Nanostructured-lattices produced by surface mechanical attrition treatment method
10253383 ยท 2019-04-09
Assignee
Inventors
Cpc classification
C21D10/00
CHEMISTRY; METALLURGY
C21D2211/00
CHEMISTRY; METALLURGY
International classification
Abstract
The present invention is about the design and manufacturing method of constructing nano-structured lattices. The design of the four periodic two-dimensional lattices (hexagonal, triangulated, square and Kagome) is described; and the process of making nano-structured lattices is outlined in the present invention.
Claims
1. A nano-structured lattice generated by surface mechanical attrition treatment (SMAT), comprising: a plurality of bar members having end portions; and one or more holes embedded inside the nano-structured lattice, wherein the lattice is two-dimensional; wherein one or more of the bar members comprise one or more nodes for connecting one or more other bar members; and wherein one or more of the bar members are partly treated at each of the end portions around the one or more nodes by the SMAT.
2. The lattice of claim 1, wherein a grain size at a surface of the one or more SMAT treated bar members has been reduced to form at least one nano-structured layer with grain size in nanometer after being treated by the SMAT.
3. The lattice of claim 1, wherein the lattice is a square lattice comprising the one or more holes in a square shape, and wherein the one or more holes comprises at least two holes being periodically located along two principal axes of planar space.
4. The lattice of claim 3, one of the two principal axes defining a horizontal axis, wherein the one or more SMAT treated bar members are horizontal bar members for being subjected to an applied loading along the horizontal axis of the square lattice.
5. The lattice of claim 3, wherein the one or more SMAT treated bar members are partly treated at their end portion within a circle around the one or more nodes.
6. The lattice of claim 5, wherein the circle has a radius (R) calculated by:
R=(11/k)l/2 where k is SMAT duration in minutes, and l is length of each bar member in millimeters.
7. The lattice of claim 1, wherein the one or more SMAT treated bar members are treated by the SMAT based on being subjected to a maximum axial stress.
8. The lattice of claim 7, wherein the maximum axial stress is uniaxial.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) Embodiments of the present invention are described in more detail hereinafter with reference to the drawings, in which:
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DETAILED DESCRIPTION OF PREFERRED EMBODIMENTS
(20) In the following description, nanostructured lattices, and the corresponding embodiments of the fabrication methods are set forth as preferred examples. It will be apparent to those skilled in the art that modifications, including additions and/or substitutions, may be made without departing from the scope and spirit of the invention. Specific details may be omitted so as not to obscure the invention; however, the disclosure is written to enable one skilled in the art to practice the teachings herein without undue experimentation.
(21) The present invention is the combination of lattice topologies and nano-structured materials induced by the SMAT process. On one hand, the SMAT method increases significantly the strength of metallic materials. On the other hand, lattice topologies possess variety in designing the mass and geometries of these structures. As combined, the SMAT-lattice structures are much stronger, and can be of various geometrical sizes and masses.
(22) The present invention concerns with the design and manufacturing of lattice architectures from the nano-structured materials produced by SMAT process. The methodology of generating solid nano-structured materials by SMAT process is outlined in the prior art, U.S. Pat. No. 7,691,211. This method has been proved to increase significantly the strength of metallic materials such as stainless steel sheets, see Chan et al., (2010) and Chen et al., (2011).
(23) Nano-structured materials have been effectively generated by the surface mechanical attrition treatment method, see Lu and Lu (1999 & 2004) and U.S. Pat. No. 7,691,211. In the SMAT process, a number of spherical projectiles are actuated by a vibration generator to impact the material surface at various angles, as schematically shown in
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(25) In this invention, holes of regular polygonal shapes (triangle, square or hexagon) are embedded inside the solid nano-structured materials in uniform and periodic patterns in order to reduce the overall mass and to create light-weight structures. There are four types of the lattice designs as exhibited in
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(30) For each type of the lattice, the remaining solid framework of bars is characterized by three geometrical parameters (t, l, r): l is the designed central-line length of each bar member in the lattice; t is the designed thickness of each bar member of the lattice; r is the designed radius of the blunting round-off at each nodal corner of the lattice. This round-off is designed to reduce the stress concentration at the nodal positions of the lattice.
(31) The mass of each lattice depends mainly upon t and l, and can be varied by changing the values of these two parameters. For example, the lattice can be considered as being thin (low mass) if the ratio l/t30, while it can be thick (high mass) if 4l/t10. The designed ratio of t/r is in the range of 1 to 2.
(32) According to an embodiment of the presently claimed invention, the manufacturing method of nano-structured lattices is shown as follows. Firstly, the initial solid material is treated by SMAT process to produce nano-structured material following the prior art, U.S. Pat. No. 7,691,211. Secondly, the type of the lattice is chosen, and the values of the three parameters (l, t, r) are designed in order to determine the dimensions of the holes, which will be removed from the solid SMAT material. The three designed values of (l, t, r) are also used to construct the drawing of the lattice for programming in the CNC water-cutting machine. Finally, the designed holes are wire-cut off from the solid nano-structured material by the CNC machine, and the nano-structured lattice is consequently achieved.
(33) In the present invention, nano-structured materials produced by surface mechanical attrition treatment method are particularly explored for two periodic lattice topologies: square and Kagome. Selected SMAT strategies are applied to bar members in the unit cell of each topology considered. The maximum axial stress in these bars is calculated as a function of the macroscopic in-plane principal stresses. A simple yield criterion is used to determine the elastic limit of the lattice with each SMAT strategy, and the relative merits of the competing strategies are discussed in terms of the reinforced yield strength and the SMAT efficiency. Experiments of selected SMAT strategies on both square and Kagome lattices made from stainless steel sheets are performed to assess the analytical predictions for the loading case of uni-axial tension.
(34) Experiments on the uni-axial tension of square and Kagome lattices treated with SMAT are shown as follows.
(35) Experimental tests have been performed to explore the strengthening effect of SMAT method upon the two lattices considered. The specimens of square and Kagome topologies arranged in selected directions were manufactured and treated with SMAT. These lattice samples were subjected to uni-axial tension test in turn, and the SMAT effect was assessed for each lattice topology.
(36) Square lattices: 0/90 versus 45, are tested and studied as follows.
(37) A series of SMAT strategies applied to each unit cell of the square lattice is introduced as follows. (i) Strategy N: no SMAT; this is for comparison purposes. (ii) Strategy AI: all bar members in the lattice are completely treated with SMAT, see
(38) Geometries of tensile dog-bone specimens are shown in
(39) Three identical 0/90 square lattice plates were manufactured for three cases considered: no SMATstrategy N, fully SMATstrategy AI, and partly SMATstrategy AII. The SMAT-treated surface areas of strategies AI and AII are shown in
(40) All samples were cut from AISI 304 stainless steel sheets of thickness d=1 mm. The manufacturing route is as follows. First, steel sheets were wire-cut into three identical dog-bone plates for the 0/90 square lattice, and into three identical rectangular plates for the 45 square lattice. For the no SMAT specimens, the central areas of the plates were wire-cut into the designed patterns, recall
(41) The manufactured samples were in turn subjected to the quasi-static tensile test (along the x.sub.1-axis shown in
(42) Consider first the results of the 0/90 square lattice. The lattice has a strut-stretching response to the uni-axial tension, and all samples exhibit an initial linear elastic behavior followed by a hardening response, see
(43) The analysis is applied here to calculate the stress-strain relation of the 0/90 square lattice under uni-axial tension. The horizontal bars a and a resist directly the applied stretching load along the x.sub.1-axis, while the vertical bars b and b carry negligible forces, see
(44) Now consider the 45 square lattice. Under the uni-axial load along the x.sub.1-axis (
(45) Deformation analyses using infinitesimal calculations are also included in
(46) In the final stretching-dominated regime of the 45 square lattice specimen, the material properties in the analytical model are taken as those of the 0/90 square lattice specimen. It is shown in
(47) Kagome lattices: horizontal and vertical directions, are tested and studied as follows.
(48) SMAT strategies are selected to apply to each unit cell of the Kagome lattice as follows. (i) Strategy : no SMAT, as for comparison purposes. (ii) Strategy BI: SMAT is applied to all bar members of the lattice, see
(49) Geometries of the horizontal and vertical Kagome lattice specimens are shown in
(50) Three identical horizontal Kagome specimens were manufactured for three cases considered: no SMATstrategy , fully SMATstrategy BI, and partly SMATstrategy BII. The SMAT areas are shown in
(51) The manufacturing and testing processes of the 0/90 square lattice specimens were repeated for all Kagome lattice samples. These Kagome plates were also cut from AISI 304 stainless steel sheets of thickness d=1 mm. The SMAT duration was 3 minutes for all samples, and the untreated surface areas of the partly SMAT specimens were protected by cloths during the treatment process. The servo-hydraulic test machine and the extensometer of gauge length 50 mm were used to measure the nominal stress and strain of the Kagome specimens. The measured results are shown in
(52) The Kagome lattice is a stretching-governed structure, so both horizontal and vertical Kagome plates exhibit an initial linear behavior, followed by a hardening response, see
(53) The analytical predictions using infinitesimal calculations are also included in
(54) Last, consider the analysis of the vertical Kagome lattice. As analyzed, the stretching of the diagonal bars (b, b, c and c) is the dominant response to the tension loads along the x.sub.1-axis shown in
(55) In the present invention, the strengthening effect of SMAT method is explored for two types of lattices: square and Kagome by analysis and experiment. It is found that the SMAT method is most efficient when it is applied to the locations of high stress concentrations. For bending-dominated structures (the 45 square lattice under uni-axial tension), the highest reinforcing efficiency is achieved by applying SMAT to the vicinity of bar ends where stresses are most concentrated. In this case, the yield strength of lattice specimens made from 304 stainless steel sheets is increased by a factor of k.sub.b=2 through the SMAT process used in the current study. For stretching-dominated structures (the 0/90 square lattice under axial deformation and the Kagome lattice under any macroscopic loading), the strengthening efficiency is maximised when the SMAT is applied over the entire bar members whose axial stresses exceed the elastic limit of the parent materials. In this case, the SMAT strengthening factor upon the yield stress is k.sub.s=3.5 for all steel lattice samples tested.
INDUSTRIAL APPLICABILITY
(56) The ability to create structural materials of high yield strength and yet high ductility has been a dream for materials scientists for a long time. The study of mechanical behavior of the surface nanostructured materials using SMAT shows significant enhancements in mechanical properties of the nanostructured surface layer in different materials.
(57) Deformation regimes of the 45 square lattice under uni-axial tension are discussed as follows.
(58) The 45 square lattice has two dominant regimes of deformation: (i) the initial strut-bending and (ii) the final strut-stretching. The stress-strain analysis using infinitesimal calculations is performed here for each mode of deformation.
(59) Regime I: Strut-Bending Deformation Mode
(60) The initial bar-bending response of the 45 square lattice to the uni-axial tension load is illustrated in
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where d is the depth of the lattice, and l is the length of each bar member. The nominal strain of the lattice *.sub.1 is associated with the tip deflection as
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(63) Recall from the experiments that d=1 mm is the thickness of the 304 stainless steel sheets, whilst t=1.6 mm and l=9 mm are the width and length of each bar member in the designed lattice specimens. Due to the stubbiness of the bar members, the bar length in our calculations is taken as l=lt=7.4 mm.
(64) The inelastic bending of a cantilever beam made from a bi-linear material is analysed by Fertis (1999) using the method of the equivalent systems. The lengthy process of this approximation method is omitted and the reader is referred to Feris (1999) for more details. Here, their methodology to determine the relation of the load P and the tip deflection for two cases is applied: the beam is untreated with SMAT, and the beam is fully treated with SMAT. Again, the bi-linear material approximations are applied for these two cases considered. For the no SMAT lattice, the material properties are those of the original steel sheets: E.sub.s=200 GPa, .sub.y=0.001 and E.sub.t=2 GPa. For the fully SMAT lattice, the initial Young's modulus and yield strain are unchanged as E.sub.s=200 GPa and .sub.y=0.001. The two SMAT parameters are obtained by curve-fitting with the measured data as k=k.sub.b=2 and E.sub.t.sup.SMAT=2 GPa. The nominal stress and strain (*.sub.1,*.sub.1) of the lattice derived are shown in
(65) Regime II: Strut-Stretching Deformation Mode
(66) Suppose that all nodes in the 45 square lattice are pin-jointed. Under the infinitesimal tension force, the bar members are pulled from the initial diamond shape into a straight configuration due to the collapse mechanism of the lattice, see
h.sub.L=h.sub.0+h.sub.L=h.sub.0(1+*.sub.L)(A.3)
where h.sub.0=l/{square root over (2)} and the locking strain is
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The nominal strain of the lattice is determined as
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where =h/h.sub.L is the engineering strain of the bar member. The nominal stress of the lattice *.sub.1 is related to the stretching stress of the bar member as
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(70) The initial height of the 45 square lattice specimens is h.sub.0=l/{square root over (2)}=6.4 mm. The bar members are relatively stubby, so the locking length is taken as h.sub.L=lt/2=8.2 mm leading to the locking strain *.sub.L=h.sub.L/h.sub.0l=0.29. The material properties of the specimens are taken as those given: E.sub.s=200 GPa, .sub.y=0.001 and E.sub.t=2 GPa for the no SMAT sample; and E.sub.s=200 GPa, .sub.y=0.001, k.sub.s=3.5 and E.sub.t.sup.SMAT=1.7 GPa for the fully SMAT sample. The stress-strain relations of the lattice derived are shown in
(71) The foregoing description of the present invention has been provided for the purposes of illustration and description. It is not intended to be exhaustive or to limit the invention to the precise forms disclosed. Many modifications and variations will be apparent to the practitioner skilled in the art.
(72) The embodiments were chosen and described in order to best explain the principles of the invention and its practical application, thereby enabling others skilled in the art to understand the invention for various embodiments and with various modifications that are suited to the particular use contemplated. It is intended that the scope of the invention be defined by the following claims and their equivalence.
(73) Disclosure of the following references are hereby incorporated by reference in their entirety:
REFERENCE
(74) Chan, H. L., Ruan, H. H., Chen, A. Y., Lu, J., 2010. Optimization of strain-rate to achieve exceptional mechanical properties of 304 stainless steel using high speed ultrasonic SMAT. Acta Mater. 15, 5086-5096. Chen, A. Y., Ruan, H. H., Wang, J., Chan, H. L., Wang, Q., Li, Q., Lu, J., 2011. The influence of strain rate on the microstructure transition of 304 stainless steel. Acta Mater. 59, 3697-3709. Fleck, N. A., Deshpande, V. S., Ashby, M. F., 2010. Micro-architectured materials: past, present and future. Proc. R. Soc. Lond. A. 466, 2495-2516. Gibson, L. J., Ashby, M. F., 1997. Cellular Solids: Structure and Properties, second edition. Cambridge University Press. Lu, K., Lu, J., 1999. Surface nanocrystallization (SNC) of metallic materialspresentation of the concept behind a new approach. J. Mater. Sci. Technol. 15, 193-197. Lu, K., Lu, J., 2004. Nanostructured surface layer on metallic materials induced by surface mechanical attrition treatment. Mater. Sci. Eng. A. 375, 38-45. Lu J., Lu K., 2010. Method for generating nanostructures and device for generating nanostructures. U.S. Pat. No. 7,691,211.