Process of Preparing a Malt-Based Beverage

Abstract

A process of preparing a malt-based beverage includes at least two flavour components A and B in a weight ratio A/B of X.sub.final.The method includes the following steps. Brewing and fermenting a wort is performed to obtain a fermented malt-based beverage having at least two water-soluble components A and B, other than alcohol or water, in a weight ratio A/B of X1>X.sub.final. Then, adjusting the weight ratio of A/B at concentrating said fermented malt-based beverage by removal of water therefrom to obtain a concentrated malt-based beverage having a weight ration A/B of X.sub.final occurs. The ratio A/B of X.sub.1 is determined in anticipation of adjusting the amount of component A in the beverage during concentrating.

Claims

1. A process of preparing a malt-based beverage comprising at least two flavour components A and B in a weight ratio A/B of .sub.Xfinal, said method comprising the steps of: brewing and fermenting a wort to obtain a fermented malt-based beverage comprising at least two water-soluble components A and B, other than alcohol or water, in a weight ratio A/B of X.sub.1>X.sub.final, adjusting the weight ratio of A/B at concentrating said fermented malt-based beverage by removal of water therefrom to obtain a concentrated malt-based beverage having a weight ration A/B of X.sub.final, wherein the ratio A/B of X.sub.1 is determined in anticipation of adjusting the amount of component A in the beverage during concentrating.

2. The process according to claim 1, the concentration step comprising one or more of freeze concentration, concentration by reverse osmosis, nanofiltration, ultrafiltration or distillation.

3. The process according to claim 1, the concentration step comprising a 2-step concentration comprising a first concentration by filtration, resulting in a concentrated retentate and a permeate; and a second concentration step removing water from the permeate thereby obtaining a concentrated alcohol containing fraction to be added with the retentate of the first concentration step prior to dilution, during dilution or after dilution to obtain the malt-based beverage.

4. The process according to claim 1, said component A having an average mean size of 150 Da or smaller.

5. The process according to claim 1, said component A having a boiling point of 100 C. or higher.

6. The process according to claim 1, said component A being one of: an ester, iso-alfa acid, dymethylsulfide.

7. The process according to claim 6, said ester being chosen from the group of: ethylformate, n-amyl acetate, isoamyl acetate, isobutyl propionate, methyl butyrare, ethyl butyrate, n-butyl butyrate, n-amyl butyrate, isoamyl valerate, methyl salicylate and/or combinations thereof.

8. The process according to claim 1, the concentration step concerning a concentration of the beverage solids by a factor of at least 3, preferably at least 4, and most preferably at least 6 in view of the fermented malt-based beverage prior to concentration.

9. The process according to claim 1, said component B being maltotetraose.

10. The process according to claim 1, the fermented malt-based beverage having an original extract level A.sub.fermented in a range of 10 P-20 P.

11. The process according to claim 1, comprising the step of diluting the concentrated malt-based beverage by the addition of diluent.

12. The process according to claim 11, comprising selecting the amount of diluent for dilution of the concentrated malt-based beverage to obtain a beverage having an original extract level A.sub.beverage in a range of 4 P-20 P.

13. The process according to claim 12, the original extract level A.sub.beverage being smaller than or equal to A.sub.fermented.

14. The process according to claim 10, the diluent being water.

15. The process according to claim 10, the diluent comprising CO, N.sub.2 or N.sub.2O dissolved therein.

16. The process according to claim 2, said component A having an average mean size of 150 Da or smaller.

17. The process according to claim 3, said component A having an average mean size of 150 Da or smaller.

18. The process according to claim 2, said component A having a boiling point of 100 C. or higher.

19. The process according to claim 3, said component A having a boiling point of 100 C. or higher.

20. The process according to claim 4, said component A having a boiling point of 100 C. or higher.

Description

DETAILED DESCRIPTION OF A PREFERRED EMBODIMENT

[0023] The present invention concerns a process of preparing a malt-based beverage, the process comprising the steps of brewing a wort, preferably based on malt-based mash, boiling said wort and subsequently fermenting the wort. After fermentation the fermented broth is filtered and subsequently stabilized (eg with PVPP or kieselguhr) to obtain the fermented beverage.

[0024] The fermented beverage comprises at least two water-soluble components A and B, other than alcohol or water, in a weight ratio A/B of X.sub.1, whereby component A preferably has an average mean size of 150 Da or less such as one of: an ester, dimethylsulfide or an iso-alfa acid and the component B is a component having an average means size of larger than 150 Da such as maltotetraose. The fermented beverage preferably has an original extract level of between 10 Plato and 20 Plato.

[0025] Following the stabilisation, the fermented beverage is concentrated, i.e. water is removed from the beverage, thereby concentrating the component B, for example at least 3 times, preferably at least 4 times or even up to 6 times or more in comparison with the fermented beverage after stabilisation.

[0026] According to the invention the ratio X.sub.1 of the weight in which components A/B are present in the fermented beverage is adjusted during the concentration step to a ratio X.sub.final. In practice, X.sub.final will be smaller than X1 as during concentration, a fraction of the component A in the beverage will be allowed to be removed together with the water. Such removal during concentration allows for tweaking the brewing and fermentation of the malt-based beverage to allow a more cost-efficient brewing and fermentation process. As an example, adjusting the amount of dimethylsulfide (DMS) in the fermented beverage, by allowing selective removal of DMS together with water during for example a nanofiltration step allows reducing the boiling time of the wort, as in brewing of regular beer, DMS is removed during boiling and the boiling of the wort will only be stopped once the DMS levels are below a given threshold value. Experiments have shown that with nanofiltration, the DMS level in the beer can be reduced with about 91% for Stella Artois and with about 83% for Leffe, whilst with a concentration step comprising freeze concentration the DMS levels can be reduced by about 27% (weight %) for Stella Artois and about 15% for Leffe.

[0027] According to another example, the fermentation conditions can be altered by applying more stress on the yeast (less stringent temperature conditions during fermentation), resulting in a malt-based beverage having a higher concentration of esters such as eg. ethylformate, n-amyl acetate, isoamyl acetate, isobutyl propionate, methyl butyrare, ethyl butyrate, n-butyl butyrate, n-amyl butyrate, isoamyl valerate, methyl salicylate and/or combinations thereof. During the total weight amount of eg isoamylacetate can be lowered by 15% (weight %) for Stella Artois when using freeze concentration and even up to 60% (weight %) with nanofiltration, whilst for Leffe, the isoamylacetate can be lowered by 11% by freeze concentration and by 60% with nanofiltration.

[0028] The amount of maltotetraose is not or only in a very limited amount affected by the concentration of the malt-based beverage. As such the ratio A/B is adjusted during concentration to a level X.sub.final lower than X.sub.1.

[0029] After concentration the malt-based beverage is preferably packed in packaging providing adequate gas and light barrier properties. And for consumption, the malt based beverage concentrate is preferably rediluted, either with water or another liquid (alcohol, beer, cider, . . . ) to obtain a malt-based beverage having a ratio of A/B of X.sub.final. The amount of diluent is hereby preferably chosen to match or to be slightly lower than the amount of water removed during concentration. The original extract level of the final malt based beverage preferably ranging between 4 Plato and 20 Plato.

[0030] The diluent may optionally have CO.sub.2, N.sub.2 or N.sub.2O dissolved therein.

[0031] The method of concentration of the fermented malt-based beverage is preferably one or more of freeze concentration, concentration by reverse osmosis, nanofiltration, ultrafiltration or distillation.

[0032] A preferred method for obtaining a concentration level of at least 3, preferably 4 and most preferably 6 or more concerns a 2-step concentration method, said method comprising the steps of:

a) Subjecting beer or cider to a first concentration step comprising nanofiltration or reverse osmosis to obtain a retentate and a fraction comprising alcohol and volatile flavour components, wherein the retentate is characterised by the concentration of unfilterable compounds equal to or higher than 20% (w/w), preferably 30% (w/w), most preferably 40% (w/w), as calculated from density measurement corrected for the alcohol amount;
b) Subjecting the fraction comprising alcohol and volatile flavour components to a next concentration step comprising freeze concentration, distillation, fractionation, or reverse osmosis, to obtain a concentrated fraction comprising alcohol and volatile flavour components and a leftover fraction;
c) Combining the retentate from a) with the concentrated fraction comprising alcohol and volatile flavour components from b) to obtain the beer concentrate.

[0033] In a particular embodiment, the method for preparing alcohol-enriched beer concentrate, said method comprising the steps of:

a) Subjecting beer or cider to a first concentration step comprising nanofiltration to obtain a retentate and a fraction comprising alcohol and volatile flavour components, wherein the retentate is characterised by the concentration of unfilterable compounds equal to or higher than 30% (w/w), preferably 35% (w/w), most preferably 40% (w/w), as calculated from density measurement corrected for alcohol amount;
b) Subjecting the fraction comprising alcohol and volatile flavour components to a next concentration step comprising freeze concentration, distillation, fractionation, or reverse osmosis, to obtain a concentrated fraction comprising alcohol and volatile flavour components and a leftover fraction;
c) Combining the retentate from a) with the concentrated fraction comprising alcohol and volatile flavour components from b) to obtain the beer concentrate.

[0034] In some cases it is desired to store the retentate and concentrated fraction comprising alcohol separately until redilution of the beer, in such instance the ratio Xfinal is the one measured after recombining the retentate and the concentrated fraction comprising alcohol together with a diluent.