Method and apparatus for producing iron powder

10421126 ยท 2019-09-24

Assignee

Inventors

Cpc classification

International classification

Abstract

A method of producing iron powder by a water atomization process may include preparing a molten metal in a tundish, discharging the molten metal in a free-falling manner by opening an orifice formed on a bottom of the tundish, and producing iron powder by spraying water onto the free-falling molten metal using a pair of water spraying nozzles, an angle formed by the water spraying nozzles being at least 45.

Claims

1. An apparatus for producing iron powder by a water atomization process, the apparatus comprising: a pair of nozzles disposed in a lower portion of a tundish to face each other with a free-falling molten metal interposed therebetween, for spraying water onto the molten metal, wherein the nozzles are disposed such that a distance therebetween is adjustable, and wherein each of the nozzles comprises: a fixed body including a thread formed on an outer peripheral surface of the fixed body, a first side of the fixed body being fixed to the lower portion of the tundish; a water spraying nozzle including a thread formed on an inner peripheral surface of the water spraying nozzle, the thread engaging with the thread formed on the outer peripheral surface of the fixed body, the water spraying nozzle being disposed on a second side of the fixed body and spraying the water onto the molten metal discharged from the tundish to produce the iron powder; and a spring disposed around the outer peripheral surface of the fixed body to fix a position of the water spraying nozzle, the spring providing an elastic force to the water spraying nozzle.

2. The apparatus according to claim 1, wherein an atomization angle formed by streams of water sprayed from the pair of water spraying nozzles ranges from 45 to 50.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

(1) FIG. 1 is a view for illustrating a conventional method of producing metal powder by a water atomization process.

(2) FIG. 2 is a schematic view for illustrating that build-up of molten metal occurs due to a water splash phenomenon in the related art.

(3) FIG. 3 is a view schematically illustrating nozzles according to various embodiments of the present invention.

(4) FIG. 4 is a view schematically illustrating nozzles according to various embodiments of the present invention.

(5) FIG. 5 is a flowchart illustrating a method of producing iron powder according to various embodiments of the present invention.

(6) FIG. 6 is a view for illustrating a relationship of a distance between water spraying nozzles, a spraying distance of water, and an atomization angle formed by streams of water according to various embodiments of the present invention.

DETAILED DESCRIPTION

(7) Reference will now be made in detail to various embodiments of the present invention(s), examples of which are illustrated in the accompanying drawings and described below. While the invention(s) will be described in conjunction with exemplary embodiments, it will be understood that the present description is not intended to limit the invention(s) to those exemplary embodiments. On the contrary, the invention(s) is/are intended to cover not only the exemplary embodiments, but also various alternatives, modifications, equivalents and other embodiments, which may be included within the spirit and scope of the invention as defined by the appended claims.

(8) An apparatus for producing iron powder according to various embodiments of the present invention is an apparatus for producing iron powder by a water atomization process, and includes a pair of nozzles 10 which are disposed to face each other with a molten metal 3, falling downward from a tundish 1, interposed therebetween so as to spray water onto a linear region of the flow of the molten metal 3 falling downward from the tundish 1.

(9) In this case, the nozzles 10 are disposed such that the distance therebetween varies with the flow of the molten metal 3 falling free interposed therebetween, and thus form an atomization angle of 45 to 50. Consequently, it is possible to reduce occurrence of water splash and increase a recovery rate of iron powder.

(10) FIG. 3 is a view schematically illustrating nozzles according to various embodiments of the present invention.

(11) As illustrated in FIG. 3, each of nozzles 10 according to various embodiments of the present invention includes a fixed body 12 having a thread formed on the outer peripheral surface thereof while one side of the fixed body 12 is fixed to a lower portion of a tundish (e.g., tundish 1), a water atomization nozzle 11a having a thread which is formed on the inner peripheral surface thereof and engages with the thread formed on the outer peripheral surface of the fixed body 12, the water atomization nozzle 11a being coupled to the other side of the fixed body 12 and spraying water onto the flow of a molten metal 3, and a spring 13 installed around the outer peripheral surface of the fixed body 12 to provide an elastic force to the water atomization nozzle 11a.

(12) In this case, the distance between the pair of water spraying nozzles 11a may be adjusted while the nozzles 11a rotate on the other sides of the respective fixed bodies 12.

(13) FIG. 4 is a view schematically illustrating nozzles according to various embodiments of the present invention.

(14) As illustrated in FIG. 4, each of nozzles 10 according to various embodiments of the present invention includes a spacer 14, one side of which is fixed to the lower portion of a tundish (e.g., tundish 1), having a variable length, a water spraying nozzle 11b installed to the other side of the spacer 14 to spray water onto the flow of a molten metal 3, and a length adjustment member 15 which adjusts the length of the spacer 14.

(15) In some embodiments, the spacer 14 may have, for example, a spring structure having elasticity such that the length thereof varies. The length adjustment member 15 may be a bolt, and one side thereof is inserted into the spacer 14 to fix the length of the spacer 14, thereby enabling the distance between the water spraying nozzles 11b to be adjusted.

(16) In various embodiments of the present invention, the atomization angle formed by the streams of water sprayed from the pair of water spraying nozzles 11 (11a or 11b) may be an angle of 45 to 50, and the atomization pressure P of water is deduced and controlled by the following Equation (1). Description thereof will be given in detail with reference to a method of producing iron powder.

(17) log P log P 0 = D D 0 , [ Equation ( 1 ) ]
where P: atomization pressure (bar), P.sub.0: initial atomization pressure (bar), D: spraying distance (mm), and D.sub.0: initial spraying distance (mm).

(18) Hereinafter, a method of producing iron powder according to various embodiments of the present invention will be described with reference to the drawings.

(19) FIG. 5 is a flowchart illustrating a method of producing iron powder according to various embodiments of the present invention.

(20) As illustrated in FIG. 5, the method of producing iron powder according to various embodiments of the present invention is a method of producing iron powder by a water atomization process, and includes a molten metal preparation process of preparing a molten metal 3 in a tundish 1, a molten metal discharge process of discharging the molten metal 3 in the downward direction of the tundish 1 for the free fall thereof, and a powder formation process of forming iron powder by spraying water onto the flow of the molten metal 3 falling free.

(21) In the molten metal preparation process, scraps of iron are melted and stored in the tundish 1 having an orifice 5 formed on the bottom thereof.

(22) When the molten metal preparation process is completed, the molten metal 3 accommodated in the tundish 1 falls free by opening the orifice 5 on the bottom of the tundish 1.

(23) When the opening of the orifice 5 is completed, iron powder is produced in the powder formation process in which water 7 is sprayed onto the flow of the molten metal 3 falling free from the tundish 1 using a pair of water spraying nozzles 11 (11a or 11b), transforms the molten metal 3 into droplet form by colliding therewith, and then solidifies the same.

(24) In this case, the atomization angle formed by the streams of water sprayed from the water spraying nozzles 11 may be an angle of 45 or more. The reason is because the recovery rate of iron powder is decreased when the atomization angle is an angle less than 45.

(25) In some embodiments, the method of producing iron powder according to various embodiments of the present invention may further include an atomization angle adjustment process of adjusting a distance between the water spraying nozzles 11 to adjust the atomization angle formed by the streams of water 7 colliding with the molten metal 3, prior to the molten metal discharge process.

(26) In the atomization angle adjustment process, a point at which iron powder is formed by collision of the flow of the free-falling molten metal 3 with water 7 sprayed from each the water spraying nozzles 11 may be constant, namely a vertical distance between the water spraying nozzle 11 and the formation point of iron powder may be constant.

(27) That is, in the atomization angle adjustment process, the atomization angle may be adjusted by increasing and decreasing the distance between the water spraying nozzles 11.

(28) If only the atomization angle is adjusted in the state in which the positions of the water spraying nozzles 11 are fixed, the formation point of iron powder is adjacent to the water spraying nozzles 11. Hence, water splash or build-up of the molten metal 3 in the water spraying nozzles 11 occurs, which may lead to equipment damage and a decrease in recovery rate.

(29) Accordingly, in the present invention, in order to prevent the recovery rate of iron powder from decreasing while preventing equipment damage and work accidents such as operation stop, the atomization angle is adjusted by increasing and decreasing the distance A between water spraying nozzles while the formation point of iron powder is constantly maintained.

(30) This is because the acceleration of water is increased even when the spraying distance of water D sprayed from each water spraying nozzle 11 becomes shorter, and thus the upward vertical vector value of the impact force of water is increased as indicated by the following Equation (2).

(31) F y = F cos ( 2 ) = m cos ( 2 ) = m ( d 2 D dr 2 ) cos ( 2 ) , [ Equation ( 2 ) ]
where : atomization angle, : acceleration of water, m: mass of water, D: spraying distance, and t: time.

(32) Accordingly, in the method of producing iron powder according to various embodiments of the present invention, the atomization angle is adjusted by increasing and decreasing the distance A between water spraying nozzles while the formation point of iron powder is constantly maintained.

(33) The following Equations (3) and (4) refer to a relationship of an atomization angle, a distance A between water spraying nozzles, and an injection distance D.

(34) sin ( 2 ) = A 2 D [ Equation ( 3 ) ] 4 D 2 - A 2 = constant [ Equation ( 4 ) ]

(35) FIG. 6 is a view for explaining the relationship of the distance between water spraying nozzles, the spraying distance of water, and the atomization angle formed by streams of water.

(36) As illustrated in FIG. 6, the atomization angle is an angle formed by a pair of water spraying nozzles, and is two times the angle formed by a stream of water sprayed from each water spraying nozzle 11 and an imaginary center line.

(37) When the distance between the pair of water spraying nozzles 11, i.e. the distance A between water spraying nozzles, is increased in the state in which the atomization angle is fixed, the spraying distance D from each water spraying nozzle 11 to the point at which the water 7 sprayed therefrom collides with the molten metal 3 is increased compared to the initial distance. In this case, when the atomization pressure P of each water spraying nozzle 11 is constant, a sufficient pressure may not be maintained when the water 7 collides with the molten metal 3. Hence, efficiency in producing iron powder may be deteriorated or iron powder may not be formed.

(38) In order for the atomization angle formed by the streams of water 7 to be an angle of 45 to 50 in the method of producing iron powder according to various embodiments of the present invention, after the distance A between water spraying nozzles is adjusted in the atomization angle adjustment process, each water spraying nozzle 11 is controlled by calculating the atomization pressure P of water sprayed from the water spraying nozzle 11, based on the distance A between water spraying nozzles and the spraying distance D.

(39) In more detail, according to various embodiments of the present invention, the atomization pressure P of the water spraying nozzle 11 is deduced from the following Equation (1).

(40) log P log P 0 = D D 0 , [ Equation ( 1 ) ]
where P: atomization pressure (bar), P.sub.0: initial atomization pressure (bar), D: spraying distance (mm), and D.sub.0: initial spraying distance (mm).

(41) That is, in order for the ratio between the atomization pressure P and the spraying distance D to be equal to the ratio between the initial atomization pressure P.sub.0 and the initial spraying distance D.sub.0 as reference values, the atomization pressure P of the water spraying nozzle 11 is controlled based on the spraying distance D of the water 7 increased as the distance between water spraying nozzles A is increased, and the atomization pressure P is set such that the spraying distance D is increased/decreased by increasing/decreasing the distance A between water spraying nozzles in order to increase the atomization angle . Consequently, it is possible to increase the recovery rate of iron powder while preventing water splash from occurring.

(42) TABLE-US-00001 TABLE 1 Distance between water Atomization Spraying Atomization Recovery Sort spraying nozzles (A) angle () distance (D) pressure (P) rate (%) Comp. Ex. 1 94 mm 38 144 94 bar 80.5 Comp. Ex. 2 94 mm 45 113 100 bar Nozzle clogging Comp. Ex. 3 94 mm 50 101 100 bar Nozzle clogging Example 1 100 mm 40 146 100 bar 84.1 Example 2 113 mm 45 148 107 bar 88.3 Example 3 128 mm 50 151 117 bar 94.5

(43) As indicated by Table 1, in the comparative examples of the related art, it can be seen that, when the atomization angle is increased in the state in which the distance A between water spraying nozzles is fixed, work accidents, such as the clogging of the water spraying nozzles 11, occur as the spraying distance D becomes shorter. In addition, it can be seen that the recovery rate of iron powder is reduced to 80.5%.

(44) On the other hand, according to various embodiments of the present invention, it can be seen that when the atomization angle is increased by increasing the distance A between water spraying nozzles, the spraying distance D and the atomization pressure P are increased together. Therefore, it is possible to reduce occurrence of water splash and simultaneously prevent work accidents such as the clogging of the water spraying nozzles 11 while the recovery rate is increased to maximum 94.5% by adjusting the atomization pressure.

(45) For convenience in explanation and accurate definition in the appended claims, the terms upper or lower, inner or outer and etc. are used to describe features of the exemplary embodiments with reference to the positions of such features as displayed in the figures.

(46) The foregoing descriptions of specific exemplary embodiments of the present invention have been presented for purposes of illustration and description. They are not intended to be exhaustive or to limit the invention to the precise forms disclosed, and obviously many modifications and variations are possible in light of the above teachings. The exemplary embodiments were chosen and described in order to explain certain principles of the invention and their practical application, to thereby enable others skilled in the art to make and utilize various exemplary embodiments of the present invention, as well as various alternatives and modifications thereof. It is intended that the scope of the invention be defined by the Claims appended hereto and their equivalents.