SHORT PATH DISTILLATION HEAD

Abstract

A distillation head for distilling a distillate from a vaporous distilland. The distillation head including a headspace chamber within a condenser surface. An inlet port having an extended portion below and to but not into the headspace, to receive the vaporous distilland and pass it into the headspace. A collection surface below the headspace to collect the distillate. And an outlet port, to receive the distillate from the collection surface and pass it out of the distillation head.

Claims

1: A distillation head (10, 30, 50) for distilling a distillate from a vaporous distilland, comprising: a headspace chamber (16, 36, 56) at least partially encompassed by an actively cooled condenser surface (18, 38, 58); an inlet port (12, 32, 52) having an extended portion (26, 36, 56) below and to but not into a volume encompassed by said actively cooled condenser surface (18, 38, 58), to receive the vaporous distilland and pass it into said headspace chamber (16, 36, 56); a collection surface (22, 42, 62) below said headspace chamber (16, 36, 56) to collect the distillate, wherein said collection surface has a sloped lower surface; a separable upper surface (28, 68, 70) above said headspace chamber (16, 36, 56); and an outlet port (24, 44, 64), to receive the distillate from said collection surface (22, 42, 62) and pass it out of the distillation head (10, 30, 50).

2: The distillation head (10, 30, 50) of claim 1, wherein said headspace chamber (16, 36, 56) and said condenser surface (18, 38, 58) have a vertical common first axis (14), said extended portion (26, 36, 56) of said inlet port (12, 32, 52) has a vertical second axis (14), and said first axis (14) and said second axis (14) are coaxial.

3. (canceled)

4. (canceled)

5. (canceled)

6: The distillation head (10, 30, 50) of claim 1, wherein the condenser surface (18, 38, 58) is of a corrosion resistant metal alloy.

7: The distillation head (10, 30, 50) of claim 1, further comprising a cooler (20, 40, 60) attached to said condenser surface (18, 38, 58).

8. (canceled)

9: The distillation head (10, 30, 50) of claim 7, wherein said cooler (20, 40, 60) receives a flowing medium to cool said condenser surface (18, 38, 58) and thereby also to cool portions of the distilland that contact said condenser surface (18, 38, 58).

10: The distillation head (10, 30, 50) of claim 9, wherein said medium is a member of the set consisting of a liquid and a gas.

11: The distillation head (10, 30, 50) of claim 7, wherein said cooler (60) includes at least one fin (60) attached to said condenser surface (18, 38, 58).

12: The distillation head (10, 30, 50) of claim 1, further comprising a sight portal (28, 68) above said headspace chamber (16, 36, 56).

13. (canceled)

14: A process for distilling a distillate from a vaporous distilland, the process comprising the steps of: (a) directing the vaporous distilland into a distillation head via an inlet port; (b) receiving the vaporous distilland via an extended portion of said inlet port into a headspace chamber of said distillation head, wherein: (1) said headspace chamber is at least partially encompassed by a condensing surface that is actively cooled and has a separable upper surface; and (2) said extended portion of said inlet port extends below and to but not into a volume encompassed by said condenser surface that is actively cooled; (c) condensing portions of the vaporous distilland onto said condensing surface such that it falls as distillate onward to a collecting surface, wherein said collection surface has a sloped lower surface; (d) collecting the distillate that falls onto said collecting surface; (e) receiving the distillate collected in (c) into an outlet port; and (f) directing the distillate received in (d) out of said distillation head.

15: The process of claim 14, wherein said condensing surface is actively cooled by a flowing medium that is a member of the set consisting of a liquid and a gas.

16: The distillation head (10, 30, 50) of claim 1, wherein said separable upper surface (28, 68, 70) encompasses the entire upper-most surface area of said headspace chamber (16, 36, 56) with no inward restriction from said condensation surface (18, 38, 58).

17: The process of claim 14, wherein said separable upper surface encompasses the entire upper-most surface area of said headspace chamber with no inward restriction from said condensation surface.

Description

BRIEF DESCRIPTION OF THE SEVERAL VIEWS OF THE DRAWING(S)

[0021] The purposes and advantages of the present invention will be apparent from the following detailed description in conjunction with the appended figures of drawings in which: FIGS. 1a (Prior Art) and 1b (Prior Art) are schematic diagrams of an essentially same shot-path distillation approach, wherein FIG. 1a (Prior Art) is taken from “SHORT-PATH DISTILLATION—WIKIPEDIA”; FIG. 1B (Prior Art) is FIG. 1 (Prior Art) from U.S. Pat. No. 10,493,374 by Wells, et al.; and FIG. 1c (Prior Art) is FIG. 2 also from U.S. Pat. No. 10,493,374 by Wells, et al.

[0022] FIG. 2a is a schematic side cut away view of a first embodiment of a short path distillation head in accord with the present invention, and FIG. 2b is a schematic perspective cut away view of the same distillation head;

[0023] FIG. 3 is a schematic side cut away view of a second distillation head embodiment in accord with the present invention;

[0024] FIG. 4 is a schematic side cut away view of a third distillation head embodiment in accord with the present invention; and

[0025] FIG. 5 is a flow chart depicting a process in accord with the present invention.

[0026] In the various figures of the drawings which are prior art (i.e., FIGS. 1a-c), references are included from the originals.

DETAILED DESCRIPTION OF THE INVENTION

[0027] A preferred embodiment of the present invention is a short path distillation head. As illustrated in the various drawings herein, and particularly in the view(s) of FIGS. 2a-b, an embodiment of the invention is depicted by the general reference character (10).

[0028] FIG. 2a is a schematic side cut away view of a first embodiment of a short path distillation head 10 in accord with the present invention. A vaporous distilland in a distillation process enters the distillation head 10 via an inlet port 12 (e.g., a “vapor tube”) from a lower boiling flask (not shown; the boiling flask may be conventional in the existing distillation arts). As depicted here, the distillation head 10 and many elements of it can be largely symmetrical about a common axis 14.

[0029] The entering vaporous distilland expands into a headspace 16 (i.e., the interior of or a chamber in the distillation head 10) it comes into contact with a condenser surface 18 where at least one component of the vapor is commenced to a distillate in liquid state. The condenser surface 18 is held at a desired temperature by a cooler 20 (e.g., a liquid jacket to receive a cooling medium as depicted in FIG. 2a-b) The distillate then flows down the condenser surface 18 and onto a collection surface 22 which is angled toward an outlet port 24. Concurrently, an extended portion 26 above the inlet port 12 prevents any of the distillate from flowing back into the boiling flask. The outlet port 24 may be angled (as shown) to help the liquid distillate flow and may also be of a large enough diameter to allow uncondensed gasses to escape. An optional sight portal 28 (e.g., a “sight glass”) can be provided to allow the process to be observed. FIG. 2b is a schematic perspective cut away view of the same distillation head 10 in FIG. 2a.

[0030] FIG. 3 is a schematic side cut away view of a second embodiment in accord with the present invention, here of a distillation head 30. A vaporous distilland in a distillation process here enters the distillation head 30 via an inlet port 32 by flowing up from a lower boiling flask (not shown). As the vapor expands into a headspace 36 it comes into contact with a condenser surface 38 where some of the components of the vapor are commenced to a distillate in liquid state. The condenser surface 38 here is held at a desired temperature by flowing a coolant through a cooler 40. The distillate then flows down the condenser surface 38 and onto a collection surface 42 which here is angled toward an outlet port 44. Concurrently, an extended portion 46 above the inlet port 32 prevents the distillate from flowing back into the boiling flask. The outlet port 44 is here also angled to help liquid flow and is of a large enough diameter to allow uncondensed gasses to escape. In contrast with the embodiment depicted in FIGS. 2a-b, an optional sight portal is not provided in the embodiment depicted in FIG. 3.

[0031] Returning to the condenser surface 38, it is intentionally here depicted having a tubular lower portion 38a and a hemispherical upper portion 38b.

[0032] FIG. 4 is a schematic side cut away view of a third embodiment in accord with the present invention, here of a distillation head 50. A vaporous distilland in a distillation process here enters the distillation head 50 via an inlet port 52 by flowing up from a lower boiling flask (not shown). As the vapor expands into a headspace 56 it comes into contact with a condenser surface 58 where some of the components of the vapor are commenced to a distillate in liquid state. The condenser surface 58 here has an attached cooler 60 (here including a fin or fins) to hold the condenser surface 58 at a temperature in a desired range. The distillate then flows down the condenser surface 58 and onto a collection surface 62 which here is angled toward an outlet port 64. Concurrently, an extended portion 66 above the inlet port 52 prevents the distillate from flowing back into the boiling flask. The outlet port 64 is here also angled to help liquid flow and is of a large enough diameter to allow uncondensed gasses to escape. Similar to the embodiment depicted in FIGS. 2a-b, and in contrast with the embodiment depicted in FIG. 3, an optional sight portal 68 is provided in the embodiment depicted in FIG. 4. Additionally, a removable element 70 can be provided above the headspace 56, to provide access to it, and this removable element 70 may be or include the optional sight portal 68 as is the case depicted in FIG. 4.

[0033] FIG. 5 is a flow chart depicting a process 80 in accord with the present invention. In a step 82 the process 80 starts. In an optional step 84 a condensing surface of a distillation apparatus is cooled. In a step 86 a vaporous distilland is directed into the distillation apparatus. In a step 88 a distillate is condensed out of the vaporous distilland. In a step 90 that distillate is collected. In a step 92 this distillate is received into an outlet from the distillation apparatus. In a step 94 the final distillate is directed out of the distillation apparatus. And in a step 96 the process 80 stops.

[0034] We return now briefly to some of the prior art. U.S. Pat. No. 10,493,374 by Wells, et al. was previously introduced. It can now be appreciated that distilland inlet conduit (102) extends into its condensate chamber (111), thus considerably lengthening its distillation path. In contrast, in the present invention the extended portion 28, 46, 66 of the inlet port 12, 32, 52 ends at or below the headspace 16, 36, 56 within the condenser surface 18, 38, 58, thus permitting the present invention to comport with the primary defining goal of “short path” distillation.

[0035] U.S. Pat. No. 10,279,281 by Kremerman was also previously noted. It has a “fraction collector” that directs fluid to a side port where its condenser is located. In contrast the inventive distillation head 10, 30, 50 disclosed herein has its condenser surface 18, 38, 58 generally coaxial with respect to and located above its outlet port 24, 44, 64.

[0036] While multiple embodiments have been described above, it should be understood that these have been presented by way of examples only, and that the breadth and scope of the present invention should not be limited by the above described exemplary embodiments but should instead be defined only in accordance with the following claims and their equivalents.