DIFFERENTIAL PRESSURE DETECTION ELEMENT, FLOW RATE MEASUREMENT DEVICE, AND METHOD OF MANUFACTURING DIFFERENTIAL PRESSURE DETECTION ELEMENT
20180245955 ยท 2018-08-30
Assignee
Inventors
Cpc classification
B81B3/0072
PERFORMING OPERATIONS; TRANSPORTING
G01L13/02
PHYSICS
B81C1/00666
PERFORMING OPERATIONS; TRANSPORTING
B81B3/00
PERFORMING OPERATIONS; TRANSPORTING
B81C2201/0173
PERFORMING OPERATIONS; TRANSPORTING
International classification
G01F1/38
PHYSICS
B81B3/00
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A differential pressure detection element includes: a support portion having an opening; a cantilever portion supported in a cantilever manner by the support portion so as to protrude into the opening; a diffusion layer including a piezoresistive portion provided at a fixed end of the cantilever portion; a pair of wiring portions electrically connected to the diffusion layer; a first insulating layer covering the diffusion layer; and a second insulating layer laid on the first insulating layer. A linear expansion coefficient of the first insulating layer is smaller than a linear expansion coefficient of a material of which the cantilever portion is composed, and a linear expansion coefficient of the second insulating layer is larger than the linear expansion coefficient of the first insulating layer.
Claims
1. A differential pressure detection element comprising: a support portion having an opening; a cantilever portion supported in a cantilever manner by the support portion so as to protrude into the opening; a diffusion layer including a piezoresistive portion provided at a fixed end of the cantilever portion; a pair of wiring portions electrically connected to the diffusion layer; a first insulating layer covering the diffusion layer; and a second insulating layer laid on the first insulating layer, wherein a linear expansion coefficient of the first insulating layer is smaller than a linear expansion coefficient of a material of which the cantilever portion is composed, and a linear expansion coefficient of the second insulating layer is larger than the linear expansion coefficient of the first insulating layer.
2. The differential pressure detection element according to claim 1, wherein the cantilever portion is composed of silicon, the first insulating layer is a silicon oxide layer, and the second insulating layer is a silicon nitride layer.
3. The differential pressure detection element according to claim 1, wherein the following Mathematical Formula (1) is satisfied, and
4. The differential pressure detection element according to claim 1, wherein the diffusion layer includes a lead portion electrically connecting a pair of the wiring portions and the piezoresistive portion in series, and an impurity concentration in the lead portion is higher than an impurity concentration in the piezoresistive portion.
5. A flow rate measurement device configured to detect a flow rate of a fluid flowing through a main flow passage, comprising: the differential pressure detection element according claim 1; a bypass passage communicating with the main flow passage through a pair of communication ports and being provided with the differential pressure detection element; and a flow rate calculation unit calculating the flow rate of the fluid on the basis of an output of the differential pressure detection element.
6. A method of manufacturing the differential pressure detection element according to claim 1, comprising: a first step of forming the diffusion layer by doping one silicon layer of the SOI substrate with impurities; a second step of forming the first insulating layer on the diffusion layer; and a third step of forming the second insulating layer on the first insulating layer, wherein a first layer formation temperature in the second step is 1200 C. or less, and a second layer formation temperature in the third step is 800 C. or less.
7. The method of manufacturing the differential pressure detection element according to claim 6, wherein the following Mathematical Formula (2) is satisfied,
8. The method of manufacturing the differential pressure detection element according to claim 6, wherein the first step includes forming a thermal silicon oxide layer by performing a thermal oxidation process on the silicon layer, the second step includes: forming a deposited silicon oxide layer on the thermal silicon oxide layer by a CVD method; and forming the first insulating layer by performing an annealing process on the thermal silicon oxide layer and the deposited silicon oxide layer, the third step includes forming the silicon nitride layer by a CVD method, the first layer formation temperature in the second step is a temperature of the annealing process in the second step, and the second layer formation temperature in the third step is a temperature of the CVD method in the third step.
Description
BRIEF DESCRIPTION OF DRAWINGS
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[0019]
[0020]
[0021]
[0022]
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[0024]
[0025]
DETAILED DESCRIPTION
[0026] Hereinafter, embodiments of the invention will be described with reference to the drawings.
[0027]
[0028] As illustrated in
[0029] Although
[0030] The flow rate measurement device 1 detects a pressure difference between an upstream opening 5 and a downstream opening 6 of the bypass passage 4 by elastic deformation of the cantilever portion 12 of the differential pressure detection element 10, and the flow rate calculation unit 20 calculates the flow rate of the fluid flowing through the main flow passage 2 on the basis of the pressure difference.
[0031] In the example illustrated in
[0032]
[0033] As illustrated in
[0034] As described later, the support substrate 11 and the cantilever portion 12 are integrally formed by processing an SOI (Silicon on Insulator) wafer 30. The support substrate 11 is configured as a laminate including a first silicon layer 31, a silicon oxide layer 32, and a second silicon layer 33. A rectangular opening 111 penetrating the support substrate 11 is formed on the support substrate 11.
[0035] On the other hand, the cantilever portion 12 includes only the first silicon layer 31. The cantilever portion 12 is supported in a cantilever manner by the support substrate 11 at the fixed end 121 of the cantilever portion 12 so as to protrude into the opening 111 of the support substrate 11. Therefore, except for the fixed end 121 of the cantilever portion 12, a gap 122 is secured between the outer edge of the cantilever portion 12 and the inner wall surface of a through-hole 111. Although not particularly limited, the gap 122 has a width of, for example, about 1 m to 100 m.
[0036] The diffusion layer 13 includes piezoresistive portions 131 and 132 and lead portions 133 to 135. A pair of the piezoresistive portions 131 and 132 is electrically connected in series to the wiring portions 16 and 17 described later by the lead portions 133 to 135. The piezoresistive portions 131 and 132 are formed by doping the first silicon layer 31 (n-type semiconductor) with p-type impurities. The piezoresistive portions 131 and 132 are provided at the fixed end 121 where the stress is at maximum in the cantilever portion 12 at the time of pressure application. The resistance values of the piezoresistive portions 131 and 132 are changed in accordance with the elastic deformation of the cantilever portion 12.
[0037] The wiring portions 133 to 135 of the diffusion layer 13 are also formed by doping the first silicon layer 31 with p-type impurities. However, the impurity concentration in the lead portions 133 to 135 is higher than the impurity concentration in the piezoresistive portions 131 and 132. Namely, in one or more embodiments, the piezoresistive portions 131 and 132 of the diffusion layer 13 are composed of a p.sup. type semiconductor, whereas the lead portions 133 to 135 of the diffusion layer 13 are composed of a p.sup.+ type semiconductor. As a result, the electrical resistance values of the piezoresistive portions 131 and 132 are higher than the electrical resistance values of the lead portions 133 to 135.
[0038] The first lead portion 133 electrically connects one end (upper end in
[0039] The diffusion layer 13 may be formed by doping the first silicon layer 31 (p-type semiconductor) with n-type impurities. In this case, the piezoresistive portions 131 and 132 are composed of an n.sup. type semiconductor, and the wiring portions 133 to 135 are composed of an n.sup.+ type semiconductor.
[0040] The diffusion layer 13 is covered with the first insulating layer 14, so that electrical insulation properties of the piezoresistive portions 131 and 132, the lead portions 133 to 135, and the wiring portions 16 and 17 are secured. The first insulating layer 14 is configured as a layer having a linear expansion coefficient smaller than the linear expansion coefficient of silicon, and specifically, the first insulating layer is configured as a silicon oxide (SiO.sub.2) layer. The first insulating layer 14 has a thickness w.sub.1 of, for example, about 0.5 nm to 200 nm. In one or more embodiments, the first insulating layer 14 is formed on the fixed end 121 of the cantilever portion 12 including the diffusion layer 13 and the support substrate 11.
[0041] Furthermore, in one or more embodiments, the second insulating layer 15 is laid on the first insulating layer 14. The second insulating layer 15 is configured as a layer having a linear expansion coefficient larger than the linear expansion coefficient of the first insulating layer 14, and specifically, the second insulating layer configured as a silicon nitride (SiN) layer. The second insulating layer 15 has a thickness w.sub.2 of, for example, about 3 nm to 100 nm.
[0042] As described in one or more embodiments above, if an insulating film is configured with a silicon oxide layer having a linear expansion coefficient smaller than the linear expansion coefficient of silicon, in the cooling process after the formation of the insulating film, the cantilever is greatly contracted in comparison with the insulating film. Therefore, the cantilever warps to the side opposite to the insulating film in the differential pressure detection element having a structure in the related art that has no second insulating layer. If the cantilever greatly warps in the offset state as described above, a large initial stress occurs in the piezoresistive portions formed at the base of the cantilever, so that the offset voltage (the output voltage of the differential pressure detection element in the offset state) increases. As the offset voltage increases, in some cases, the correction of the output of the differential pressure detection element or the like is adversely affected, so that the detection accuracy of the differential pressure detection element is deteriorated.
[0043] In contrast, in one or more embodiments, the second insulating layer 15 is laid on the first insulating layer 14, and the linear expansion coefficient of the second insulating layer 15 is set to be larger than the linear expansion coefficient of the first insulating layer 14. Therefore, in the cooling process after the formation of the second insulating layer 15, the second insulating layer 15 is also greatly contracted in comparison with the first insulating layer 14. As a result, the warp of the cantilever portion 12 can be canceled out, so that the offset voltage of the differential pressure detection element 10 can be reduced.
[0044] In this case, in one or more embodiments, the relationship between the thickness w.sub.1 of the first insulating layer 14 and the thickness w.sub.2 of the second insulating layer 15 satisfies the following Mathematical Formula (3). Therefore, the warp of the cantilever portion 12 can be more appropriately canceled out by the second insulating layer 15, and the symmetry of the sensitivity of the differential pressure detection element 10 with respect to the pressure application direction can be further improved.
[0045] More specifically, as illustrated in
[0046] On the other hand, as illustrated in
[0047] Furthermore, as illustrated in
[0048] In
[0049] The first wiring portion 16 is provided on the upper surface 112 of the support substrate 11 through the openings 141 and 151 of the first and second insulating layers 14 and 15 so as to be in contact with the end portion (lower end in
[0050] As illustrated in
[0051] In the case where the fluid flows through the main flow passage 2, pressure loss occurs due to friction with the wall surface, and thus, the pressure becomes small toward the downstream side, so that the pressure of the downstream opening 6 of the bypass passage 4 is lower than the pressure of the upstream opening 5. On the other hand, the gap 122 of the differential pressure detection element 10 is narrowed to such a degree that almost no fluid flows. Therefore, the pressure of the upstream opening 5 is applied to the upstream side of the cantilever portion 12, whereas the pressure of the downstream opening 6 is applied to the downstream side of the cantilever portion 12. The cantilever portion 12 of the differential pressure detection element 10 is elastically deformed in accordance with the pressure difference between the openings 5 and 6, and thus, distortion occurs in the piezoresistive portions 131 and 132.
[0052] The flow rate calculation unit 20 detects changes in the resistance values of the piezoresistive portions 131 and 132 corresponding to the differential pressure through the wiring portions 16 and 17. The flow rate calculation unit 20 calculates the flow rate of the fluid on the basis of the differential pressure in the main flow passage 2 by using the fact that there is a correlation between the pressure loss of the fluid and the flow rate. The flow rate calculation unit 20 can be configured with, for example, a computer, an analog circuit, or the like.
[0053] Hereinafter, a method of manufacturing the differential pressure detection element 10 according to one or more embodiments will be described with reference to
[0054]
[0055] First, in step S11 of
[0056] As a method of forming the SOI wafer 30, there may be exemplified a method of bonding another silicon substrate to a silicon substrate having a silicon oxide layer formed thereon, an SIMOX (Separation by Implanted Oxygen) method, a smart cut method, or the like.
[0057] Next, in step S12 of
[0058] More specifically, as illustrated in
[0059] Next, as illustrated in
[0060] Next, as illustrated in the same figure, the lead portions 133 to 135 are formed by doping the first silicon layer 31 with p-type impurities through the opening of the first resist layer 51, and after that, the first resist layer 51 is removed.
[0061] Next, as illustrated in
[0062] Next, as illustrated in the same figure, the first silicon layer 31 is doped with p-type impurities through the opening of the second resist layer 52 to form the piezoresistive portions 131 and 132, and after that, the second resist layer 52 is removed.
[0063] As a method of doping the first silicon layer 31 of the SOI wafer 30 with impurities, there are exemplified an ion implantation method and the like. At this time, ion implantation is controlled so that the impurity concentration in the wiring portions 133 to 135 is higher than the impurity concentration in the piezoresistive portions 131 and 132.
[0064] Next, as illustrated in step S13 of
[0065] More specifically, as illustrated in
[0066] Next, as illustrated in
[0067] Next, in step S14 of
[0068] Herein, if it is assumed that the linear expansion coefficient is constant with respect to temperature, in the cooling process after the formation of the first insulating layer 14 (that is, after the annealing process in the above-described step S13), a thermal stress .sub.1 occurring in the first insulating layer 14 can be expressed by the following Mathematical Formula (4).
[0069] In the above Mathematical Formula (4), au is a linear expansion coefficient of the material of which the cantilever portion 12 is composed, .sub.1 is a linear expansion coefficient of the first insulating layer 14, v.sub.1 is a Poisson's ratio of the first insulating layer 14, E.sub.1 is a Young's modulus of the first insulating layer 14, and dT.sub.1 is a temperature difference in the cooling process after the formation of the first insulating layer 14 (that is, a difference between the maximum temperature in the annealing process in step S13 described above and the room temperature).
[0070] On the other hand, in the cooling process after the formation of the second insulating layer 15 (that is, after the second insulating layer 15 is formed by an LPCVD method in the above-described step S14), a thermal stress .sub.2 occurring in the second insulating layer 15 can be expressed by the following Mathematical Formula (5).
[0071] Herein, in the above Mathematical Formula (5), .sub.2 is a linear expansion coefficient of the second insulating layer 15, v.sub.2 is a Poisson's ratio of the second insulating layer 15, E.sub.2 is a Young's modulus of the second insulating layer 15, and dT.sub.2 is a temperature difference in the cooling process after the formation of the second insulating layer 15 (that is, a difference between the maximum temperature in the LPCVD method in step S14 described above and the room temperature).
[0072] Since both the first and second insulating layers 14 and 15 are thin films, if the film stress is approximated to be uniformly distributed in the film cross section, an equilibrium equation such as the following Mathematical Formula (6) is derived. In the case where Mathematical Formula (6) is satisfied, the warp amount of the cantilever portion 12 becomes zero due to the equilibrium of the film stress.
[0073] [Math. 6]
.sub.1w.sub.1+.sub.2w.sub.2=0(6)
[0074] Therefore, in one or more embodiments, the above-described steps S13 and S14 are executed so as to satisfy the following Mathematical Formula (7) on the basis of the above-described Mathematical Formulas (3) to (6). As a result, the warp of the cantilever portion 12 can be more appropriately canceled out by the second insulating layer 15, and thus, the symmetry of the sensitivity of the differential pressure detection element 10 in the pressure application direction can be further improved.
[0075] In one or more embodiments, the thickness w.sub.1 of the first insulating layer 14 in the above-described Mathematical Formulas (6) and (7) is defined as a sum of the thickness of the thermal silicon oxide layer 41 formed in the above-described step S12 and the thickness of the deposited silicon oxide layer 42 formed in the above-described step S13.
[0076] Next, in step S15 of
[0077] More specifically, as illustrated in
[0078] Next, as illustrated in the same figure, an etching process is performed on the first and second insulating layers 14 and 15 through the opening of the third resist layer 53. Therefore, the opening 141, 142, 151, and 152 of the first and second insulating layers 14 and 15 are formed.
[0079] Next, as illustrated in
[0080] Next, in step S16 of
[0081] More specifically, as illustrated in
[0082] Next, as illustrated in the same figure, an etching process is performed on the first and second insulating layers 14 and 15 through the opening of the fourth resist layer 54. As a result, in the first silicon layer 31, a region including the cantilever portion 12 excluding the fixed end 121 is exposed from the first and second insulating layers 14 and 15.
[0083] Next, as illustrated in
[0084] Next, as illustrated in the same figure, an etching process is performed on the first silicon layer 31 through the opening of the fifth resist layer 55. Therefore, the cantilever portion 12 is defined by the gap 122. At this time, the silicon oxide layer 32 of the SOI wafer 30 functions as an etching stopper.
[0085] Next, in step S17 of
[0086] More specifically, as illustrated in
[0087] Next, as illustrated in the same figure, an etching process is performed on the second silicon layer 33 from the lower side. At this time, the silicon oxide layer 32 of the SOI wafer 30 functions as an etching stopper.
[0088] Next, after removing the sixth resist layer 56, as illustrated in
[0089] By executing steps S11 to S17 described above, a large number of differential pressure detection elements 10 are collectively formed on one SOI wafer 30. Therefore, in step S18 of
[0090] As described above, in one or more embodiments, the second insulating layer 15 is laid on the first insulating layer 14, and the linear expansion coefficient of the second insulating layer 15 is set to be larger than the linear expansion coefficient of the first insulating layer 14. Therefore, the warp of the cantilever portion 12 can be canceled out, and thus, the offset voltage of the differential pressure detection element 10 can be reduced.
[0091] Furthermore, in one or more embodiments, since the silicon nitride layer 15 is laid on the silicon oxide layer 14, it is possible to prevent the phenomenon that the cantilever portion is deflected as time elapses due to penetration of moisture into the silicon oxide layer and expansion of the silicon oxide layer. As a result, for example, it is possible to prevent the position of the cantilever portion 12 in the offset state from changing with time.
[0092] Step S12 of
[0093] It should be noted that the embodiments described above are described for the better understanding of the invention and are not described for the limitation of the invention. Therefore, each component disclosed in one or more embodiments described above includes all design changes and equivalents belonging to the technical scope of the invention.
[0094] For example, in one or more embodiments described above, the first insulating layer 14 is formed by annealing the two layers of the thermal silicon oxide layer 41 formed by the thermal oxidation process and the deposited silicon oxide layer 42 formed by the CVD method. However, the method of forming the first insulating layer 14 is not particularly limited thereto. For example, the first insulating layer 14 may be configured with a single layer of a silicon oxide layer formed by any of a thermal oxidation method, a CVD method, a spin coating method, or the like.
EXPLANATIONS OF LETTERS OR NUMERALS
[0095] 1: flow rate measurement device [0096] 2: main flow passage [0097] 3: orifice [0098] 4: bypass passage [0099] 5: upstream opening [0100] 6: downstream opening [0101] 10: differential pressure detection element [0102] 11: support substrate [0103] 111: through-hole [0104] 112: upper surface [0105] 12: cantilever portion [0106] 121: fixed end [0107] 122: gap [0108] 13: diffusion layer [0109] 131, 132: piezoresistive portion [0110] 133 to 135: lead portion [0111] 14: first insulating layer [0112] 141, 142: opening [0113] 15: second insulating layer [0114] 151, 152: opening [0115] 16, 17: wiring portion [0116] 20: flow rate calculation unit [0117] 30: SOI wafer [0118] 31: first silicon layer [0119] 32: silicon oxide layer [0120] 33: second silicon layer [0121] 41: thermal silicon oxide layer [0122] 42: deposited silicon oxide layer [0123] 51 to 56: first to sixth resist layers
[0124] Although the disclosure has been described with respect to only a limited number of embodiments, those skill in the art, having benefit of this disclosure, will appreciate that various other embodiments may be devised without departing from the scope of the present invention. Accordingly, the scope of the invention should be limited only by the attached claims.