Part consisting of a ceramic material, comprising a base and a wall
10138739 ยท 2018-11-27
Assignee
Inventors
Cpc classification
C04B38/06
CHEMISTRY; METALLURGY
C04B2111/00405
CHEMISTRY; METALLURGY
B32B18/00
PERFORMING OPERATIONS; TRANSPORTING
C04B38/06
CHEMISTRY; METALLURGY
F01D9/02
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
C04B2237/76
CHEMISTRY; METALLURGY
B28B1/001
PERFORMING OPERATIONS; TRANSPORTING
F01D5/284
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
International classification
B28B1/00
PERFORMING OPERATIONS; TRANSPORTING
C04B38/06
CHEMISTRY; METALLURGY
B32B18/00
PERFORMING OPERATIONS; TRANSPORTING
F01D9/02
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
F01D5/28
MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
Abstract
A part made of a ceramic material, including a portion forming a base and a portion forming a wall, wherein the base consists of a low-porosity ceramic material and the wall is obtained by powder sintering and includes an envelope and a core, the core being within the envelope, the porosity of the core being higher than that of the base and increasing the further it is from the base.
Claims
1. A turbine blade made of ceramic material, comprising: a root; and an airfoil, wherein the root is made of ceramic material and the airfoil is obtained by ceramic powder sintering, and wherein the airfoil includes an envelope and a core, the core being positioned within the envelope and a porosity of the core being greater than a porosity of the root, the porosity of the core increasing along the airfoil along an axis in a direction of centrifugal forces which the turbine blade is subjected to during operation.
2. The turbine blade according to claim 1, wherein the root is produced by ceramic powder sintering.
3. The turbine blade according to claim 1, the porosity of the material forming the root being less than 3%.
4. The turbine blade according to claim 1, wherein the porosity of the core is greater than 5%.
5. The turbine blade according to claim 4, wherein the porosity of the core is between 10 and 50%.
6. The turbine blade according to claim 1, wherein the core comprises a porous material made of ceramic grains which are bound by partial sintering.
7. The turbine blade according to claim 1, wherein the core comprises cavities separated by partitions, a material forming the partitions having a porosity of less than 3%.
8. The turbine blade according to claim 1, wherein the core has portions having different cavities, sizes of the cavities increasing along the airfoil along the axis.
9. The turbine blade according to claim 1, further comprising a heel at a free end of the airfoil, a porosity of the heel being lower than the porosity of the core.
10. The turbine blade according to claim 9, wherein the heel includes sealing strips.
11. A method for manufacturing a turbine blade according to claim 1, comprising: forming the airfoil using a sintering tray containing powder with which the root is flush at a beginning of the forming; and selective sintering of the powder in successive layers by a laser beam or electron beam, the successive layers being obtained by making the turbine blade move progressively downwards in the sintering tray.
12. The method according to claim 11, including producing the root separately by powder sintering and then forming the airfoil by depositing successive layers of ceramic powder and binding the root and the airfoil by sintering.
Description
BRIEF DESCRIPTION OF THE FIGURES
(1) The invention will be better understood and other aims, details, features and advantages thereof will emerge more clearly in the following detailed explanatory description of an embodiment of the invention given by way of purely illustrative and non-limiting example, with reference to the accompanying schematic drawings, in which:
(2)
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DETAILED DESCRIPTION OF EMBODIMENTS OF THE INVENTION
(7) With reference to
(8) According to the invention, this part which is made of ceramic material has a density which varies along its axis XX. The variation in density is schematically shown by the sections along the planes which are transverse relative to the axis XX: A, B, C and D of the part along the axis XX.
(9) The base 11 is of maximum density. This is, for example, an element obtained by shaping a ceramic powder in a mould, said powder optionally being combined with a binder. This step is followed by sintering heat treatment of the unfinished blank produced by the mould. According to the composition of the material used, the treatment may include intermediate debinding steps. The porosity of this element is preferably less than 3%.
(10) The wall 13 has an envelope 13E and a core 13N. The envelope forms the outer surface of the wall. It is thin, for example less than 1 mm, preferably approximately 0.5 mm, and of low porosity like the base. The envelope delimits the core 13N, of which the porosity is greater. This porosity is greater than 5%, preferably between 10 and 50%. Correspondingly, its density is lower, providing the above-mentioned advantages of reducing the centrifugal mechanical stress on the base, when the part, as in this example, is mounted on a rotor. Advantageously, the density is not the same along the entirety of the axis. As can be seen in sections B and C, said density is represented schematically by different grid patterns having a smaller or larger mesh size. The heel, shown by the section D, may have a lower density than that of the base and a greater density than that of the wall. It is produced by sintering grains of ceramic powder.
(11) Such a part is produced in part by powder sintering, of which the method set out below is recalled in relation with the device from
(12) A laser-beam or electron-beam generator 1 emits a beam 2 of appropriate power, which it directs towards an arrangement of reflecting mirrors 3, of which the last mirror 4 can pivot so as to ensure that the surface of the part to be produced, for example the blade 10 mentioned above, is swept.
(13) The portion of the part P which has already been formed is immersed in a tray 6 such that it can be covered with a layer of the powder 7 which is suitable for sintering at regular intervals. A second tray 8, for supplying powder, is positioned to the side of the sintering tray 6 and is filled with this sintering powder 7. A device forming a piston 9 makes it possible to move a given quantity of powder 7 from the supply tray 8 to the sintering tray 6, in order to cover the portion of the part P with a layer of powder of a given thickness. The thickness of this layer corresponds to that of which can be increased that of the portion of the part during a sintering pass between the grains by the beam 2. Devices for lowering the sintering tray 6 and raising the supply tray 8 make it possible, on one hand, to keep the portion of the part to be sintered P flush with the sides of the tray 6 and, on the other hand, to bring a layer of powder 7 having the correct thickness to be opposite the piston 9 of the supply tray 8.
(14) The sintering and binding of the grain to form the part 10 is carried out in a succession of basic operations which take place in the following manner: since the portion of the part P is flush with the sides of the sintering tray 6, the piston 9 is moved towards this tray 6 so that it deposits the desired thickness of powder 7 on the portion of the part P, and is then returned to a stand-by position at the end of the supply tray 8. The laser beam or electron beam 2 sweeps the surface of the portion of the part P using the oscillating mirror 4, thereby causing partial meltingor an increase in temperature such that the diffusion between the grains is activatedof the surface layers of the layer and causing said layer to aggregate to the part P, and the thickness is increased. The portion of the part P formed is then moved downwards to compensate the increase in its thickness and so that its surface is once more flush with the sintering tray 6, whereas the supply tray 8 is raised to provide an adequate quantity of powder 7 opposite the piston 9. This process is repeated the number of times that are required to arrive at the desired geometry and dimensions for the complete part 10.
(15) According to the invention, the base 11 of the part to be produced is firstly arranged in the sintering tray 6. This base 11 which is shown in
(16) The base is arranged in the sintering tray together with the ceramic powder such that the planar-surface portion is flush with the surface of the powder. The method then includes producing the wall 13 on this base 11 (
(17) The surface of the envelope 13E is thus produced for the layer being constructed at a given porosity, in particular a porosity of less than 3%, similar to that of the base. Below this surface, the core 13N is constructed such that its porosity is greater than that of the surface. A lower density is obtained by keeping the energy of the beam at a lower level in order to obtain partial sintering. The porosity is greater than that of the base. It is at least 5%, preferably between 10 and 50%. Constructing the part layer by layer moreover allows layers to be produced which have a core of which the porosity varies along the axis XX. This porosity advantageously increases between the base and the heel.
(18) According to a variant of the core of the wall, the movement of the laser beam is controlled so as to produce partitions which form cavities therebetween in the manner of a honeycomb structure. The partitions are made of a dense material, like the surface forming the envelope. The size of the cavities may advantageously change, preferably increase, between the base and the heel of the blade.
(19) The ceramic material used may be of any kind. Preferably, ceramics are selected which can be used at temperatures of greater than 1000 C.; these are, for example, carbides such as SiC, oxides such as Al.sub.2O.sub.3 or nitrides such as Si.sub.3N.sub.4. Eutectic ceramics are also suitable.
(20) The granulometry of the powders is selected in order for it to be possible for sintering to be carried out by means of a laser or an electron beam. It is observed that the lower the size of the powder, the easier it is to produce partial sintering at a low temperature.
(21) The laser beam or electron beam is adapted to the material which is treated. For example, in the case of alumina Al.sub.2O.sub.3, a YAG laser emitting at 9400 cm.sup.1, having a power of between 10 and 30 W and together with optimal movement at a speed of 96 mm/s is suitable for this application.
(22) The ceramics may be part of a mixture having a hot-melt precursor which forms a binder and which is optionally eliminated subsequently by appropriate heat treatment.
(23) Final machining is optionally provided if it is necessary for the roughness to be reduced.
(24) The method used to manufacture these parts results in significant residual stress which is due to the thermal gradients generated by the successive melting of the layers. These gradients may increase as a function of the geometry, the thickness and changes in section of the parts to be produced. Depending on the materials, the residual stress arising from these gradients may result in deformations of the part during construction, and in fissuring or cracking during use. It is therefore important to control the temperature during the sintering process and to maintain a uniform temperature in the powder in order to minimise the residual stress during solidification. An appropriate heating means, for example a resistive heating means, is used for this purpose.
(25) According to a variant of the invention, the part is a pair of turbine blades as shown in