Proofing dyeing cup for supercritical fluid dyeing and finishing

Abstract

The invention discloses a proofing dyeing cup for supercritical fluid waterless dyeing and finishing, which achieves separate or simultaneous filling of the medium into multiple dyeing units, and simultaneous heating of the dyeing units for proofing processing. Efficiency of proofing processing such as high-pressure supercritical fluid waterless dyeing and thus the utilization rate of the medium boosting and filling system and separation and recycling system are significantly improved, so that the proofing requirements of commercial production of textile waterless dyeing and finishing are met. Furthermore, dye chemicals at the bottom of the cup can be stirred to facilitate dissolution, and the dye chemicals at the bottom of the cup can be swept and cleaned. Thus, defects of an existing fixed supercritical fluid dyeing proofing device or an equipment system thereof, such as low utilization efficiency, complex cleaning and incapability of meeting the proofing requirements of commercial production, are overcome.

Claims

1. A proofing dyeing cup for supercritical fluid waterless dyeing and finishing, comprising a high-pressure dyeing cup body (6), a high-pressure dyeing cup seal cover (4), a high-pressure fluid delivery tube (7), a first high-pressure pipe (8), a second high-pressure pipe (9), a first high-pressure stop valve (1) and a second high-pressure stop valve (5), wherein: the high-pressure dyeing cup seal cover covers an upper cup opening of the high-pressure dyeing cup body, one end of the first high-pressure pipe being connected with an upper end of the high-pressure dyeing cup seal cover, the other end of the first high-pressure pipe being connected to an external gas source or filling system, and the first high-pressure stop valve being mounted on the first high-pressure pipe; the inner bottom of the high-pressure dyeing cup body is in the shape of a concave circular arc, a medium outlet (10) being provided on a side wall of the high-pressure dyeing cup body at a position adjacent to the cup opening, one end of the second high-pressure pipe being connected at the medium outlet, the other end of the second high-pressure pipe being connected to an external separation and recycling system, and the second high-pressure stop valve being mounted on the second high-pressure pipe; the high-pressure fluid delivery tube is connected with a lower end of the high-pressure dyeing cup seal cover, and the high-pressure fluid delivery tube being vertically suspended in the high-pressure dyeing cup body; the proofing dyeing cup for supercritical fluid waterless dyeing further comprises a wireless integrated pressure and temperature sensor (2) and a safety valve (3), the wireless integrated pressure and temperature sensor being mounted on the first high-pressure pipe or the second high-pressure pipe, and the safety valve being mounted on the first high-pressure pipe or the second high-pressure pipe; both the wireless integrated pressure and temperature sensor and the safety valve are mounted on the second high-pressure pipe, a four-way connector (12) being mounted on the second high-pressure pipe between the medium outlet and the second high-pressure stop valve, and the wireless integrated pressure and temperature sensor and the safety valve being mounted at two opposite joints of the four-way connector respectively; and an upper end of the high-pressure fluid delivery tube is threadedly connected with the first high-pressure pipe on the high-pressure dyeing cup seal cover, and a lower end of the high-pressure fluid delivery tube being at a distance of 0.5-5 cm from the bottom of the high-pressure dyeing cup body.

2. The proofing dyeing cup for supercritical fluid waterless dyeing and finishing as claimed in claim 1, wherein both the wireless integrated pressure and temperature sensor and the safety valve are mounted on the first high-pressure pipe, a four-way connector being mounted on the first high-pressure pipe between the high-pressure dyeing cup seal cover and the first high-pressure stop valve, and the wireless integrated pressure and temperature sensor and the safety valve being mounted at two opposite joints of the four-way connector respectively.

3. The proofing dyeing cup for supercritical fluid waterless dyeing and finishing as claimed in claim 1, wherein the wireless integrated pressure and temperature sensor is mounted on the first high-pressure pipe and the safety valve is mounted on the second high-pressure pipe, a first three-way connector (13) being mounted on the first high-pressure pipe between the high-pressure dyeing cup seal cover and the first high-pressure stop valve, the wireless integrated pressure and temperature sensor being mounted at a middle joint of the first three-way connector, a second three-way connector (14) being mounted on the second high-pressure pipe between the medium outlet and the second high-pressure stop valve, and the safety valve being mounted at a middle joint of the second three-way connector.

4. The proofing dyeing cup for supercritical fluid waterless dyeing and finishing as claimed in claim 1, wherein the wireless integrated pressure and temperature sensor is mounted on the second high-pressure pipe and the safety valve is mounted on the first high-pressure pipe, a first three-way connector (13) being mounted on the first high-pressure pipe between the high-pressure dyeing cup seal cover and the first high-pressure stop valve, the safety valve being mounted at a middle joint of the first three-way connector, a second three-way connector (14) being mounted on the second high-pressure pipe between the medium outlet and the second high-pressure stop valve, and the wireless integrated pressure and temperature sensor being mounted at a middle joint of the second three-way connector.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

(1) FIG. 1 is a schematic view of a proofing dyeing cup for supercritical fluid waterless dyeing and finishing according to embodiment 1 of the present invention;

(2) FIG. 2 is a schematic view of a proofing dyeing cup for supercritical fluid waterless dyeing and finishing according to embodiment 2 of the present invention;

(3) FIG. 3 is a schematic view of a proofing dyeing cup for supercritical fluid waterless dyeing and finishing according to embodiment 3 of the present invention; and

(4) FIG. 4 is a schematic view of a proofing dyeing cup for supercritical fluid waterless dyeing and finishing according to embodiment 4 of the present invention.

(5) In the drawings: 1. first high-pressure stop valve; 2. wireless integrated pressure and temperature sensor; 3. safety valve; 4. high-pressure dyeing cup seal cover; 5. second high-pressure stop valve; 6. high-pressure dyeing cup body; 7. high-pressure fluid delivery tube; 8. first high-pressure pipe; 9. second high-pressure pipe; 10. medium outlet; 12. four-way connector; 13. first three-way connector; and 14. second three-way connector.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENTS

(6) The invention will be further illustrated in more detail with reference to the accompanying drawings and embodiments. It is noted that, the following embodiments only are intended for purposes of illustration, but are not intended to limit the scope of the present invention.

Embodiment 1

(7) As shown in FIG. 1, a proofing dyeing cup for supercritical fluid waterless dyeing and finishing includes a high-pressure dyeing cup body 6, a high-pressure dyeing cup seal cover 4, a high-pressure fluid delivery tube 7, a first high-pressure pipe 8, a second high-pressure pipe 9, a first high-pressure stop valve 1 and a second high-pressure stop valve 5. The high-pressure dyeing cup seal cover covers the upper cup opening of the high-pressure dyeing cup body. One end of the first high-pressure pipe is connected with the upper end of the high-pressure dyeing cup seal cover, and the other end of the first high-pressure pipe is connected to an external gas source or filling system. The first high-pressure stop valve is mounted on the first high-pressure pipe.

(8) The first high-pressure stop valve can achieve the filling of a medium into the dyeing cup, and the separation and disconnection of the dyeing cup from the gas source or filling system.

(9) The inner bottom of the high-pressure dyeing cup body is in the shape of a concave circular arc. A medium outlet 10 is provided on the side wall of the high-pressure dyeing cup body at a position adjacent to the cup opening. One end of the second high-pressure pipe is connected at the medium outlet, and the other end of the second high-pressure pipe is connected to an external separation and recycling system. The second high-pressure stop valve is mounted on the second high-pressure pipe.

(10) The second high-pressure stop valve can achieve the pressure relief and output of the medium in the dyeing cup, and the separation and disconnection of the dyeing cup from the separation and recycling system.

(11) The high-pressure fluid delivery tube is connected with the lower end of the high-pressure dyeing cup seal cover, and the high-pressure fluid delivery tube is vertically suspended in the high-pressure dyeing cup body.

(12) The proofing dyeing cup for supercritical fluid waterless dyeing further includes a wireless integrated pressure and temperature sensor 2 and a safety valve 3. Both the wireless integrated pressure and temperature sensor and the safety valve are mounted on the second high-pressure pipe. A four-way connector 12 is mounted on the second high-pressure pipe. The four-way connector is located between the medium outlet and the second high-pressure stop valve. The wireless integrated pressure and temperature sensor and the safety valve are mounted at two opposite joints of the four-way connector respectively.

(13) The wireless integrated pressure and temperature sensor can achieve remote transmission of the pressure of the medium in the dyeing cup. The safety valve can achieve emergency pressure relief when the pressure in the cup exceeds a safety pressure.

(14) The upper end of the high-pressure fluid delivery tube is threadedly connected with the first high-pressure pipe on the high-pressure dyeing cup seal cover, and The lower end of the high-pressure fluid delivery tube is at a distance of 0.5-5 cm from the bottom of the high-pressure dyeing cup body.

(15) When the medium is filled into the dyeing cup, chemicals such as dye at the bottom of the cup can be stirred to facilitate dissolution. During the cleaning of the dyeing cup, the chemicals such as dye at the bottom of the cup can also be swept effectively, and thus the cleaning efficiency is improved.

(16) Certainly, the mounting positions of the wireless integrated pressure and temperature sensor and the safety valve are not limited to that described in this embodiment 1, and may also be other positions. Some of the other mounting positions of the wireless integrated pressure and temperature sensor and the safety valve are provided in the following embodiments.

Embodiment 2

(17) As shown in FIG. 2, both the wireless integrated pressure and temperature sensor and the safety valve are mounted on the first high-pressure pipe. A four-way connector 12 is mounted on the first high-pressure pipe. The four-way connector is located between the high-pressure dyeing cup seal cover and the first high-pressure stop valve. The wireless integrated pressure and temperature sensor and the safety valve are mounted at two opposite joints of the four-way connector respectively.

Embodiment 3

(18) As shown in FIG. 3, the wireless integrated pressure and temperature sensor is mounted on the first high-pressure pipe, and the safety valve is mounted on the second high-pressure pipe. A first three-way connector 13 is mounted on the first high-pressure pipe. The first three-way connector is located between the high-pressure dyeing cup seal cover and the first high-pressure stop valve. The wireless integrated pressure and temperature sensor is mounted at a middle joint of the first three-way connector. A second three-way connector 14 is mounted on the second high-pressure pipe. The second three-way connector is located between the medium outlet and the second high-pressure stop valve, and the safety valve is mounted at a middle joint of the second three-way connector.

Embodiment 4

(19) As shown in FIG. 4, the wireless integrated pressure and temperature sensor is mounted on the second high-pressure pipe and the safety valve is mounted on the first high-pressure pipe. A first three-way connector 13 is mounted on the first high-pressure pipe. The first three-way connector is located between the high-pressure dyeing cup seal cover and the first high-pressure stop valve. The safety valve is mounted at a middle joint of the first three-way connector. A second three-way connector 14 is mounted on the second high-pressure pipe. The second three-way connector is located between the medium outlet and the second high-pressure stop valve, and the wireless integrated pressure and temperature sensor is mounted at a middle joint of the second three-way connector.

(20) When the proofing dyeing cup for supercritical fluid waterless dyeing and finishing of the present invention operates, firstly, quantitative textile products on which proofing treatment such as dyeing needs to be performed and quantitative dye chemicals such as dye are placed in the high-pressure dyeing cup body 6. The high-pressure dyeing cup seal cover 4 is used to seal the high-pressure dyeing cup body, and other components are connected and assembled correspondingly. Then, the second high-pressure stop valve 5 is closed, the upper end of the first high-pressure pipe connected with the first high-pressure stop valve 1 is communicated with the gas source of the processing medium or the medium filling system, and the first high-pressure stop valve 1 is opened to perform quantitative medium filling on the dyeing cup system. After the filling is finished, the first high-pressure stop valve 1 is closed, and the dyeing cup system is separated from the filling system. The above operations are repeated, to fill the medium into a series of dyeing cups on which proofing treatment needs to be performed. Subsequently, the prepared dyeing cups to be heated for proofing are placed in a heating system or other heating baths, and proofing treatment is performed in a centralized manner according to a predetermined heating program and proofing conditions.

(21) After the proofing is finished, the dyeing cups may be separately or simultaneously connected into a dedicated separation and recycling system through the second high-pressure pipe at a lateral end of the second high-pressure stop valve 5, to separate and recycle the dyeing medium. Furthermore, according to the actual proofing requirements, the dyeing cup may also be communicated with the gas source of the processing medium or the medium filling system through the upper end of the first high-pressure pipe connected with the first high-pressure stop valve 1, to clean unfixed dye or other residual dye chemicals on a sample in the dyeing cup and residual dye chemicals in the cup by using the clean fluid medium. The medium for cleaning flows through the medium outlet 10 at the upper end and on the outer side surface of the high-pressure dyeing cup body 6, and is then treated by the separation and recycling system.

(22) After the separation and recycling and/or cleaning is finished, first, the first high-pressure stop valve 1 disposed on each dyeing cup needs to be closed, and then, a gas pump provided for the separation and recycling system is used to fully recycle and reduce the pressure of the medium in each dyeing cup. When a pressure displayed by the wireless integrated pressure and temperature sensor 2 is equal to or less than the atmospheric pressure, the gas pump of the separation and recycling system is stopped. Then, the dedicated gas source of the processing medium or the medium filling system as well as the separation and recycling system connected to the dyeing cup are respectively disconnected and separated, the high-pressure dyeing cup seal cover 4 is opened and the sample is taken out, to accomplish the sample proofing for waterless dyeing and finishing. By repeating the above operations, the next sample proofing of supercritical fluid waterless dyeing and finishing can be implemented continuously.

(23) The above description is only preferred embodiments of the present invention and not intended to limit the present invention, it should be noted that those of ordinary skill in the art can further make various modifications and variations without departing from the technical principles of the present invention, and these modifications and variations also should be considered to be within the scope of protection of the present invention.