COLORANT COMPOSITIONS CONTAINING C. TERNATEA DERIVED BOTANICAL EXTRACTS AND PROCESSES FOR THEIR PRODUCTION

20180199600 ยท 2018-07-19

    Inventors

    Cpc classification

    International classification

    Abstract

    Compositions containing extract of C. ternatea flower and methods of extracting the extract and forming such composition are disclosed. Such compositions contain superior attributes as colorants, and may also include one or more of beta-carotene, beta-carotene extract, turmeric extract, or annatto extract and/or other suitable known colorants. Such compositions may be stabilized in a powder, crystal, or other solid form, or may be dissolved, suspended, or otherwise contained in solution. The extract may be produced via certain methods such as polar solvent extract, supercritical fluid extraction, expression, enfleurage, as well as other techniques. The stabilized compositions may further include a pH-modifying component for establishing or changing a pH level of a solution into which the composition is placed.

    Claims

    1. A composition comprising: C. ternatea flower extract; and one or more of: turmeric extract, beta carotene, beta-carotene extract, safflower extract, lutein, Marigold Extract, saffron extract, yellow gardenia, turmeric extract, annatto extract.

    2. The composition of claim 1, wherein the composition is stabilized in a powder form.

    3. The composition of claim 2, wherein the composition is stabilized in a powder form via partial evaporation of a solvent and dehydration.

    4. The composition of claim 2, wherein the compositions is stabilized in a powder form via partial evaporation of a solvent and crystallization.

    5. The composition of claim 3, wherein the composition further comprises one or more saccharides for heterogeneous nucleation of the components of the C. ternatea flower extract.

    6. The composition of claim 5, wherein the one or more saccharides are chosen from the group of: dextrose, maltodextrin, or combinations thereof.

    7. The composition of claim 1, wherein the composition is stabilized via placement into an 11% ethanol solution.

    8. The composition of claim 1, wherein the composition is stabilized via placement into a 51% glycerine solution.

    9. The composition of claim 1, wherein the composition is stabilized via placement into a 25% propylene glycol solution.

    10. The composition of claim 1, wherein the composition is stabilized in a solid form.

    11. The composition of claim 1, wherein the C. ternatea flower extract is extracted via use of an aqueous solvent.

    12. The composition of claim 1, wherein the C. ternatea flower extract is extracted via use of a polar solvent other than water.

    13. The composition of claim 1, wherein the C. ternatea flower extract is extracted via use of a nonpolar solvent.

    14. The composition of claim 1, wherein the C. ternatea flower extract is extracted via use of a combination of polar and nonpolar solvents.

    15. The composition of claim 1, wherein the C. ternatea flower extract is extracted and purified via distillation.

    16. The composition of claim 1, wherein the C. ternatea flower extract is extracted via a supercritical fluid extraction technique.

    17. The composition of claim 1, wherein the C. ternatea flower extract is extracted via an expression technique.

    18. The composition of claim 1, wherein the C. ternatea flower extract is extracted via an enfleurage technique.

    19. The composition of claim 1, further comprising a pH-modifying component for establishing or changing a pH level of a solution into which the composition is placed.

    20. The composition of claim 19, wherein the pH-modifying component comprises a buffering agent.

    Description

    DETAILED DESCRIPTION

    [0016] According to one contemplated embodiment of the present disclosure, it is contemplated that an aqueous extract of C. ternatea flower may be stabilized in solution via the addition of one or more of: Ethanol, Glycerine, Propylene Glycol, Sodium Benzoate, Potassium Sorbate and/or food grade acids, Sugar, or via adjusting the pH content. In one embodiment, the aqueous extract of C. ternatea flower may be stabilized via placement into an 11% ethanol solution. It may also be seen that in other embodiments, the aqueous extract of C. ternatea flower may be stabilized via placement in a minimum 51% glycerine solution or a minimum 20% propylene glycol solution.

    [0017] According to other embodiments, it is contemplated that an aqueous extract of C. ternatea flowers may be stabilized in a powder or other solid form via known techniques, such as partial evaporation of the aqueous solvent and subsequent dehydration or crystallization. According to various embodiments, it is contemplated that the processes for dehydration may include the addition of one or more saccharides such as dextrose or maltodextrin, which may serve various purposes, including but not limited to a filler-binder for the resulting powder or solid, or to aid in heterogeneous nucleation of the components of the aqueous extract of C. ternatea.

    [0018] According to further embodiments, it is contemplated that extraction of the botanical extract from C. ternatea flowers may not necessarily be via an aqueous solvent process, but may be performed according to other known methods of extraction, including via other polar solvents than water, via nonpolar solvents, via combinations of polar and nonpolar solvents, or via other known extraction processes other than solvent extraction for extracting botanical extracts, including but not limited to distillation, supercritical fluid extraction, expression, or enfleurage techniques.

    [0019] It may additionally be seen that the C. ternatea flower extract may be standardized across batches via adjustment of a number of factors, including adjustment of the amounts of the individual extract components, adjusting the temperature at which extraction is performed, adjustment of the pH of the extract in solution, or other methods.

    [0020] It may further be seen that the C. ternatea flower extract may be compounded with other substances, including but not limited to extracts of other botanical substances. For example, it is contemplated that according to certain embodiments, the C. ternatea flower extract may be compounded with, for example, beta-carotene or beta-carotene-containing botanical extracts, turmeric extracts, or annatto extracts. It may further be seen that compounding of C. ternatea flower extracts with these aforementioned compounds or botanical extracts, and other compounds or botanical extracts, may impart or change various properties of the resulting C. ternatea flower extract-containing compositions from those understood to be present in a pure conventional C. ternatea flower extract. Such imparted or changed properties may include the colorant properties, the flavor properties, and the medicinal properties, among other properties. For example, it may be seen that the interplay between the pigmentation properties of the various components of a mixed C. ternatea flower extract-containing compositions may result in changes from the conventional C. ternatea flower extract color properties, both when held at constant pH levels and when the pH levels are altered.

    [0021] According to one exemplary process for recovering the natural blue color from C. Ternatea, an extraction from the fresh or dried flowers (biomass) may be performed whereby the biomass is placed in contact with water, preferably at elevated temperature, to allow the color to dissolve away from the biomass and separate into the water. The biomass is separated from the solvent by physical means, and the solvent containing the color may be further processed to concentrate and stabilize the color. A counter current extraction may be performed where portions of fresh solvent are placed in contact with the biomass until most of the available color is removed. These washes may be recycled onto a fresh batch of the biomass to increase the concentration of the color in the individual wash portions, or the wash portions may be combined and some of the solvent removed via distillation to concentrate the color.

    [0022] A preferred method of accomplishing such a current extraction is to use a vacuum soxhlet type extractor where the biomass is held in a porous container and fresh solvent (which in the preferred method is water) is distilled from the solvent reservoir, condensed above the porous container, and allowed to flow through the biomass before returning via a siphon to the solvent reservoir. This process allows exhaustive extraction of the biomass with smaller amounts of solvent, effectively concentrating the coloring material in the solvent. The use of a vacuum soxhlet extractor has the added advantage of minimizing exposure to heat, which can cause degradation of the color, while effectively concentrating the color from the biomass.

    [0023] Water may be an effective solvent for the removal of the blue color from C. Ternatea, and indeed may be the preferred solvent where final application of the color is in foods and beverages, but it is not the only solvent that can be used. Other polar solvents, alone or in combinations, may be used.

    [0024] A further advantage of a C. Ternatea extract is that it can be used in combination with natural yellow colorants (which may include turmeric extract, beta carotene, safflower extract, lutein, Marigold Extract, saffron extract, yellow gardenia and other permitted food colorants) to obtain various shades of green. Food and beverage manufacturers today are driven to replace synthetic colors with naturally derived food colorants. The most available natural green color is Chlorophyll, which is difficult to use in many applications due to stability issues related to pH, heat exposure, and light exposure. It is also known to give less vivid green colors.

    [0025] Green colors based on C. Ternatea L. extract may be formulated which have advantages over Chlorophyll-based colors regarding heat and light stability. They may also be less susceptible to pH stability issues than Chlorophyll. Finally, they may produce more vivid shades of green depending on the application conditions.