MICRO CHANNEL CARTRIDGE FOR MASS SPECTROMETER
20240194467 ยท 2024-06-13
Assignee
Inventors
Cpc classification
H01J49/025
ELECTRICITY
International classification
Abstract
A cartridge assembly for a mass spectrometer includes two detector plates. Each of the two detector plates includes (a) an active area defining a plurality of channels from a first side of each of the two detector plates to a second side of each of the two detector plates, and (b) a plurality of clamping areas. A spacer is disposed between the two detector plates and includes a plurality of clamping tabs aligned with each of the plurality of clamping areas. A washer is disposed proximate a second detector plate and includes a plurality of clamping blocks aligned with each of the plural-ity of clamping tabs. A cartridge housing includes a first portion disposed adjacent a first detector plate, and a second portion disposed adjacent the second detector plate, and fasteners span the first and second portions. A biasing element is disposed between the washer and the first portion.
Claims
1. A cartridge assembly for a mass spectrometer, the cartridge assembly comprising: two detector plates, each of the two detector plates comprising (a) an active area defining a plurality of channels from a first side of each of the two detector plates to a second side of each of the two detector plates, and (b) a plurality of clamping areas; a spacer disposed between the two detector plates, the spacer comprising a plurality of clamping tabs, wherein each of the plurality of clamping tabs are aligned with each of the plurality of clamping areas; a washer disposed proximate a second detector plate of the two detector plates, wherein the washer comprises a plurality of clamping blocks, wherein each of the plurality of clamping blocks are aligned with each of the plurality of clamping tabs; a cartridge housing comprising: a first housing portion disposed adjacent a first detector plate of the two detector plates; and a second housing portion disposed adjacent the second detector plate; a plurality of fasteners spanning the first housing portion and the second housing portion; and a biasing element disposed between the washer and the first housing portion.
2. The cartridge assembly of claim 1, wherein the plurality of clamping areas are disposed proximate a perimeter of the each of the two detector plates.
3. The cartridge assembly of claim 1, wherein the plurality of clamping areas comprise channelless portions of each of the two detector plates.
4. The cartridge assembly of claim 1, wherein each of the plurality of clamping tabs extend outward from a perimeter of the spacer.
5. The cartridge assembly of claim 1, wherein the washer comprises an inner ring and an outer ring, and wherein the clamping blocks extend from the inner ring.
6. The cartridge assembly of claim 5, wherein the inner ring is raised relative to the second detector plate.
7. The cartridge assembly of claim 1, wherein the biasing element comprises an axial canted coil spring disposed proximate an outer portion of the washer.
8. A cartridge assembly for a mass spectrometer, the cartridge assembly comprising: an input detector plate, wherein the input detector plate defines a plurality of input plate channels extending from an input side of the input detector plate to an output side of the input detector plate; an output detector plate, wherein the output detector plate defines a plurality of output plate channels extending from an input side of the output detector plate to an output side of the output detector plate, and wherein the input detector plate and the output detector plate are aligned along a common axis; a spacer in contact with the output side of the input detector plate and the input side of the output detector plate; a washer disposed in contact with the output side of the output detector plate; an input housing portion disposed in contact with the input side of the input detector plate; and a biasing element in contact with the washer for biasing each of the washer, the output detector plate, the spacer, and the input detector plate towards the input housing portion.
9. The cartridge assembly of claim 8, wherein each of the plurality of input plate channels and each of the plurality of output plate channels comprises: a channel axis disposed at an angle to the common axis; an input channel mouth defined by the input side of each of the input plate and the output plate, respectively; and an output channel mouth defined by the output side of each of the input plate and the output plate, respectively.
10. The cartridge assembly of claim 9, wherein the plurality of input plate channels comprise a housing subset of input plate channels, wherein the input channel mouth of the housing subset of input plate channels is obstructed by the input housing portion, and wherein the output channel mouth of the housing subset of input plate channels is unobstructed.
11. The cartridge assembly of claim 9, wherein the plurality of input plate channels comprises a spacer subset of input plate channels, wherein the input channel mouth of the spacer subset of input plate channels is unobstructed, and wherein the output channel mouth of the spacer subset of input plate channels is obstructed by the spacer.
12. The cartridge assembly of claim 9, wherein the plurality of output plate channels comprises a spacer subset of output plate channels, wherein the input channel mouth of the spacer subset of output plate channels is obstructed by the spacer, and wherein the output channel mouth of the spacer subset of output plate channels is unobstructed.
13. The cartridge assembly of claim 9, wherein the plurality of output plate channels comprises a washer subset of output plate channels, wherein the input channel mouth of the washer subset of output plate channels is unobstructed, and wherein the output channel mouth of the washer subset of output plate channels is obstructed by the washer.
14. The cartridge assembly of claim 8, wherein the output detector plate comprises a clamping area characterized by an absence of the plurality of output plate channels.
15. The cartridge assembly of claim 14, wherein the washer contacts the clamping area on an output side of the output detector plate and the spacer contacts the clamping area on an input side of the output detector plate.
16. The cartridge assembly of claim 8, wherein the biasing element comprises an axial canted coil spring having an inner diameter greater than an inner diameter of the washer.
17. The cartridge assembly of claim 16, further comprising an output housing portion, wherein the axial canted coil spring biases the washer away from the output housing portion.
18. A method of assembling a cartridge, the method comprising: positioning an input detector plate against an input housing portion, wherein the input detector plate comprises a plurality of input plate clamping areas, and wherein the input housing portion comprises a plurality of plate support features; positioning a spacer against the input detector plate, wherein the spacer comprises a plurality of clamping tabs; positioning an output detector plate against the spacer, wherein the output detector plate comprises a plurality of output plate clamping areas; positioning a washer against the output detector plate, wherein the washer comprises a plurality of clamping blocks; positioning a biasing element against the washer; and positioning an output housing portion against the biasing element, wherein the plurality of plate support features, the plurality of input plate clamping areas, the plurality of clamping tabs, the plurality of output plate clamping areas, and the plurality of clamping blocks are aligned.
19. The method of claim 18, further comprising fastening the output housing portion to the input housing portion, wherein fastening the output housing portion to the input housing portion applies a biasing force from the biasing element to each of the washer, the output detector plate, the spacer, the input detector plate, and the input housing portion.
20. The method of claim 18, further comprising applying a biasing force with the biasing element proximate a perimeter of each of the input housing portion, the input detector plate, the spacer, the output detector plate, and the washer.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION
[0016] Careful assembly of an MCP cartridge is critical for proper performance and to prevent damage to the MCPs. For example, the MCPs should be clamped in such a way to achieve maximum flatness of the plates. The mount and stack configuration must not trap gas in the MCP channels, which can cause a damaging discharge in the MCP channels to occur. The creepage paths around the edge of each MCP from the top metallization to the bottom metallization should not be shorted out by contact with any conductor. The clamping force must be sufficient to prevent movement of the MCP in response to shock and vibration. Finally, electrical contact must be made to the upper and lower MCPs to energize them to perform their electron multiplication function.
[0017] The cartridges described herein include a number of features to limit or eliminate damage to the MCPs or other components of an MCP cartridge or detector system, or which otherwise improve performance. In examples, the cartridges may include one or more of the following features. An input housing portion may include plate support features to contact the solid mounting pads or clamping areas on an input MCP. An input housing portion may also include an opening having a raised circular lip in contact with the circumference of the input MCP. A similar structure may be present on the output housing portion as well. A spacer may include clamping tabs aligned to the clamping area on the input and output MCPs. A portion of the housing may act as an insulator around the MCPs to confine the MCPs, align the spacer, and insulate the input housing from the output housing, and the edges of the MCPs from both housings. A biasing element in the form of a canted coil spring may be utilized to provide even and well-controlled force pressing a washer against the output MCP. The output housing portion compresses and holds the spring, washer, MCPs, and spacer in place. The components are configured such that no micro-channels are obstructed at both ends by contacting components. Alignment markings may be included to facilitate correct angular alignment of the MCPs, which may be important to achieving correct ventilation of the channels. Further, all parts are made with precision tolerance to ensure flatness.
[0018] As noted above, the configuration of the cartridges described herein ensures that no micro-channels are blocked on both ends. This allows faster pump down of the detector instrument to a safe operating condition and minimizes the risk of a discharge in the MCPs. Further, it provides for maximum flatness for the input MCP, thus reducing warp-induced jitter in the time-of-flight (ToF) measurement. For the user of the detector, this minimizes pump down time to the ready state, avoids the cost and inconvenience of premature MCP failure, and maximizes the resolution of the instrument.
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[0021] The cartridge 200 includes a plurality of components that form a housing 202 thereof. An input housing portion of the housing includes components 202a and 202b. Both of input housing portions 202a and 202b define an opening 204a, 204b therein. The lower input housing portion 202a includes a plurality of flanges 206 that may be secured to the standoffs 112 depicted in
[0022] The input MCP 212 is a micro-channel plate, a planar component used for detection of single particles (e.g., ions, electrons, neutrons, etc.) and low intensity impinging radiation. The input MCP 212 includes a body 214 made from highly resistive material and may have a thickness of about 2 mm. The body 214 includes a regular array of tiny tubes or slots (e.g., micro-channels) in a so-called active area of the body 214. The active area is not specifically depicted but may be considered any portion of the body 214 where one or more micro-channels are present. Each micro-channel is defined on an input side of the input MCP 212 by an input channel mouth and on an output side of the input MCP 212 by an output channel mouth. The micro-channels are densely distributed over a significant portion of the surface of the body 214, and may be approximately 5 micrometers in diameter. Micro-channels may be spaced apart by approximately 6 micrometers and may be distributed substantially parallel to each other. In examples, the micro-channels may enter the MCP 212 at a small angle to the surface (e.g., about 12? from normal), or orthogonal thereto (e.g., if the input beam is at an angle to the MCP 212). Although the micro-channels cannot be accurately depicted in
[0023] The input MCP 212 also includes a plurality of clamping areas 218 positioned proximate a perimeter or periphery of the input MCP 212. Four clamping areas 218 are depicted but any number may be utilized. The clamping areas 218 are characterized by an absence of any micro-channels 216 therein, thus rendering the clamping areas 218 channelless. When the cartridge 200 is assembled, each clamping area 218 is aligned with one of the plate support features 210 on the input housing portion 202a, 202b. As described in more detail herein, this alignment help ensure the clamping force of the cartridge 200 is distributed at the appropriate areas of the input MCP 212.
[0024] A spacer 220 is positioned adjacent the input MCP 212. The spacer 220 includes an outer diameter Dso less than an outer diameter of the input MCP 212. Extending from an outer perimeter or periphery of the spacer 220 are a plurality of clamping tabs 222. When the cartridge 200 is assembled, each clamping tab 222 is aligned with one of the clamping areas 218 on the input MCP 212. Further, the spacer 220 defines a central opening 224 which may at least partially define a significant portion of the active area described above (with regard to the input MCP 212). More specifically, the opening 224 is sized such that the vast majority of micro-channels in the input MCP 212 are unobstructed by the spacer 220 itself. A micro-channel must be entirely unobstructed on both the input side and output side to detect ions. It may be advantageous to size the spacer 220 and arrange the micro-channels such that as large a number of the micro-channels as possible are unobstructed on both sides. The clamping tabs 222 are configured and positioned to contact discrete and predetermined portions of an output MCP 226.
[0025] The output detector plate 226 is a micro-channel plate, generally similar or identical to the input MCP 212. The output MCP 226 also includes a plurality of clamping areas 232 positioned proximate a perimeter or periphery of the input MCP 226. Four clamping areas 232 are depicted but any number may be utilized. The clamping areas 232 are characterized by an absence of any micro-channels 230 therein, thus rendering the clamping areas 232 channelless. When the cartridge 200 is assembled, each clamping area 232 is aligned with one of the clamping tabs 222 on the spacer 220. As described in more detail herein, this alignment help ensure the clamping force of the cartridge 200 is distributed at the appropriate areas of the output MCP 226.
[0026] A washer 234 is positioned adjacent the output MCP 226. The washer 234 includes an inner ring 236 and an outer ring 238, which are described further with regard to
[0027] The biasing element 244 may be an axial canted coil spring in contact with the washer 234 that distributes biasing force evenly across the washer 234. Thus, the force distribution against the remaining components between the washer 234 and the input housing portion 202a, 202b also remains even and consistent. The force of the spring biasing element 244 against the washer 234 is at least partially caused by contact between the spring 244 and the output housing portion 246. The outer housing portion 246 includes a number of flanges 248 configured to receive a mechanical fastener 250 such as a bolt or screw. The bolt or screw 250 extends from the output housing portion 248 and is secured to the input housing portion 202a, 202b, to draw the two housing portions 248, 202a, 202b together. This, in turn, evenly applies force of the spring 244 against the internal components of the cartridge 200. Notably, the force is applied primarily along the contact surfaces of the various components, that is, the clamping blocks 240, the clamping areas 232, the clamping tabs 222, the clamping areas 218, and the plate support features 210.
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[0029] While the spring force is distributed downward (towards the input I side) evenly proximate the perimeter of the input MCP 214 and the output MCP 226, the cartridge 200 is configured such that compression force F is transmitted through particular locations of the cartridge 200 (generally aligned with the clamping areas 232, 218). Relevant to this distribution of compression force F,
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[0034] This disclosure described some examples of the present technology with reference to the accompanying drawings, in which only some of the possible examples were shown. Other aspects can, however, be embodied in many different forms and should not be construed as limited to the examples set forth herein. Rather, these examples were provided so that this disclosure was thorough and complete and fully conveyed the scope of the possible examples to those skilled in the art.
[0035] Although specific examples were described herein, the scope of the technology is not limited to those specific examples. One skilled in the art will recognize other examples or improvements that are within the scope of the present technology. Therefore, the specific structure, acts, or media are disclosed only as illustrative examples. Examples according to the technology may also combine elements or components of those that are disclosed in general but not expressly exemplified in combination, unless otherwise stated herein. The scope of the technology is defined by the following claims and any equivalents therein.