Ion milling system
10361065 ยท 2019-07-23
Assignee
Inventors
Cpc classification
H01J37/3056
ELECTRICITY
H01J2237/31745
ELECTRICITY
H01J37/09
ELECTRICITY
H01J37/20
ELECTRICITY
International classification
H01J37/20
ELECTRICITY
Abstract
To provide an ion milling system that can suppress an orbital shift of an observation electron beam emitted from an electron microscope column, the ion milling system includes: a Penning discharge type ion gun 100 that includes a permanent magnet 114 and that generates ions for processing a sample; and a scanning electron microscope for observing the sample, in which a magnetic shield 172 for reducing a leakage magnetic field from the permanent magnet 114 to the electron microscope column is provided.
Claims
1. An ion milling system comprising: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, wherein the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, the ion gun includes an accelerating electrode that accelerates the ions, and the magnetic shield is the accelerating electrode configured with a ferromagnetic material.
2. The ion milling system according to claim 1, wherein the ion gun includes an ion gun base that holds the permanent magnet and the accelerating electrode, and a ferromagnetic material is disposed on a surface, on a side of which the accelerating electrode is disposed, of the ion gun base.
3. The ion milling system according to claim 1, wherein the ion gun includes an ion gun base that holds the permanent magnet and the accelerating electrode, and the magnetic shield is configured with the ferromagnetic material with which an outer peripheral surface of the accelerating electrode and a surface, on a side of which the accelerating electrode is disposed, of the ion gun base are covered.
4. The ion milling system according to claim 1, wherein the ion gun includes an ion gun base that holds the permanent magnet and the accelerating electrode, and the magnetic shield is configured with the ferromagnetic material with which an inner peripheral surface of the accelerating electrode and a surface, on a side of which the accelerating electrode is disposed, of the ion gun base are covered.
5. The ion milling system according to claim 1, wherein the magnetic shield is configured with permalloy, pure iron, nickel, copper, molybdenum, and a material that contains at least one type of permalloy, pure iron, nickel, copper, and molybdenum as a main component.
6. The ion milling system according to claim 1, wherein the ion gun includes an ion gun base that holds the permanent magnet and the accelerating electrode, the accelerating electrode is a structure split into three parts that are an accelerating electrode guide member, a first accelerating electrode member, and a second accelerating electrode member, the accelerating electrode guide member is formed from a material other than a ferromagnetic substance and secured to the ion gun base, the first accelerating electrode member is formed from the ferromagnetic substance and installed on an outer side of the accelerating electrode guide member, the second accelerating electrode member is formed from the ferromagnetic substance and installed by being positioned by the accelerating electrode guide member and the first accelerating electrode member, and the first and second accelerating electrode members are secured by a magnetic field of the permanent magnet.
7. The ion milling system according to claim 1, wherein the magnetic shield includes a magnetic shield guide member that is disposed to surround an outer side of the permanent magnet and that is formed from a material other than a ferromagnetic material; and a magnetic shield member that is disposed to surround an outer side of the magnetic shield guide member and that is formed from the ferromagnetic material.
8. An ion milling system comprising: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, wherein the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, the ion gun includes an accelerating electrode that accelerates the ions; and an ion gun base that holds the permanent magnet and the accelerating electrode, and the magnetic shield is configured with a ferromagnetic material disposed on a surface, on a side of which the accelerating electrode is disposed, of the ion gun base, and a ferromagnetic material with which the accelerating electrode is covered and which is disposed apart from the accelerating electrode.
9. An ion milling system comprising: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, wherein the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, the ion gun includes a cathode ring that is disposed on an outer peripheral surface of the permanent magnet, and the magnetic shield is the cathode ring configured with a ferromagnetic material.
10. An ion milling system comprising: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, wherein the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, the magnetic shield is configured with a ferromagnetic material that surrounds an outer periphery of the permanent magnet and that is disposed apart from the permanent magnet, and the magnetic shield is on an inner side of an accelerating electrode.
11. An ion milling system comprising: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, wherein the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, and the magnetic shield configures a magnetic field control board that controls an axial magnetic field within the ion gun by changing a structure of the magnetic shield.
12. An ion milling system comprising an ion gun that includes a permanent magnet and that generates ions for processing a sample, wherein a magnetic field control board is disposed in such a manner that magnetic field control board surrounds an outer periphery of the permanent magnet, is formed from a ferromagnetic material, and controls an axial magnetic field intensity within the ion gun.
13. The ion milling system according to claim 12, wherein the ion gun includes an accelerating electrode that accelerates the ions; and an ion gun base that holds the permanent magnet and the accelerating electrode, and the magnetic field control board is also disposed on a surface, on a side of which the accelerating electrode is disposed, of the ion gun base.
14. The ion milling system according to claim 12, wherein the axial magnetic field intensity within the ion gun is controlled by changing a structure of the magnetic field control board.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1)
(2)
(3)
(4)
(5)
(6)
(7)
(8)
(9)
(10)
(11)
(12)
(13)
(14)
(15)
(16)
MODES FOR CARRYING OUT THE INVENTION
(17) After conducting a study about the problems, the inventors have decided to add a magnetic shield to a Penning discharge type ion gun. It is thereby possible to reduce a leakage magnetic field from a permanent magnet installed within the ion gun.
(18) Specifically, the ion gun includes, for example, a gas supply mechanism that supplies gas into the ion gun; an anode which is disposed within the ion gun and to which a positive voltage is applied; two cathodes that generate a potential difference between the anode and the cathodes; a cathode ring and an insulator; and a permanent magnet, causes electrons emitted from the two cathodes to turn by the magnetic field, ionizes the gas by the turning electrons, and emits generated ions to outside of the ion gun by an accelerating electrode, in which the accelerating electrode is formed from a ferromagnetic material. This configuration thereby reduces the leakage magnetic field from the ion gun and sufficiently suppresses an orbital shift of an electron beam emitted from an electron microscope column.
(19) In that case, the ferromagnetic material can be formed on a surface, on which the accelerating electrode is disposed, of an ion gun base.
(20) Alternatively, an outer peripheral surface of the accelerating electrode formed from stainless steel and the surface, on which the accelerating electrode is disposed, of the ion gun base can be covered with the ferromagnetic material.
(21) Alternatively, an inner peripheral surface of the accelerating electrode formed from stainless steel and the surface, on which the accelerating electrode is disposed, of the ion gun base can be covered with the ferromagnetic material.
(22) Alternatively, a magnetic shield structure formed from a ferromagnetic material can be formed on an outer side of the ion gun, and the ferromagnetic material can be formed on the surface, on which the accelerating electrode is disposed, of the ion gun base.
(23) Alternatively, the cathode ring can be formed from the ferromagnetic material.
(24) In another alternative, the magnetic shield structure formed from the ferromagnetic material can be formed on an inner side of the accelerating electrode.
(25) Preferably, the ferromagnetic material includes permalloy, pure iron, nickel, copper, molybdenum, and a material containing at least one type of permalloy, pure iron, nickel, copper, and molybdenum as a main component.
(26) Adding the magnetic shield structure to the ion gun makes it possible to sufficiently reduce the leakage magnetic field from the permanent magnet disposed within the ion gun.
(27) Furthermore, changing a structure of a magnetic shield electrode added to the ion gun makes it possible to control an axial magnetic field intensity within the ion gun. It is thereby possible to select an optimum axial magnetic field intensity for deriving an ion gun performance; thus, it is possible to obtain a far higher milling rate than that according to a conventional technique.
(28) Preferred embodiments of the present invention will be explained hereinafter with reference to the drawings. It is noted that the same reference characters denote the same constituent elements.
First Embodiment
(29) An ion milling system will be explained with reference to the drawings.
(30)
(31) The first cathode 111 and the second cathode 112 are made of pure iron that is a ferromagnetic substance, and form, along with the permanent magnet 114 that is a magnetomotive force, a magnetic circuit. On the other hand, the accelerating electrode 115, the cathode ring 119, and the ion gun base 117 are made of stainless steel (SUS: Steel Special Use Stainless), and the accelerating electrode 115, the cathode ring 119, and the ion gun base 117 as well as the insulator 116 made of alumina and the anode 113 made of aluminum are not, therefore, included in the magnetic circuit.
(32) Since the Penning discharge type ion gun as described above is configured such that the permanent magnet is provided inside, a leakage magnetic field from the ion gun has an influence on the electron beam during electron microscope observation. Even a slight electron beam orbital shift causes a problem particularly when a specific microscopic region is observed. Since an electron emitted from the electron microscope column takes on a property that an orbit thereof is curved by a very weak magnetic field, the electron beam is largely curved during conversion of the accelerating voltage or the like and an observation image that is being observed is largely shifted, accordingly in the ion milling system in which the electron microscope is mounted. To avoid this observation image shift, it is necessary to suppress the leakage magnetic field from the ion gun.
(33)
(34) Alternatively, in the magnetic shield structure ion gun 100, forming the magnetic shield 171 made of, for example, pure iron in place of the magnetic shield made of permalloy as the accelerating electrode makes it possible to obtain a magnetic shielding effect, reduce the leakage magnetic field from the magnetic shield structure ion gun 100, and sufficiently suppress the orbital shift of the electron beam 162 emitted from the electron microscope column 161 (configuration 2).
(35)
(36)
(37)
(38)
(39)
(40)
(41)
(42) As described so far, according to the present embodiment, it is possible to provide the ion milling system that includes the Penning discharge type ion gun and that can reduce the leakage magnetic field from the ion gun and sufficiently suppress the orbital shift of the electron beam emitted from the electron microscope column.
(43)
(44) A result of conducting a study about a relationship between the axial magnetic field intensity and performances of the permanent magnet 114 will next be explained. Table 1 shows a list of performance figures of magnets used.
(45) TABLE-US-00001 TABLE 1 magnet magnet A magnet B C magnet D maximum energy product: 302-334 223-247 175-191 127-143 (BH)max (kJ/m3) residual magnetic 1250-1320 1080-1150 950 850 flux density: Br (mT) coercive force: HcB (kA/m) 859 796 637 660 axial magnetic flux 220 200 160 145 density (mT)
(46) On the other hand,
(47)
(48) As explained so far, according to the present embodiment, it is possible to provide the ion milling system that can suppress the orbital shift of the electron beam emitted from the electron microscope column by adding the magnetic shield structure to the ion gun. It is also possible to control the axial magnetic field intensity within the ion gun to have an optimum value by adding the magnetic shield structure to the ion gun. Furthermore, it is thereby possible to provide the Penning discharge type ion milling system that can obtain the milling rate far higher than that according to the conventional technique or obtain the optimum value of the milling rate in response to the various materials or the like.
Second Embodiment
(49) An ion milling system according to a second embodiment of the present invention will be explained. It is noted that matters that are described in the first embodiment but not described in the present embodiment are also applicable to the present embodiment unless there are exceptional circumstances.
(50)
(51) The accelerating electrode guide member 181 is made of a material, for example, stainless steel, other than the ferromagnetic substance and secured to the ion gun base 117 by being screwed (or fitted) thereinto. The first accelerating electrode member 182 is formed from the ferromagnetic substance, for example, pure iron, installed by being fitted along an outer periphery of the accelerating electrode guide member 181, and secured by the magnetic field of the permanent magnet 114. The second accelerating electrode member 183 is formed from the ferromagnetic substance, for example, pure iron, and has a structure such that the second accelerating electrode member 183 is positioned with respect to the magnetic shield structure ion gun 100 by being fitted into grooves formed in tip end portions of the accelerating electrode guide member 181 and the first accelerating electrode member 182. Configuring the shield type accelerating electrode to have the structure split into the three parts can facilitate attaching the accelerating electrode guide member 181 formed from the material other than the ferromagnetic substance first without influence of the permanent magnet 114 and attaching the first and second accelerating electrode members that are the magnetic material next using this accelerating electrode guide member. In other words, the magnetic shield type accelerating electrode 180 that is the ferromagnetic material can be detached without interference of the permanent magnet 114 and maintainability can be ensured.
(52)
(53) The accelerating electrode guide member 181 is made of a material, for example, stainless steel other than the ferromagnetic substance and secured to the ion gun base 117 by being screwed thereinto. The accelerating electrode member 182 is formed from the ferromagnetic substance, for example, pure iron, and has a structure such that the accelerating electrode member 182 is installed by being fitted into the ion gun base 117 along the outer periphery of the accelerating electrode guide member 181 and is positioned with respect to the magnetic shield structure ion gun 100 by being secured to the ion gun base 117 by the magnetic field of the permanent magnet 114. Configuring the shield type accelerating electrode 180 to have the structure split into the two parts can facilitate attaching the accelerating electrode guide member 181 formed from the material other than the ferromagnetic substance first without influence of the permanent magnet 114 and attaching the accelerating electrode member 182 that is the magnetic material next using this accelerating electrode guide member 181. In other words, the magnetic shield type accelerating electrode 180 that is the ferromagnetic material can be detached without the interference of the permanent magnet 114 and the maintainability can be ensured. While the accelerating electrode guide member is provided because of use of the accelerating electrode as the magnetic shield in the present embodiment, similar effects can be basically obtained by providing a magnetic shield guide member formed from a material other than the ferromagnetic substance.
(54) As explained so far, the present embodiment can exhibit similar effects to those of the first embodiment. Furthermore, providing the magnetic shield guide member such as the accelerating electrode guide member formed from the material other than the ferromagnetic substance makes it possible to facilitate attaching or detaching the ferromagnetic magnetic shield and ensure maintainability.
(55) The present invention is not limited to the embodiments described above but encompasses various modifications. For example, the abovementioned embodiments have been explained in detail for explaining the present invention so that the present invention is easy to understand. The present invention is not always limited to the examples having all the configurations described so far. Furthermore, the configuration of the certain embodiment can be partially replaced by the configuration of the other embodiment or the configuration of the other embodiment can be added to the configuration of the certain embodiment. Moreover, for part of the configuration of each embodiment, additions, omissions, and substitutions of the other configurations can be made.
(56) While the present invention has been explained in detail, the present invention includes the following aspects.
(57) (1) An ion milling system including: an ion gun that includes a permanent magnet and that generates ions for processing a sample; and a scanning electron microscope that observes the sample, in which
(58) the ion milling system includes a magnetic shield that reduces a leakage magnetic field from the permanent magnet, and
(59) the magnetic shield configures a magnetic field control board that controls an axial magnetic field within the ion gun by changing a structure of the magnetic shield.
(60) (2) An ion milling system including an ion gun that includes a permanent magnet and that generates ions for processing a sample, in which
(61) a magnetic field control board is disposed in such a manner that magnetic field control board surrounds an outer periphery of the permanent magnet, is formed from a ferromagnetic material, and controls an axial magnetic field intensity of the ion gun.
(62) (3) The ion milling system according to (2), in which
(63) the ion gun includes an accelerating electrode that accelerates the ions; and an ion gun base that holds the permanent magnet and the accelerating electrode, and
(64) the magnetic field control board is also disposed on a surface, on a side of which the accelerating electrode is disposed, of the ion gun base.
(65) (4) The ion milling system according to (2), in which
(66) the axial magnetic field intensity within the ion gun is controlled by changing a structure of the magnetic field control board.
DESCRIPTION OF REFERENCE CHARACTERS
(67) 100: Magnetic shield structure ion gun 101: Ion gun 102: Ion beam 103: Ion gun control section 104: Vacuum chamber 105: Evacuation system 106: Sample 107: Sample stage 108: Sample stage drive section 109: Sample stage drive control section 111: First cathode 112: Second cathode 113: Anode 114: Permanent magnet 115: Accelerating electrode 116: Insulator 117: Ion gun base 118: Ionization chamber 119: Cathode ring 121: Discharge power source 122: Accelerating power source 131: Anode outlet hole 132: Cathode outlet hole 133: Accelerating electrode outlet hole 141: Gas supply mechanism 142: Gas source 151: Current measurement means 152: Current probe drive section 153: Current probe 161: Electron microscope column 162: Electron beam 171, 172, 173, 174, 175, 176, 177: Magnetic shield 181: Magnetic shield type accelerating electrode 181: Accelerating electrode guide member 182, 183: Accelerating electrode member