PREPARATION METHOD OF SCRIBING RUBBER CEMENT OF TIRE TREAD

Abstract

The present invention discloses a preparation method of scribing rubber cement of a tire tread. The scribing rubber cement of the tire tread is prepared from the following raw materials in parts by weight: 100 parts of natural rubber; 3.5 to 4.5 parts of zinc oxide; 1.5 to 2.5 parts of stearic acid; 15 to 25 parts of titanium white; 2.5 to 3.5 parts of insoluble sulfur; 0.9 to 1.1 parts of accelerant DM; 0.9 to 1.1 parts of rosin; and 15 to 25 parts of color masterbatch. The preparation method of the scribing rubber cement comprises the following steps: step 1) preparing rubber compound; and step 2) preparing the scribing rubber cement. The scribing rubber cement of the tire tread prepared by the present invention has high aesthetic degree and does not influence the product quality.

Claims

1. A preparation method of scribing rubber cement of a tire tread, comprising the following raw materials in parts by weight: 100 parts of natural rubber; 3.5 to 4.5 parts of zinc oxide; 1.5 to 2.5 parts of stearic acid; 15 to 25 parts of titanium white; 2.5 to 3.5 parts of insoluble sulfur; 0.9 to 1.1 parts of accelerant DM; 0.9 to 1.1 parts of rosin; and 15 to 25 parts of color masterbatch; the preparation method of the scribing rubber cement comprising the following steps: step 1) preparing rubber compound: preparing raw rubber: performing tire baking using natural rubber in a tire baking room with a temperature of 50 C. to 70 C., wherein the tire baking time in three seasons, i.e. spring, summer and autumn is 24 h to 36 h and the tire baking time in winter is 36 h to 72 h, cutting the rubber after the rubber is baked, weighing, and plasticating; preparing a compounding agent: weighing all raw materials by weight parts; preparing the rubber compound: preparing by adopting an open mill, performing roll covering on the plasticated natural rubber, and then successively adding the stearic acid, the accelerant DM, the zinc oxide, the rosin, the titanium white, the color masterbatch, and insoluble sulfur; and sheeting after the cement is uniformly mixed, wherein the thickness of a rubber sheet is 2.0 mm to 4.0 mm, and the storage time is 8 h to 48 h; step 2) preparing the scribing rubber cement preparing rubber blocks: cutting the uniformly mixed scribing rubber cement into small rubber sheets, wherein the thickness is 2.0 mm to 4.0 mm, the width is 10 mm to 20 mm, and the length is 20 mm to 50 mm; preparing the scribing rubber cement: putting the prepared rubber sheet into a beating machine; then adding gasoline, wherein a mass ratio of the rubber sheet to the gasoline is 1: (2 to 4); covering an opening of the beating machine, and beginning to stir; gradually dissolving the rubber under the continuous stirring of blades of the beating machine, and preparing the uniform scribing rubber cement; and storing the rubber cement: after the scribing rubber cement is prepared, storing the scribing rubber cement in a closed cement storing container, and placing the container in a shade place with a temperature of 20 C. for 24 h to 36 h.

2. The preparation method of the scribing rubber cement of the tire tread according to claim 1, wherein the gasoline is national standard No. 93 or No. 97 or No. 120 gasoline.

3. The preparation method of the scribing rubber cement of the tire tread according to claim 1, wherein the weight ratio of the rubber sheet to the gasoline is 1:3.

4. The preparation method of the scribing rubber cement of the tire tread according to claim 2, wherein the weight ratio of the rubber sheet to the gasoline is 1:3.

5. The preparation method of the scribing rubber cement of the tire tread according to claim 1, wherein the Williames plasticity of the scribing rubber cement is 1.5 to 4.

6. The preparation method of the scribing rubber cement of the tire tread according to claim 2, wherein the Williames plasticity of the scribing rubber cement is 1.5 to 4.

7. The preparation method of the scribing rubber cement of the tire tread according to claim 5, wherein the pH of the scribing rubber cement is 7 to 10.

8. The preparation method of the scribing rubber cement of the tire tread according to claim 5, wherein the pH of the scribing rubber cement is 7 to 10.

Description

DETAILED DESCRIPTION

[0018] The present invention is further described below through embodiments.

Embodiment 1

[0019] A preparation method of scribing rubber cement of a tire tread comprises the following raw materials in parts by weight:

[0020] 100 parts of natural rubber; 3.5 parts of zinc oxide; 1.5 parts of stearic acid; 15 parts of titanium white; 2.5 parts of insoluble sulfur; 0.9 part of accelerant DM; 0.9 part of rosin; and 15 parts of color masterbatch.

[0021] The preparation method of the scribing rubber cement comprises the following steps:

[0022] step 1) preparing rubber compound:

[0023] preparing raw rubber: performing tire baking using natural rubber in a tire baking room with a temperature of 50 C., wherein the tire baking time is 36 h, cutting the rubber after the rubber is baked, weighing, and plasticating;

[0024] preparing a compounding agent: weighing all raw materials by weight parts;

[0025] preparing the rubber compound: preparing by adopting an open mill, performing roll covering on the plasticated natural rubber, and then successively adding the stearic acid, the accelerant DM, the zinc oxide, the rosin, the titanium white, the color masterbatch, and insoluble sulfur; and sheeting after the cement is uniformly mixed, wherein the thickness of a rubber sheet is 2.0 mm, and the storage time is 8 h;

[0026] step 2) preparing the scribing rubber cement

[0027] preparing rubber blocks: cutting the uniformly mixed scribing rubber cement into small rubber sheets, wherein the thickness is 2.0 mm, the width is 10 mm, and the length is 20 mm;

[0028] preparing the scribing rubber cement: putting the prepared rubber sheet into a beating machine; then adding gasoline, wherein a mass ratio of the rubber sheet to the gasoline is 1:2; covering an opening of the beating machine, and beginning to stir; gradually dissolving the rubber under the continuous stirring of blades of the beating machine, and preparing the uniform scribing rubber cement; and

[0029] storing the rubber cement: after the scribing rubber cement is prepared, storing the scribing rubber cement in a closed cement storing container, and placing the container in a shade place with a temperature of 20 C. for 24 h.

[0030] The gasoline is national standard No. 93 or No. 97 or No. 120 gasoline.

[0031] The Williames plasticity of the scribing rubber cement is 1.5 to 4.

[0032] The pH of the scribing rubber cement is 7.

Embodiment 2

[0033] A preparation method of scribing rubber cement of a tire tread comprises the following raw materials in parts by weight:

[0034] 100 parts of natural rubber; 4 parts of zinc oxide; 2 parts of stearic acid; 20 parts of titanium white; 3 parts of insoluble sulfur; 1 part of accelerant DM; 1 part of rosin; and 20 parts of color masterbatch.

[0035] The preparation method of the scribing rubber cement comprises the following steps:

[0036] step 1) preparing rubber compound:

[0037] preparing raw rubber: performing tire baking using natural rubber in a tire baking room with a temperature of 60 C., wherein the tire baking time is 60 h and the tire baking time in winter is 36 h to 72 h, cutting the rubber after the rubber is baked, weighing, and plasticating;

[0038] preparing a compounding agent: weighing all raw materials by weight parts;

[0039] preparing the rubber compound: preparing by adopting an open mill, performing roll covering on the plasticated natural rubber, and then successively adding the stearic acid, the accelerant DM, the zinc oxide, the rosin, the titanium white, the color masterbatch, and insoluble sulfur; and sheeting after the cement is uniformly mixed, wherein the thickness of a rubber sheet is 3.0 mm, and the storage time is 24 h;

[0040] step 2) preparing the scribing rubber cement

[0041] preparing rubber blocks: cutting the uniformly mixed scribing rubber cement into small rubber sheets, wherein the thickness is 3.0 mm, the width is 15 mm, and the length is 40 mm;

[0042] preparing the scribing rubber cement: putting the prepared rubber sheet into a beating machine; then adding gasoline, wherein a mass ratio of the rubber sheet to the gasoline is 1:3; covering an opening of the beating machine, and beginning to stir; gradually dissolving the rubber under the continuous stirring of blades of the beating machine, and preparing the uniform scribing rubber cement; and

[0043] storing the rubber cement: after the scribing rubber cement is prepared, storing the scribing rubber cement in a closed cement storing container, and placing the container in a shade place with a temperature of 20 C. for 30 h.

[0044] The gasoline is national standard No. 93 or No. 97 or No. 120 gasoline.

[0045] The weight ratio of the rubber sheet to the gasoline is 1:3.

[0046] The Williames plasticity of the scribing rubber cement is 3.

[0047] The pH of the scribing rubber cement is 10.

Embodiment 3

[0048] A preparation method of scribing rubber cement of a tire tread comprises the following raw materials in parts by weight:

[0049] 100 parts of natural rubber; 4.5 parts of zinc oxide; 2.5 parts of stearic acid; 25 parts of titanium white; 3.5 parts of insoluble sulfur; 1.1 parts of accelerant DM; 1.1 parts of rosin; and 25 parts of color masterbatch.

[0050] The preparation method of the scribing rubber cement comprises the following steps:

[0051] step 1) preparing rubber compound:

[0052] preparing raw rubber: performing tire baking using natural rubber in a tire baking room with a temperature of 70 C., wherein the tire baking time is 72 h, cutting the rubber after the rubber is baked, weighing, and plasticating;

[0053] preparing a compounding agent: weighing all raw materials by weight parts;

[0054] preparing the rubber compound: preparing by adopting an open mill, performing roll covering on the plasticated natural rubber, and then successively adding the stearic acid, the accelerant DM, the zinc oxide, the rosin, the titanium white, the color masterbatch, and insoluble sulfur; and sheeting after the cement is uniformly mixed, wherein the thickness of a rubber sheet is 4.0 mm, and the storage time is 48 h;

[0055] step 2) preparing the scribing rubber cement

[0056] preparing rubber blocks: cutting the uniformly mixed scribing rubber cement into small rubber sheets, wherein the thickness is 4.0 mm, the width is 20 mm, and the length is 50 mm;

[0057] preparing the scribing rubber cement: putting the prepared rubber sheet into a beating machine; then adding gasoline, wherein a mass ratio of the rubber sheet to the gasoline is 1:4; covering an opening of the beating machine, and beginning to stir; gradually dissolving the rubber under the continuous stirring of blades of the beating machine, and preparing the uniform scribing rubber cement; and

[0058] storing the rubber cement: after the scribing rubber cement is prepared, storing the scribing rubber cement in a closed cement storing container, and placing the container in a shade place with a temperature of 20 C. for 36 h.

[0059] The gasoline is national standard No. 93 or No. 97 or No. 120 gasoline.

[0060] The Williames plasticity of the scribing rubber cement is 4.

[0061] The pH of the scribing rubber cement is 10.

TABLE-US-00001 Control indexes of the scribing rubber cement Name of Rubber sheet: Concentration Williames rubber gasoline (B) PH plasticity Scribing 1: (2-4) 30-45 7-11 1.5-4 rubber cement