, wherein the element of parallelepipedal shape or does not contain a body of type i) to iii) as described in claim 17.
26. The method as claimed in claim 16, wherein a first stack is assembled principally comprising body elements of type i) or of type ii) or of type iii) as described in claim 2 and a second stack is assembled principally comprising body elements of type i) or type ii) or type iii) as described in claim 2 so that a lateral face of the second stack is substantially in contact with a lateral face of the first stack.
27. The method as claimed in claim 26, wherein a third stack is assembled principally comprising body elements of type i) or of type ii) or of type iii) as described in claim 2 so that a lateral face of the second stack is substantially in contact with a lateral face of the third stack.
28. The method as claimed in claim 26, wherein the first stack principally contains body elements of type i) and/or the second stack principally contains body elements of type ii) and/or the third stack principally contains body elements of type iii).
29. The method as claimed in claim 28, wherein an element of the first stack or the second stack contains an air compressor intended to feed with air elements of the stack of bodies of type i) or ii).
30. The method as claimed in claim 16, wherein: according to the variant a) of claim 16, the first and/or second element is taken up in a manufacturing center or a logistical platform, and/or according to the variant b) of claim 16, the first and/or second element is deposited in a/the manufacturing center or a/the logistical platform, the manufacturing center or the logistical platform containing a plurality of elements identical to the first element and/or a plurality of elements identical to the second element.
31. The method as claimed in Claim Error! Reference source not found., wherein a first and/or second element is unfastened from a first device in accordance with the step b) of claim 1, the unfastened element is deposited in a manufacturing center or a logistical platform, the unfastened element is possibly reconditioned there, the unfastened element is taken up in the center or the platform to transport it to a second device where it is fixed in accordance with the step a) of claim 1 to another element to form part of the second device.
32. A device for the exchange of mass and/or of heat constructed or modified by a method as claimed in claim 16.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0198] The present invention will be clearly understood and its advantages will arise from the description which follows, given merely as a non-limitative example, and with reference to the attached drawings in which
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DETAILED DESCRIPTION
[0218] The invention will be described in more detail with reference to
[0219]
[0220] The modular element 10 is an element enabling an exchange of material and/or of heat. It is composed of a box 2 of parallelepipedal shape, formed for example of metal beams. The element includes eight container type ISO 101 corners fixed to the box 2 and has a width oriented horizontally relative to the ground, a length oriented horizontally relative to the ground and a height oriented vertically relative to the ground, when it is installed to form part of a device.
[0221] ISO containers are subject to specific construction standards and performance tests. The same applies to ISO corners.
[0222] ISO corners are certified by an internationally recognized organization to enable their multimodal use in maritime, road, rail or even air transport.
[0223] Steel, aluminum or stainless steel ISO corners are commercially available according to their specified use.
[0224] The element comprises a box having opposite horizontal upper and lower faces, two opposite vertical end faces and two opposite vertical lateral faces, the upper and lower faces of the box being defined by the length and the width of the box, the two end faces of the box by the length and the height of the modular element and the two lateral faces of the box by the width and the height of the box. The lateral and end walls are for example made of sheet metal. The faces formed by the width and the length of the element are open to enable the passage of fluids. Alternatively, the opening may be smaller than the surface of the lower and/or upper face, covering at least part of the insulation 3 and possibly a part of the zone 4.
[0225] It is obvious that the height and the width of the element are not necessarily identical, and so the lateral walls may all be rectangular without being square. The walls may also be smaller than the box of the element. The walls are preferably fixed to the inside of the box 2, but may be fixed to its outside. Insulation 3 lines the inside of the box 2, at least on the vertical sides of the parallelepiped. The upper and/or lower surface may also comprise a wall and be insulated. The insulation 3 can be pressed onto a plate which bears on the box 2 to make a fluid seal between the interior and the surroundings. The insulation 3 can also provide this sealing function directly, together with the structural wall function. By default, a fluid-tight wall, for example a metal plate, may be applied on the interior side to the insulation 3. The box 2 and the insulation 3 delimit an internal zone. The box 2, the wall and/or the insulation 3 can be sized to contain any overpressure inside the internal zone.
[0226] The internal zone surrounds a zone 4. This zone 4 contains a body that enables transfer of mass and/or heat, for example a structured packing for distillation, an exchanger matrix with plates and fins for exchange of heat, adsorbent in ball or structured form for adsorption. This zone can also contain a support zone, for example in the lower part, fluid distribution zones, for example in the lower and/or upper part. It can also be divided into a plurality of parts, for example vertically, with walls that may be fluid-tight and/or structural walls (for example to resist a pressure difference) and/or thermally insulative walls. The body preferably fills all the section of the zone 4.
[0227] At least one fluid circulates up or down through the zone 4. In some cases, for example that of distillation, a fluid, for example a gas, circulates upward and another, for example a liquid, downward through the zone 4.
[0228] The internal zone may consist entirely of the zone 4. However, as shown, it can equally well contain at least one other zone, for example here a fluid circulation zone 5, delimited by a fluid-tight and possibly insulating wall 6, in some kind of duct. The part in contact with the insulation 3 can be delimited by a fluid-tight, for example metal, wall, if the insulation does not provide this function. In the situation in the figure, two fluid circulation zones 5 are delimited by a vertical fluid tight wall 6. This enables replacement of gas or liquid conduits of a conventional device by causing circulation of at least one fluid that has to be sent to a higher or lower modular element and not treated by exchange of mass and/or of heat in the element through which it or they circulate(s).
[0229] It is equally feasible for the internal zone to comprise a plurality of zones 4. For example, there could be a first zone 4 and a second zone separated from one another, each containing structured packing for out distillation or an exchanger matrix with plates and fins for exchange of heat or adsorbent in ball or structured form for adsorption.
[0230] Similarly, the at least two zones could each have a different function or different dimensions, one containing structured packing and the other an exchanger matrix with plates and fins.
[0231] The fluid directed to the zone 5 can be directly in contact with the walls of the zone, which separate the zone from the insulation. Otherwise the fluid can be contained in a conduit that passes through the zone.
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[0234] A barrier 6 divides the chamber 5 in two to form two gas paths, one of the two paths being again divided in two by the barrier 6, the barriers 6, 6 forming a T. The gas arriving from outside the element rises or descends in the path.
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[0237] The stack of two modular elements 10 and 20 of parallelepipedal shape forms an assembly of two modular elements interconnected by mechanical connecting parts 141 at the level of the ISO corners 101. The opening between the two modular elements of parallelepipedal shape, generated by the connecting part 141 and/or by the separation of the beams between the frameworks of the two modular elements, is filled in by an element 131 that provides both the seal with respect to the exterior and the continuity of the insulation between the two modular elements 10 and 20 of parallelepipedal shape. The element 131 can consist of a plurality of sub-elements, for example one providing the insulation function and another the sealing function. The connecting part 141 can be made so that the upper and lower ISO corners are in contact, for example, via a mechanical connection inside the ISO corners or outside it and using the lateral holes of the ISO corners. The opening between the two modular elements of parallelepipedal shape is then reduced to its minimum, of approximately 2 cm, corresponding to the positioning separation of the horizontal metal beams and the ISO corner 101, generally around 1 cm.
[0238] Other ways of assembling the modular elements and/or of providing the seal between the modular elements may be envisaged, for example welding and/or a seal, for example made of PTFE or its derivatives and/or adhesive bonding as well as or instead of a mechanical connection. The beams can be interconnected via a mechanical system, typically using nuts and bolts, like a pipe flange, to reinforce the seal if necessary.
[0239] Obviously more than two elements can be assembled in this manner.
[0240] As the two elements have the same length and the same width, it suffices to fix one element to the other by the contiguous corners 101 in order to attach the elements together. The space between the elements is filled at least with the seal 131 so that the fluids in the zones 4 cannot escape from the assembly of elements but pass entirely from one element to the other.
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[0242] This figure shows the location of the sealing element, for example a seal 131, at the interface between two modular elements 10, 20 of parallelepipedal shape. The element 131 bears on the insulation, and preferably also on the box 2, except for the ISO corners 101. Other elements 132, 133 and 134, possibly of the same kind as the element 131, are going to provide fluid continuity between the two modular elements 10, 20 of parallelepipedal shape, in terms of sealing and possibly insulation: the element 132 when the zone 4 has been divided into a plurality of parts, for example vertically, with walls that can be fluid-tight, the element 133 when it is wished to channel a fluid leaving the zone 4, typically following heat transfer, the element 134 for the fluid circulation zones 5.
[0243] These elements 131, 132, 133 and 134 can be installed when assembling the two modular elements 10, 20 of parallelepipedal shape. These elements 131, 132, 133 and 134 can possibly constitute one and the same piece.
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[0245] In this case, an element of a separation device is sufficiently small or too complex to be divided into a plurality of sections, each of which would be found in a respective modular element. This is typically the case of heat exchangers used as boilers or as condensers.
[0246] At least one fluid circulates up or down through the interface between two modular elements of parallelepipedal shape, at the level of the zone 4, the two modular elements of parallelepipedal shape being of the
[0247] In
[0248] For example, the modular elements 11 and 12 may have the dimensions of a standardized container 40 feet long and the other modular elements 21, 22, 23, 24, 31, 32, 33, 41, 42, 43, 44, 45, 46, 47 and 48 the dimensions of a standardized container 20 feet long.
[0249] The circulation of the fluids respectively in a first stack composed of the modular elements 21, 22, 23 and 24, a second stack composed of the modular elements 31, 32 and 33, a third stack composed of the modular elements 41, 42, 43, 44, 45, 46, 47 and 48 is effected essentially vertically in each modular element and each stack, and essentially vertically at the interface 11, 12 between two modular elements of the stack. Each stack is disposed so that the longest edge of the modular elements is parallel to the ground.
[0250] In the case of separation of air, the first stack 21, 22, 23 and 24 can essentially provide the pre-cooling and head purification function, the second stack 31, 32 and 33 the heat exchange function and the third stack 41, 42, 43, 44, 45, 46, 47 and 48 the cryogenic distillation function between nitrogen and oxygen.
[0251] The third stack could constitute a single column operating at low pressure or a plurality of columns at different pressures, each constituted by a few elements from the stack.
[0252] The modular elements 11 and 12 notably enable the fluids to be caused to circulate horizontally through rectangular ducts and/or round pipes so as to transfer the fluids respectively between the first stack 21, 22, 23 and 24 and the second stack 31, 32 and 33, the second stack 31, 32 and 33 and the third stack 41, 42, 43, 44, 45, 46, 47 and 48. The modular elements 11 and 12 can also provide process and/or control and/or utilities functions. For example they can contain command and/or control and/or analysis and/or instrumentation and/or utility, such as electricity or instrument air supply means.
[0253] The modular element 11 straddles the modular elements 24 and 33, above the first and second stacks, and the modular element 12 straddling the modular elements 31 and 41 under the second and third stack. The modular elements 11 and 12 preferably include intermediate ISO corners 102 to facilitate assembly respectively with the modular elements 24 and 33, with the modular elements 31 and 41.
[0254] The modular element 11, 12 can be insulated in various ways. It can be insulated by depositing insulation on the outside of the box. It can be insulated by covering the inside of the end and lateral faces with insulation and likewise the upper or lower face if the latter is exposed. Another possibility is to insulate the at least one conduit or the at least one duct inside the element 11, 12.
[0255] As the elements 11, 12 comprise only two openings, these openings being found in the lower face and the upper face respectively, the elements 11, 12 essentially serve to transfer a fluid from one stack to the adjacent stack, and possibly to change the direction of flow of the fluids passing through the stacks. Thus a fluid passing upwards through the first stack can pass downwards through the second stack. Nevertheless it should be noted that a fluid can pass through both stacks in the same direction. For example, a gas passes through the first stack and is directed to the second stack by passing through the element 11. It then descends to the element 31 via the zone 5 of the elements 33, 32, 31 before being directed to the chamber of the element 31.
[0256] This would make it possible, for example, to constitute a distillation column, using two stacks of elements, for example the two first stacks from
[0257] The column constituted in this way would have a particularly low height.
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[0259] The modular element 43 from
[0260] The modular element 13 is placed inside the third stack (between the modular elements 42 and 44) and inside the supplementary fourth stack (between the modular elements 53 and 54). If necessary the modular element 13 enables fluids to be caused to circulate vertically between the lower part of the third stack 41 and 42 and the higher part of the third stack 44, 45, 46, 47 and 48. In this case the modular element 13 enables division of the gases coming from only one stack between two stacks. Here for example a gas from an intermediate point of the third stack, constituting a simple low-pressure distillation column, is enriched with argon. This gas continues its path in part toward the top of the single column, that is to say the elements 45 to 48, but is also directed toward the top of the supplementary fourth stack 54, 55, 56, 57, 58, 59, 60, 61 and 62.
[0261] On the other hand, no fluid passes from the element 53 to the element 54 through the element 13. In other configurations, at least one fluid can pass from the element 53 to the element 54 through the element 13 and vice versa.
[0262] The elements 51 to 53 can have a number of variants. They can be simple supports in which case they do not even contain insulation, being simple empty boxes. They can contain other elements useful for the process, for example pumps. The elements 51 to 53 can be modular elements according to the invention as shown in
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[0264] In contrast to
[0265] To fix ideas, the modular elements 21, 22, 23, 24, 31, 32, 33, 41, 42, 43, 44, 45, 46, 47 and 48 have the dimensions of a 20-foot container. If the invention as described in
[0266] In
[0267] The connection between the first stack and the second stack could be produced thanks to a single modular element 11a, and that between the second stack and the third stack by a single modular element 12a, the modular element 12b then being reducible to its structural function alone.
[0268] In contrast to
[0269]
[0270] The modular element 12 preferably includes intermediate ISO corners 102 to facilitate assembly with the modular elements 31 and 41.
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[0272] The modular element 12 preferably includes ISO intermediate corners 102.
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[0274] The modular elements 11a, 11b, 11c, 12a, 12b and 12c can have the same height as the other modular elements, or preferably a reduced height, for example half the height, as shown in
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[0279] The modular elements are stacked in three vertical stacks. Each stack is composed only of elements of one of the two sizes. The modular elements arrive from a manufacturing center CF and/or a logistical platform PL where a plurality of elements of each of the two sizes are stored. A plurality of examples of each element and each body type are stocked, in order to be able to replace any defective element. Thus a single manufacturing center and/or logistical platform is able to serve a plurality of devices in locations that are very far apart, stocking replacement elements. A quality control process makes it possible to ensure that each modular element is functional.
[0280] The various modular elements are assembled on site by stacking them to constitute at least one part of the device.
[0281] The first stack comprises an element A, surmounted by three elements B and part of the element C.
[0282] In the case of a cryogenic atmosphere gas separation device, the modular element A can contain an air blower and a pre-cooling unit, the modular elements B adsorbent to purify the air coming from the blower in A and the modular element C ducts for transfer of fluid from the first stack to the second stack and/or from the second stack to the first stack.
[0283] The modular elements are designed so that the air rises from the lowest modular element B, to the middle modular element B and then to the top modular element B, becoming purified of water and carbon dioxide and some of the secondary air impurities. The purified air is then transferred from the top modular element B to the ducts of the modular element C to pass into the second stack. The regeneration nitrogen is transferred by the modular element C of the second stack to the modular elements B.
[0284] The second stack is placed beside the first stack so that the side walls of the modular elements of the two stacks touch, possibly with a small clearance between the two.
[0285] The second stack comprises part of the modular element C containing the ducts described above, the three modular elements D each containing a heat exchange section, and part of the modular element E containing ducts for transferring at least one fluid from the second stack to the third stack and/or at least one fluid from the third stack to the second stack.
[0286] The purified air passes into the modular elements D to be cooled to a cryogenic temperature and fluids resulting from the distillation pass from the modular element E to the modular elements D to be heated.
[0287] The third stack is placed beside the second stack so that the side walls of the modular elements of the two stacks touch, possibly with a small clearance between the two.
[0288] The third stack, higher than the other two, comprises at the bottom a part of the modular element E with its fluid transfer ducts. On top of E is the modular element F, which is an evaporator. On top of F are found the stacked three modular elements G each containing a distillation section. The modular element H contains a condenser and possibly a distillation section and is found on top of the lowest of the modular elements G. Then there come the three modular elements I each containing a distillation section. On top of the higher section of the modular element I is a condenser J. Disposed beside the other sections are the modular element K that contains a heat pump for distillation and the modular element L that contains a heat pump for the refrigerating balance of the device.
[0289] It is obvious that the diagram could be simplified by eliminating the modular elements L, K and/or the condenser J. The number of modular elements B, D, G and I can be modified to produce required products or to modify the heights of the modular elements.
[0290] The installation of the device is limited to disposing the modular elements on top of one another and ensuring that they are securely attached and sealed from one another and that the stack is correctly fixed to the ground. This can be carried out by relatively unskilled labor.
[0291]
[0292] In the case of a cryogenic atmospheric gas separation device, the modular element I can contain a distillation section (minaret) with the aim of producing pure nitrogen.
[0293] To reduce the energy consumption of a device there may be added:
[0294] An evaporator/condenser modular element at the head of the column and/or in the tank of the column or at an intermediate level of the column to reduce the pinch effect on the evaporator and/or condenser or to add a supplementary intermediate evaporator or condenser function.
[0295] A modular element containing one or more distillation sections.
[0296] An exchange line modular element to the heat exchanger elements to reduce its pinch effect and therefore to reduce the consumption of the heat balance pump.
[0297] A modular element containing a low-energy heat pump or a modular element containing a heat pump connected in parallel with an existing heat pump or connected in part to a supplementary evaporator or condenser.
[0298] To reduce the energy consumption of a device modular elements can be replaced by modular elements of higher performance.
[0299] To modify the device to produce impure oxygen, a distillation modular element can be removed.
[0300] The modular element added or removed can also contain a liquid product pump, a liquefaction unit or a product compressor.
[0301]
[0302] It can also be decided to replace the modular element L that is still functional with a new modular element L of better energy performance for example, or better performance in terms of capacity (debottlenecking).
[0303] This maintenance operation can obviously be effected for any element A, B, C, D, E, F, G, H, J or K of the device.
[0304]
[0305] In the case of a cryogenic atmosphere gas separation device, energy consumption can for example be reduced on the one hand by duplicating the evaporator by adding a modular element F and/or by duplicating the condenser by adding a modular element J, enabling the thermal pinch effect on these exchangers to be reduced, on the other hand, by duplicating the heat pump for distillation by adding a modular element K, enabling the heat pump to function with greater efficiency.
[0306] Here again the installation of the new elements is easy and it suffices to remove the other elements to dispose the new element just above or just below another modular element having the same function (and therefore identified by the same letter) or not having the same function.
[0307]
[0308] In the case of a cryogenic atmosphere gas separation device, argon may be produced for example: the modular element M can contain transfer ducts and is of the larger size. The fourth stack comprises at the bottom the modular element P that contains a liquid lifter pump, then the three stacked modular elements O each containing a distillation section. Part of the modular element M, which is inserted into the third stack, is found on top of the top modular element O. There are then found on top of the part of the modular element M in the fourth stack eight stacked modular elements N each containing a distillation section. The head of the fourth stack is surmounted by a condenser H, relocated from the existing third stack in
[0309]
[0310] While the invention has been described in conjunction with specific embodiments thereof, it is evident that many alternatives, modifications, and variations will be apparent to those skilled in the art in light of the foregoing description. Accordingly, it is intended to embrace all such alternatives, modifications, and variations as fall within the spirit and broad scope of the appended claims. The present invention may suitably comprise, consist or consist essentially of the elements disclosed and may be practiced in the absence of an element not disclosed. Furthermore, if there is language referring to order, such as first and second, it should be understood in an exemplary sense and not in a limiting sense. For example, it can be recognized by those skilled in the art that certain steps can be combined into a single step.
[0311] The singular forms a, an and the include plural referents, unless the context clearly dictates otherwise.
[0312] Comprising in a claim is an open transitional term which means the subsequently identified claim elements are a nonexclusive listing (i.e., anything else may be additionally included and remain within the scope of comprising). Comprising as used herein may be replaced by the more limited transitional terms consisting essentially of and consisting of unless otherwise indicated herein.
[0313] Providing in a claim is defined to mean furnishing, supplying, making available, or preparing something. The step may be performed by any actor in the absence of express language in the claim to the contrary.
[0314] Optional or optionally means that the subsequently described event or circumstances may or may not occur. The description includes instances where the event or circumstance occurs and instances where it does not occur.
[0315] Ranges may be expressed herein as from about one particular value, and/or to about another particular value. When such a range is expressed, it is to be understood that another embodiment is from the one particular value and/or to the other particular value, along with all combinations within said range.
[0316] All references identified herein are each hereby incorporated by reference into this application in their entireties, as well as for the specific information for which each is cited.