FILLING SYSTEM FOR A TEXTURED BEVERAGE
20180338509 ยท 2018-11-29
Assignee
Inventors
Cpc classification
A23C9/156
HUMAN NECESSITIES
B67C2007/0066
PERFORMING OPERATIONS; TRANSPORTING
A23C9/1544
HUMAN NECESSITIES
B65D85/73
PERFORMING OPERATIONS; TRANSPORTING
A23G1/56
HUMAN NECESSITIES
A23V2002/00
HUMAN NECESSITIES
B67C3/02
PERFORMING OPERATIONS; TRANSPORTING
A23C9/154
HUMAN NECESSITIES
A23C2240/20
HUMAN NECESSITIES
B67C2007/006
PERFORMING OPERATIONS; TRANSPORTING
A23F5/243
HUMAN NECESSITIES
A23C2270/10
HUMAN NECESSITIES
International classification
A23F5/24
HUMAN NECESSITIES
B67C3/02
PERFORMING OPERATIONS; TRANSPORTING
B67C7/00
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A process for packaging pressurized beverages. The process includes mixing liquid, a solute that depresses the freezing point of the liquid, and gas. Next, the liquid-gas mixture is allowed to rest. Then, retail containers are filled with the mixture. During the mixing and filling steps of the process, the liquid-gas mixture is subjected to pressures that are higher than atmospheric pressure. Unfortunately, such pressure cannot be maintained when the container is transferred from the filling station to the sealing station causing dissolved gas to leave the liquid and foam to overflow the container during the transfer. To prevent such an overflow, prior to the transfer, the dissolved gas is put to sleep by reducing the temperature of the liquid to below 0 C. (32 F.) and optionally allowing the liquid-gas mixture to rest. The liquid beverage may include milk, coffee, tea, fruit juice, chocolate or mixtures thereof, and may include a gum.
Claims
1. A process for the packaging of a pressurized liquid, containing a gas and a solute that depresses the freezing point of the liquid, the process comprising: mixing the liquid and the solute to create a liquid mixture; introducing the gas to the liquid mixture, under greater than 101325 Pa (1 atmosphere) of pressure; agitating the liquid mixture, to create a liquid-gas mixture; cooling the liquid-gas mixture to less than 0 C. (32 F.) to create a cooled liquid-gas mixture; transferring the cooled liquid-gas mixture to a container; subjecting the cooled liquid-gas mixture in the container to atmospheric pressure; and sealing the cooled liquid-gas mixture in the container wherein the pressure inside the container after sealing is greater than 101325 Pa (1 atmosphere).
2. The process of claim 1, wherein the liquid mixture is cooled to less than 0 C. (32 F.) prior to the introduction of the gas.
3. The process of claim 1, wherein the liquid is agitated at substantially the same time the gas is introduced to the liquid mixture.
4. The process of claim 4, wherein the liquid, solute, and gas are all mixed together at substantially the same time
5. The process of claim 1, wherein the liquid includes milk, coffee, fruit juice, chocolate or mixtures thereof.
6. The process of claim 1, wherein the liquid includes a gum selected from the group consisting of acacia gum, guar gum, locust bean gum, carrageenan, pectin, xanthan gum, or mixtures thereof.
7. The process of claim 1, wherein the solute includes salt, sugar, electrolytes, alcohol, or mixtures thereof.
8. The process of claim 1, wherein the gas includes nitrous oxide.
9. The process of claim 1, wherein the container is a can, bottle, or keg.
10. A process for the packaging of a pressurized liquid, containing a gas and solute that depresses the freezing point of the liquid, the process comprising: mixing the liquid and the solute to create a liquid mixture; filling a container with the liquid mixture; sealing the container with a first cap that contains a one-way valve; introducing the gas through the one-way valve to the liquid mixture, under greater than 101325 Pa (1 atmosphere) of pressure; agitating the liquid mixture, to create a liquid-gas mixture; cooling the liquid gas mixture to less than 0 C. (32 F.) to create a cooled liquid-gas mixture; removing the first cap, thereby subjecting the cooled liquid-gas mixture in the container to atmospheric pressure; and sealing the cooled liquid-gas mixture in the container with a second cap which does not contain a one-way valve, wherein the pressure inside the container after sealing is greater than 101325 Pa (1 atmosphere).
11. The process of claim 10, wherein the liquid mixture is cooled to less than 0 C. (32 F.) prior to the introduction of the gas.
12. The process of claim 10, wherein the liquid is agitated at substantially the same time the gas is introduced to the liquid mixture.
13. The process of claim 10, wherein the liquid includes milk, coffee, fruit juice, chocolate, tea, or mixtures thereof.
14. The process of claim 10, wherein the liquid includes a gum selected from the group consisting of acacia gum, guar gum, locust bean gum, carrageenan, pectin, xanthan gum, or mixtures thereof.
15. The process of claim 10, wherein the solute includes salt, sugar, electrolytes, alcohol, or mixtures thereof.
16. The process of claim 10, wherein the gas includes nitrous oxide.
17. The process of claim 10, wherein the second container is a can, bottle, or keg.
18. A system for packaging a pressurized liquid comprising: an ingredient mixing tank into which a drinkable liquid and a solute that reduces the freezing point of the liquid are introduced to create a liquid mixture; a gas saturation tank in fluid communication with the ingredient mixing tank permitting the liquid mixture to flow from the ingredient mixing tank to the gas saturation tanks, the gas saturation tank receiving a gas introduced to the liquid mixture at pressures greater than 101325 Pa (1 atmosphere) and in which the liquid mixture is agitated to create a gas-liquid mixture; a heat exchanger in contact with the gas saturation tank such that the temperature of the gas-liquid mixture is reduced to less than 0 C. (32 F.) to create a cooled gas-liquid mixture; a pressurized filler in fluid communication with the gas saturation tank which permits the cooled gas-liquid mixture to flow from the gas saturation tank to the pressurized filler; a container receiving the cooled gas-liquid mixture from the pressurized filler at a pressure greater than 101325 Pa (1 atmosphere) to create a filled container; a conveyor transmitting the filled container from the pressurized filler during which time the filled container is subject to atmospheric pressure; and a sealer which seals the container.
19. The system of claim 18, further comprising a heat exchanger that contacts the liquid mixture as the liquid mixture flows between the mixing tank and the gas saturation tank.
Description
BRIEF DESCRIPTION OF DRAWING
[0015] The invention is best understood from the following detailed description when read in conjunction with the accompanying drawings. It is emphasized that, according to common practice, the various features of the drawing are not to scale. On the contrary, the various features are arbitrarily expanded or reduced for clarity. Included in the drawing are the following figures:
[0016]
[0017]
[0018]
DETAILED DESCRIPTION
[0019] Embodiments of the invention include beverages packaged in a sealed, pressurized container that contains no fixed valves or apertures. When the container is opened, the contents, comprising liquid and gas, expand in volume as the internal pressure of the container is released, thereby permitted the gas saturated in the liquid to expand. This causes the liquid to separate into a liquid phase and a stable textured drinkable foam phase above the liquid phase. The beverage may include milk or a milk substitute, and may also include coffee or tea. Embodiments further include processes and systems for achieving the result described above. Specifically, the embodiments employ temperatures from about 0 C. to below the liquid-gas mixture's freezing point. Pursuant to gas laws, such as Henry's Law and the Stokes' Equation, such a decrease in temperature slows the creation, buildup, and eventual overflow of foam caused by the rapid release of saturated or super saturated gas in the beverage. By delaying foam creation and buildup, even if the delay achieved is less than eight (8) seconds, the container may be sealed before significant gas loss and/or overflow, thereby avoiding the waste associated with, and damage caused by, foam overflowing the container and the loss of an amount of dissolved gas, which negatively affects foam formation when the liquid beverage is eventually consumed. Although a longer delay of foam overflow is desired, delays of as short as four (4) seconds have provided the necessary window to seal the retail container before significant overflow or gas loss occurs.
[0020] Referring now to the drawings, in which like reference numbers refer to like elements throughout the various views that comprise the drawings,
[0021] Mixing Tank
[0022] At the first step 110 of the process 100, a beverage container is filled with a beverage and a solute that depresses the freezing point of the liquid. The beverage container may be one of any number of vessels suitable for mixing or storage. It can also be sealed or unsealed, and pressurized or open.
[0023] In some embodiments, the liquid beverage may include at least a base liquid and optionally a gum. In other embodiments, the gum may not be included. In an exemplary embodiment, the gum is acacia gum (also referred to as gum arabic), guar gum (also referred to as guaran), locust bean gum (also known as carob gum), pectin, xanthan gum, or mixtures thereof. Other gums are also suitable, such as carrageenan. The gum may be added to the liquid beverage in a concentration ranging from approximately 0.05 wt. % to approximately 10 wt. %. As described in more detail below, the gum is added as a popping inhibitor which allows bubbles to form and grow into a stable drinkable foam when the beverage container is opened. In one non-limiting embodiment, the gum further acts as an emulsifier.
[0024] The amount of gum added to the beverage will depend on the base liquid, as well as the desired characteristics of the foam. Base liquids that are naturally more viscous will require less gum, or in some cases no gum at all, in order to achieve the same effect.
[0025] The addition of gum to the base liquid serves at least three purposes. First, it thickens the base liquid in a way that may be more palatable. Second, once the container is opened, the gum traps the gas that exits the base liquid and forms bubbles. Some base liquids are sufficiently viscous to foam without the addition of gum, but the foam phase duration is greatly increased by the gum. The gum further serves as a limiter on bubble size by forming a stronger, thicker bubble wall which resists stretching by the trapped gas. This results in finer bubbles which are perceived as silkier and creamier than foams with large bubbles. In situations where the resulting beverage will be consumed immediately, the foam phase may persist for a sufficient duration without the addition of gum to the liquid beverage.
[0026] In an exemplary embodiment, the base liquid of the liquid beverage is milk. In some embodiments, the term milk refers to dairy milk and non-dairy milk. For example, dairy milk can be an animal milk including milk proteins and fat, such as, for example, cow's milk. In other embodiments, the milk may be a reconstituted mixture of milk proteins and milk fat. In further embodiments, the liquid may include one or more non-dairy milks such as almond milk, coconut milk, soy milk, etc. The non-dairy milks have fat and protein concentrations similar to dairy milk. In still other embodiments, the liquid may include other dairy products such as yogurt. The milk used in the liquid beverage may initially have any concentration of fat including approximately 1 wt. % or approximately 2 wt. % (e.g., reduced fat milks), approximately 3.25 wt. % (e.g., whole milk), approximately 10.5 wt. % to approximately 18 wt. % (e.g., half and half), or greater than approximately 18 wt. % (e.g., cream).
[0027] Non-dairy liquids are also suitable as the base liquid of the liquid beverage, such as water, coffee, tea, or fruit juices (e.g., orange juice). The liquid beverage may further include solutes that depress the freezing point of the liquid such as sweeteners (e.g., sugar, honey, artificial, non-saccharide sweeteners, etc.) and artificial or natural flavoring agents (e.g., mint, cinnamon, caramel, hazelnut, chocolate, etc.). The solutes may also be sugars, salts, acids, gas, gums, stabilizers, emulsifiers, flavors, preservatives, starches, flours, electrolytes, alcohol, or a mixture thereof. In a non-limiting embodiment, the solutes may comprise between about 0.05% and about 5.0% of the total weight of the liquid. In another embodiment, the solutes comprise between about 0.1% and about 3.0% of the total weight of the liquid. In another embodiment, the solutes comprise between about 0.3% and about 1.5% of the total weight of the liquid.
[0028] In an exemplary embodiment, the liquid beverage is a mixture of milk or milk substitute and coffee in any suitable ratio. For example, coffee is mixed with whole milk at a milk-to-coffee weight ratio ranging from approximately 4:1 to approximately 5:1. In other words, the liquid beverage may include approximately 15 wt. % to approximately 25 wt. % of coffee and approximately 80 wt. % to approximately 90 wt. % milk or milk substitute. The coffee may be brewed using any suitable method known to one of ordinary skill in the art, including, but not limited to, espresso, drip brewing, or cold brewing. In a preferred embodiment, the coffee is cold brewed with a brew strength, measured as the percentage of total dissolved solids, of approximately 7 parts per million (ppm).
[0029] The liquid beverage may be prepared by slowly mixing the gum and the base liquid until the gum is well dissolved. The base liquid and gum are mixed at a rate low enough to avoid dissolving air into the mixture at 15.6 C. (60 F.) and 101325 Pa (1 atmosphere). Where the base liquid is a mixture of liquids, the gum may be dissolved into a first liquid before a second liquid is added to the mixture. For example, for a mixture of coffee and milk, the gum may first be dissolved in the coffee. The milk is then added to the coffee-gum mixture and again slowly mixed to incorporate without dissolving air in the mixture. In other embodiments, the liquid beverage may be mixed in any other order, including first mixing together the milk and the coffee and then adding the gum. In some embodiments, the liquid beverage may be ultrasonicated to remove any dissolved air before or after filling the retail container, but before sealing the retail container.
[0030] Gas Saturation Tank
[0031] At the second step 120 of the process 100, the mixing tank is sealed or the liquid mixture is transferred to a sealed gas saturation tank such that the tank forms a gas tight system. It will be understood that the mixing tank and the gas saturation tank may be the same tank. In one exemplary embodiment, the tank is a circulatory agitation system which includes a tank and a pump, in which the liquid beverage and gas are able travel from the tank and through the pump before returning to the tank. Once sealed, the headspace may contain air at approximately atmospheric pressure (i.e., approximately 14.7 pounds per square inch (psi) at sea level). In another embodiment, the headspace may be purged of air such that the headspace has a reduced pressure of less than atmospheric pressure.
[0032] A volume of a gas is introduced into the gas saturation tank through a valve. In one embodiment, the gas is nonreactive to prevent the gas from altering the flavor of the liquid beverage. In an exemplary embodiment, the gas is nitrous oxide (N.sub.2O), nitrogen (N.sub.2), carbon dioxide (CO.sub.2) or argon (Ar). In contrast to a nonreactive gas like nitrous oxide, carbon dioxide reacts with water to form carbonic acid, which may alter the flavor of the beverage. Accordingly, in another embodiment, carbon dioxide may be used to increase the acidity or alter the flavor of the liquid beverage. After the gas is introduced into the tank, it may naturally collect in the headspace rather than being dissolved into the liquid resulting in a head pressure of equal to or greater than 101325 Pa (1 atmosphere).
[0033] At the third step 130 of the process 100, the liquid beverage, now sealed in the tank, is agitated to dissolve a portion of the gas in the liquid beverage. The liquid beverage may be agitated by agitating the tank or by agitating only the liquid beverage within the tank. As the gas is dissolved, it will move from the headspace into the liquid beverage, thereby reducing the pressure in the headspace. Further gas is added and the beverage container is agitated until the liquid beverage is fully saturated by the gas. Saturation may be determined by measuring the pressure within the headspace. When the pressure in the headspace is not reduced by further agitation, no more gas can be dissolved into the liquid beverage. The gas may be added to the sealed beverage container continuously while agitating the liquid beverage or in a stepwise manner, where gas is added to the tank between periods of agitation. Simultaneous addition of gas and agitation is preferred. After the liquid beverage is fully saturated by the gas, the pressure in the tank ranges from approximately 137895 Pa (20 psi) to 586054 Pa (85 psi), from approximately 137895 Pa (20 psi) to 413685 Pa (60 psi), or from approximately 137895 Pa (20 psi) to 275790 Pa (40 psi). Without agitation, the gas will collect in the headspace rather than dissolve in the liquid beverage. Because undissolved gas will not form bubbles in the liquid beverage once the beverage container is opened, reducing or eliminating agitation will result in reduced foam production.
[0034] Because the amount of the gas which can be dissolved in the liquid beverage is dependent on the temperature of the liquid beverage, steps 120 and 130 may occur at the temperature at which the product will be stored and served to prevent too little or too much of the gas being dissolved in the liquid beverage during packaging. In some embodiments, the liquid beverage has a temperature ranging from approximately 28.9 C. (20 F.) to approximately 4.4 C. (40 F.) during gassing and agitation. Alternatively, the liquid beverage has a temperature ranging from approximately 17.8 C. (0 F.) to approximately 4.4 C. (40 F.) during gassing and agitation. In another alternative, the liquid beverage has a temperature ranging from approximately 3.9 C. (25 F.) to approximately 4.4 C. (40 F.) during gassing and agitation. The liquid beverage may have a temperature ranging from approximately 3.9 C. (25 F.) to approximately 0.5 C. (33 F.) during gassing and agitation. In an exemplary embodiment, the liquid-gas mixture may be frozen.
[0035] In some embodiments, the liquid-gas mixture may be allowed to rest. Such resting may occur for anywhere up to about 15, 30, 45, 60, 75, 90, 105, or 120 minutes. In other embodiments, the liquid-gas mixture is permitted to rest for up to about 3, 4, 5, or 6 hours. In an exemplary embodiment, the liquid-gas mixture may be frozen during the time it is resting. Such resting may occur before, during, or after the cooling step. In another embodiment, the resting may occur before or after the filing step, but prior to the exposure of the liquid-gas mixture to atmospheric pressure.
[0036] Heat Exchanger
[0037] At the fourth step 140 of the process 100, the temperature of the liquid-gas mixture is reduced to about 0 C. (32 F.). At constant pressure, Henry's Law teaches that as the temperature goes down the solubility of the gas increases. When pressure is reduced, however, solubility will decrease and dissolved gas will begin to flow out of the liquid phase. By increasing the pressure the applicant is increasing the solubility before reducing the pressure, which will in turn decrease the solubility.
[0038] In certain embodiments, heat exchangers 320, such as glycol heat exchangers, may be used to reduce the temperature of the liquid. Heat exchangers 320 may be placed between the mixing tank and the gas saturation tank 330 or between the gas saturation tank 330 and the pressurized filler 340 discussed below.
[0039] Pressurized Filler
[0040] At the fifth step 150 of the process 100, the cooled liquid-gas mixture is introduced to a retail container. As the cooled liquid-gas mixture contains dissolved gas, turbulence, which would start the foaming process, should be avoided. In addition, the container may be only partially filled with the liquid beverage such that a headspace remains above the liquid beverage. In an exemplary embodiment, the volume of the liquid beverage ranges from approximately 65% to approximately 95% of the volume of the beverage container, with the headspace forming the balance of the volume of the beverage container (i.e., approximately 5% to approximately 35% of the volume).
[0041] The retail container may be one of any number of vessels suitable for packaging beverages that may be sealed, pressurized with a gas, and reopened as described in more detail below, such as cans, bottles, kegs, etc. In the exemplary embodiment, the container is a metal (e.g., aluminum) can, bottle, or keg. Glass or ceramic bottles may also be used.
[0042] In one embodiment of this invention turbulence is avoided by minimizing the height difference between the surface of the liquid in the can and the surface of the liquid in the tank. Such minimization can be accomplished in one of two ways, both of which require monitoring of the height of the surface in the tank. First, as the cooled liquid-gas mixture flows out of the tank, the tank may be lifted via a motorized tank elevation system. Second, the flow of the cooled liquid-gas mixture to the tank could be set to equal the flow of the cooled liquid-gas mixture to the filler thereby maintaining a steady height. Regardless of the strategy employed, it is desirable to maintain the difference in the height of the surface of the liquid in the tank and the container between approximately 5.1 cm (2 in) and 30.5 cm (12 in).
[0043] In another embodiment of this invention, the liquid mixture may bypass the gas saturation tank 330 and be introduced directly to a container via the pressurized filler 340. The container may be initially sealed with a cap containing a one-way valve. The cap may be a one-time use cap or reusable. Gas is then introduced to the liquid mixture in the container and the liquid mixture is agitated to create a gas-liquid mixture. The temperature of the gas-liquid mixture is then reduced to about 0 C. (32 F.) to put the dissolved gas to sleep. The introduction of the gas may occur at substantially the same time that the liquid mixture is agitated or cooled. In addition, the gas may be introduced into the liquid mixture, the mixture may be agitated, and the temperature of the gas-liquid mixture may be reduced to about 0 C. (32 F.) all at substantially the same time.
[0044] In a further non-limiting embodiment, the temperature of the gas-liquid mixture is reduced below the freezing point of the gas-liquid mixture. While the gas-liquid mixture is frozen, a cap containing a one-way valve may be removed and replaced with a standard cap.
[0045] The use of a reusable cap with a one-way valve permits the container to be adapted to allow gas to be introduced into the container after it is sealed. In an exemplary embodiment, the one-way valve is incorporated into the top of the cap. However, other embodiments may include the one-way valve located in any other suitable location, for example the side of the cap. The one-way valve, for example, may be a permeable membrane through which a syringe can be introduced into the interior of the first container but which does not allow gas or liquid to exit the first container. The one-way valve may be an FDA-approved gassing valve. In other embodiments, any other one-way valve may be used.
[0046] Conveyor
[0047] At the sixth step 160 of the process 100, the retail containers containing the cooled gas-liquid mixture are transmitted from the filler to the sealer. On the conveyor and in the sealer, the pressure that the containers are subject to is reduced to atmospheric pressure. In one embodiment of this invention, the conveyor is approximately 1.2 m (4 ft) long. In such embodiments the containers traverse the length of the conveyor in approximately 2 seconds. It is during this time that the gas dissolved in the liquid-gas mixture comes out of solution and begins to create a foam which will eventually overflow the container if the container is not sealed.
[0048] Sealer
[0049] At the seventh step 170 of the process 100, the container containing the liquid-gas mixture is sealed so that pressure cannot escape. When the containers reach the sealer they are almost immediately sealed. Once sealed, the gas that has been released as a result of the drop in pressure to atmospheric pressure equilibrates as certain amounts dissolve back into the liquid-gas mixture thereby preserving the ability of the liquid-gas mixture to separate into a delicious liquid and foam upon the opening of the sealed container.
[0050] In other embodiments in which the container is initially sealed with a cap containing a one-way valve, the cap containing a one-way valve is removed and a new cap, which does not contain a one-way valve, is used to seal the container. Once sealed, the gas that has been released as a result of the drop in pressure to atmospheric pressure equilibrates as certain amounts dissolve back into the liquid-gas mixture thereby preserving the ability of the liquid-gas mixture to separate into a delicious liquid and foam upon the opening of the sealed container. The cap containing the one-way valve may then be sterilized and reused.
[0051] During the sealing process additional gas and/or beverage product may be introduced to the container. In some embodiments, additional gases are introduced to the beverage after the beverage is exposed to reduced atmospheric pressure (i.e., prior to sealing). These gases may be introduced in solid, liquid or gas form. For example, in one embodiment a drop of liquid nitrogen is introduced to the beverage before sealing. In another embodiment, dry ice could be introduced to the beverage before sealing.
EXAMPLES
[0052] In the following three experiments, the freezing point and gas stability of various beverages was tested.
Experiment 1Solute Effect on Freezing Points
[0053] In the first set of experiments, the freezing point of three different compositions was investigated. The first composition was a La Colombe Original Draft Latte. The second and third compositions added different solutes (sugar and alcohol) to composition 1. During the experiment, each preparation was carefully weighed and poured into a transparent container equipped with a valve. Next, the container was gassed and shaken with nitrous oxide at 45 psi until saturation occur. Then the gas-liquid mixture was cooled in a freezer. Finally, when the preparation began to freeze, the temperature was recorded using a laser gun thermometer. The results of the first set of experiments is recorded in Table 1 below:
TABLE-US-00001 TABLE 1 Original Draft Latte Sugar Alcohol Freezing Point Compo- 270 grams 0 grams 0 grams 2.2 C. (28 F.) sition 1 Compo- 270 grams 10 grams 0 grams 2.8 C. (27 F.) sition 2 Compo- 270 grams 0 grams 10 grams 3.9 C. (25 F.) sition 3
Experiment 2Temperature and Resting Time Effect on Gas Retention
[0054] In the second set of experiments, the effect of temperature and rest on the gas retention of the three different compositions was investigated. The basic manipulation included first getting a composition ready and gassed in a first 8 fluid oz. container at 45 PSI, which may be considered as a large scale production container connected to a filler. Next, the container (and the composition) was placed in various conditions of temperature and rest in order to test the effect of these 2 parameters. Specifically, the container was opened to expose the composition to an atmospheric pressure. The composition was poured from the first container into a second 8 fluid oz. container without a valve to simulate the agitation produced by a production filler. The second container was then sealed. To test the gas lost from the exposure to atmospheric pressure, the second container was permitted to rest until it reaches a consuming temperature (45 F.) at which time the container was opened and poured into a beaker. The quantity of foam obtained from each composition was measured in milliliters at set intervals and is listed in Tables 2 below:
TABLE-US-00002 TABLE 2 Measured at 45 F., volume of foam in ml after: Composition Temperature Rest Time 0 s 15 s 30 s 1 min 3 min 5 min 10 min 15 min 1 0.6 C. (33 F.) 15 min 500 480 470 410 360 250 40 0 0.6 C. (33 F.) 30 min 510 500 490 450 380 270 40 0 0.6 C. (33 F.) 90 min 600 580 570 560 440 300 50 0 7.2 C. (45 F.) 15 min 450 430 350 300 250 150 10 0 7.2 C. (45 F.) 30 min 430 400 330 290 210 150 10 0 7.2 C. (45 F.) 90 min 450 440 350 300 230 150 10 0 15.6 C. (60 F.) 15 min 150 75 50 50 10 0 0 0 15.6 C. (60 F.) 30 min 480 390 350 310 125 60 0 0 15.6 C. (60 F.) 90 min 550 470 400 350 180 100 10 0 2 0 C. (32 F.) 15 min 620 610 610 560 470 430 140 10 0 C. (32 F.) 30 min 620 620 610 600 500 400 190 0 0 C. (32 F.) 90 min 600 590 590 570 490 370 150 10 7.2 C. (45 F.) 15 min 500 480 470 430 340 280 80 0 7.2 C. (45 F.) 30 min 560 550 530 510 420 320 130 0 7.2 C. (45 F.) 90 min 500 490 480 450 360 300 100 10 15.6 C. (60 F.) 15 min 370 350 330 290 200 140 10 0 15.6 C. (60 F.) 30 min 400 340 320 280 180 110 10 0 15.6 C. (60 F.) 90 min 390 370 350 300 190 140 0 0 3 1.1 C. (30 F.) 15 min 620 620 600 580 470 300 40 0 1.1 C. (30 F.) 30 min 630 630 600 580 500 330 60 10 1.1 C. (30 F.) 90 min 630 630 610 570 500 410 140 10 7.2 C. (45 F.) 15 min 480 450 430 310 270 200 30 0 7.2 C. (45 F.) 30 min 510 490 470 440 330 210 40 0 7.2 C. (45 F.) 90 min 530 500 470 450 340 210 50 0 15.6 C. (60 F.) 15 min 450 420 420 350 240 180 50 0 15.6 C. (60 F.) 30 min 470 440 400 360 250 180 10 0 15.6 C. (60 F.) 90 min 470 450 400 340 240 190 30 0
[0055] As can be seen above, decreased temperature and rest puts the gas-liquid mixture to sleep, which permits more gas to be retained in between filling and sealing of the container.
Experiment 3Temperature and Resting Time Effect on Switch Cap System
[0056] In the third set of experiments, the effect of temperature and rest on the gas retention of the original draft latte (Composition 1) using the switch cap system was investigated. The basic manipulation included first getting a composition ready and gassed in a first 12 fluid oz. container at 45 PSI. The container rests for 90 minutes and the temperature is lowered to 0.6 C. (33 F.). The cap is removed, exposing the liquid to atmospheric pressure. The container is then sealed with a standard cap lacking a valve. To test the gas lost from the exposure to atmospheric pressure, the container was permitted to rest until it reaches a consuming temperature (45 F.) at which time the container was opened and poured into a beaker. The quantity of foam obtained from each composition was measured in milliliters at set intervals and is listed in Tables 3 below:
TABLE-US-00003 TABLE 3 Measured at 45 F., volume of foam in ml after: Composition Temperature Rest Time 0 s 15 s 30 s 1 min 3 min 5 min 10 min 15 min 1 0.6 C. (33 F.) 90 min 810 780 770 690 640 510 340 90 0.6 C. (33 F.) 90 min 800 790 780 730 650 520 340 110 0.6 C. (33 F.) 90 min 800 790 750 780 580 480 280 80 0.6 C. (33 F.) 90 min 810 800 780 750 650 520 300 90 0.6 C. (33 F.)) 90 min 800 790 780 670 550 490 320 90 0.6 C. (33 F.) 90 min 780 770 670 650 530 490 250 40
[0057] Although illustrated and described above with reference to certain specific embodiments, the present invention is nevertheless not intended to be limited to the details shown. Rather, various modifications may be made in the details within the scope and range of equivalents of the claims and without departing from the spirit of the invention. It is also expressly intended that the steps of the methods of using the various devices disclosed above are not restricted to any particular order.