Cold cathode ionization vacuum gauge
10352811 ยท 2019-07-16
Assignee
Inventors
- Gerardo A. Brucker (Longmont, CO)
- Timothy C. Swinney (Fort Collins, CO)
- Brandon J. Kelly (Longmont, CO, US)
- Alfred A. Funari (Fort Collins, CO, US)
- Michael N. Schott (Loveland, CO)
- Kristian S. Schartau (Erie, CO, US)
Cpc classification
H01J9/50
ELECTRICITY
Y02W30/82
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
G01L19/06
PHYSICS
International classification
H01J9/50
ELECTRICITY
G01L19/06
PHYSICS
Abstract
A cold cathode ionization vacuum gauge includes an extended anode electrode and a cathode electrode surrounding the anode electrode along its length and forming a discharge space between the anode electrode and the cathode electrode. The vacuum gauge further includes an electrically conductive guard ring electrode interposed between the cathode electrode and the anode electrode about a base of the anode electrode to collect leakage electrical current, and a discharge starter device disposed over and electrically connected with the guard ring electrode, the starter device having a plurality of tips directed toward the anode and forming a gap between the tips and the anode.
Claims
1. A cold cathode ionization vacuum gauge assembly comprising: a cold cathode ionization vacuum gauge comprising: an extended anode electrode; and a cathode electrode surrounding the anode electrode along its length; an electronics module configured to be coupled to the vacuum gauge in either of first and second configurations, in the first configuration the electronics module being displaced from the vacuum gauge and coupled to the vacuum gauge by a cable and in the second configuration the electronics module being directly coupled to the vacuum gauge with an interface of physical mating surfaces complementary to physical mating surfaces of the vacuum gauge, the electronics module including electronics adapted to operate and read the vacuum gauge and further including an interlock on the electronics module configured to detect the presence of the vacuum gauge or the first end of the cable; and the cable coupled between the electronics module and the vacuum gauge in the first configuration with the vacuum gauge and the electronics module displaced from each other, the cable having a first end and a second end, the first end being configured to imitate physical mating surfaces of the vacuum gauge to mate to the electronics module, and the second end being configured to imitate physical mating surfaces of the electronics module to mate to the vacuum gauge.
2. The cold cathode ionization vacuum gauge assembly of claim 1, wherein the cold cathode ionization vacuum gauge further comprises an anode guard ring and the first end of the cable comprises a central anode connection pin, an anode guard ring insulator spaced from and surrounding the anode connection pin and a guard ring connection surrounding and spaced from the anode guard ring insulator.
3. The cold cathode ionization vacuum gauge assembly of claim 2, wherein the first end of the cable further comprises an outer cylindrical insert having an interlock groove for detection by the electronics module.
4. The cold cathode ionization vacuum gauge assembly of claim 1, wherein the cold cathode ionization vacuum gauge further comprises an anode guard ring and the second end of the cable comprises a central anode connection sleeve, a guard ring insulator mating sleeve and a guard ring mating sleeve.
5. A cable for connecting an electronics module to a cold cathode ionization vacuum gauge, with the vacuum gauge and electronics module displaced from each other in a first configuration, where the electronics module is configured to be displaced from the vacuum gauge, the electronics module also being configured to be directly coupled to the vacuum gauge with an interface complementary to the vacuum gauge, the cable having a first end and a second end, the first end being configured to imitate physical mating surfaces of the vacuum gauge to mate to the electronics module, and the second end being configured to imitate physical mating surfaces of the electronics module to mate to the vacuum gauge; wherein the first end of the cable comprises a central anode connection pin, an anode guard ring insulator spaced from and surrounding the anode connection pin, a guard ring connection surrounding and spaced from the anode guard ring insulator, and a cathode electrode connection, and the second end of the cable comprises a central anode connection sleeve, a guard ring insulator mating sleeve, a guard ring mating sleeve, and a cathode electrode connection; and wherein the first end of the cable further comprises an interlock feature to enable detection by the electronics module.
6. The cable of claim 5, wherein the first end further comprises an outer cylindrical insert and the interlock feature is an interlock groove on the cylindrical insert.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) The foregoing will be apparent from the following more particular description of example embodiments of the invention, as illustrated in the accompanying drawings in which like reference characters refer to the same parts throughout the different views. The drawings are not necessarily to scale, emphasis instead being placed upon illustrating embodiments of the present invention.
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DETAILED DESCRIPTION OF THE INVENTION
(27) A description of example embodiments of the invention follows.
(28) The cold cathode ionization vacuum gauge described herein relies on the inverted magnetron principle. The gauge is of cylindrical symmetry. A large voltage potential difference (i.e., radial electric field) between the anode pin (located at the axis) and the cathode cylindrical envelope provides energy to the electrons for the ionization events to occur. A crossed axial magnetic field provides the electron trajectory path length required to maintain a discharge inside the envelope. The discharge current is the measured quantity that is proportional to the pressure in the system.
(29) The discharge is established through an avalanche ionization process that generally starts with a single electron being released into the ionization volume of the gauge. The process responsible for releasing an electron can include a field emission event or a cosmic ray ionization process. The avalanche process relies on the long path length for the electron trajectories that leads to many ionization processes per electron. Each ionization process releases an ion as well as an additional electron that is added into the discharge. As the ions collide with the cathode internal walls, additional electrons are also released into the discharge, thereby contributing to the total charge. The electrical discharge consisting of ions and electrons reaches an ion density that is proportional to the pressure in the system.
(30) The cold cathode ionization vacuum gauge described herein relies on the double inverted magnetron principle introduced by Drubetsky in 1995. See U.S. Pat. No. 5,568,053. The double inverted magnetron design, shown in
(31) Accordingly, in one aspect, shown in
(32) The removable and replaceable anode sleeve 110b may be a thin walled tube that slides onto the anode post 110, providing electrical connection to the anode post and shielding the post surface from contamination build-up. The anode sleeve 110b may simply be held in place with a friction fit. The anode sleeve 110b may also include a hole 110c on the top end that can be used to hook the sleeve in order to pull it out of the gauge structure. The bottom end of the anode sleeve 110b may include a flare 110d. The anode sleeve flare 110d can inhibit deposits from falling into the starter device 150.
(33) Once a gauge shows signs of contamination, it should be possible to quickly and easily clean the contaminated areas of the gauge and restore it to a fully functional condition. The anode in a CCIVG is expected to build a layer of hydrocarbon or silicone contaminants very quickly in a vacuum system. A removable anode sleeve 110b can be used in CCIVGs to protect and shield the anode post from contamination build up during the operation of the gauge. Used in combination with the removable cathode 120, it provides a fast and easy method of field servicing a CCIVG and a CCIVG user is able to restore the entire gauge in a matter of a few minutes. This method of servicing a CCIVG has several advantages over previous methods. Using a removable and replaceable anode sleeve 110b and cathode eliminates the need to use abrasive materials to clean the anode post and cathode once they are contaminated. Abrasive cleaners may abrade away too much material from the internal surfaces of the gauge and significantly impact their mechanical and chemical characteristics. With a removable sleeve and cathode, the contaminated surfaces can be easily removed and replaced with a clean set. The contaminated cathode cage and the anode sleeve do not have to be cleaned by means of abrasive treatments. In most cases, the cleaning can be done in an ultrasonic cleaner with the help of proper chemicals. One way to eliminate hydrocarbon build up on the anode post is to use alkaline cleaners such as a concentrated solution of NaOH followed by a rinsable cleaning solution. Using a removable anode sleeve and cathode reduces the possibility of affecting the concentric alignment between the anode and the cathode because the gauge does not need to be fully disassembled. The maintenance cost is minimal. A user with access to an extra anode sleeve/cathode combination can quickly do a swap each time maintenance is required.
(34) As discussed above, a crossed axial magnetic field provides the electron trajectory path length required to maintain a discharge inside the discharge space 130. The magnetic field is created by magnet assembly 115, shown in
(35) The electrically conductive guard ring electrode 140 is interposed between the cathode electrode 120 and the anode electrode 110 about a base of the anode electrode 110 to collect leakage electrical current that would otherwise tend to flow between the anode electrode 110 and the cathode electrode 120 if electrically conductive deposits accumulate over time on surfaces of the cathode-guard ring insulator 103 exposed to the discharge space 130 during operation of the vacuum gauge 100.
(36) A discharge starter device 150 is disposed over and electrically connected with the guard ring electrode 140. As shown in
(37) During operation of the vacuum gauge 100, electrical contacts to the anode electrode 110 and guard ring electrode 140 are made by the anode connection 110a and the guard ring connection 102, respectively. Electrical contact to the cathode electrode 120, which is grounded, is made either by a spring clip 310 shown in
(38) As shown in
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where E is the electric field (MV/m), is the work function of the material (eV), is the field enhancement factor, and A is the effective emitting area (m.sup.2). As shown in
(40) Since the start times of a cold cathode ionization vacuum gauge are of a statistical nature, meaning that under the same conditions different start times will be measured each time, if enough samples are measured, a distribution of start times is generated. While it is difficult to specify a start time from a histogram of start times, if a cumulative probability is used, which is the normalized integral of the starting time histogram, the starting probability can be predicted at any time and voltage at a given pressure. Starting times are measured by turning off all sources of ions in a vacuum chamber; after a waiting period, the high voltage power supply (HVPS) 430 to the gauge is turned on, and both the cathode discharge current I.sub.D and the guard ring current I.sub.GR are measured; when the cathode current jumps from its nominal baseline of 10ths of nanoamperes to operational values several decades larger, the start time is logged. The system is automated to repeat this collection method, so that start time statistics can be accumulated.
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(42) Turning to
(43) Cold cathode ionization vacuum gauges presently available commercially typically have 1) a gauge connected to a controller through a cable interconnect, or 2) a gauge connected directly to an electronics module, i.e. with no cable interconnect. The choice between the two technologies seems to be defined by (1) the need to bake out the gauge while the gauge is operating and (2) a need to operate the electronics remotely from the gauge. Most modular CCIVGs require a direct connection between the gauge and the module, and tools are often required to separate the gauge from the controller. In some cases the magnet assembly is part of the electronics module, and in some other cases the magnets are part of the gauge which might require an additional tool to separate them from the gauge tube. CCIVGs with modular configurations generally include o-ring or compressed glass fittings and generally do not allow extensive and/or high temperature bakeouts. The lack of flexibility of modular designs limits their applicability and drives many users to more complicated and costlier products that include remote controllers.
(44) The cold cathode ionization vacuum gauge described herein combines the best features of the commercially available vacuum gauges described above by including both an optional cable and an electronics module. As shown in
(45) As shown in
(46) To detect the interlock of the vacuum gauge with the electronics module, the position of the plate 960 is detected. To detect the position of the plate, a finger 990a is carried by the plate 960. When the interlock 945 is not engaged, the gauge detector finger 990a depresses a gauge detector button shown schematically at 990b; that is, the button is pushed up in
(47) The design shown in
(48) As shown in
(49) The cable 1105 also includes a second end 1150, shown in
(50) Methods of operating a cold cathode ionization vacuum gauge described herein include setting a voltage potential difference to form an electrical discharge between the anode electrode and the cathode electrode, measuring a discharge impedance between the anode electrode and the cathode electrode, and deriving a pressure reading therefrom.
(51) In one aspect, a method of operating a cold cathode ionization vacuum gauge includes switching the voltage potential difference between a high voltage setting and a low voltage setting at a lower pressure than that of a high voltage measurement anomaly and at a higher pressure than that of a low voltage measurement anomaly. Measurement anomalies or discontinuities in the calibration curves for current and voltage as a function of pressure in cold cathode ionization vacuum gauges are well known. See P. A. Redhead, Instabilities in crossed-field discharges at low pressures, Vacuum vol. 38 pp. 901-908 (1988). These measurement anomalies are dependent on the specific geometry of the gauge, and occur over a limited pressure range at particular voltages. For example, as shown in
(52) The high voltage measurement anomaly and the low voltage measurement anomaly can be discharge current anomalies, or discharge impedance anomalies. As shown in
(53) Turning back to
(54) In order to avoid discontinuities, it is important to avoid reaching the voltages that lead to discontinuities at pressures that support those discontinuities. One possible solution to avoid discontinuities is to operate the CCIVGs with low anode voltages and the smallest possible current limiting resistor, for example, by using a 2.0 kV High Voltage Supply and a 20 M limiting resistor to make sure that the anode voltage remains below the discontinuity voltage throughout the entire range of the gauge. Operating the CCIVG with a low High Voltage supply, such that the anode voltage remains below the voltages that lead to discontinuities, is a good approach, because the resulting current and impedance curves do not have large discontinuities. However, the sensitivity of the gauge is lower at a low anode voltage potential difference, as a result of the reduced electric field inside the ionization volume. For example, the cold cathode ionization vacuum gauge described herein has a sensitivity as large as 12 A/Torr for a 5 kV high voltage setting, but decreases to 1 A/Torr at 2 kV. The solution described herein is to operate the gauge at two different voltage settings, a high voltage setting at low pressure, and a low voltage setting at higher pressure. The high voltage setting can be in a range of about 3.5 kV to about 6 kV, and the low voltage setting can be in a range of about 2 kV to about 3 kV. Turning back to
(55) In addition to avoiding discontinuities, the dual voltage mode of operation provides several additional advantages: 1. It provides the ability to increase the anode voltage levels at low pressures without having to worry about the effects of higher pressures. This is ideal for UHV operation where a gauge could operate at a very high voltage for UHV measurement and switches to a much lower voltage before the discontinuity is reached. This provides high sensitivity at UHV, avoids the discontinuities, and provides protection of the gauge at higher pressures where a low voltage minimizes sputtering. Operation at high voltage at UHV provides better sensitivity and also faster start times. 2. It provides the ability to avoid discontinuities providing improved accuracy and repeatability. 3. It provides lower wear and tear at high pressures by minimizing sputtering.
(56) Minimizing sputtering is important for the lifetime of a cold cathode ionization vacuum gauge, but there are circumstances when a higher discharge current is tolerable during normal operation of the vacuum gauge. Another method of operating a cold cathode ionization vacuum gauge includes measuring a leakage electrical current between an electrically conductive guard ring electrode interposed between the cathode electrode and the anode electrode about a base of the anode electrode, and triggering a gauge maintenance alarm if the pressure reading is less than an oscillatory discharge current pressure level and the leakage electrical current is greater than a maximum allowable leakage current limit. The oscillatory discharge current pressure level can be about 510.sup.6 Torr. The maximum allowable leakage current limit can be about 1 A. Turning back to
(57) Oscillatory discharge currents are not expected below a certain pressure, which is dependent on the particular design of the vacuum gauge. Therefore, if the maximum allowable leakage current limit is exceeded and the pressure is less than the oscillatory discharge current pressure level, i.e., where oscillatory discharge currents are not expected, then it is likely that the gauge has developed excessive feedthrough leakage current and/or starter field emission current and a gauge maintenance alarm is triggered. If, on the other hand, the maximum allowable leakage current limit is exceeded and the pressure is higher than the oscillatory discharge current pressure level, then it is likely that oscillatory discharge currents are responsible for the increase in current and no gauge maintenance alarm is triggered. The specific oscillatory discharge current pressure level depends on the gauge design and operational conditions. To check on the operational viability of the gauge, the gauge needs to be evacuated to a pressure below the oscillator discharge current pressure level and the feedthrough leakage current needs to be measured and compared to the maximum allowable leakage current limit.
(58) Yet another method of estimating the operational viability of a cold cathode ionization vacuum gauge includes measuring a discharge current between the anode electrode and the cathode electrode, and deriving a pressure reading therefrom, recording the discharge current as a function of time, and integrating the discharge current over time to obtain a pressure dose for the vacuum gauge. Pressure dose as a measure of the effective lifetime of cold cathode ionization vacuum gauges was introduced by Wilfert and Schindler in 2004. See St. Wilfert and N. Schindler, Applied Physics A vol. 78, pp. 993-666 and 691-694 (2004). Wilfert and Schindler integrated the measured pressure over time to obtain the pressure dose PD(T) according to the expression
PD(T)=.sub.0.sup.TP(t)dt(2)
where P(t) is the pressure measured at time t, and T is the elapsed time (hours) since the beginning of measurements. They concluded that a cold cathode ionization vacuum gauge operated in a typical residual gas environment has an accuracy degradation in a range of about 10% to about 30% after a pressure dose of 1.1 mbar*h.
(59) Integrating the measured pressure is not suitable at high pressures for cold cathode ionization vacuum gauges that have limiting resistors, because, as discussed above, for such vacuum gauges the pressure is not directly related to the discharge current, and it is more likely that the discharge current is responsible for the accuracy degradation of the gauge due to sputtering of the cathode. The pressure dose expression converted to discharge current is
PD(T)=.sub.0.sup.TI.sub.D(t)dt(3)
where I.sub.D(t) is the discharge current at time t, and T is the elapsed time since the beginning of measurements. The Wilfert and Schindler 1.1 mbar*h converts to an integrated charge of about 3,600 Coulombs.
(60) The method can further include recording and integrating a gas factor as a function of time, to account for gas species dependent sputtering rates, using the expression
PD(T)=f.sub.0.sup.TG(t)I.sub.D(t)dt(4)
where G(t) is a gas species factor at time t (default is equal to 1 for nitrogen), I.sub.D(t) is the discharge current at time t, and T is the elapsed time since the beginning of measurements.
(61) The method can further include recording and integrating an ion energy factor as a function of time, because the ion energy is likely to affect the sputtering rate of the cathode. The integration over time of the sputtering rate provides a closer approximation of the pressure dose. The sputtering rate depends on the discharge current (i.e., the number of ions hitting the cathode per unit time) and it is weighted by the gas species and the energy of the ions reaching the cathode. An energy factor is therefore introduced to account for the fact that the energy of the ions depends on the pressure (i.e., the anode voltage changes with pressure, due to the limiting resistor discussed above). The expression including the energy factor is
PD(T)=f.sub.0.sup.TE(t)G(t)I.sub.D(t)dt(5)
where E(t) is the energy factor at time t, G(t) is a gas species factor at time t (default is equal to 1 for nitrogen), I.sub.D(t) is the discharge current at time t, and T is the elapsed time since the beginning of measurements. The energy factor is higher at lower pressures and lower at higher pressures where the anode voltage decreases relative to the high voltage power supply output (see
(62) Additionally, the method can include determining a remaining service life for the vacuum gauge based on the pressure dose. The remaining service life is calculated using
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where EF is an environmental factor (default=1), and PD.sub.max is the maximum acceptable dose (default is 3,600 Coulombs as discussed above). The environmental factor can be adjustable, enabling adjustment in the rate at which the remaining service life decreases as the pressure dose increases. An environmental factor greater than 1 allows a larger maximum pressure dose, increasing the service life of the vacuum gauge. Vacuum gauge that operate in more benign environments or ones that can tolerate larger changes in sensitivity before replacement of the vacuum gauge can use an EF>1. On the other hand, vacuum gauges that operate in harsher environments (e.g., including exposure to corrosive gases, such as chlorine) or ones that need to provide higher accuracy can use an EF<1, leading to more frequent replacement of the vacuum gauge. The remaining service life diminishes from 100% to 0% as the pressure dose progresses from 0 Coulombs to (PD.sub.max*EF).
(64) The relevant teachings of all patents, published applications and references cited herein are incorporated by reference in their entirety.
(65) While this invention has been particularly shown and described with references to example embodiments thereof, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the scope of the invention encompassed by the appended claims.