System method and capsules for producing sparkling drinks
10143977 ยท 2018-12-04
Assignee
Inventors
Cpc classification
A23V2002/00
HUMAN NECESSITIES
A47J31/44
HUMAN NECESSITIES
B65D85/804
PERFORMING OPERATIONS; TRANSPORTING
A47J31/407
HUMAN NECESSITIES
B01F2101/14
PERFORMING OPERATIONS; TRANSPORTING
A23V2002/00
HUMAN NECESSITIES
B01F23/236
PERFORMING OPERATIONS; TRANSPORTING
International classification
A47J31/40
HUMAN NECESSITIES
B65D85/804
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A system and a method for the production and provision of CO.sub.2 gas are disclosed. A sealable chamber is equipped with heating means and when a CO.sub.2 carrier material, such as sodium bicarbonate is placed in it and heated to its decomposition temperature CO.sub.2 gas is released. The released gas is conveyed into liquid within a container and when the pressure of the gas in the container raises more and more CO.sub.2 gas is dissolved. The heating may be done by conduction mechanism, a microwave heating mechanism or by induction mechanism. The sodium bicarbonate or any other material including carbon dioxide may be disposed in powder, solid, suspension, emulsion, solution or wet powder form. It may be disposed in thin envelope case.
Claims
1. Capsule for providing carbon dioxide gas for the production of sparkling drinks, the capsule comprising: a single reactive substance configured to release carbon dioxide upon heating, the single reactive substance is sodium bicarbonate in one of solid, dry powder, wet powder, solution, emulsion and suspension form.
2. The capsule of claim 1, further comprising: at least one non-reactive additive from a list consisting of: taste additive, flavor additive, color additive; or chips of ferrous material.
3. The capsule of claim 1, encapsulated in a thin envelope of non-ferrous material, said envelope having one or more punctures made in its wall to allow releasing of gas produced in the envelope.
4. The capsule of claim 1, having one face formed with protrusions and recesses to fit onto an inner face of a base element of a pressure chamber made with suitable recesses and protrusions.
5. The capsule of claim 3, wherein said thin envelope comprises more than one compartment and wherein at least one of said compartments comprise a carbon dioxide carrier material in a dry form and at least another of said compartments comprise a fluid to wet the dry form carbon dioxide carrier prior to heating.
6. The capsule of claim 5, wherein the fluid is one or more of a group consisting of: water, edible oil and aromatic oil.
7. The capsule of claim 4, wherein at least one of the recesses in the capsule is configured to loosely fit to at least one heat fin protruding into the pressure chamber.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) The subject matter regarded as the invention is particularly pointed out and distinctly claimed in the concluding portion of the specification. The invention, however, both as to organization and method of operation, together with objects, features, and advantages thereof, may best be understood by reference to the following detailed description when read with the accompanying drawings in which:
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(11) It will be appreciated that for simplicity and clarity of illustration, elements shown in the figures have not necessarily been drawn to scale. For example, the dimensions of some of the elements may be exaggerated relative to other elements for clarity. Further, where considered appropriate, reference numerals may be repeated among the figures to indicate corresponding or analogous elements.
DETAILED DESCRIPTION OF THE INVENTION
(12) In the following detailed description, numerous specific details are set forth in order to provide a thorough understanding of the invention. However, it will be understood by those skilled in the art that the present invention may be practiced without these specific details. In other instances, well-known methods, procedures, and components have not been described in detail so as not to obscure the present invention.
(13) Although embodiments of the present invention are not limited in this regard, the terms plurality and a plurality as used herein may include, for example, multiple or two or more. The terms plurality or a plurality may be used throughout the specification to describe two or more components, devices, elements, units, parameters, or the like. Unless explicitly stated, the method embodiments described herein are not constrained to a particular order or sequence. Additionally, some of the described method embodiments or elements thereof can occur or be performed at the same point in time.
(14) Heating of compositions to a temperature that is higher than the thermal decomposition temperature of that composition, in order to decomposite it is well known. Similarly heating compositions to a temperature that is higher than the phase transition temperature, in order to cause the composition to undergo phase transition is well known. For example, heating a composition that includes CO.sub.2 to a temperature that is higher than the thermal decomposition temperature may decomposite it and thus may cause the decomposed material to release CO.sub.2. |In many cases such a process that is known as calcination, or calcination reaction. For example, when limestone is calcinated the chemical reaction is expressed:
CaCO.sub.3.fwdarw.CaO+CO.sub.2(g)
That is, the calcination process decomposed the lime stone to lime (calcium oxide) and carbon dioxide. Well known examples of calcination processes, mostly held in large (industrial) scales are meant to remove certain undesired components from the composition. One example is decomposition of hydrated minerals, as in the calcination of bauxite and gypsum, to remove crystalline water. Another example is the decomposition of volatile matter contained in raw petroleum coke and yet another example is the removal of ammonium ions in the synthesis of zeolites.
(15) Many devices and methods for carbonating liquids are known. Some require complicated and bulky apparatuses and multi stage methods, even for the production of carbonated beverage for personal use. Several known devices and methods disclose the use of pairs of reagents that when chemically activated release carbon dioxide that may be used for the carbonation of the liquid, to create gaseous beverage. Other devices and methods make use of pre-pressurized CO.sub.2 that is contained in high pressure containers from which the pressurized CO.sub.2 may be released into a container holding the beverage in order to carbonate it. Use of pairs of reagents for the production of CO.sub.2 requires means for keeping the reagents apart from each other until the chemical reaction takes place and in many devices known in the art complicated and bulky carbonating apparatuses are required in order to control the process of the carbonation. Use of pressurized CO.sub.2 containers is typically less complicated then the use of carbonating devices based on chemical reaction of pairs of reagents, however handling the containers of the pressurized CO.sub.2 is typically inconvenient andwith non-disposable containers there is the burden of carrying the filled containers from the store and the empty ones back there.
(16) The inventor of the invention embodiments of which are described herein below has discovered that the amount of CO.sub.2 that may be released from a relatively small amount of sodium bicarbonate during calcination process is relatively very large. For example, from a tablet of sodium bicarbonate weighing 35 grams, when calcinated at temperatures of about 60-200 degrees centigrade CO.sub.2 is released in an amount that is enough to carbonate water or similar liquid in the amount of 1.5 liter having carbonation level of about 2 to 4 volumes, and temperature of 2 to 15 degrees. This ratio of CO.sub.2 production is very high compared to other known methods. This allows producing, at the desire of a user, amount of CO.sub.2 that is enough for a 1 liter container from a sodium bicarbonate tablet weighing about 25 g.
(17) Heating of materials such as sodium bicarbonate (NaHCO3) or other substances that include Carbon dioxide (CO.sub.2), herein after referred to as CO.sub.2 carrier, may release CO.sub.2 gas. For example, when heating sodium bicarbonate in solid form in a closed vessel to temperature higher than the decomposition temperature the following applies:
2NaHCO.sub.3(s)Na2CO.sub.3(s)+H.sub.2O(g)+CO.sub.2(g)
The same applies, with the required changes, to sodium bicarbonate in other states and forms, such as in dry or wet powder or in solution or emulsion state.
(18) According to embodiments of the present invention, sparkling drinks, also referred to as carbonated drinks, may be produced by heating CO.sub.2 carrier and by dissolving the released CO.sub.2 gas in water or other liquid such as juice or wine.
(19) At temperatures above 70? C. (degrees Celsius) sodium bicarbonate gradually decomposes into sodium carbonate, water and carbon dioxide. The conversion is fast at 200? C. For example, heating 8 grams of sodium bicarbonate at 180 degrees Celsius may produce 1.5 liters of CO.sub.2 gas. To reach high carbonation level of commercial sparkling drinks, 3 to 4 liters of gas are needed for each 2 liters of liquid. Therefore, heating of about 16-35 grams of sodium bicarbonate may produce enough gas for 2 liters of sparkling drink.
(20) According to experiments conducted by the inventor of the present invention, the use of wet powder, suspension or solution of CO.sub.2 carrier, such as sodium bicarbonate, may allow the production of similar amounts of CO.sub.2 gas, at the same production rate, while heating the solution, suspension or wet powder to a lower temperature compared to production from dry powder. For example, heating 25 grams of dry sodium bicarbonate powder to a temperature of 180? C. will yield 2 liters of CO.sub.2 gas in approximately 100-130 seconds. Using the same amount of sodium bicarbonate in a solution form will produce the same volume of CO.sub.2 gas, in similar rate, when heated to a temperature lower than 180? C. It would be appreciated that heating the solution to higher temperatures will provide a higher gas production rate. It should be noted, however, that heating sodium bicarbonate to a temperature of over 200? C. (degrees Celsius) may cause the sodium bicarbonate particles to be sealed and the CO.sub.2 may then be trapped within the particles of the powder.
(21) According to embodiments of the present invention, when using a CO.sub.2 carrier in a solution, a suspension, an emulsion or a wet powder state, the solvent used for the solution or suspension or the fluid used to wet the powder may be water, edible oil or aromatic oils. Alternatively or additionally, the fluid used as a solvent or to wet the powder may be a flavored fluid.
(22) Reference is made now to
(23) Reference is made to
(24) As is well known in the art, the boiling point of a substance is the temperature at which the vapor pressure of the liquid equals the pressure surrounding the liquid and the liquid changes into a vapor. Thus, raising the pressure surrounding the liquid will result in raising the temperature in which the fluid reaches the boiling point. That is, a liquid at high surrounding pressure has a higher boiling point than when that liquid is at atmospheric pressure.
(25) According to some embodiments of the present invention, CO.sub.2 carrier material may be placed within CO.sub.2 carrier material unit 205 inside pressure chamber 204 and may be wet prior to heating. When heating CO.sub.2 carrier material in wet form, the fluid serves as a thermal conductor as long as the fluid that wets the CO.sub.2 carrier material remains in a liquid state. Since pressure chamber 204 is pressure sealed, heating of CO.sub.2 carrier material in pressure chamber 204 raises the pressure in the chamber 204, and thus raises the temperature in which the fluid in chamber 204 vapors. Thus, the fluid preserves its thermal conducting characteristics at higher temperatures than under atmospheric pressure and thus remains effective as a thermal conductor during the heating process of the CO.sub.2 carrier material to temperatures of over 100? C.
(26) According to some embodiments of the present invention, heating device 207 may be an induction heating device. According to other embodiments heating device 207 may be a microwave heater.
(27) System 200 may include a temperature regulator 206 that may include a temperature sensor to measure the temperature inside chamber 204 and provide feedback to heating device 207 so as to regulate the temperature to be, for example, between 150 to 400 degrees Celsius. It would be appreciated that when CO.sub.2 carrier material in unit 205 is in a wet form lower temperatures may be required. Furthermore, as noted above, when carrier material is sodium bicarbonate, heating to a temperature of over 200 degrees Celsius is not beneficial.
(28) CO.sub.2 carrier material unit 205 may be provided in any suitable form such as powder (either dry or wet), tablet, capsule etc. CO.sub.2 carrier material unit 205 may be mixed or otherwise provided with various other flavoring materials that may be released as gas and mix with the drink. For example, a tablet may include a layer of sodium bicarbonate and a plurality of layers of additives.
(29) Reference is now made to
(30) Reference is made now to
(31) According to one embodiment of the present invention, gas production unit 20 may further have an inlet (not shown) for introducing fluid from a source (such as liquid container 100), external to gas production unit 20, into pressure tight chamber 21, to wet a CO2 carrier material placed within chamber 21 in solid or dry powder form. It would be appreciated by those skilled in the art that the inlet into chamber 21 may further comprise a unidirectional valve (not shown) to prevent gas produced in chamber 21 to exit through the unidirectional valve.
(32) According to some embodiments, fluid introduced into chamber 21 may be water. According to other embodiments the fluid introduced into chamber 21 may be water with additives, such as flavor and/or color additives. In yet additional embodiments of the present invention, fluid introduced into chamber 21 may be edible oil and/or aromatic oil. According to other embodiments, the fluid may be an emulsion of water and oil such as aromatic oil. It would be appreciated that other fluids may be used.
(33) System 400 may further comprise circulation means 40, such as a pump, that is adapted to pump liquid from container 100 via conduit 40A, the distal end of which is adapted to be submerged in the liquid in container 100 and to return that liquid via conduit 40B into container 100. According to one embodiment conduits 40A and 40B may pass via disposing plug 24, however other embodiments may be utilized. According to another or additional embodiment, conduits 40A and 40B may pass through a heat exchanger (not shown) to cool down the fluid in conduits 40A and 40B to a desired temperature. The end of conduit 40B that is distal from circulation means 40 may be in a distance from plug 24 that will ensure that it will remain out of the liquid in container 100 when container 100 is substantially in upright position. The liquid that is returned via conduit 40B may be sprayed into the headspace of container 100, for example by forming the distal end of conduit 40B to provide liquid in the form of a spray. Circulation caused by the operation of circulation means 40 may improve (i.e. expend the amount of CO.sub.2 gas dissolved in the container) and speed up the dissolving of CO.sub.2 in the liquid. The inventor of the invention described in this application has discovered that when system 400 is in pressure equilibrium with the pressure inside container 100, after certain amount of gas was dissolved, the activation of circulation means 40 so that carbonated liquid is pumped from container 100 and sprayed back to its headspace enhances the rate of dissolving the gas in the liquid so that the pressure inside container 100 drops, due to the additional gas that was dissolved in the liquid and therefore the pressure produced by CO.sub.2 production unit 20 is now higher than that inside container 100, and therefore additional amount of gas is provided to container 100. Thus, circulation means 40 may be activated continuously or periodically during the production of gas by gas production unit 20 to enable dissolving of larger amounts of gas in the liquid. An acidity indicator that was placed in container 100 indicated repeating raise of acidity of the liquid in container 100 as the activation of circulation means continued, which indicates that the amount of CO.sub.2 gas in container 100 grew with the activation of circulation means 40. It would be appreciated that any other system and method known in the art for dissolving CO.sub.2 gas in the liquid in container 100 may be used.
(34) Reference is made now to
(35) Heat may be transferred to tablets, according to embodiments of the present invention, in one or more from a list of various heating methods. Reference is made now to
(36) Heat may be produced, according to embodiments of the present invention, inside the tablet in the gas production unit, using induction heating mechanism. Reference is made now to
(37) Tablets made for use with induction heating may comprise certain amount of ferrous chips calculated to provide enough heating within defined period of time. According to another embodiment the heat generating material may be carbon chips. The size, spherical density and the level of unity of dispersion of the chips in the tablet may be selected to achieve the required level of heating and the time required for that heating. According to some embodiments tablets for the production of CO.sub.2 gas may further comprise taste additives, flavor additives, color additives, and the like.
(38) In experiments carried out by the inventor of the present invention he discovered that when heating the tablet using induction mechanism the rate of decomposition of the tablet and the rate of gas production may be kept same as in conduction heating with lower temperatures of the heating chamber.
(39) Heating chamber units 720A and 720B may be made of non-ferrous metals which will minimize its heating when electromagnetic energy is activated.
(40) Reference is now made to
(41) According to some embodiments of the method according to the present invention, introducing fluid into the pressure chamber may precede the heating of the CO2 carrier within the pressure chamber.
(42) While embodiments of the present invention were described with relation to preparation of sparkling drinks, embodiments of the present invention are not limited to this application. Carbonated liquids may be produced according to embodiments of the present invention for any other suitable application in which carbonated liquids are required.