Filling device and use thereof for dispensing a fluid

Abstract

The invention relates to a filling device (1) for dispensing a fluid into at least one container, where the filling device (1) has a weighing system (2) and a filling-needle system (3). The weighing system (2) has a positioning device (4) which can be adapted to a container diameter and which may have an annular design. The weighing system (2) is arranged on an accommodation platform (7) which can be moved vertically by means of a linear unit. The filling-needle system (3) is arranged on a displacement unit in a position at a distance in the axial direction above the positioning device (4).

Claims

1. A filling device (1) for dispensing a fluid into at least one container, comprising a weighing scale (2), which has at least one container positioning receptacle (4) which is adapted to a container diameter, where the weighing scale (2) is arranged on an accommodation platform (7) which is movable vertically along a linear track (6) and where a filling-needle (3) is arranged on a displacement block (8) in a position at a distance in the axial direction above the positioning receptacle (4).

2. The filling device (1) according to claim 1, comprising two or more weighing scales (2), where the weighing scales (2) are each arranged on an accommodation platform (7) which is movable vertically by, in each case, one linear track (6).

3. The filling device (1) according to claim 1, wherein the filling-needle (3) is present in combination with an inertisation needle (12).

4. The filling device (1) according to claim 1, wherein the filling-needle (3) is arranged in a clamping block (13) which is removable from the displacement block (8).

5. The filling device (1) according to claim 1, wherein components of the filling-needle (3) which may come into contact with the respective fluid used during the filling operation consist of stainless steel and/or polytetrafluoroethylene (PTFE).

6. The filling device (1) according to claim 1, wherein a membrane valve is installed upstream of the filling-needle (3).

7. The filling device (1) according to claim 6, wherein a filter unit (9) is installed upstream of the membrane valve.

8. The filling device (1) according to claim 1, wherein ionisers are present laterally, above and/or below the filling-needle (3) and are capable of emitting a directed stream of ionised air against the filling-needle (3).

9. The filling device (1) according to claim 1, wherein protective walls (16) having an antistatic coating are arranged laterally to the filling-needle (3).

10. The filling device (1) according to claim 1, wherein the positioning receptacle (4) has an annular shape.

11. The filling device (1) according to claim 1, further comprising a drop-catching vessel (5), which is attached to a swivel arm, and which vessel is capable of being swiveled beneath the filling-needle (3) if no container is located in the positioning receptacle (4) or after the filling operation is complete.

12. A method for dispensing a fluid into at least one container, comprising dispensing said fluid into the at least one container by the filling device (1) according to claim 1.

13. A method for dispensing a liquid-crystal mixture, comprising dispensing said liquid-crystal mixture by the filling device (1) according to claim 1.

14. The method according to claim 12, which is carried out in a clean room.

15. The method according to claim 13, which is carried out in a clean room.

Description

BRIEF DESCRIPTION OF DRAWINGS

(1) FIG. 1 shows an illustrative depiction of a filling device according to the invention, and

(2) FIG. 2 shows an illustrative depiction of a filling-needle system for the filling device shown in FIG. 1.

(3) FIG. 1 shows a diagrammatic representation of a preferred filling device 1. The filling device 1 comprises two separate weighing systems 2, two filling-needle systems 3, two positioning devices 4 which can be adapted to a container diameter, and two drop-catching systems 5.

(4) The container positioning device 4 has an annular design and has bulges of different size, so that containers having different sizes or diameters can be introduced and fixed reliably in the respective positioning device.

(5) In order to enable the two weighing systems 2 to be moved vertically, the two weighing systems 2 are arranged on an accommodation platform 7 which can be moved vertically by means of a linear unit 6. The two weighing systems 2 can be adapted uniformly to different container sizes by means of the common accommodation platform 7, where automatic or manual displacement of the accommodation platform 7 can take place.

(6) In the case where a plurality of containers of different size are to be filled independently of one another and if possible simultaneously with one or more fluids, each weighing system 2 could, contrary to the illustrative variant depicted by way of example, be arranged on an assigned accommodation platform 7 each, where the accommodation tables 7 can be moved vertically independently of one another by means of in each case one linear unit 6. This enables the accommodation tables 7 to be moved into different positions, enabling the filling of different container sizes.

(7) The filling-needle systems 3 are each arranged in a position at a distance in the axial direction above the positioning devices 4 on a displacement unit 8 which can be moved horizontally. This enables each filling-needle system 3 and the assigned weighing system 2 to be adapted to different container sizes. The adjustment of the filling-needle system 3 takes place via a fine adjustment which enables horizontal displacement of the system 3 in the X and Z directions. Simultaneous horizontal and vertical movability of the filling-needle system 3 may optionally also be provided. It has been found that this enables it to be ensured that the filling-needle system 3 penetrates to an optimum extent into the opening of a container and efficient and lossfree filling is possible.

(8) In order to prevent fluid residues dripping out of the filling-needle system 3 onto the weighing system 2 after filling of a container, the drop-catching system 5, which is attached to a swivel arm and includes a vessel, can advantageously be swivelled beneath the associated filling-needle system 3 after filling. It can thus be ensured that the weighing system 2 is not contaminated by fluid residues and the weighing of a current or future filling operation is thereby falsified. The drop-catching system 5 may of course also be designed in such a way that it swivels automatically beneath the filling-needle system 3 as soon as or if no container is located in the positioning device 4.

(9) Before filling of a container located in the positioning device 4, the fluid to be dispensed is advantageously purified using a filter unit 9. The filter unit 9, preferably an ultrafine filter, can be mounted on the side of the filling device 1 in a filter holder 10. The filter unit 9 can be prepared before beginning the filling and inserted rapidly into the filter holder 10, in particular via clamp connections.

(10) Different properties of the fluids and in particular liquid-crystal mixtures to be dispensed require adaptation of the filling to the differing properties of the fluids in question. The specific filling parameters, such as, for example, adjustment of the weighing system, the container size, a filling speed and optionally ionisation, can be determined in advance and stored in a database. During initialisation of the filling device, these parameters can be input into the filling device 1, for example via a touch-screen monitor 11. The filling device 1 subsequently automatically adjusts all relevant parameters correspondingly. However, it may also be advantageous for the product-specific data to be input via a reader, for example a barcode reader (not depicted), from a barcode on documents accompanying the batch, on containers to be filled or on a storage container of the fluid to be dispensed. The barcode reader can thus be an advantageous supplement of the filling device 1 and may be connected, for example, to the touch-screen monitor 11. The filling device 1 is arranged in a switching cabinet 15, which also accommodates circuitry of supply and discharge lines of the filling device 1.

(11) Side walls 16 which have an antistatic coating may be arranged laterally alongside the weighing systems 2 or alongside the filling-needle systems 3, so that electrostatic charges formed by a laminar flow of the liquid to be dispensed are prevented.

(12) FIG. 2 shows an enlarged representation of the filling-needle system 3. The filling-needle system 3 comprises a combined filling and inertisation needle 12. Filling and inertisation of a container are thus possible using the filling-needle system 3 of the filling device without the container having to be transported to a further station for this purpose.

(13) The filling-needle system 3 is fixed in a clamping block 13 and may be assembled outside the filling device 1. The clamping block 13 can be mounted on the displacement unit (not depicted in FIG. 2) using attachment means, for example screws. The installation of the filling-needle system 3 in the clamping block 13 is carried out in an advantageous manner by means of clamp connections, enabling rapid assembly and disassembly. The filling-needle system 3 may furthermore have screws 14 for the fine adjustment of the filling-needle system 3 on the displacement unit, so that the position of the combined filling and inertisation needle 12 in the opening of a container is achieved. The fine adjustment preferably enables the filling-needle system 3 and/or the clamping block 13 to be moved horizontally and/or vertically on the displacement unit.

(14) The filling device described above is particularly suitable for liquid-crystal mixtures. In particular, liquid-crystal mixtures comprising at least two organic substances, preferably mesogenic, in particular liquid-crystalline substances, are used here, where the organic substances are preferably selected from the compounds of the general formula I,

(15) ##STR00001##
in which R.sup.1 and R.sup.2 each, independently of one another, denote H, an alkyl radical having up to 15 C atoms which is unsubstituted, monosubstituted by CN or CF.sub.3 or at least monosubstituted by halogen, where, in addition, one or more CH.sub.2 groups in these radicals may be replaced by O, S,

(16) ##STR00002##
CC, CHCH, CF.sub.2O, OCF.sub.2, OCO or OCO in such a way that 0 atoms are not linked directly to one another, and one of the radicals R.sup.1 and R.sup.2 also denotes F, Cl, CN, SF.sub.5, NCS, SCN, OCN, rings A, B, C, D and E each, independently of one another, denote

(17) ##STR00003## ##STR00004## ##STR00005## r, s and t each, independently of one another, denote 0, 1, 2 or 3, where r+s+t3, Z.sup.1-4 each, independently of one another, denote COO, OCO, CF.sub.2O, OCF.sub.2, CH.sub.2O, OCH.sub.2, CH.sub.2CH.sub.2, (CH.sub.2).sub.4, CHCHCH.sub.2O, C.sub.2F.sub.4, CH.sub.2CF.sub.2, CF.sub.2CH.sub.2, CFCF, CHCF, CFCH, CHCH, CC or a single bond, and L.sup.1 and L.sup.2 each, independently of one another, denote H or F.

(18) In the case where r+s+t=0, Z.sup.1 and Z.sup.4 are preferably selected in such a way that, if they do not denote a single bond, they are not linked to one another via two O atoms.

(19) The liquid-crystal mixtures employed comprising the individual mesogenic substances may additionally also comprise one or more polymerisable compounds, so-called reactive mesogens (RMs), for example as disclosed in U.S. Pat. No. 6,861,107, in concentrations of, preferably, 0.12-5% by weight, particularly preferably 0.2-2% by weight, based on the mixture. Mixtures of this type can be used for so-called polymer stabilised VA (PS-VA) modes, negative IPS (PS-IPS) or negative FFS (PS-FFS) modes, in which polymerisation of the reactive mesogens is intended to take place in the liquid-crystalline mixture. The prerequisite for this is that the liquid-crystal mixture does not itself comprise any individual polymerisable substances.

(20) The polymerisable mesogenic or liquid-crystalline compounds, also known as reactive mesogens (RMs), are preferably selected from the compounds of the formula II
R.sup.a-A.sup.1-(Z.sup.1-A.sup.2).sub.m-R.sup.bII
in which the individual radicals have the following meanings: A.sup.1 and A.sup.2 each, independently of one another, denote an aromatic, heteroaromatic, alicyclic or heterocyclic group, preferably having 4 to 25 C atoms, which may also contain fused rings and which is optionally mono- or polysubstituted by L, Z.sup.1 on each occurrence, identically or differently, denotes O, S, CO, COO, OCO, OCOO, OCH.sub.2, CH.sub.2O, SCH.sub.2, CH.sub.2S, CF.sub.2O, OCF.sub.2, CF.sub.2S, SCF.sub.2, (CH.sub.2).sub.n, CF.sub.2CH.sub.2, CH.sub.2CF.sub.2, (CF.sub.2).sub.n, CHCH, CFCF, CC, CHCHCOO, OCOCHCH, CR.sup.0R.sup.00 or a single bond, L, R.sup.a and R.sup.b each, independently of one another, denote H, halogen, SF.sub.5, NO.sub.2, a carbon group or hydrocarbon group, where the compounds contain at least one radical L, R.sup.a and R.sup.b which denotes or contains a P-Sp-group, R.sup.0 and R.sup.00 each, independently of one another, denote H or alkyl having 1 to 12 C atoms, P denotes a polymerisable group, Sp denotes a spacer group or a single bond, m denotes 0, 1, 2, 3 or 4, n denotes 1, 2, 3 or 4.

(21) The polymerisable compounds may contain one polymerisable group (monoreactive) or two or more (di- or multireactive), preferably two, polymerisable groups.

(22) Above and below, the following meanings apply:

(23) The term mesogenic group is known to the person skilled in the art and is described in the literature, and denotes a group which, due to the anisotropy of its attracting and repelling interactions, essentially contributes to causing a liquid-crystal (LC) phase in low-molecular-weight or polymeric substances. Compounds containing mesogenic groups (mesogenic compounds) do not necessarily have to have an LC phase themselves. It is also possible for mesogenic compounds to exhibit LC phase behaviour only after mixing with other compounds and/or after polymerisation. Typical mesogenic groups are, for example, rigid rod- or disc-shaped units. An overview of the terms and definitions used in connection with mesogenic or LC compounds is given in Pure Appl. Chem. 73(5), 888 (2001) and C. Tschierske, G. Pelzl, S. Diele, Angew. Chem. 2004, 116, 6340-6368.

(24) The term spacer group, also referred to as Sp above and below, is known to the person skilled in the art and is described in the literature, see, for example, Pure Appl. Chem. 73(5), 888 (2001) and C. Tschierske, G. Pelzl, S. Diele, Angew. Chem. 2004, 116, 6340-6368. Unless indicated otherwise, the term spacer group or spacer above and below denotes a flexible group which connects the mesogenic group and the polymerisable group(s) in a polymerisable mesogenic compound (RM) to one another. Sp preferably denotes a single bond or a 1-16 C alkylene, in which one or more CH.sub.2 groups may be replaced by O, CO, COO or OCO in such a way that two O atoms are not connected directly to one another.

(25) The term organic group denotes a carbon or hydrocarbon group.

(26) The term carbon group denotes a mono- or polyvalent organic group containing at least one carbon atom which either contains no further atoms (such as, for example, CC) or optionally contains one or more further atoms, such as, for example, N, O, S, P, Si, Se, As, Te or Ge (for example carbonyl, etc.). The term hydrocarbon group denotes a carbon group which additionally contains one or more H atoms and optionally one or more heteroatoms, such as, for example, N, O, S, P, Si, Se, As, Te or Ge.

(27) Halogen denotes F, Cl, Br or I.

(28) The terms alkyl, aryl, heteroaryl, etc., also encompass polyvalent groups, for example alkylene, arylene, heteroarylene, etc.

(29) The term alkyl in this application encompasses straight-chain and branched alkyl groups having 1 to 9 carbon atoms, preferably the straight-chain groups methyl, ethyl, propyl, butyl, pentyl, hexyl, heptyl, octyl and nonyl. Groups having 1 to 5 carbon atoms are particularly preferred.

(30) The term alkenyl in this application encompasses straight-chain and branched alkenyl groups having 2 to 9 carbon atoms, preferably the straight-chain groups having 2 to 7 carbon atoms. Particularly preferred alkenyl groups are C.sub.2-C.sub.7-1E-alkenyl, C.sub.4-C.sub.7-3E-alkenyl, C.sub.5-C.sub.7-4-alkenyl, C.sub.6-C.sub.7-5-alkenyl and C.sub.7-6-alkenyl, in particular C.sub.2-C.sub.7-1E-alkenyl, C.sub.4-C.sub.7-3E-alkenyl and C.sub.5-C.sub.7-4-alkenyl. Examples of preferred alkenyl groups are vinyl, E-propenyl, 1E-butenyl, 1E-pentenyl, 1E-hex-enyl, 1E-hept-enyl, 3-butenyl, 3E-pentenyl, 3E-hexenyl, 3E-heptenyl, 4-pentenyl, 4Z-hexenyl, 4E-hexenyl, 4Z-hep-tenyl, 5-hexenyl, 6-heptenyl and the like. Groups having up to 5 carbon atoms are particularly preferred.

(31) The term fluoroalkyl in this application encompasses straight-chain groups having a terminal fluorine, i.e. fluoromethyl, 2-fluoroethyl, 3-fluoropropyl, 4-fluoro-butyl, 5-fluoro-pentyl, 6-fluorohexyl and 7-fluoroheptyl. However, other positions of the fluorine are not excluded.

(32) The term oxaalkyl or alkoxy in this application encompasses straight-chain radicals of the formula C.sub.nH.sub.2n+1O(CH.sub.2).sub.m, in which n and m each, independently of one another, denote 1 to 6. Preferably, n=1 and m=1 to 6.

(33) The term aryl denotes an aromatic carbon group or a group derived therefrom. The term heteroaryl denotes aryl in accordance with the above definition containing one or more heteroatoms.

(34) The polymerisable group P is a group which is suitable for a polymerisation reaction, such as, for example, free-radical or ionic chain polymerisation, polyaddition or polycondensation, or for a polymer-analogous reaction, for example addition or condensation onto a main polymer chain. Particular preference is given to groups for chain polymerisation, in particular those containing a CC double bond or a CC triple bond, and groups which are suitable for polymerisation with ring opening, such as, for example, oxetane or epoxide groups.

(35) The polymerisable compounds are prepared analogously to processes which are known to the person skilled in the art and are described in standard works of organic chemistry, such as, for example, in Houben-Weyl, Methoden der organischen Chemie [Methods of Organic Chemistry], Thieme-Verlag, Stuttgart.

(36) Typical and preferred reactive mesogens (RMs) are described, for example, in WO 93/22397, EP 0 261 712, DE 195 04 224, WO 95/22586, WO 97/00600, U.S. Pat. No. 5,518,652, U.S. Pat. No. 5,750,051, U.S. Pat. No. 5,770,107 and U.S. Pat. No. 6,514,578. Very particularly referred reactive mesogens are shown on Table E.

(37) The process is used for the preparation of a mixture consisting of organic compounds, one or more of which are preferably mesogenic, preferably liquid-crystalline, per se. The mesogenic compounds preferably include one or more liquid-crystalline compounds. The process product is preferably a homogeneous, liquid-crystalline mixture. In the broader sense, the process also encompasses the preparation of mixtures which consist of organic substances in the homogeneous liquid phase and comprise additives which are insoluble therein (for example small particles). The process can thus also be used for the preparation of suspension-like or emulsion-like mixtures based on a continuous homogeneous organic phase. However, process variants of this type are generally less preferred.

(38) By means of suitable additives, the liquid-crystal phases according to the invention can be modified in such a way that they can be employed in any type of LCD display that has been disclosed to date, for example, ECB, VAN, IPS, FFS, TN, TN-TFT, STN, OCB, GH, PS-IPS, PS-FFS, PS-VA or ASM-VA displays.

(39) The liquid-crystal mixtures may also comprise further additives known to the person skilled in the art and described in the literature, such as, for example, UV stabilisers, such as, for example, Tinuvin from Ciba, antioxidants, free-radical scavengers, nanoparticles, microparticles, one or more dopants, etc. For example, 0-15% of pleochroic dyes may be added, furthermore conductive salts, preferably ethyldimethyldodecylammonium 4-hexoxybenzoate, tetrabutylammonium tetraphenylboranate or complex salts of crown ethers (cf., for example, Haller et al., Mol. Cryst. Liq. Cryst. Volume 24, pages 249-258 (1973)) in order to improve the conductivity, or substances can be added in order to modify the dielectric anisotropy, the viscosity and/or the alignment of the nematic phases. Substances of this type are described, for example, in DE-A 22 09 127, 22 40 864, 23 21 632, 23 38 281, 24 50 088, 26 37 430 and 28 53 728.

(40) Suitable stabilisers and dopants which can be combined with the compounds of the formula I in the mixing container in the preparation of the liquid-crystal mixtures are indicated below in Tables C and D.

(41) The following examples are intended to explain the invention without limiting it. Above and below, percentages are percent by weight and all temperatures are indicated in degrees Celsius.

(42) Throughout the patent application, 1,4-cyclohexylene rings and 1,4-phenylene rings are depicted as follows:

(43) ##STR00006##

(44) The cyclohexylene rings are trans-1,4-cyclohexylene rings.

(45) In the present application and in the following examples, the structures of the liquid-crystal compounds are indicated by means of acronyms, with the transformation into chemical formulae taking place in accordance with Tables A and B below. All radicals C.sub.nH.sub.2n+1 and C.sub.mH.sub.2m+1 are straight-chain alkyl radicals having n and m C atoms respectively; n, m, k and z are integers and preferably denote 0, 1, 2, 3, 4, 5, 6, 7, 8, 9, 10, 11 or 12. The term (O)C.sub.mH.sub.2m+1 means OC.sub.mH.sub.2m+1 or C.sub.mH.sub.2m+1. The coding in Table B is selfevident.

(46) In Table A, only the acronym for the parent structure is indicated. In individual cases, this is followed, separated from the acronym for the parent structure by a dash, by a code for the substituents R.sup.1*, R.sup.2*, L.sup.1* and L.sup.2*:

(47) TABLE-US-00001 Code for R.sup.1*, R.sup.2*, L.sup.1*, L.sup.2*, L.sup.3* R.sup.1* R.sup.2* L.sup.1* L.sup.2* nm C.sub.nH.sub.2n+1 C.sub.mH.sub.2m+1 H H nOm C.sub.nH.sub.2n+1 OC.sub.mH.sub.2m+1 H H nO .Math. m OC.sub.nH.sub.2n+1 C.sub.mH.sub.2m+1 H H n C.sub.nH.sub.2n+1 CN H H nN .Math. F C.sub.nH.sub.2n+1 CN F H nN .Math. F .Math. C.sub.nH.sub.2n+1 CN F F F nF C.sub.nH.sub.2n+1 F H H nCl C.sub.nH.sub.2n+1 Cl H H nOF OC.sub.nH.sub.2n+1 F H H nF .Math. F C.sub.nH.sub.2n+1 F F H nF .Math. F .Math. C.sub.nH.sub.2n+1 F F F F nOCF.sub.3 C.sub.nH.sub.2n+1 OCF.sub.3 H H nOCF.sub.3 .Math. C.sub.nH.sub.2n+1 OCF.sub.3 F H F n-Vm C.sub.nH.sub.2n+1 CHCHC.sub.mH.sub.2m+1 H H nV-Vm C.sub.nH.sub.2n+1CHCH CHCHC.sub.mH.sub.2m+1 H H

(48) Preferred mesogenic or liquid-crystalline substances which are suitable for the preparation of liquid-crystal mixtures and can be used in the purification process according to the invention are listed, in particular, in Tables A and B:

(49) TABLE-US-00002 TABLE A embedded image PYP PYRP BCH 0 CBC CCH CCP CPTP CEPTP ECCP CECP EPCH PCH CH 0 PTP CCPC CP BECH EBCH CPC B FET-nF CGG CGU 0 CFU

(50) TABLE-US-00003 TABLE B embedded image APU-n-OXF ACQU-n-F CPU-n-OXF APUQU-n-F BCH-nFm CFU-n-F CBC-nmF CCP-nOCF.sub.3 CCP-nOCF.sub.3F 0 ECCP-nm CCZU-n-F ECCP-nOCF.sub.3 ECCP-nFF PGP-n-m CGU-n-F CGUQU-n-F CLUQU-n-F CDUQU-n-F CDU-n-F 0 DCU-n-F CGG-n-F CPZG-n-OT CC-nV-Vm CCP-Vn-m CCG-V-F CCP-nV-m CC-n-V embedded image CCQU-n-F CC-n-Vm 0 CPPC-nV-Vm CCQG-n-F CQU-n-F CP-1V-m CP-2V-m CP-V2-m CP-1V-N CP-V2-N CCP-nF CCP-nFF 0 BCH-nFFF CCP-nFFF BCH-nFF Dec-U-n-F CWCU-n-F CPGP-n-m CWCG-n-F GPP-n-m CCOC-n-m CPTU-n-F 0 GPTU-n-F PQU-n-F PUQU-n-F PGU-n-F CGZP-n-OT PGU-n-OXF CCGU-n-F CUQU-n-F embedded image CCCQU-n-F CPGU-n-OT 0 CPGU-n-F CVCP-1V-OT GGP-n-Cl PP-nV-Vm PP-1-nVm CWCQU-n-F PPGU-n-F PGUQU-n-F GPQU-n-F MPP-n-F 00 PGP-n-kVm 01 PP-n-kVm 02 PCH-nCl 03 GP-n-Cl 04 PCH-nF 05 PCH-n 06 PCH-nNFF 07 GGP-n-F 08 PGIGI-n-F 09 AlK-n-F 0 BCH-nm BCH-nF/CPP-n-F BCN-nm CY-n-Om/PCH-nOmFF embedded image CP(F,Cl)n-Om CP(Cl,F)-n-Om CCY-n-Om CCY-n-m CAIY-n-Om CAIY-n-m 0 CCP(Cl,F)-n-Om CCP(F,Cl)n-Om CCY-V-m CCY-Vn-m CCY-V-Om CCY-Vn-Om CCY-n-OmV CBC-nm CCP-V-m CCP-Vn-m 0 CCP-n-m/CCP-nm CPYC-n-m CYYC-n-m CCYY-n-(O)m CCY-n-O2V CY-n-m CCH-nm/CC-n-m CCH-nOm/CC-n-Om CEY-n-Om embedded image CC-n-V1 0 CY-n-OV CC-2V-V2 CVC-n-m CC-n-mV CC-n-mV1 CP-nOmFF CH-nm CEY-V-n CVY-V-n CY-V-On 0 CY-n-OC(CH.sub.3)CH.sub.2 CY-n-O1V CCN-nm CY-1V-O1V CCPC-nm CCY-n-zOm CPY-n-m CPY-n-Om CPY-V-Om CPP(Cl,F)-n-(O)m 0 CPY-1V-Om CQY-n-(O)m CPP(F,Cl)n-(O)m CQIY-n-(O)m CCQY-n-(O)m embedded image CCQIY-n-(O)m CPQY-n-(O)m CPQIY-n-(O)m CPYG-n-(O)m CCY-V-Om 0 D-nOmFF MEnNF CY-nV-Om PCH-nm/CP-n-m CY-zVn-Om PY-zVn-Om PY-V-Om PY-1V-Om PCH-nOm/CP-n-Om DPGU-n-F 0 DPGU-n-OT PP-n-m PYP-n-mV CYLI-n-m CENap-n-Om LY-n-(O)m CCNap-n-Om CNap-n-Om YPY-n-mV CETNap-n-Om 0 CTNap-n-Om embedded image CK-n-F YPY-n-m LYLI-n-m C-DFDBF-n-(O)m B-nO-Om CPYG-n-(O)m DFDBC-n(O)-(O)m CCY-V2-(O)m CCY-1V2-(O)m 00 CCY-3V-(O)m 01 PYP-nF 02 MUQU-n-F 03 NUQU-n-F 04 COChrom-n-Om 05 COChrom-n-m 06 CCOChrom-n-Om 07 CCOChrom-n-m 08 CONaph-n-Om 09 CCONaph-n-Om 0 CLY-n-Om CLY-n-m LYLI-n-m CYLI-n-m embedded image LY-n-(O)m COYOICC-n-m COYOIC-n-V CCOY-V-O2V CCOY-V-O3V COY-n-Om 0 CCOY-n-Om PGIY-n-Om PYP-n-m PYP-n-Om YPY-n-m YPY-n-mV Y-nO-Om Y-n-Om PY-n-m PY-n-Om 0 PY-V2-Om C-DFDBF-n-(O)m DFDBC-n(O)-(O)m DFDBC-n(O)-(O)m CPU-n-VT CPU-n-AT DGUQU-n-F C-n-V C-n-XF C-n-m 0 CC-n-2V1 embedded image CCVC-n-V DPGU-n-OT PTP-nOm PTP-nm CPTP-nOm PTP-nOmFF CPTP-nOmFF CPTP-n-m PPTUI-n-m (n = 1-15; (O)C.sub.nH.sub.2n+1 means C.sub.nH.sub.2n+1 or OC.sub.nH.sub.2n+1)

(51) Particular preference is given to liquid-crystalline mixtures which comprise at least one, two, three, four or more compounds from Table B besides one or more compounds of the formula I.

(52) TABLE-US-00004 TABLE C Table C indicates possible dopants, which are generally added to the liquid-crystalline mixtures. The mixtures preferably comprise 0-10% by weight, in particular 0.01-5% by weight and particularly preferably 0.01-3% by weight, of dopants. 0 embedded image C 15 CB 15 CM 21 R/S-811 CM 44 CM 45 CM 47 CN R/S-2011 R/S-3011 0 R/S-4011 R/S-5011 R/S-1011

(53) Stabilisers, which can be added, for example, to the liquid-crystalline mixtures in amounts of 0-10% by weight, are shown below.

(54) TABLE-US-00005 TABLE D Stabilizers, which can be added, for example, to the liquid-crystalline mixtures in amounts of 0-10% by weight, are shown below. embedded image n = 1, 2, 3, 4, 5, 6 or 7 n = 1, 2, 3, 4, 5, 6 or 7 n = 1, 2, 3, 4, 5, 6 or 7 0 0 0 00 (n = 1-12)

(55) Suitable polymerisable compounds (reactive mesogens) for use in the mixtures according to the invention, preferably in PSA and PS-VA applications or PS-IPS/FFS applications, are shown below in Table E:

(56) TABLE-US-00006 TABLE E Table E shows example compounds which can preferably be used as reactive mesogenic compounds in the liquid-crystalline mixtures according to the invention. If the liquid-crystalline mixtures comprise one or more reactive compounds, they are preferably employed in amounts of 0.01-5% by weight. It may be necessary also to add an initiator or a mixture of two or more initiators for the polymerisation. The initiator or the initiator mixture is preferably added in amounts of 0.001-2% by weight, based on the mixture. A suitable initiator is, for example, Irgacure (BASF) or Irganox (BASF). 01 embedded image RM-1 02 RM-2 03 RM-3 04 RM-4 05 RM-5 06 RM-6 07 RM-7 08 RM-8 09 RM-9 0 RM-10 RM-11 RM-12 RM-13 RM-14 RM-15 RM-16 RM-17 RM-18 RM-19 0 RM-20 RM-21 RM-22 RM-23 RM-24 RM-25 RM-26 RM-27 RM-28 RM-29 0 RM-30 RM-31 RM-32 RM-33 RM-34 RM-35 RM-36 RM-37 RM-38 RM-39 0 RM-40 embedded image RM-41 RM-42 RM-43 RM-44 RM-45 RM-46 RM-47 RM-48 RM-49 0 RM-50 RM-51 RM-52 RM-53 RM-54 RM-55 RM-56 RM-57 RM-58 RM-59 0 RM-60 RM-61 RM-62 RM-63 RM-64 RM-65 RM-66 RM-67 RM-68 RM-69 0 RM-70 RM-71 RM-72 RM-73 RM-74 RM-75 RM-76 RM-77 RM-78 RM-79 0 RM-80 RM-81 embedded image RM-82 RM-83 RM-84 RM-85 RM-86 RM-87 RM-88 RM-89 0 RM-90 RM-91 RM-92 RM-93 RM-94 RM-95

(57) Table E shows example compounds which can preferably be used as reactive mesogenic compounds in the liquid-crystalline mixtures according to the invention. If the liquid-crystalline mixtures comprise one or more reactive compounds, they are preferably employed in amounts of 0.01-5% by weight. It may be necessary also to add an initiator or a mixture of two or more initiators for the polymerisation. The initiator or the initiator mixture is preferably added in amounts of 0.001-2% by weight, based on the mixture. A suitable initiator is, for example, Irgacure (BASF) or Irganox (BASF).

(58) In a preferred embodiment, the liquid-crystalline mixtures comprise one or more compounds selected from the group of the compounds from Table E.

EXAMPLES

(59) The following working examples are intended to explain the invention without restricting it.

(60) Above and below, percent data denote percent by weight. All temperatures are indicated in degrees Celsius. m.p. denotes melting point, cl.p.=clearing point. Furthermore, C=crystalline state, N=nematic phase, S=smectic phase and I=isotropic phase. The data between these symbols represent the transition temperatures. Furthermore, V.sub.o denotes threshold voltage, capacitive [V] at 20 C. n denotes the optical anisotropy measured at 20 C. and 589 nm denotes the dielectric anisotropy at 20 C. and 1 kHz cl.p. denotes clearing point [ C.] K.sub.1 denotes elastic constant, splay deformation at 20 C., [pN] K.sub.3 denotes elastic constant, bend deformation at 20 C., [pN] .sub.1 denotes rotational viscosity measured at 20 C. [mPa.Math.s], determined by the rotation method in a magnetic field LTS denotes low-temperature stability (nematic phase), determined in test cells.

(61) The following examples are intended to explain the invention without limiting it.

(62) Above and below, percentages are percent by weight. All temperatures are indicated in degrees Celsius.

Working Examples

Example 1

(63) A liquid-crystalline mixture, preferably for PS-VA applications, of the composition

(64) TABLE-US-00007 CCH-35 9.47% CCH-501 4.99% CCY-2-1 9.47% CCY-3-1 10.47% CCY-3-O2 10.47% CCY-5-O2 9.47% CPY-2-O2 11.96% CY-3-O4 8.97% CY-5-O4 10.97% RM-1 0.30% PCH-53 13.46%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 2

(65) A liquid-crystalline mixture, preferably for PS-VA applications, of the composition

(66) TABLE-US-00008 BCH-32 7.48% CCH-23 21.93% CCH-34 3.49% CCY-3-O3 6.98% CCY-4-O2 7.98% CPY-2-O2 10.97% CPY-3-O2 10.97% CY-3-O2 15.45% RM-1 0.30% PCH-301 12.46% PCH-302 1.99%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 3

(67) A liquid-crystalline mixture, preferably for PS-VA applications, of the composition

(68) TABLE-US-00009 CC-3-V1 7.98% CCH-23 17.95% CCH-34 3.99% CCH-35 6.98% CCP-3-1 4.99% CCY-3-O2 12.46% CPY-2-O2 7.98% CPY-3-O2 10.97% CY-3-O2 15.45% RM-1 0.30% PY-3-O2 10.97%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 4

(69) A liquid-crystalline mixture, preferably for PS-VA applications, of the composition

(70) TABLE-US-00010 CC-3-V1 8.97% CCH-23 12.96% CCH-34 6.23% CCH-35 7.73% CCP-3-1 3.49% CCY-3-O2 12.21% CPY-2-O2 6.73% CPY-3-O2 11.96% CY-3-O2 11.47% RM-1 0.30% PP-1-2V1 4.24% PY-3-O2 13.71%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 5

(71) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(72) TABLE-US-00011 CBC-33 3.50% CC-3-V 38.00% CC-3-V1 10.00% CCP-V-1 3.00% CCP-V2-1 9.00% PGP-2-3 5.00% PGP-2-4 5.00% PGU-2-F 8.00% PGU-3-F 9.00% PUQU-3-F 9.50%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 6

(73) A liquid-crystalline mixture, preferably for IPS or FFS applications, of the composition

(74) TABLE-US-00012 APUQU-3-F 4.50% CC-3-V 44.00% CC-3-V1 12.00% CCP-V-1 11.00% CCP-V2-1 9.00% PGP-2-3 6.00% PGUQU-3-F 6.00% PP-1-2V1 7.00% PPGU-3-F 0.50%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 7

(75) A liquid-crystalline mixture, preferably for IPS or FFS applications, of the composition

(76) TABLE-US-00013 APUQU-3-F 8.00% CBC-33 3.00% CC-3-V 34.00% CC-3-V1 2.50% CCGU-3-F 4.00% CCP-30CF.sub.3 4.00% CCP-3F.F.F 4.50% CCP-50CF.sub.3 3.00% CCP-V-1 10.00% CCQU-3-F 10.00% CPGU-3-OT 6.00% PGUQU-3-F 4.00% PUQU-3-F 7.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 8

(77) A liquid-crystalline mixture, preferably for IPS or FFS applications, of the composition

(78) TABLE-US-00014 APUQU-2-F 5.00% APUQU-3-F 7.50% BCH-3F.F.F 7.00% CC-3-V 40.50% CC-3-V1 6.00% CCP-V-1 9.50% CPGU-3-OT 5.00% PGP-2-3 6.00% PGP-2-4 6.00% PPGU-3-F 0.50% PUQU-3-F 7.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 9

(79) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(80) TABLE-US-00015 APUQU-2-F 8.00% APUQU-3-F 8.00% BCH-32 7.00% CC-3-V 43.00% CCP-V-1 9.00% PGP-2-3 7.00% PGP-2-4 6.00% PUQU-2-F 5.00% PUQU-3-F 7.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 10

(81) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(82) TABLE-US-00016 BCH-5F.F 8.00% CBC-33F 3.00% CC-3-V 22.00% CCGU-3-F 6.00% CCP-3F.F.F 8.00% CCP-5F.F.F 4.00% CCP-V-1 13.00% CCP-V2-1 11.00% CCQU-3-F 5.00% CCQU-5-F 4.00% PUQU-3-F 16.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 11

(83) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(84) TABLE-US-00017 CBC-33F 3.00% CBC-53F 3.00% CC-3-V 17.00% CC-3-V1 4.00% CCP-3F.F.F 8.00% CCPC-33 3.00% CCPC-34 3.00% CCP-V-1 5.00% CCP-V2-1 2.00% CCQU-2-F 1.50% CCQU-3-F 10.00% CCQU-5-F 10.00% CGU-3-F 6.00% PGP-2-3 7.50% PP-1-2V1 7.00% PUQU-3-F 10.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 12

(85) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(86) TABLE-US-00018 APUQU-2-F 1.00% BCH-3F.F.F 15.00% CC-3-V 33.50% CC-3-V1 2.00% CCGU-3-F 1.00% CCPC-33 2.00% CCP-V-1 4.50% BCH-2F 5.00% BCH-3F 5.00% PGP-2-3 8.50% PGUQU-3-F 7.80% PP-1-2V1 11.00% PPGU-3-F 0.20% PUQU-3-F 3.50%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 13

(87) A liquid-crystalline mixture, preferably for IPS or FFS applications, of the composition

(88) TABLE-US-00019 APUQU-2-F 2.00% APUQU-3-F 6.00% CC-3-V 42.00% CCP-3-1 3.00% CCP-3-3 3.00% CCP-3F.F.F 8.00% CCP-V-1 1.50% CCQU-3-F 7.00% CCQU-5-F 3.00% CPGU-3-OT 6.50% PGUQU-3-F 5.00% PGUQU-4-F 4.00% PGUQU-5-F 4.00% PPGU-3-F 0.50% PUQU-3-F 4.50%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 14

(89) A liquid-crystalline mixture, preferably for TN-TFT applications, of the composition

(90) TABLE-US-00020 CC-3-V 49.50% CCP-3-1 1.50% CCP-V-1 6.00% CPGU-3-OT 7.00% PGP-2-3 8.50% PGP-2-4 5.50% PGUQU-3-F 7.00% PGUQU-4-F 4.00% PP-1-2V1 2.50% PPGU-3-F 0.50% PUQU-3-F 8.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 15

(91) A liquid-crystalline mixture, preferably for VA applications, of the composition

(92) TABLE-US-00021 BCH-32 6.00% CCH-23 18.00% CCH-34 8.00% CCP-3-1 12.00% CCP-3-3 3.00% CCY-3-O2 6.00% CPY-2-O2 6.00% CPY-3-O2 7.00% CY-3-O2 14.00% CY-3-O4 8.00% CY-5-O2 9.00% PYP-2-3 3.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 16

(93) A liquid-crystalline mixture, preferably for PS-VA applications, of the composition

(94) TABLE-US-00022 CC-3-V1 7.98% CCH-23 17.95% CCH-34 3.99% CCH-35 6.98% CCP-3-1 4.99% CCY-3-O2 12.46% CPY-2-O2 7.98% CPY-3-O2 10.97% CY-3-O2 15.45% RM-17 0.30% PY-3-O2 10.97%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

Example 17

(95) A liquid-crystalline mixture, preferably for VA applications, of the composition

(96) TABLE-US-00023 CC-3-V 29.50% PP-1-3 11.00% PY-3-O2 12.00% CCP-3-1 9.50% CCOY-2-O2 18.00% CCOY-3-O2 13.00% GPP-5-2 7.00%
is dispensed into a container using the filling device described in FIG. 1 and FIG. 2.

(97) Mixture Examples 1 to 17 may additionally also comprise one or more, preferably one or two, stabiliser(s) and/or a dopant from Tables C and D.

(98) The liquid-crystal mixtures of Examples 18-168 shown below are dispensed into a container analogously using the filling device described in FIG. 1 and FIG. 2.

Example 18

(99) TABLE-US-00024 CCY-3-O1 7.50% Clearing point [ C.]: 81.5 CCY-4-O2 3.50% n [589 nm, 20 C.]: 0.1082 CLY-3-O2 7.00% [1 kHz, 20 C.]: 2.7 CPY-2-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.4 CPY-3-O2 10.00% .sub. [1 kHz, 20 C.] 6.1 PYP-2-3 9.00% .sub.1 [mPa .Math. s, 20 C.]: 88 CC-3-V 45.00% K.sub.1 [pN, 20 C.]: 13.4 PY-1-O4 4.00% K.sub.3 [pN, 20 C.]: 15.3 PY-3-O2 2.00% V.sub.0 [20 C., V]: 2.53 Y-4O-O4 2.00%

Example 19

(100) TABLE-US-00025 CCY-3-O1 7.50% Clearing point [ C.]: 81 CCY-4-O2 5.00% n [589 nm, 20 C.]: 0.1054 CLY-3-O2 7.00% [1 kHz, 20 C.]: 2.6 CPY-2-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.4 CPY-3-O2 8.50% .sub. [1 kHz, 20 C.]: 6.0 PYP-2-3 9.00% .sub.1 [mPa .Math. s, 20 C.]: 86 CC-3-V 45.50% K.sub.1 [pN, 20 C.]: 13.3 PY-1-O4 5.00% K.sub.3 [pN, 20 C.]: 15.1 Y-4O-O4 2.50% V.sub.0 [20 C., V]: 2.54

Example 20

(101) TABLE-US-00026 CC-3-2V1 4.00% Clearing point [ C.]: 100 CC-3-V 37.50% n [589 nm, 20 C.]: 0.1047 CC-3-V1 5.00% [1 kHz, 20 C.]: 3.9 CCP-V-1 13.00% .sub.|| [1 kHz, 20 C.]: 6.6 CCP-V2-1 7.50% .sub. [1 kHz, 20 C.]: 2.7 CCVC-3-V 6.00% .sub.1 [mPa .Math. s, 20 C.]: 72 CDUQU-3-F 1.00% K.sub.1 [pN, 20 C.]: 15.1 CPGP-5-2 3.00% K.sub.3 [pN, 20 C.]: 17.4 DGUQU-4-F 2.00% V.sub.0 [20 C., V]: 2.07 PGP-2-3 5.00% PGP-2-4 3.00% PGUQU-3-F 4.00% PGUQU-4-F 3.50% PPGU-3F 0.50% PUQU-3F 5.00%

Example 21

(102) TABLE-US-00027 APUQU-2-F 1.50% Clearing point [ C.]: 100 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1056 CC-3-2V1 4.00% [1 kHz, 20 C.]: 4.0 CC-3-V 36.00% .sub.|| [1 kHz, 20 C.]: 6.8 CC-3-V1 5.00% .sub. [1 kHz, 20 C.]: 2.8 CCP-V-1 13.00% .sub.1 [mPa .Math. s, 20 C.]: 71 CCP-V2-1 9.50% K.sub.1 [pN, 20 C.]: 15.4 CCVC-3-V 4.00% K.sub.3 [pN, 20 C.]: 17.7 CDUQU-3-F 3.00% V.sub.0 [20 C., V]: 2.07 DGUQU-4-F 2.00% PGP-1-2V 5.50% PGP-2-2V 7.00% PPGU-3-F 0.50% PUQU-3-F 4.00%

Example 22

(103) TABLE-US-00028 CC-3-V1 9.00% Clearing point [ C.]: 74.7 CCH-23 18.00% n [589 nm, 20 C.]: 0.0982 CCH-34 3.00% [1 kHz, 20 C.]: 3.4 CCH-35 7.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCP-3-1 5.50% .sub. [1 kHz, 20 C.]: 6.9 CCY-3-O2 11.50% .sub.1 [mPa .Math. s, 20 C.]: 108 CPY-2-O2 8.00% K.sub.1 [pN, 20 C.]: 14.9 CPY-3-O2 11.00% K.sub.3 [pN, 20 C.]: 15.9 CY-3-O2 15.50% V.sub.0 [20 C., V]: 2.28 PY-3-O2 11.50%

Example 22a

(104) The mixture from Example 22 is additionally mixed with 0.001% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.45% of RM-1.

Example 23

(105) TABLE-US-00029 CC-3-V 15.00% Clearing point [ C.]: 85 CPGP-4-3 2.00% n [589 nm, 20 C.]: 0.1981 CPGP-5-2 2.00% [1 kHz, 20 C.]: 9.9 CPTP-301 6.00% .sub.|| [1 kHz, 20 C.]: 13.6 DGUQU-4-F 3.00% .sub. [1 kHz, 20 C.]: 3.7 PCH-301 7.00% .sub.1 [mPa .Math. s, 20 C.]: 123 PGP-2-2V 14.50% K.sub.1 [pN, 20 C.]: 15.1 PGUQU-3-F 7.50% K.sub.3 [pN, 20 C.]: 15.1 PGUQU-4-F 7.00% V.sub.0 [20 C., V]: 1.29 PGUQU-5-F 6.00% PP-1-2V1 12.00% PTP-102 6.00% PTP-201 6.00% PUQU-3-F 6.00%

Example 24

(106) TABLE-US-00030 CC-3-V 28.00% Clearing point [ C.]: 84.8 CC-3-V1 3.00% n [589 nm, 20 C.]: 0.1078 CCP-3-1 3.00% [1 kHz, 20 C.]: 4.1 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-4-O2 9.00% .sub. [1 kHz, 20 C.]: 7.8 CLY-3-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 122 CLY-3-O3 6.00% K.sub.1 [pN, 20 C.]: 14.8 CPY-2-O2 7.00% CPY-3-O2 9.00% PY-3-O2 8.00% PY-4-O2 4.00% PYP-2-4 2.50% Y-4O-O4 5.50%

Example 24a

(107) The mixture from Example 24 is additionally stabilised with

(108) 0.04% of

(109) ##STR00396##
and
0.01% of

(110) ##STR00397##

Example 25

(111) TABLE-US-00031 CC-3-V 28.00% Clearing point [ C.]: 80 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1082 CCP-3-1 2.50% [1 kHz, 20 C.]: 4.1 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.8 CCY-4-O2 2.50% .sub. [1 kHz, 20 C.]: 7.9 CLY-3-O2 6.50% .sub.1 [mPa .Math. s, 20 C.]: 113 CLY-3-O3 6.50% K.sub.1 [pN, 20 C.]: 14.5 CPY-2-O2 9.00% CPY-3-O2 10.00% PY-3-O2 10.00% PY-4-O2 5.00% Y-4O-O4 5.00%

Example 25a

(112) The mixture from Example 25 is additionally stabilised with

(113) 0.04% of

(114) ##STR00398##
and
0.01% of

(115) ##STR00399##

Example 26

(116) TABLE-US-00032 CC-3-V 29.00% Clearing point [ C.]: 75.1 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1075 CCP-3-1 3.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.8 CLY-3-O2 6.00% .sub. [1 kHz, 20 C.]: 7.7 CLY-3-O3 6.00% .sub.1 [mPa .Math. s, 20 C.]: 103 CPY-2-O2 9.00% K.sub.1 [pN, 20 C.]: 14.3 CPY-3-O2 10.00% PY-3-O2 10.00% PY-4-O2 7.00% Y-4O-O4 5.00%

Example 26a

(117) The mixture from Example 26 is additionally stabilised with

(118) 0.04% of

(119) ##STR00400##
and
0.015% of

(120) ##STR00401##

Example 27

(121) TABLE-US-00033 CC-3-V 29.00% Clearing point [ C.]: 80.1 CCY-3-O1 8.00% n [589 nm, 20 C.]: 0.1052 CCY-3-O2 6.00% [1 kHz, 20 C.]: 4.7 CCY-4-O2 2.00% .sub.|| [1 kHz, 20 C.]: 3.9 CLY-3-O2 8.50% .sub. [1 kHz, 20 C.]: 8.7 CLY-3-O3 7.50% .sub.1 [mPa .Math. s, 20 C.]: 125 CPY-2-O2 10.00% K.sub.1 [pN, 20 C.]: 14.0 CPY-3-O2 7.50% CY-3-O2 6.50% PY-3-O2 10.00% Y-4O-O4 5.00%

Example 27a

(122) The mixture from Example 27 is additionally stabilised with

(123) 0.04% of

(124) ##STR00402##
and
0.02% of

(125) ##STR00403##

Example 28

(126) TABLE-US-00034 CC-3-V 37.00% Clearing point [ C.]: 75.2 CCY-3-O1 5.00% n [589 nm, 20 C.]: 0.1012 CCY-3-O2 5.00% [1 kHz, 20 C.]: 3.8 CCY-4-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.6 CLY-3-O2 7.00% .sub. [1 kHz, 20 C.]: 7.5 CPY-2-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 97 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 13.3 CY-3-O2 12.00% K.sub.3 [pN, 20 C.]: 15.3 PY-3-O2 11.00% V.sub.0 [20 C., V]: 2.12

Example 28a

(127) The mixture from Example 28 is additionally stabilised with

(128) 0.04% of

(129) ##STR00404##
and
0.015% of

(130) ##STR00405##

Example 29

(131) TABLE-US-00035 CY-3-O2 15.00% Clearing point [ C.]: 80.4 CY-5-O2 12.50% n [589 nm, 20 C.]: 0.1038 CCY-3-O1 2.50% [1 kHz, 20 C.]: 3.3 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 137 CCY-2-1 6.00% K.sub.1 [pN, 20 C.]: 14.2 CCY-3-1 6.00% K.sub.3 [pN, 20 C.]: 14.2 CCH-23 15.00% V.sub.0 [20 C., V]: 2.18 CCH-34 5.00% CCH-301 1.50% BCH-32 15.50%

Example 29a

(132) The mixture from Example 29 is additionally stabilised with

(133) 0.01% of

(134) ##STR00406##

Example 30

(135) TABLE-US-00036 CY-3-O2 15.00% Clearing point [ C.]: 100 CY-3-O4 20.00% n [589 nm, 20 C.]: 0.0968 CY-5-O2 7.50% [1 kHz, 20 C.]: 5.9 CCY-3-O2 6.50% .sub.|| [1 kHz, 20 C.]: 4.0 CCY-3-O3 6.50% .sub. [1 kHz, 20 C.]: 9.9 CCY-4-O2 6.50% .sub.1 [mPa .Math. s, 20 C.]: 324 CCY-5-O2 6.50% K.sub.1 [pN, 20 C.]: 15.1 CPY-2-O2 5.50% K.sub.3 [pN, 20 C.]: 17.2 CPY-3-O2 5.00% V.sub.0 [20 C., V]: 1.80 CC-4-V 3.00% CH-33 3.00% CH-35 2.00% CH-43 3.00% CH-45 2.00% CCPC-33 4.00% CCPC-34 4.00%

Example 31

(136) TABLE-US-00037 CY-3-O2 11.00% Clearing point [ C.]: 101 CY-3-O4 18.00% n [589 nm, 20 C.]: 0.1662 CCY-3-O2 6.00% [1 kHz, 20 C.]: 6.1 CCY-3-O3 6.00% .sub.|| [1 kHz, 20 C.]: 4.2 CCY-4-O2 6.00% .sub. [1 kHz, 20 C.]: 10.3 CCY-5-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 363 CPY-3-O2 6.00% K.sub.1 [pN, 20 C.]: 16.5 CC-4-V 3.00% K.sub.3 [pN, 20 C.]: 22.00 CPTP-3-1 5.00% V.sub.0 [20 C., V]: 2.00 PTP-302FF 10.00% PTP-502FF 10.00% CPTP-302FF 5.00% CPTP-502FF 5.00% CCPC-33 3.00%

Example 32

(137) TABLE-US-00038 CY-3-O2 8.00% Clearing point [ C.]: 101 CY-3-O4 13.00% n [589 nm, 20 C.]: 0.0970 CCY-3-O2 6.50% [1 kHz, 20 C.]: 2.1 CPY-2-O2 3.50% .sub.|| [1 kHz, 20 C.]: 3.2 CPY-3-O2 8.00% .sub. [1 kHz, 20 C.]: 5.3 CCH-301 5.00% .sub.1 [mPa .Math. s, 20 C.]: 136 CC-4-V 12.00% K.sub.1 [pN, 20 C.]: 14.8 CC-5-V 8.00% K.sub.3 [pN, 20 C.]: 18.3 CCP-V-1 13.00% V.sub.0 [20 C., V]: 3.11 CCP-V2-1 13.00% BCH-32 5.00% CCPC-33 5.00%

Example 33

(138) TABLE-US-00039 CY-3-O4 12.00% Clearing point [ C.]: 101 CC-4-V 13.00% n [589 nm, 20 C.]: 0.1660 CC-5-V 9.50% [1 kHz, 20 C.]: 2.1 CCP-V-1 10.50% .sub.|| [1 kHz, 20 C.]: 3.4 CCP-V2-1 10.00% .sub. [1 kHz, 20 C.]: 5.5 PTP-102 3.00% .sub.1 [mPa .Math. s, 20 C.]: 151 CPTP-3-1 5.00% K.sub.1 [pN, 20 C.]: 16.2 CPTP-3-2 5.00% K.sub.3 [pN, 20 C.]: 19.8 PTP-302FF 9.50% V.sub.0 [20 C., V]: 3.25 PTP-502FF 9.50% CPTP-302FF 6.50% CPTP-502FF 6.50%

Example 34

(139) TABLE-US-00040 CY-3-O2 15.00% Clearing point [ C.]: 71.9 CCY-3-O1 6.00% n [589 nm, 20 C.]: 0.1203 CCY-3-O2 8.00% [1 kHz, 20 C.]: 8.1 CCY-3-O3 5.50% .sub.|| [1 kHz, 20 C.]: 5.2 CCY-4-O2 8.00% .sub. [1 kHz, 20 C.]: 13.3 CCY-5-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 253 CPY-2-O2 1.50% K.sub.1 [pN, 20 C.]: 13.2 CPY-3-O2 10.00% K.sub.3 [pN, 20 C.]: 15.7 CLY-3-O2 8.00% V.sub.0 [20 C., V]: 1.46 PY-3-O2 6.00% PY-1-O4 8.00% PY-4-O2 8.00% Y-4O-O4 8.00%

Example 35

(140) TABLE-US-00041 CC-3-V1 8.00% Clearing point [ C.]: 75.5 CCH-23 18.00% n [589 nm, 20 C.]: 0.0978 CCH-34 4.00% [1 kHz, 20 C.]: 3.5 CCH-35 7.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCP-3-1 5.00% .sub. [1 kHz, 20 C.]: 6.9 CCY-3-O2 12.50% .sub.1 [mPa .Math. s, 20 C.]: 111 CPY-2-O2 8.00% K.sub.1 [pN, 20 C.]: 14.9 CPY-3-O2 11.00% K.sub.3 [pN, 20 C.]: 15.8 CY-3-O2 15.50% V.sub.0 [20 C., V]: 2.26 PY-3-O2 11.00%

Example 35a

(141) The mixture from Example 35 is additionally mixed with 0.3% of RM-1

(142) ##STR00407##

Example 36

(143) TABLE-US-00042 BCH-32 1.50% Clearing point [ C.]: 74.8 CC-3-V 15.50% n [589 nm, 20 C.]: 0.1035 CC-3-V1 11.00% [1 kHz, 20 C.]: 3.1 CCH-23 12.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCH-34 3.50% .sub. [1 kHz, 20 C.]: 6.5 CCY-3-O2 11.50% .sub.1 [mPa .Math. s, 20 C.]: 95 CCY-5-O2 0.50% K.sub.1 [pN, 20 C.]: 14.1 CPY-2-O2 8.50% K.sub.3 [pN, 20 C.]: 15.4 CPY-3-O2 12.00% V.sub.0 [20 C., V]: 2.36 CY-3-O2 9.50% PY-3-O2 11.50% PYP-2-3 3.00%

Example 36a

(144) The mixture from Example 36 is additionally mixed with 0.001% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.

Example 37

(145) TABLE-US-00043 CC-3-V 30.50% Clearing point [ C.]: 79.8 CC-3-V1 4.50% n [589 nm, 20 C.]: 0.1022 CCY-3-O1 5.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O3 4.00% .sub. [1 kHz, 20 C.]: 7.6 CLY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 114 CPY-2-O2 8.00% K.sub.1 [pN, 20 C.]: 14.5 CPY-3-O2 11.00% K.sub.3 [pN, 20 C.]: 16.7 CY-3-O2 15.00% V.sub.0 [20 C., V]: 2.14 PY-3-O2 8.00%

Example 38

(146) TABLE-US-00044 CY-3-O2 15.00% Clearing point [ C.]: 80.4 CY-5-O2 12.50% n [589 nm, 20 C.]: 0.1038 CCY-3-O1 2.50% [1 kHz, 20 C.]: 3.3 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 137 CCY-2-1 6.00% K.sub.1 [pN, 20 C.]: 14.2 CCY-3-1 6.00% K.sub.3 [pN, 20 C.]: 14.2 CCH-23 15.00% V.sub.0 [20 C., V]: 2.18 CCH-34 5.00% CCH-301 1.50% BCH-32 15.50%

Example 39

(147) TABLE-US-00045 CY-3-O2 15.00% Clearing point [ C.]: 80.5 CY-3-O4 4.00% n [589 nm, 20 C.]: 0.1025 CY-5-O2 6.50% [1 kHz, 20 C.]: 3.4 CCY-3-O1 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-O3 2.00% .sub. [1 kHz, 20 C.]: 6.9 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 141 CPY-2-O2 7.00% K.sub.1 [pN, 20 C.]: 14.0 CPY-3-O2 7.00% K.sub.3 [pN, 20 C.]: 14.1 CCY-2-1 6.00% V.sub.0 [20 C., V]: 2.16 CCY-3-1 6.00% CCH-23 15.50% CCH-34 5.00% BCH-32 13.00% PP-1-4 2.00%

Example 40

(148) TABLE-US-00046 PGUQU-3-F 4.00% Clearing point [ C.]: 85.4 CCQU-3-F 7.50% n [589 nm, 20 C.]: 0.1028 PUQU-3-F 15.50% [1 kHz, 20 C.]: 9.9 APUQU-2-F 4.00% .sub.|| [1 kHz, 20 C.]: 13.3 APUQU-3-F 7.50% .sub. [1 kHz, 20 C.]: 3.4 CC-3-V 27.50% .sub.1 [mPa .Math. s, 20 C.]: 82 CCP-3-V1 6.00% K.sub.1 [pN, 20 C.]: 12.6 CCP-V-1 13.00% K.sub.3 [pN, 20 C.]: 15.3 CCP-V2-1 10.00% V.sub.0 [20 C., V]: 1.19 PPGU-3-F 0.50% BCH-3F.F 4.50%

Example 40a

(149) The mixture from Example 40 is additionally stabilised with

(150) 0.01% of

(151) ##STR00408##

Example 41

(152) TABLE-US-00047 CC-3-V 30.50% Clearing point [ C.]: 80.1 CC-3-V1 4.50% n [589 nm, 20 C.]: 0.1033 CCY-3-O1 6.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.6 CLY-3-O2 8.00% .sub. [1 kHz, 20 C.]: 7.6 CPY-2-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 113 CPY-3-O2 12.00% K.sub.1 [pN, 20 C.]: 14.4 CY-3-O2 15.00% K.sub.3 [pN, 20 C.]: 17.0 PY-3-O2 8.00% V.sub.0 [20 C., V]: 2.16

Example 41a

(153) The mixture from Example 41 is additionally stabilised with

(154) 0.3% of

(155) ##STR00409##

Example 42

(156) TABLE-US-00048 CC-3-V 28.50% Clearing point [ C.]: 74.6 CC-3-V1 7.00% n [589 nm, 20 C.]: 0.1040 CCY-3-O2 12.50% [1 kHz, 20 C.]: 3.0 CCY-4-O2 5.25% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-3-O2 9.75% .sub. [1 kHz, 20 C.]: 6.5 CY-3-O2 15.00% .sub.1 [mPa .Math. s, 20 C.]: 98 CY-3-O4 4.75% K.sub.1 [pN, 20 C.]: 13.2 CY-5-O2 1.00% K.sub.3 [pN, 20 C.]: 15.5 PCH-301 3.25% V.sub.0 [20 C., V]: 2.4 PPGU-3-F 0.50% PYP-2-3 12.50%

Example 42a

(157) The mixture from Example 42 is additionally mixed with 0.001% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.45% of RM-1.

Example 43

(158) TABLE-US-00049 CC-3-V 36.50% Clearing point [ C.]: 75 CC-3-V1 2.00% n [589 nm, 20 C.]: 0.1015 CCY-3-O1 8.00% [1 kHz, 20 C.]: 3.7 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-4-O2 2.50% .sub. [1 kHz, 20 C.]: 7.3 CLY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 97 CLY-3-O3 2.00% K.sub.1 [pN, 20 C.]: 13.8 CPY-2-O2 10.00% K.sub.3 [pN, 20 C.]: 15 CPY-3-O2 3.00% V.sub.0 [20 C., V]: 2.14 CY-3-O2 5.50% PY-3-O2 13.00% PY-1-O4 3.50%

Example 44

(159) TABLE-US-00050 BCH-32 4.50% Clearing point [ C.]: 75.5 CCH-23 14.00% n [589 nm, 20 C.]: 0.0938 CCH-301 7.00% [1 kHz, 20 C.]: 2.5 CCH-34 9.00% .sub.|| [1 kHz, 20 C.]: 3.3 CCH-35 5.50% .sub. [1 kHz, 20 C.]: 5.8 CCP-3-1 10.00% .sub.1 [mPa .Math. s, 20 C.]: 89 CY-3-O2 5.00% K.sub.1 [pN, 20 C.]: 13.5 CY-V-O2 7.00% K.sub.3 [pN, 20 C.]: 14.5 CCY-3-O1 5.00% V.sub.0 [20 C., V]: 2.54 CCY-3-O2 9.00% CPY-V-O2 10.00% PCH-302 5.00% PY-V2-O2 9.00%

Example 45

(160) TABLE-US-00051 BCH-32 1.50% Clearing point [ C.]: 75 CC-3-V 37.00% n [589 nm, 20 C.]: 0.0960 CCP-3-1 8.00% [1 kHz, 20 C.]: 2.6 CY-3-O2 15.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-O1 7.00% .sub. [1 kHz, 20 C.]: 6.0 CCY-3-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 79 CPY-3-O2 8.50% K.sub.1 [pN, 20 C.]: 13.0 PCH-302 5.50% K.sub.3 [pN, 20 C.]: 16.0 PY-V-O2 8.00% V.sub.0 [20 C., V]: 2.6

Example 46

(161) TABLE-US-00052 BCH-32 1.00% Clearing point [ C.]: 75 CC-3-V 41.00% n [589 nm, 20 C.]: 0.0948 CCP-3-1 8.50% [1 kHz, 20 C.]: 2.3 CY-3-O2 13.00% .sub.|| [1 kHz, 20 C.]: 3.2 CCY-3-O1 6.50% .sub. [1 kHz, 20 C.]: 5.5 CCY-3-O2 8.50% .sub.1 [mPa .Math. s, 20 C.]: 70 CPY-3-O2 6.00% K.sub.1 [pN, 20 C.]: 13.4 PCH-302 7.00% K.sub.3 [pN, 20 C.]: 16.5 PY-1V-O2 8.50% V.sub.0 [20 C., V]: 2.84

Example 47

(162) TABLE-US-00053 PY-3-O2 7.50% Clearing point [ C.]: 74 PY-1V-O2 4.00% n [589 nm, 20 C.]: 0.1094 CY-3-O2 14.50% [1 kHz, 20 C.]: 3.0 CCY-3-O1 3.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O2 9.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-2-O2 7.50% .sub.1 [mPa .Math. s, 20 C.]: 85 CPY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 12.9 CC-3-V 37.00% K.sub.3 [pN, 20 C.]: 14.6 BCH-32 8.00% V.sub.0 [20 C., V]: 2.34 PPGU-3-F 0.50%

Example 48

(163) TABLE-US-00054 PY-3-O2 8.00% Clearing point [ C.]: 74.5 PY-3V-O2 5.00% n [589 nm, 20 C.]: 0.1086 CY-3-O2 11.50% [1 kHz, 20 C.]: 3.0 CCY-3-O1 10.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O2 4.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-2-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 87 CPY-3-O2 7.00% K.sub.1 [pN, 20 C.]: 12.9 CC-3-V 37.50% K.sub.3 [pN, 20 C.]: 14.1 BCH-32 6.50% V.sub.0 [20 C., V]: 2.30 PPGU-3-F 0.50%

Example 49

(164) TABLE-US-00055 PY-V2-O2 12.00% Clearing point [ C.]: 76 CY-V-O2 9.00% n [589 nm, 20 C.]: 0.1087 CCY-3-O1 9.00% [1 kHz, 20 C.]: 3.1 CCY-V2-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 6.9 CPY-V-O2 10.50% .sub.1 [mPa .Math. s, 20 C.]: 83 CC-3-V 36.50% K.sub.1 [pN, 20 C.]: 12.4 BCH-32 6.50% K.sub.3 [pN, 20 C.]: 14.7 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.28

Example 50

(165) TABLE-US-00056 PY-V2-O2 11.50% Clearing point [ C.]: 75.5 CY-3-O2 11.00% n [589 nm, 20 C.]: 0.1074 CCY-3-O1 9.00% [1 kHz, 20 C.]: 3.1 CCY-3-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 12.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 87 CC-3-V 37.00% K.sub.1 [pN, 20 C.]: 13.0 BCH-32 6.00% K.sub.3 [pN, 20 C.]: 14.7 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.29

Example 51

(166) TABLE-US-00057 PY-1V-O2 10.50% Clearing point [ C.]: 72 CY-3-O2 18.00% n [589 nm, 20 C.]: 0.1068 CCY-3-O1 7.00% [1 kHz, 20 C.]: 3.1 CCY-3-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.6 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 6.7 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 78 CC-3-V 41.00% K.sub.1 [pN, 20 C.]: 12.6 BCH-32 3.00% K.sub.3 [pN, 20 C.]: 14.6 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.30

Example 52

(167) TABLE-US-00058 PY-V2-O2 10.50% Clearing point [ C.]: 75 CY-3-O2 10.00% n [589 nm, 20 C.]: 0.1070 CCY-3-O1 6.00% [1 kHz, 20 C.]: 3.3 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 7.0 CPY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 90 CC-3-V 35.00% K.sub.1 [pN, 20 C.]: 12.7 BCH-32 6.50% K.sub.3 [pN, 20 C.]: 14.5 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.23 Y-4O-O4 2.50% LTS (bulk) [20 C.]: >1000 h LTS (bulk) [30 C.]: >1000 h

Example 53

(168) TABLE-US-00059 PY-1V-O2 10.00% Clearing point [ C.]: 73.5 CY-3-O2 18.00% n [589 nm, 20 C.]: 0.1084 CCY-3-O1 6.00% [1 kHz, 20 C.]: 3.2 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.6 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 82 CC-3-V 40.00% K.sub.1 [pN, 20 C.]: 12.8 BCH-32 3.50% K.sub.3 [pN, 20 C.]: 14.9 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.3

Example 54

(169) TABLE-US-00060 PY-V2-O2 11.50% Clearing point [ C.]: 74.5 CY-3-O2 10.00% n [589 nm, 20 C.]: 0.1071 CCY-3-O1 4.50% [1 kHz, 20 C.]: 3.4 CCY-3-O2 11.00% .sub.|| [1 kHz, 20 C.]: 3.8 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 7.1 CPY-3-O2 12.50% .sub.1 [mPa .Math. s, 20 C.]: 91 CC-3-V 34.50% K.sub.1 [pN, 20 C.]: 12.7 BCH-32 6.00% K.sub.3 [pN, 20 C.]: 14.6 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.2 Y-4O-O4 2.50%

Example 55

(170) TABLE-US-00061 PY-V2-O2 14.00% Clearing point [ C.]: 74.5 CY-3-O2 10.50% n [589 nm, 20 C.]: 0.1075 CCY-3-O1 5.00% [1 kHz, 20 C.]: 3.2 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.6 CPY-2-O2 9.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 90 CC-3-V 36.50% K.sub.1 [pN, 20 C.]: 11.7 BCH-32 2.50% K.sub.3 [pN, 20 C.]: 14.1 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.21

Example 56

(171) TABLE-US-00062 PY-3V-O2 10.50% Clearing point [ C.]: 74.5 CY-3-O2 15.00% n [589 nm, 20 C.]: 0.1073 CCY-3-O1 7.50% [1 kHz, 20 C.]: 3.0 CCY-3-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.6 CPY-2-O2 11.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 84 CC-3-V 40.50% K.sub.1 [pN, 20 C.]: 12.8 BCH-32 3.00% K.sub.3 [pN, 20 C.]: 14.1 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.29

Example 57

(172) TABLE-US-00063 CC-3-V 36.50% Clearing point [ C.]: 73 CY-3-O2 10.00% n [589 nm, 20 C.]: 0.1081 CCY-3-O1 6.50% [1 kHz, 20 C.]: 3.3 CCY-3-O2 11.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 6.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 8.50% .sub.1 [mPa .Math. s, 20 C.]: 90 PY-3-O2 4.00% K.sub.1 [pN, 20 C.]: 13.2 PY-3V-O2 6.50% K.sub.3 [pN, 20 C.]: 15.0 PY-1-O4 4.50% V.sub.0 [20 C., V]: 2.25 PYP-2-3 3.00% PP-1-2V1 3.50%

Example 58

(173) TABLE-US-00064 PY-V2-O2 7.00% Clearing point [ C.]: 75.5 CY-3-O2 10.00% n [589 nm, 20 C.]: 0.1086 CY-1V2-O2 6.00% [1 kHz, 20 C.]: 2.7 CCY-3-O1 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-O2 2.00% .sub. [1 kHz, 20 C.]: 6.2 CPY-2-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 85 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 12.8 CC-3-V 37.00% K.sub.3 [pN, 20 C.]: 14.5 BCH-32 10.50% V.sub.0 [20 C., V]: 2.45 PPGU-3-F 0.50% LTS (bulk) [20 C.]: >1000 h

Example 59

(174) TABLE-US-00065 PY-V-O2 5.00% Clearing point [ C.]: 75 PY-V2-O2 5.00% n [589 nm, 20 C.]: 0.1087 PY-3-O2 3.00% [1 kHz, 20 C.]: 3.1 CY-V-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CY-3-O2 3.00% .sub. [1 kHz, 20 C.]: 6.8 CCY-3-O1 3.50% .sub.1 [mPa .Math. s, 20 C.]: 83 CCY-3-O2 7.00% K.sub.1 [pN, 20 C.]: 12.6 CCY-4-O2 5.00% K.sub.3 [pN, 20 C.]: 14.2 CPY-2-O2 8.00% V.sub.0 [20 C., V]: 2.28 CPY-3-O2 10.00% LTS (bulk) [20 C.]: >1000 h CC-3-V 38.00% BCH-32 6.00% PPGU-3-F 0.50% Y-4O-O4 2.00%

Example 60

(175) TABLE-US-00066 PY-V2-O2 5.50% Clearing point [ C.]: 75.5 PY-3-O2 8.00% n [589 nm, 20 C.]: 0.1075 CY-V-O2 6.00% [1 kHz, 20 C.]: 3.1 CCY-3-O1 5.50% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 5.00% .sub. [1 kHz, 20 C.]: 6.8 CCY-4-O2 4.00% .sub.1 [mPa .Math. s, 20 C.]: 88 CPY-2-O2 8.00% K.sub.1 [pN, 20 C.]: 12.6 CPY-3-O2 9.00% K.sub.3 [pN, 20 C.]: 14.0 CC-3-V 35.00% V.sub.0 [20 C., V]: 2.26 BCH-32 8.00% LTS (bulk) [20 C.]: >1000 h PPGU-3-F 0.50% LTS (bulk) [30 C.]: >1000 h Y-4O-O4 2.00%

Example 61

(176) TABLE-US-00067 PY-V-O2 5.50% Clearing point [ C.]: 74.5 PY-3-O2 4.50% n [589 nm, 20 C.]: 0.1098 CY-3-O2 11.00% [1 kHz, 20 C.]: 3.0 CCY-3-O2 10.50% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 10.00% .sub. [1 kHz, 20 C.]: 6.7 CPY-3-O2 11.00% .sub.1 [mPa .Math. s, 20 C.]: 85 CC-3-V 37.00% K.sub.1 [pN, 20 C.]: 12.9 BCH-32 8.00% K.sub.3 [pN, 20 C.]: 14.5 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.31 Y-4O-O4 2.00% LTS (bulk) [20 C.]: >1000 h LTS (bulk) [30 C.]: >1000 h

Example 62

(177) TABLE-US-00068 PY-3-O2 6.00% Clearing point [ C.]: 75 PY-V2-O2 6.00% n [589 nm, 20 C.]: 0.1079 CY-3-O2 12.00% [1 kHz, 20 C.]: 3.2 CCY-3-O1 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 9.50% .sub. [1 kHz, 20 C.]: 6.9 CPY-2-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 91 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 13.1 CC-3-V 35.50% K.sub.3 [pN, 20 C.]: 14.9 BCH-32 7.00% V.sub.0 [20 C., V]: 2.29 PPGU-3-F 0.50% LTS (bulk) [20 C.]: >1000 h LTS (bulk) [30 C.]: >1000 h

Example 63

(178) TABLE-US-00069 PY-3-O2 6.00% Clearing point [ C.]: 75 PY-1V2-O2 6.50% n [589 nm, 20 C.]: 0.1088 CY-3-O2 13.00% [1 kHz, 20 C.]: 3.3 CCY-3-O2 12.00% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 6.9 CPY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 93 CC-3-V 36.00% K.sub.1 [pN, 20 C.]: 13.5 BCH-32 6.00% K.sub.3 [pN, 20 C.]: 15.6 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.32

Example 64

(179) TABLE-US-00070 PY-3-O2 4.50% Clearing point [ C.]: 75 PY-V2-O2 6.00% n [589 nm, 20 C.]: 0.1078 CY-3-O2 10.00% [1 kHz, 20 C.]: 3.1 CCY-3-O1 2.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 11.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-2-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 88 CPY-3-O2 12.00% K.sub.1 [pN, 20 C.]: 13.0 CC-3-V 36.00% K.sub.3 [pN, 20 C.]: 14.8 BCH-32 8.00% V.sub.0 [20 C., V]: 2.31 PPGU-3-F 0.50% LTS (bulk) [30 C.] >1000 h Y-4O-O4 2.00%

Example 64a

(180) The mixture from Example 64 is additionally stabilised with

(181) 0.01% of

(182) ##STR00410##

Example 65

(183) TABLE-US-00071 BCH-32 6.00% Clearing point [ C.]: 77 CCH-23 16.00% n [589 nm, 20 C.]: 0.0953 CCH-301 3.50% [1 kHz, 20 C.]: 2.5 CCH-34 6.00% .sub.|| [1 kHz, 20 C.]: 3.3 CCH-35 6.00% .sub. [1 kHz, 20 C.]: 5.8 CCP-3-1 12.00% .sub.1 [mPa .Math. s, 20 C.]: 96 CY-3-O2 15.00% K.sub.1 [pN, 20 C.]: 14.6 CCY-3-O1 5.00% K.sub.3 [pN, 20 C.]: 15.6 CCY-3-O2 7.00% V.sub.0 [20 C., V]: 2.66 CPY-3-O2 8.50% LTS (bulk) [20 C.] >1000 h PCH-302 6.00% LTS (bulk) [30 C.] >1000 h PY-V2-O2 9.00%

Example 66

(184) TABLE-US-00072 BCH-32 4.00% Clearing point [ C.]: 76 CC-3-V 34.50% n [589 nm, 20 C.]: 0.0955 CCP-3-1 10.00% [1 kHz, 20 C.]: 2.5 CY-3-O2 14.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 5.9 CCY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 82 CPY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 13.4 PCH-302 4.50% K.sub.3 [pN, 20 C.]: 16.2 PY-V2-O2 9.00% V.sub.0 [20 C., V]: 2.66 LTS (bulk) [20 C.]: >1000 h LTS (bulk) [30 C.]: >1000 h

Example 67

(185) TABLE-US-00073 BCH-32 6.50% Clearing point [ C.]: 76.5 CCH-23 16.00% n [589 nm, 20 C.]: 0.0933 CCH-301 4.50% [1 kHz, 20 C.]: 2.5 CCH-34 8.00% .sub.|| [1 kHz, 20 C.]: 3.3 CCH-35 6.00% .sub. [1 kHz, 20 C.]: 5.8 CCP-3-1 8.50% .sub.1 [mPa .Math. s, 20 C.]: 96 CY-3-O2 15.00% K.sub.1 [pN, 20 C.]: 14.3 CCY-3-O1 5.50% K.sub.3 [pN, 20 C.]: 15.0 CCY-3-O2 8.00% V.sub.0 [20 C., V]: 2.57 CPY-3-O2 9.00% PCH-302 4.50% PY-V2-O2 8.50%

Example 68

(186) TABLE-US-00074 Y-4O-O4 7.00% Clearing point [ C.]: 75.5 PY-1-O4 2.00% n [589 nm, 20 C.]: 0.1062 CCY-3-O1 2.50% [1 kHz, 20 C.]: 2.2 CCY-3-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.4 CPY-3-O2 10.00% .sub. [1 kHz, 20 C.]: 5.5 PYP-2-3 8.50% .sub.1 [mPa .Math. s, 20 C.]: 90 CCH-23 19.00% K.sub.1 [pN, 20 C.]: 14.5 CCH-34 6.00% K.sub.3 [pN, 20 C.]: 14.2 CCH-35 6.00% V.sub.0 [20 C., V]: 2.70 PCH-302 8.00% BCH-32 7.00% CCP-3-1 10.00% PY-V2-O2 6.00%

Example 69

(187) TABLE-US-00075 BCH-32 7.00% Clearing point [ C.]: 75 CCH-23 16.00% n [589 nm, 20 C.]: 0.0930 CCH-301 3.50% [1 kHz, 20 C.]: 2.5 CCH-34 6.50% .sub.|| [1 kHz, 20 C.]: 3.3 CCH-35 6.50% .sub. [1 kHz, 20 C.]: 5.8 CCP-3-1 9.50% .sub.1 [mPa .Math. s, 20 C.]: 93 CY-3-O2 7.50% K.sub.1 [pN, 20 C.]: 13.7 CY-V1-O2 7.00% K.sub.3 [pN, 20 C.]: 14.1 CCY-3-O1 6.00% V.sub.0 [20 C., V]: 2.52 CCY-3-O2 9.00% LTS (bulk) [20 C.] >1000 h CPY-3-O2 7.00% PCH-302 5.00% PY-V2-O2 9.50%

Example 70

(188) TABLE-US-00076 BCH-32 7.00% Clearing point [ C.]: 74 CCH-23 15.00% n [589 nm, 20 C.]: 0.0921 CCH-301 4.00% [1 kHz, 20 C.]: 2.5 CCH-34 8.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCH-35 7.00% .sub. [1 kHz, 20 C.]: 5.9 CCP-3-1 8.00% .sub.1 [mPa .Math. s, 20 C.]: 95 CY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 13.4 CY-V1-O2 7.00% K.sub.3 [pN, 20 C.]: 14.1 CCY-3-O1 9.00% V.sub.0 [20 C., V]: 2.49 CCY-3-O2 7.00% CPY-1V-O1 7.00% PCH-302 4.00% PY-V2-O2 8.00%

Example 71

(189) TABLE-US-00077 BCH-32 7.00% Clearing point [ C.]: 77 CCH-23 13.00% n [589 nm, 20 C.]: 0.0935 CCH-301 3.00% [1 kHz, 20 C.]: 2.4 CCH-34 10.00% .sub.|| [1 kHz, 20 C.]: 3.3 CCH-35 6.00% .sub. [1 kHz, 20 C.]: 5.7 CCP-3-1 10.50% .sub.1 [mPa .Math. s, 20 C.]: 97 CY-3-O2 8.50% K.sub.1 [pN, 20 C.]: 14.1 CY-V1-O2 5.50% K.sub.3 [pN, 20 C.]: 14.6 CCY-3-O1 10.00% V.sub.0 [20 C., V]: 2.62 CCY-3-O2 6.00% CPY-1V-O1 5.50% PCH-302 6.00% PY-V2-O2 9.00%

Example 72

(190) TABLE-US-00078 CY-3-O2 9.50% Clearing point [ C.]: 75 PY-V-O2 9.50% n [589 nm, 20 C.]: 0.1101 CCY-3-O2 9.00% [1 kHz, 20 C.]: 3.0 CCY-4-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 5.00% .sub. [1 kHz, 20 C.]: 6.5 CPY-3-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 100 CCH-34 10.00% K.sub.1 [pN, 20 C.]: 13.4 CCH-23 21.00% K.sub.3 [pN, 20 C.]: 14.3 PYP-2-3 7.00% V.sub.0 [20 C., V]: 2.31 CCP-3-1 3.00% PCH-301 10.50%

Example 73

(191) TABLE-US-00079 PY-3-O2 11.00% Clearing point [ C.]: 75 PY-1V-O2 8.00% n [589 nm, 20 C.]: 0.1100 CY-3-O2 5.00% [1 kHz, 20 C.]: 3.4 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 6.9 CPY-2-O2 7.00% .sub.1 [mP .Math. s, 20 C.]: 107 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 14.3 CCH-34 10.00% K.sub.3 [pN, 20 C.]: 15.2 CCH-23 21.00% V.sub.0 [20 C., V]: 2.24 CCP-3-1 4.00% PCH-301 9.00%

Example 74

(192) TABLE-US-00080 CY-3-O2 10.00% Clearing point [ C.]: 75 PY-V-O2 9.00% n [589 nm, 20 C.]: 0.1099 CCY-3-O2 9.00% [1 kHz, 20 C.]: 3.2 CCY-4-O2 7.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 6.7 CPY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CCH-34 11.00% K.sub.1 [pN, 20 C.]: 13.2 CCH-23 20.00% K.sub.3 [pN, 20 C.]: 14.1 PYP-2-3 7.00% V.sub.0 [20 C., V]: 2.24 CCP-3-1 1.00% PCH-301 10.00%

Example 75

(193) TABLE-US-00081 CY-3-O2 12.50% Clearing point [ C.]: 74 PY-3-O2 4.00% n [589 nm, 20 C.]: 0.1026 PY-V-O2 5.00% [1 kHz, 20 C.]: 3.2 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 6.7 CCY-4-O2 2.00% .sub.1 [mPa .Math. s, 20 C.]: 102 CPY-2-O2 7.00% K.sub.1 [pN, 20 C.]: 13.5 CPY-3-O2 9.00% K.sub.3 [pN, 20 C.]: 14.1 CCH-34 10.00% V.sub.0 [20 C., V]: 2.22 CCH-23 21.00% LTS (bulk) [20 C.]: >1000 h BCH-32 5.50% PCH-301 8.00% PYP-2-3 1.00%

Example 76

(194) TABLE-US-00082 PY-3-O2 12.00% Clearing point [ C.]: 75 PY-V-O2 5.00% n [589 nm, 20 C.]: 0.1112 CCY-3-O2 10.00% [1 kHz, 20 C.]: 3.1 CCY-4-O2 9.50% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 6.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 107 CCH-34 5.50% K.sub.1 [pN, 20 C.]: 13.7 CCH-23 21.00% K.sub.3 [pN, 20 C.]: 14.4 PYP-2-3 4.50% V.sub.0 [20 C., V]: 2.29 CCH-35 4.00% PCH-301 12.00% BCH-32 1.50%

Example 77

(195) TABLE-US-00083 PY-V-O2 8.00% Clearing point [ C.]: 74.8 CY-3-O2 5.50% n [589 nm, 20 C.]: 0.1073 CY-V-O2 11.00% [1 kHz, 20 C.]: 3.1 CCY-3-O1 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 10.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 82 CPY-V-O4 7.00% K.sub.1 [pN, 20 C.]: 12.1 CC-3-V 37.00% K.sub.3 [pN, 20 C.]: 14.6 BCH-32 7.00% V.sub.0 [20 C., V]: 2.30 PPGU-3-F 0.50%

Example 78

(196) TABLE-US-00084 PY-3-O2 5.00% Clearing point [ C.]: 76 PY-V2-O2 6.50% n [589 nm, 20 C.]: 0.1082 CY-3-O2 12.00% [1 kHz, 20 C.]: 3.2 CCY-3-O1 5.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 10.00% .sub. [1 kHz, 20 C.]: 6.9 CPY-V-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 89 CPY-V-O4 10.00% K.sub.1 [pN, 20 C.]: 12.6 CC-3-V 35.00% K.sub.3 [pN, 20 C.]: 14.6 BCH-32 7.00% V.sub.0 [20 C., V]: 2.26 PPGU-3-F 0.50%

Example 78a

(197) The mixture from Example 78 is additionally stabilised with

(198) 0.01% of

(199) ##STR00411##

Example 78b

(200) The mixture from Example 78 is additionally stabilised with

(201) 0.01% of

(202) ##STR00412##

Example 79

(203) TABLE-US-00085 PY-V-O2 5.00% Clearing point [ C.]: 73.5 PY-V2-O2 5.00% n [589 nm, 20 C.]: 0.1074 PY-3-O2 3.00% [1 kHz, 20 C.]: 2.9 CY-V-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CY-3-O2 3.00% .sub. [1 kHz, 20 C.]: 6.6 CCY-3-O1 3.00% .sub.1 [mPa .Math. s, 20 C.]: 78 CCY-3-O2 6.00% K.sub.1 [pN, 20 C.]: 12.5 CCY-4-O2 5.00% K.sub.3 [pN, 20 C.]: 14.0 CPY-2-O2 7.50% V.sub.0 [20 C., V]: 2.33 CPY-3-O2 10.00% CC-3-V 39.00% BCH-32 7.00% PPGU-3-F 0.50% Y-4O-O4 2.00%

Example 80

(204) TABLE-US-00086 PY-V-O2 5.00% Clearing point [ C.]: 75 CY-3-O2 8.00% n [589 nm, 20 C.]: 0.1078 CY-V-O2 11.00% [1 kHz, 20 C.]: 3.0 CCY-3-O1 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O2 7.00% .sub. [1 kHz, 20 C.]: 6.7 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 84 CPY-V-O4 5.00% K.sub.1 [pN, 20 C.]: 11.9 CPY-V-O2 7.00% K.sub.3 [pN, 20 C.]: 14.4 CC-3-V 35.50% V.sub.0 [20 C., V]: 2.30 BCH-32 9.00% PPGU-3-F 0.50%

Example 81

(205) TABLE-US-00087 APUQU-2-F 9.00% Clearing point [ C.]: 77.5 APUQU-3-F 8.50% n [589 nm, 20 C.]: 0.1087 CC-3-V 43.50% [1 kHz, 20 C.]: 9.9 CCP-30CF.sub.3 7.50% .sub.|| [1 kHz, 20 C.]: 13.7 CCP-V-1 7.00% .sub. [1 kHz, 20 C.]: 3.8 DPGU-4-F 3.50% .sub.1 [mPa .Math. s, 20 C.]: 68 PGP-2-2V 4.00% K.sub.1 [pN, 20 C.]: 12.4 PGUQU-4-F 4.50% K.sub.3 [pN, 20 C.]: 13.1 PUQU-3-F 8.50% V.sub.0 [20 C., V]: 1.18 PY-3V-O2 4.00% LTS (bulk) [20 C.]: >1000 h LTS (bulk) [30 C.]: >1000 h

Example 82

(206) TABLE-US-00088 PY-1V-O2 4.50% Clearing point [ C.]: 73.5 PY-V2-O2 5.00% n [589 nm, 20 C.]: 0.1074 CY-3-O2 10.00% [1 kHz, 20 C.]: 2.8 CY-V-O2 4.50% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 6.4 CCY-3-O2 3.00% .sub.1 [mPa .Math. s, 20 C.]: 78 CPY-2-O2 9.00% K.sub.1 [pN, 20 C.]: 12.5 CPY-3-O2 10.00% K.sub.3 [pN, 20 C.]: 14.3 CC-3-V 39.50% V.sub.0 [20 C., V]: 2.40 BCH-32 8.00% PPGU-3-F 0.50%

Example 83

(207) TABLE-US-00089 PY-V2-O2 5.50% Clearing point [ C.]: 74 PY-3-O2 6.00% n [589 nm, 20 C.]: 0.1074 CY-V2-O2 5.00% [1 kHz, 20 C.]: 2.9 CY-3-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O1 3.00% .sub. [1 kHz, 20 C.]: 6.6 CCY-3-O2 3.00% .sub.1 [mPa .Math. s, 20 C.]: 85 CCY-4-O2 6.00% K.sub.1 [pN, 20 C.]: 12.6 CPY-2-O2 8.00% K.sub.3 [pN, 20 C.]: 13.9 CPY-3-O2 12.00% V.sub.0 [20 C., V]: 2.30 CC-3-V 36.50% BCH-32 8.50% PPGU-3-F 0.50% Y-4O-O4 2.00%

Example 84

(208) TABLE-US-00090 PY-V2-O2 6.00% Clearing point [ C.]: 74.5 PY-3-O2 6.00% n [589 nm, 20 C.]: 0.1086 CY-1V2-O2 4.50% [1 kHz, 20 C.]: 2.9 CY-3-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O1 3.00% .sub. [1 kHz, 20 C.]: 6.5 CCY-3-O2 3.00% .sub.1 [mPa .Math. s, 20 C.]: 86 CCY-4-O2 6.00% K.sub.1 [pN, 20 C.]: 12.8 CPY-2-O2 8.00% K.sub.3 [pN, 20 C.]: 14.2 CPY-3-O2 12.00% V.sub.0 [20 C., V]: 2.33 CC-3-V 37.00% BCH-32 8.00% PPGU-3-F 0.50% Y-4O-O4 2.00%

Example 85

(209) TABLE-US-00091 PY-V2-O2 6.50% Clearing point [ C.]: 74 CY-3-O2 11.00% n [589 nm, 20 C.]: 0.1068 CY-V2-O2 6.50% [1 kHz, 20 C.]: 2.8 CCY-3-O1 6.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O2 2.00% .sub. [1 kHz, 20 C.]: 6.4 CPY-2-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 85 CPY-3-O2 12.00% K.sub.1 [pN, 20 C.]: 12.3 CC-3-V 36.00% K.sub.3 [pN, 20 C.]: 14.1 BCH-32 9.50% V.sub.0 [20 C., V]: 2.35 PPGU-3-F 0.50%

Example 86

(210) TABLE-US-00092 PCH-504FF 10.00% Clearing point [ C.]: 72 PCH-502FF 8.00% n [589 nm, 20 C.]: 0.1216 PCH-304FF 4.00% [1 kHz, 20 C.]: 4.0 CCP-V2-1 6.00% .sub.|| [1 kHz, 20 C.]: 3.9 BCH-32 7.00% .sub. [1 kHz, 20 C.]: 7.9 CCH-35 5.00% .sub.1 [mPa .Math. s, 20 C.]: 125 CC-5-V 7.00% K.sub.1 [pN, 20 C.]: 14.6 CC-3-V1 10.00% K.sub.3 [pN, 20 C.]: 14.7 CPY-2-O2 10.00% V.sub.0 [20 C., V]: 2.03 CPY-3-O2 13.00% PY-V2-O2 20.00%

Example 87

(211) TABLE-US-00093 CY-3-O2 24.00% Clearing point [ C.]: 81 PY-1V2-O2 7.00% n [589 nm, 20 C.]: 0.1019 CCY-3-O3 4.00% [1 kHz, 20 C.]: 3.1 CCY-3-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-3-O2 5.00% .sub.1 [mPa .Math. s, 20 C.]: 126 CCP-3-3 9.00% K.sub.1 [pN, 20 C.]: 14.9 CCP-3-1 9.00% K.sub.3 [pN, 20 C.]: 16.0 BCH-32 5.00% V.sub.0 [20 C., V]: 2.39 CCH-34 10.00% LTS (bulk) [20 C.]: >1000 h CCH-25 10.00% PCH-301 5.00%

Example 88

(212) TABLE-US-00094 CY-3-O2 18.00% Clearing point [ C.]: 80.5 PY-1V2-O2 6.00% n [589 nm, 20 C.]: 0.0949 CCY-3-O2 8.00% [1 kHz, 20 C.]: 3.1 CCY-4-O2 4.00% .sub.|| [1 kHz, 20 C.]: 3.4 CPY-2-O2 7.00% .sub. [1 kHz, 20 C.]: 6.4 CPY-3-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 113 CCH-34 8.00% K.sub.1 [pN, 20 C.]: 14.9 CCH-23 22.00% K.sub.3 [pN, 20 C.]: 16.0 CCP-3-3 7.00% V.sub.0 [20 C., V]: 2.41 CCP-3-1 7.00% LTS (bulk) [20 C.]: >1000 h PCH-301 3.00%

Example 89

(213) TABLE-US-00095 CY-1V-O1V 20.00% Clearing point [ C.]: 82.5 PY-1V2-O2 7.00% n [589 nm, 20 C.]: 0.0987 CY-3-O2 5.00% [1 kHz, 20 C.]: 3.0 CCY-3-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-4-O2 5.00% .sub. [1 kHz, 20 C.]: 6.4 CPY-3-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 109 CCH-34 10.00% K.sub.1 [pN, 20 C.]: 14.9 CC-3-V1 11.00% K.sub.3 [pN, 20 C.]: 18.9 CC-2-V1 11.00% V.sub.0 [20 C., V]: 2.66 CCP-3-1 8.00% LTS (bulk) [20 C.]: >1000 h PCH-301 2.00% CCVC-3-V 6.00%

Example 90

(214) TABLE-US-00096 CY-1V-O1V 20.00% Clearing point [ C.]: 81 PY-1V2-O2 5.00% n [589 nm, 20 C.]: 0.0953 CY-3-O2 7.00% [1 kHz, 20 C.]: 3.0 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 6.4 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 106 CCH-34 10.00% K.sub.1 [pN, 20 C.]: 14.5 CC-3-V1 11.00% K.sub.3 [pN, 20 C.]: 18.6 CC-2-V1 11.00% V.sub.0 [20 C., V]: 2.63 CCP-3-1 8.00% LTS (bulk) [20 C.]: >1000 h PCH-301 2.00% CCVC-3-V 6.00%

Example 91

(215) TABLE-US-00097 CY-1V-O1V 20.00% Clearing point [ C.]: 81.5 PY-1V2-O2 6.00% n [589 nm, 20 C.]: 0.0947 CY-3-O2 6.00% [1 kHz, 20 C.]: 3.0 CCY-3-O2 7.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-O1 7.00% .sub. [1 kHz, 20 C.]: 6.4 CPY-3-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CCH-34 10.00% K.sub.1 [pN, 20 C.]: 14.6 CC-3-V1 12.00% K.sub.3 [pN, 20 C.]: 18.6 CC-2-V1 12.00% V.sub.0 [20 C., V]: 2.64 CCP-V2-1 4.00% CCP-V-1 4.00% CCVC-3-V 6.00%

Example 92

(216) TABLE-US-00098 CY-1V-O1V 20.00% Clearing point [ C.]: 80.5 PY-1V2-O2 5.00% n [589 nm, 20 C.]: 0.0962 CY-3-O2 12.00% [1 kHz, 20 C.]: 3.4 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 6.00% .sub. [1 kHz, 20 C.]: 6.9 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 112 CCH-34 7.00% K.sub.1 [pN, 20 C.]: 14.3 CC-3-V1 11.00% K.sub.3 [pN, 20 C.]: 18.5 CC-2-V1 11.00% V.sub.0 [20 C., V]: 2.45 CCP-3-1 6.00% CCVC-3-V 8.00%

Example 93

(217) TABLE-US-00099 CY-1V-O1V 20.00% Clearing point [ C.]: 81.5 PY-1V2-O2 7.00% n [589 nm, 20 C.]: 0.0932 CY-3-O2 7.50% [1 kHz, 20 C.]: 3.3 CCY-3-O2 10.50% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-4-O2 10.00% .sub. [1 kHz, 20 C.]: 6.7 CC-3-V2 11.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CC-3-V1 11.00% K.sub.1 [pN, 20 C.]: 14.9 CC-2-V1 11.00% K.sub.3 [pN, 20 C.]: 19.0 CCP-3-1 6.00% V.sub.0 [20 C., V]: 2.55 CCVC-3-V 6.00% LTS (bulk) [20 C.] >1000 h

Example 94

(218) TABLE-US-00100 CY-3-O2 12.00% Clearing point [ C.]: 80.0 PY-1V2-O2 11.00% n [589 nm, 20 C.]: 0.0950 CCY-3-O2 10.00% [1 kHz, 20 C.]: 3.1 CCY-4-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.3 CPY-3-O2 10.00% .sub. [1 kHz, 20 C.]: 6.4 CCH-34 8.00% .sub.1 [mPa .Math. s, 20 C.]: 111 CCH-23 22.00% K.sub.1 [pN, 20 C.]: 15.1 CCP-3-3 3.00% K.sub.3 [pN, 20 C.]: 16.6 CCP-3-1 7.00% V.sub.0 [20 C., V]: 2.46 PCH-301 7.00% LTS (bulk) [20 C.] >1000 h

Example 95

(219) TABLE-US-00101 CY-1V-O1V 18.00% Clearing point [ C.]: 80.5 PY-1V2-O2 4.00% n [589 nm, 20 C.]: 0.0943 CY-3-O2 15.00% [1 kHz, 20 C.]: 3.6 CCY-3-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 7.00% .sub. [1 kHz, C.]: 7.2 CPY-3-O2 7.00% .sub.1 [mPa .Math. s, 20 C.]: 112 CCH-34 7.00% K.sub.1 [pN, 20 C.]: 14.2 CC-3-V1 11.00% K.sub.3 [pN, 20 C.]: 18.2 CC-2-V1 11.00% V.sub.0 [20 C., V]: 2.37 CCP-3-1 3.00% CCVC-3-V 9.00%

Example 96

(220) TABLE-US-00102 CY-1V-O1V 18.00% Clearing point [ C.]: 80.5 PY-1V2-O2 3.00% n [589 nm, 20 C.]: 0.0946 CY-3-O2 16.00% [1 kHz, 20 C.]: 3.7 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 5.00% .sub. [1 kHz, 20 C.]: 7.2 CPY-3-O2 7.00% .sub.1 [mPa .Math. s, 20 C.]: 113 CC-3-V2 7.00% K.sub.1 [pN, 20 C.]: 14.2 CC-3-V1 11.00% K.sub.3 [pN, 20 C.]: 18.7 CC-2-V1 11.00% V.sub.0 [20 C., V]: 2.39 CCP-3-1 3.00% CCVC-3-V 9.00%

Example 97

(221) TABLE-US-00103 PY-3-O2 11.00% Clearing point [ C.]: 75 PY-V2-O2 6.50% n [589 nm, 20 C.]: 0.1105 CCY-3-O2 9.00% [1 kHz, 20 C.]: 3.1 CCY-4-O2 3.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-01 5.00% .sub. [1 kHz, 20 C.]: 6.6 CPY-2-O2 6.50% .sub.1 [mPa .Math. s, 20 C.]: 105 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 13.9 CCH-34 10.00% K.sub.3 [pN, 20 C.]: 14.3 CCH-23 21.00% V.sub.0 [20 C., V]: 2.28 PYP-2-3 6.00% LTS (bulk) [20 C.] >1000 h CCP-3-1 3.00% PCH-301 9.00%

Example 98

(222) TABLE-US-00104 PY-3-O2 11.00% Clearing point [ C.]: 74 PY-1V2-O2 7.50% n [589 nm, 20 C.]: 0.1107 CCY-3-O2 9.00% [1 kHz, 20 C.]: 3.0 CCY-3-O1 5.50% .sub.|| [1 kHz, 20 C.]: 3.4 CPY-2-O2 6.50% .sub. [1 kHz, 20 C.]: 6.4 CPY-3-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CCH-34 10.00% K.sub.1 [pN, 20 C.]: 14.0 CCH-23 21.00% K.sub.3 [pN, 20 C.]: 14.8 PYP-2-3 5.50% V.sub.0 [20 C., V]: 2.37 CCP-3-1 4.00% LTS (bulk) [20 C.] >1000 h PCH-301 10.00%

Example 99

(223) TABLE-US-00105 PY-3-O2 11.00% Clearing point [ C.]: 74 PY-1V2-O2 8.00% n [589 nm, 20 C.]: 0.1119 CY-3-O2 3.00% [1 kHz, 20 C.]: 3.3 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-2-O2 6.50% .sub.1 [mPa .Math. s, 20 C.]: 108 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 14.3 CCH-34 10.00% K.sub.3 [pN, 20 C.]: 15.0 CCH-23 21.00% V.sub.0 [20 C., V]: 2.26 PYP-2-3 5.00% LTS (bulk) [20 C.] >1000 h CCP-3-1 4.00% PCH-301 6.50%

Example 100

(224) TABLE-US-00106 CC-3-V 39.00% Clearing point [ C.]: 74.5 CC-3-V1 3.00% n [589 nm, 20 C.]: 0.1017 CCP-V-1 8.00% [1 kHz, 20 C.]: 3.2 CCP-V2-1 12.00% .sub.1 [mPa .Math. s, 20 C.]: 64 PGP-2-2V 3.50% K.sub.1 [pN, 20 C.]: 13 PP-1-2V1 9.00% K.sub.3 [pN, 20 C.]: 15.4 PPGU-3-F 1.00% V.sub.0 [20 C., V]: 2.13 PUQU-3-F 15.50% CCY-3-O2 9.00%

Example 101

(225) TABLE-US-00107 BCH-32 5.00% Clearing point [ C.]: 75.3 CC-3-V 41.50% n [589 nm, 20 C.]: 0.0989 CC-3-V1 8.50% [1 kHz, 20 C.]: 1.9 CCH-35 2.00% .sub.|| [1 kHz, 20 C.]: 3.2 CCP-3-1 3.00% .sub. [1 kHz, 20 C.]: 5.0 CCY-3-O2 7.00% .sub.1 [mPa .Math. s, 20 C.]: 69 CPY-2-O2 5.50% K.sub.1 [pN, 20 C.]: 14.2 CPY-3-O2 12.50% K.sub.3 [pN, 20 C.]: 15.5 PY-3-O2 15.00% V.sub.0 [20 C., V]: 3.02

Example 101a

(226) The mixture from Example 101 is additionally mixed with 0.001% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.

Example 102

(227) TABLE-US-00108 CCY-3-O1 8.00% Clearing point [ C.]: 74.9 CCY-4-O2 7.50% n [589 nm, 20 C.]: 0.1123 CPY-2-O2 10.00% [1 kHz, 20 C.]: 3.7 CPY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.7 CC-3-V 15.00% .sub. [1 kHz, 20 C.]: 7.5 PY-1-O4 5.00% .sub.1 [mPa .Math. s, 20 C.]: 121 PY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 13.2 PY-4-O2 5.00% K.sub.3 [pN, 20 C.]: 15.5 CC-3-V1 9.00% V.sub.0 [20 C., V]: 2.15 CCY-3-O2 6.50% PCH-301 15.00%

Example 102a

(228) The mixture from Example 102 is additionally stabilised with

(229) 0.01% of

(230) ##STR00413##

Example 103

(231) TABLE-US-00109 CY-3-O2 10.00% Clearing point [ C.]: 100 CY-3-O4 20.00% n [589 nm, 20 C.]: 0.0865 CY-5-O4 20.00% [1 kHz, 20 C.]: 5.4 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.9 CCY-3-O3 6.00% .sub. [1 kHz, 20 C.]: 9.3 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 347 CCY-5-O2 6.00% K.sub.1 [pN, 20 C.]: 15.6 CH-33 3.00% K.sub.3 [pN, 20 C.]: 16.6 CH-35 3.50% V.sub.0 [20 C., V]: 1.84 CH-43 3.50% CH-45 3.50% CCPC-33 4.00% CCPC-34 4.50% CCPC-35 4.00%

Example 104

(232) TABLE-US-00110 CY-3-O2 15.00% Clearing point [ C.]: 91 CY-5-O2 12.00% n [589 nm, 20 C.]: 0.105 CCY-3-O1 4.00% [1 kHz, 20 C.]: 4.5 CCY-3-O2 4.00% .sub.1 [mPa .Math. s, 20 C.]: 106 CCY-3-O3 4.00% V.sub.0 [20 C., V]: 1.32 CCY-4-O2 4.00% CLY-3-O2 10.00% CLY-3-O3 2.00% CPY-2-O2 8.00% CC-3-V 24.00% PGP-2-5 5.00%

Example 105

(233) TABLE-US-00111 CY-3-O2 14.00% Clearing point [ C.]: 84.7 CY-3-O4 4.00% n [589 nm, 20 C.]: 0.1068 CY-5-O2 7.00% [1 kHz, 20 C.]: 4.0 CCY-3-O1 4.00% .sub.1 [mPa .Math. s, 20 C.]: 138 CCY-3-O2 5.00% K.sub.1 [pN, 20 C.]: 14.1 CCY-4-O2 8.00% K.sub.3 [pN, 20 C.]: 16.2 CCY-5-O2 3.00% V.sub.0 [20 C., V]: 2.13 CPY-2-O2 9.00% CPY-3-O2 9.00% PYP-2-3 6.00% CC-3-V 22.00% CC-3-V1 3.50% CCP-V-1 5.00% PPGU-3-F 0.50%

Example 106

(234) TABLE-US-00112 CY-3-O2 15.00% Clearing point [ C.]: 80.4 CY-5-O2 12.50% n [589 nm, 20 C.]: 0.1038 CCY-3-O1 2.50% [1 kHz, 20 C.]: 3.3 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 6.8 CPY-3-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 137 CCY-2-1 6.00% K.sub.1 [pN, 20 C.]: 14.2 CCY-3-1 6.00% K.sub.3 [pN, 20 C.]: 14.2 CCH-23 15.00% V.sub.0 [20 C., V]: 2.18 CCH-34 5.00% CCH-301 1.50% BCH-32 15.50%

Example 106a

(235) The mixture from Example 106 is additionally mixed with 0.25% of RM-35

(236) ##STR00414##
and additionally stabilised with
0.025% of

(237) ##STR00415##

Example 107

(238) TABLE-US-00113 CC-3-V 34.00% Clearing point [ C.]: 100 CC-3-V1 2.50% n [589 nm, 20 C.]: 0.1003 CCP-V-1 10.00% [1 kHz, 20 C.]: 9.1 PUQU-3-F 7.00% .sub.|| [1 kHz, 20 C.]: 12.3 PGUQU-3-F 4.00% .sub. [1 kHz, 20 C.]: 3.2 CPGU-3-OT 6.00% .sub.1 [mPa .Math. s, 20 C.]: 99 CCGU-3-F 4.00% K.sub.1 [pN, 20 C.]: 14.2 APUQU-3-F 8.00% K.sub.3 [pN, 20 C.]: 17.3 CCP-3F.F.F 4.50% CCP-30CF.sub.3 4.00% CCP-50CF.sub.3 3.00% CCQU-3-F 10.00% CBC-33 3.00%

Example 107a

(239) The mixture from Example 107 is additionally stabilised with

(240) 0.03% of

(241) ##STR00416##

Example 107b

(242) The mixture from Example 107 is additionally stabilised with

(243) 0.03% of

(244) ##STR00417##

Example 108

(245) TABLE-US-00114 Y-4O-O4 4.50% Clearing point [ C.]: 100 PYP-2-3 2.00% n [589 nm, 20 C.]: 0.1716 CC-3-V 25.00% [1 kHz, 20 C.]: 1.5 CC-4-V 10.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCP-V-1 14.00% .sub. [1 kHz, 20 C.]: 4.9 PTP-302FF 10.00% .sub.1 [mPa .Math. s, 20 C.]: 114 CPTP-302FF 10.00% K.sub.1 [pN, 20 C.]: 15.2 CPTP-302FF 10.00% K.sub.3 [pN, 20 C.]: 18.5 PPTUI-3-2 14.50% V.sub.0 [20 C., V]: 3.76

Example 109

(246) TABLE-US-00115 CCH-23 25.00% Clearing point [ C.]: 70.3 CC-3-V 4.50% n [589 nm, 20 C.]: 0.0737 PCH-53 25.00% [1 kHz, 20 C.]: 1.1 CCY-2-1 12.00% .sub.|| [1 kHz, 20 C.]: 2.8 CCY-3-1 12.00% .sub. [1 kHz, 20 C.]: 3.9 CCY-3-O2 12.00% K.sub.1 [pN, 20 C.]: 11.7 CCY-3-O3 5.00% K.sub.3 [pN, 20 C.]: 13.1 CBC-33F 4.50%

Example 110

(247) TABLE-US-00116 CC-3-V1 10.25% Clearing point [ C.]: 74.7 CCH-23 18.50% n [589 nm, 20 C.]: 0.1027 CCH-35 6.75% [1 kHz, 20 C.]: 3.1 CCP-3-1 6.00% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-1 2.50% .sub. [1 kHz, 20 C.]: 6.5 CCY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CPY-2-O2 6.00% K.sub.1 [pN, 20 C.]: 15.4 CPY-3-O2 9.75% K.sub.3 [pN, 20 C.]: 16.8 CY-3-O2 11.50% V.sub.0 [20 C., V]: 2.46 PP-1-2V1 3.75% PY-3-O2 13.00%

Example 110a

(248) The mixture from Example 110 is additionally mixed with 0.01% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and 0.3% of RM-1.

Example 111

(249) TABLE-US-00117 BCH-3F.F 10.00% Clearing point [ C.]: 99.6 BCH-3F.F.F 12.00% n [589 nm, 20 C.]: 0.1122 CBC-33 3.00% [1 kHz, 20 C.]: 10.1 CBC-33F 3.00% .sub.|| [1 kHz, 20 C.]: 13.8 CCGU-3-F 8.00% .sub. [1 kHz, 20 C.]: 3.6 CCH-34 10.00% .sub.1 [mPa .Math. s, 20 C.]: 164 CCH-35 6.50% K.sub.1 [pN, 20 C.]: 11.8 CCP-1F.F.F 10.00% K.sub.3 [pN, 20 C.]: 15.9 CCP-2F.F.F 10.00% V.sub.0 [20 C., V]: 1.14 CCP-3-1 2.50% CCP-3F.F.F 8.00% CPGP-4-3 3.00% CPGP-5-2 2.00% CPGP-5-3 1.00% PUQU-2-F 1.00% PUQU-3-F 10.00%

Example 112

(250) TABLE-US-00118 CBC-53F 3.00% Clearing point [ C.]: 115.5 CC-3-2V1 1.00% n [589 nm, 20 C.]: 0.1106 CC-3-V 25.00% [1 kHz, 20 C.]: 7.0 CC-3-V1 5.00% .sub.|| [1 kHz, 20 C.]: 9.9 CCGU-3-F 5.50% .sub. [1 kHz, 20 C.]: 2.9 CCP-30CF.sub.3 4.00% .sub.1 [mPa .Math. s, 20 C.]: 118 CCP-30CF.sub.3.F 8.00% K.sub.1 [pN, 20 C.]: 17.4 CCP-40CF.sub.3 3.00% K.sub.3 [pN, 20 C.]: 20.4 CCP-50CF.sub.3 3.00% V.sub.0 [20 C., V]: 1.66 CCP-V-1 8.00% CCP-V2-1 12.00% CPGU-3-OT 5.00% PGUQU-3-F 4.00% PGUQU-4-F 4.00% PGUQU-5-F 2.00% PP-1-2V1 3.00% PPGU-3-F 0.50% PUQU-2-F 1.00% PUQU-3-F 3.00%

Example 113

(251) TABLE-US-00119 APUQU-2-F 2.50% Clearing point [ C.]: 85.8 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1106 PUQU-3-F 10.00% [1 kHz, 20 C.]: 8.6 PGUQU-3-F 5.00% .sub.|| [1 kHz, 20 C.]: 12.6 PGUQU-4-F 3.00% .sub. [1 kHz, 20 C.]: 4.0 PGUQU-5-F 2.00% .sub.1 [mPa .Math. s, 20 C.]: 92 DPGU-4-F 4.00% K.sub.1 [pN, 20 C.]: 13.0 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 15.3 CDUQU-3-F 0.05% V.sub.0 [20 C., V]: 1.30 CC-3-V 39.95% CCP-V-1 9.00% CCP-V2-1 8.00% CCP-3-1 2.00% PGP-2-3 3.00% CY-3-O2 5.00% CCY-3-O2 5.00%

Example 114

(252) TABLE-US-00120 APUQU-2-F 2.50% Clearing point [ C.]: 85.8 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1105 PUQU-3-F 12.50% [1 kHz, 20 C.]: 10.6 PGUQU-3-F 5.00% .sub.|| [1 kHz, 20 C.]: 14.8 PGUQU-4-F 4.00% .sub. [1 kHz, 20 C.]: 4.2 PGUQU-5-F 4.00% .sub.1 [mPa .Math. s, 20 C.]: 98 DPGU-4-F 4.00% K.sub.1 [pN, 20 C.]: 12.7 PPGU-3-F 0.50% K.sub.3 [pN, 20 C.]: 15.1 CDUQU-3-F 0.05% CC-3-V 34.95% CCP-V-1 7.00% CCP-V2-1 6.00% CCP-3-1 2.50% CCPC-33 2.00% CY-3-O2 5.00% CCY-3-O2 5.00%

Example 115

(253) TABLE-US-00121 APUQU-2-F 3.00% Clearing point [ C.]: 85.7 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1097 PUQU-3-F 12.00% [1 kHz, 20 C.]: 8.7 PGUQU-3-F 5.00% .sub.|| [1 kHz, 20 C.]: 12.4 PGUQU-4-F 4.00% .sub. [1 kHz, 20 C.]: 3.7 PGUQU-5-F 3.00% .sub.1 [mPa .Math. s, 20 C.]: 82 PPGU-3-F 0.50% K.sub.1 [pN, 20 C.]: 12.9 CDUQU-3-F 0.05% K.sub.3 [pN, 20 C.]: 15.7 CC-3-V 38.95% V.sub.0 [20 C., V]: 1.29 CCP-V-1 10.50% CCP-V2-1 9.00% PGP-2-3 2.00% CCY-3-O2 3.50% CPY-3-O2 3.50%

Example 116

(254) TABLE-US-00122 APUQU-2-F 3.00% Clearing point [ C.]: 85.7 APUQU-3-F 5.00% n [589 nm, 20 C.]: 0.1097 PUQU-3-F 12.00% [1 kHz, 20 C.]: 8.7 PGUQU-3-F 5.00% .sub.|| [1 kHz, 20 C.]: 12.4 PGUQU-4-F 4.00% .sub. [1 kHz, 20 C.]: 3.7 PGUQU-5-F 3.00% .sub.1 [mPa .Math. s, 20 C.]: 82 PPGU-3-F 0.50% K.sub.1 [pN, 20 C.]: 12.9 CDUQU-3-F 0.05% K.sub.3 [pN, 20 C.]: 15.7 CC-3-V 38.95% V.sub.0 [20 C., V]: 1.29 CCP-V-1 10.50% CCP-V2-1 9.00% PGP-2-3 2.00% CCY-3-O2 3.50% CPY-3-O2 3.50%

Example 117

(255) TABLE-US-00123 CC-3-V 35.00% Clearing point [ C.]: 84.6 CCY-3-O1 9.00% n [589 nm, 20 C.]: 0.1010 CCY-3-O2 8.00% [1 kHz, 20 C.]: 4.0 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.6 CLY-3-O3 11.00% .sub. [1 kHz, 20 C.]: 7.6 CPY-2-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 114 CPY-3-O2 4.00% K.sub.1 [pN, 20 C.]: 14.5 CY-3-O2 6.50% PY-3-O2 12.00%

Example 117a

(256) The mixture from Example 117 is additionally stabilised with

(257) 0.04% of

(258) ##STR00418##
and
0.015% of

(259) ##STR00419##

Example 118

(260) TABLE-US-00124 CC-3-V 33.00% Clearing point [ C.]: 84 CCY-3-O1 7.00% n [589 nm, 20 C.]: 0.1111 CCY-3-O2 7.00% [1 kHz, 20 C.]: 4.0 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 3.7 CLY-3-O3 11.00% .sub. [1 kHz, 20 C.]: 7.6 CPY-2-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 119 CPY-3-O2 8.00% K.sub.1 [pN, 20 C.]: 14.8 PP-1-2V1 1.50% PY-1-O4 8.50% PY-3-O2 10.00%

Example 118a

(261) The mixture from Example 118 is additionally stabilised with

(262) 0.04% of

(263) ##STR00420##
and
0.015% of

(264) ##STR00421##

Example 119

(265) TABLE-US-00125 APUQU-2-F 4.00% Clearing point [ C.]: 85.6 APUQU-3-F 7.00% n [589 nm, 20 C.]: 0.1021 PUQU-3-F 5.00% [1 kHz, 20 C.]: 6.9 PGUQU-3-F 4.00% .sub.|| [1 kHz, 20 C.]: 10.0 PGUQU-4-F 3.00% .sub. [1 kHz, 20 C.]: 3.1 PGUQU-5-F 3.00% .sub.1 [mPa .Math. s, 20 C.]: 71 CCP-V-1 16.00% K.sub.1 [pN, 20 C.]: 13.1 CC-3-V 40.00% K.sub.3 [pN, 20 C.]: 15.3 CC-3-V1 4.00% V.sub.0 [20 C., V]: 1.45 CC-4-V 3.00% PGP-2-3 4.00% PGP-2-4 1.00% PPGU-3-F 1.00% CCOC-4-3 5.00%

Example 119a

(266) The mixture from Example 119 is additionally mixed with 0.25% of RM-41

(267) ##STR00422##

Example 119b

(268) The mixture from Example 119 is additionally mixed with 0.3% of RM-17

(269) ##STR00423##

Example 120

(270) TABLE-US-00126 Y-4O-O4 12.00% Clearing point [ C.]: 101 CY-3-O2 14.00% n [589 nm, 20 C.]: 0.1504 CCY-3-O1 5.00% [1 kHz, 20 C.]: 6.2 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 4.5 CCY-3-O3 6.00% .sub. [1 kHz, 20 C.]: 10.7 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 281 CPY-2-O2 2.50% K.sub.1 [pN, 20 C.]: 15.7 PTP-302FF 10.00% K.sub.3 [pN, 20 C.]: 19.9 CPTP-302FF 10.00% V.sub.0 [20 C., V]: 1.90 CPTP-502FF 10.00% CC-4-V 2.50% CCP-V-1 11.50% CCPC-33 4.50%

Example 121

(271) TABLE-US-00127 Y-4O-O4 12.00% Clearing point [ C.]: 100 CCY-3-O1 5.00% n [589 nm, 20 C.]: 0.1496 CCY-3-O2 6.00% [1 kHz, 20 C.]: 4.1 CCY-3-O3 6.00% .sub.|| [1 kHz, 20 C.]: 4.0 CCY-4-O2 2.00% .sub. [1 kHz, 20 C.]: 8.1 CC-4-V 15.00% .sub.1 [mPa .Math. s, 20 C.]: 180 CCP-V-1 11.00% K.sub.1 [pN, 20 C.]: 16.1 CCP-V2-1 5.00% K.sub.3 [pN, 20 C.]: 18.5 BCH-32 5.00% V.sub.0 [20 C., V]: 2.25 PTP-302FF 10.00% PTP-502FF 3.00% CPTP-302FF 10.00% CPTP-502FF 10.00%

Example 122

(272) TABLE-US-00128 Y-4O-O4 10.00% Clearing point [ C.]: 100 CCY-3-O1 2.50% n [589 nm, 20 C.]: 0.1515 PTP-302FF 10.00% [1 kHz, 20 C.]: 2.1 PTP-502FF 3.50% .sub.|| [1 kHz, 20 C.]: 3.5 CPTP-302FF 10.00% .sub. [1 kHz, 20 C.]: 5.6 CPTP-502FF 3.50% .sub.1 [mPa .Math. s, 20 C.]: 125 CC-4-V 15.00% K.sub.1 [pN, 20 C.]: 16.6 CC-3-V1 8.00% K.sub.3 [pN, 20 C.]: 18.7 CCP-V-1 12.00% V.sub.0 [20 C., V]: 3.13 CCP-V2-1 12.00% BCH-32 5.00% CPTP-3-1 5.00% CPTP-3-2 3.50%

Example 123

(273) TABLE-US-00129 Y-4O-O4 12.00% Clearing point [ C.]: 101 CY-3-O2 6.00% n [589 nm, 20 C.]: 0.1218 CY-3-O4 15.00% [1 kHz, 20 C.]: 6.2 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 4.5 CCY-3-O3 6.00% .sub. [1 kHz, 20 C.]: 10.7 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 302 CLY-3-O2 5.00% K.sub.1 [pN, 20 C.]: 15.7 CPY-2-O2 8.00% K.sub.3 [pN, 20 C.]: 18.9 CPY-3-O2 8.00% V.sub.0 [20 C., V]: 1.83 CPTP-302FF 4.00% CPTP-502FF 4.00% CCP-V-1 11.00% CCPC-33 4.50% CCPC-34 4.50%

Example 124

(274) TABLE-US-00130 Y-4O-O4 15.00% Clearing point [ C.]: 101 CCY-3-O2 5.00% n [589 nm, 20 C.]: 0.1216 CCY-3-O3 5.00% [1 kHz, 20 C.]: 4.0 CCY-4-O2 5.00% .sub.|| [1 kHz, 20 C.]: 4.0 CLY-3-O2 4.00% .sub. [1 kHz, 20 C.]: 8.0 CPY-2-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 167 CPY-3-O2 8.00% K.sub.1 [pN, 20 C.]: 16.1 CPTP-302FF 5.00% K.sub.3 [pN, 20 C.]: 17.3 CPTP-502FF 5.00% V.sub.0 [20 C., V]: 2.19 CC-4-V 13.50% CCP-V-1 11.50% CCP-V2-1 10.00% BCH-32 5.00%

Example 125

(275) TABLE-US-00131 Y-4O-O4 10.00% Clearing point [ C.]: 100 CCY-3-O2 5.00% n [589 nm, 20 C.]: 0.1203 CCY-3-O3 3.50% [1 kHz, 20 C.]: 2.0 CPY-3-O2 5.50% .sub.|| [1 kHz, 20 C.]: 3.4 PTP-302FF 3.50% .sub. [1 kHz, 20 C.]: 5.4 CPTP-302FF 5.00% .sub.1 [mPa .Math. s, 20 C.]: 117 CPTP-502FF 5.00% K.sub.1 [pN, 20 C.]: 15.6 CCH-301 5.00% K.sub.3 [pN, 20 C.]: 18.5 CC-4-V 15.00% V.sub.0 [20 C., V]: 3.17 CC-3-V1 8.00% CCP-V-1 13.00% CCP-V2-1 13.00% BCH-32 5.00% CPTP-3-1 3.50%

Example 126

(276) TABLE-US-00132 BCH-32 16.00% Clearing point [ C.]: 10.5 BCH-52 6.50% n [589 nm, 20 C.]: 0.1503 CCY-3-O1 5.00% [1 kHz, 20 C.]: 4.2 CCY-3-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.8 CCY-3-O3 6.00% .sub. [1 kHz, 20 C.]: 8.0 CCY-4-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 297 CCY-5-O2 7.00% K.sub.1 [pN, 20 C.]: 18.3 CY-3-O4 13.00% K.sub.3 [pN, 20 C.]: 17.3 PY-3-O2 5.50% V.sub.0 [20 C., V]: 2.13 PY-4-O2 9.00% PYP-2-3 8.00% PYP-2-4 8.00%

Example 126a

(277) The mixture from Example 126 is additionally stabilised with

(278) 0.015% of

(279) ##STR00424##
and
0.015% of

(280) ##STR00425##

Example 127

(281) TABLE-US-00133 CC-3-V 35.50% Clearing point [ C.]: 79.8 CCY-3-O2 6.00% n [589 nm, 20 C.]: 0.0962 CCY-3-O3 6.00% [1 kHz, 20 C.]: 3.4 CCY-4-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-5-O2 3.50% .sub. [1 kHz, 20 C.]: 7.0 CPY-2-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 111 CPY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 13.3 CY-3-O4 10.00% K.sub.3 [pN, 20 C.]: 15.2 CY-5-O2 9.00% V.sub.0 [20 C., V]: 2.23 PGIGI-3-F 5.00%

Example 128

(282) TABLE-US-00134 CC-3-V 31.50% Clearing point [ C.]: 79.6 CCP-V-1 5.00% n [589 nm, 20 C.]: 0.1044 CCY-3-O2 6.00% [1 kHz, 20 C.]: 3.4 CCY-3-O3 6.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-4-O2 5.50% .sub. [1 kHz, 20 C.]: 7.0 CPY-2-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 115 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 13.3 CY-3-O4 7.00% K.sub.3 [pN, 20 C.]: 15.2 CY-5-O2 7.00% V.sub.0 [20 C., V]: 2.24 PGIGI-3-F 5.00% PY-3-O2 7.00%

Example 129

(283) TABLE-US-00135 CC-3-V 36.50% Clearing point [ C.]: 84.9 CCP-V-1 3.00% n [589 nm, 20 C.]: 0.1054 CCY-3-O1 6.50% [1 kHz, 20 C.]: 3.5 CCY-3-O2 3.50% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 5.00% .sub. [1 kHz, 20 C.]: 7.0 CLY-3-O3 9.00% .sub.1 [mP .Math. s, 20 C.]: 108 CPY-2-O2 11.00% K.sub.1 [pN, 20 C.]: 14.4 CPY-3-O2 9.00% K.sub.3 [pN, 20 C.]: 15.7 CY-3-O2 3.00% V.sub.0 [20 C., V]: 2.24 PY-3-O2 13.50%

Example 130

(284) TABLE-US-00136 CC-3-V 39.00% Clearing point [ C.]: 75.2 BCH-3F.F.F 8.00% n [589 nm, 20 C.]: 0.1298 PGU-2-F 6.00% [1 kHz, 20 C.]: 18.3 PGU-3-F 6.00% .sub.|| [1 kHz, 20 C.]: 22.6 APUQU-2-F 6.00% .sub. [1 kHz, 20 C.]: 4.3 APUQU-3-F 8.00% .sub.1 [mPa .Math. s, 20 C.]: 99 PGUQU-3-F 6.00% K.sub.1 [pN, 20 C.]: 10.9 PGUQU-4-F 6.00% K.sub.3 [pN, 20 C.]: 11.1 PGUQU-5-F 6.00% V.sub.0 [20 C., V]: 0.81 DPGU-4-F 9.00%

Example 131

(285) TABLE-US-00137 CC-3-V 38.50% Clearing point [ C.]: 74.9 CCY-3-O1 4.50% n [589 nm, 20 C.]: 0.1012 CCY-3-O2 4.00% [1 kHz, 20 C.]: 3.7 CCY-4-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.7 CLY-3-O2 8.00% .sub. [1 kHz, 20 C.]: 7.4 CPY-2-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 94 CPY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 13.4 PY-1-O4 7.50% K.sub.3 [pN, 20 C.]: 14.4 PY-3-O2 6.00% V.sub.0 [20 C., V]: 2.08 Y-4O-O4 4.50% LTS (bulk) [20 C.] >1000 h

Example 131a

(286) The mixture from Example 131 is additionally mixed with

(287) 0.25% of

(288) ##STR00426##
and
0.25% of

(289) ##STR00427##

Example 132

(290) TABLE-US-00138 CC-3-V 40.50% Clearing point [ C.]: 74.8 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1073 CCPC-33 3.00% [1 kHz, 20 C.]: 1.9 CCY-3-O2 9.00% .sub.|| [1 kHz, 20 C.]: 3.2 CPY-2-O2 9.00% .sub. [1 kHz, 20 C.]: 5.2 CPY-3-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 63 PP-1-2V1 6.00% K.sub.1 [pN, 20 C.]: 12.6 PY-3-O2 7.00% K.sub.3 [pN, 20 C.]: 14.1 PYP-2-3 8.00% V.sub.0 [20 C., V]: 2.86 Y-4O-O4 3.00%

Example 132a

(291) The mixture from Example 132 is additionally stabilised with

(292) 0.04% of

(293) ##STR00428##
and
0.02% of

(294) ##STR00429##

Example 133

(295) TABLE-US-00139 APUQU-2-F 2.50% Clearing point [ C.]: 97.5 APUQU-3-F 7.00% n [589 nm, 20 C.]: 0.1000 PGUQU-3-F 4.00% [1 kHz, 20 C.]: 8.0 PGUQU-4-F 4.00% .sub.|| [1 kHz, 20 C.]: 11.1 PUQU-3-F 4.00% .sub. [1 kHz, 20 C.]: 3.1 CCP-V-1 6.00% .sub.1 [mPa .Math. s, 20 C.]: 93 CCP-V2-1 14.00% K.sub.1 [pN, 20 C.]: 15.3 CCGU-3-F 3.50% K.sub.3 [pN, 20 C.]: 17.6 CCQU-3-F 10.00% V.sub.0 [20 C., V]: 1.45 PCH-302 6.50% CC-3-V 25.00% CC-3-V1 8.00% CCP-30CF.sub.3 5.00% PPGU-3-F 0.50%

Example 133a

(296) The mixture from Example 133 is additionally mixed with

(297) 0.25% of

(298) ##STR00430##

Example 134

(299) TABLE-US-00140 CY-3-O2 18.50% Clearing point [ C.]: 80 CCY-3-O2 11.00% n [589 nm, 20 C.]: 0.0896 CCY-4-O2 9.00% [1 kHz, 20 C.]: 3.4 CPY-2-O2 7.50% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-3-O2 9.00% .sub. [1 kHz, 20 C.]: 6.9 CCH-34 9.00% .sub.1 [mPa .Math. s, 20 C.]: 117 CCH-35 9.00% K.sub.1 [pN, 20 C.]: 14.4 CC-3-V 10.00% K.sub.3 [pN, 20 C.]: 15.1 CCH-301 9.00% V.sub.0 [20 C., V]: 2.23 CCH-303 5.00% PYP-2-3 3.00%

Example 134a

(300) The mixture from Example 134 is additionally mixed with

(301) 0.2% of

(302) ##STR00431##

Example 135

(303) TABLE-US-00141 CY-3-O2 10.50% Clearing point [ C.]: 79.7 PY-1-O4 5.00% n [589 nm, 20 C.]: 0.1113 PY-3-O2 7.50% [1 kHz, 20 C.]: 4.4 PY-4-O2 4.00% K.sub.1 [pN, 20 C.]: 14.5 CCY-3-O1 5.50% K.sub.3 [pN, 20 C.]: 16.7 CCY-3-O2 5.00% V.sub.0 [20 C., V]: 2.05 CCY-4-O2 4.00% CLY-3-O2 9.00% CPY-2-O2 9.00% CPY-3-O2 9.00% CC-3-V 23.50% CC-3-V1 7.00% CBC-33F 1.00%

Example 136

(304) TABLE-US-00142 APUQU-3-F 3.00% Clearing point [ C.]: 90.5 CC-3-V1 7.75% n [589 nm, 20 C.]: 0.1057 CC-4-V 10.00% [1 kHz, 20 C.]: 7.4 CC-5-V 9.25% .sub.1 [mPa .Math. s, 20 C.]: 91 CCGU-3-F 7.00% K.sub.1 [pN, 20 C.]: 13.6 CCH-34 3.00% K.sub.3 [pN, 20 C.]: 15.5 CCP-30CF.sub.3 2.50% V.sub.0 [20 C., V]: 1.43 CCP-V-1 14.00% CCP-V2-1 9.50% PCH-301 11.00% PGP-2-2V 2.00% PGUQU-3-F 5.00% PPGU-3-F 0.50% PUQU-3-F 12.00% APUQU-2-F 3.50%

Example 137

(305) TABLE-US-00143 CC-3-V 27.00% Clearing point [ C.]: 74.9 CCY-3-1 9.50% n [589 nm, 20 C.]: 0.1093 CCP-3-1 8.00% [1 kHz, 20 C.]: 3.8 CLY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 10.50% .sub. [1 kHz, 20 C.]: 7.5 CPY-3-O2 10.50% .sub.1 [mPa .Math. s, 20 C.]: 108 CY-3-O2 15.00% K.sub.1 [pN, 20 C.]: 14.1 PY-3-O2 13.50% K.sub.3 [pN, 20 C.]: 15.8 V.sub.0 [20 C., V]: 2.16

Example 138

(306) TABLE-US-00144 CC-3-V 16.00% Clearing point [ C.]: 85.4 CC-3-V1 5.00% n [589 nm, 20 C.]: 0.1060 CCH-34 7.00% [1 kHz, 20 C.]: 3.7 CCP-3-1 1.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-3-O1 6.00% .sub. [1 kHz, 20 C.]: 7.4 CCY-3-O2 7.50% .sub.1 [mPa .Math. s, 20 C.]: 114 CCY-3-O3 2.00% K.sub.1 [pN, 20 C.]: 13.4 CCY-4-O2 5.00% K.sub.3 [pN, 20 C.]: 14.5 CPY-2-O2 10.00% V.sub.0 [20 C., V]: 2.09 CPY-3-O2 9.00% CY-3-O2 10.00% CY-3-O4 6.50% CY-5-O4 6.00% PYP-2-3 5.50% PYP-2-4 3.50%

Example 138a

(307) The mixture from Example 138 is additionally stabilised with

(308) 0.04% of

(309) ##STR00432##

Example 139

(310) TABLE-US-00145 CCH-23 12.00% Clearing point [ C.]: 110.7 CCH-34 10.00% n [589 nm, 20 C.]: 0.1002 CCP-3-1 7.00% [1 kHz, 20 C.]: 2.9 CCY-3-1 10.00% .sub.|| [1 kHz, 20 C.]: 3.2 CCY-3-O1 1.50% .sub. [1 kHz, 20 C.]: 6.1 CCY-3-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 147 CCY-3-O3 7.50% K.sub.1 [pN, 20 C.]: 17.3 CCY-4-O2 9.00% K.sub.3 [pN, 20 C.]: 18.3 CPGP-4-3 2.00% V.sub.0 [20 C., V]: 2.65 CPY-2-O2 8.00% CPY-3-O2 8.00% CY-3-O2 1.50% CY-3-O4 3.00% PCH-301 10.00% PYP-2-3 1.50%

Example 139a

(311) The mixture from Example 139 is additionally stabilised with

(312) 0.04% of

(313) ##STR00433##

Example 140

(314) TABLE-US-00146 BCH-32 1.50% Clearing point [ C.]: 74.3 CC-3-V 19.50% n [589 nm, 20 C.]: 0.1089 CC-3-V1 5.50% [1 kHz, 20 C.]: 3.8 CCP-3-1 8.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCP-3-3 4.50% .sub. [1 kHz, 20 C.]: 7.5 CLY-3-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 115 CPY-2-O2 10.50% K.sub.1 [pN, 20 C.]: 13.7 CPY-3-O2 10.50% K.sub.3 [pN, 20 C.]: 16.1 CY-3-O2 15.00% V.sub.0 [20 C., V]: 2.18 CY-5-O2 9.00% PY-3-O2 10.00%

Example 141

(315) TABLE-US-00147 CY-3-O2 15.00% Clearing point [ C.]: 74.7 CY-5-O2 6.50% n [589 nm, 20 C.]: 0.1082 CCY-3-O2 11.00% [1 kHz, 20 C.]: 3.0 CPY-2-O2 5.50% .sub.|| [1 kHz, 20 C.]: 3.6 CPY-3-O2 10.50% .sub. [1 kHz, 20 C.]: 6.6 CC-3-V 28.50% .sub.1 [mPa .Math. s, 20 C.]: 97 CC-3-V1 10.00% K.sub.1 [pN, 20 C.]: 12.9 PYP-2-3 12.50% K.sub.3 [pN, 20 C.]: 15.7 PPGU-3-F 0.50% V.sub.0 [20 C., V]: 2.42

Example 142

(316) TABLE-US-00148 PGUQU-3-F 5.00% Clearing point [ C.]: 84.8 CCQU-3-F 8.00% n [589 nm, 20 C.]: 0.1035 CCQU-5-F 4.00% [1 kHz, 20 C.]: 10.1 PUQU-3-F 13.50% .sub.|| [1 kHz, 20 C.]: 13.5 APUQU-2-F 3.00% .sub. [1 kHz, 20 C.]: 3.4 APUQU-3-F 6.00% .sub.1 [mPa .Math. s, 20 C.]: 86 CC-3-V 25.50% K.sub.1 [pN, 20 C.]: 12.3 CC-3-V1 6.00% K.sub.3 [pN, 20 C.]: 15.0 CCP-V-1 13.00% V.sub.0 [20 C., V]: 1.17 CCP-V2-1 6.00% PPGU-3-F 0.50% BCH-3F.F 7.50% BCH-2F.F 2.00%

Example 142a

(317) The mixture from Example 142 is additionally mixed with

(318) 0.25% of

(319) ##STR00434##

Example 143

(320) TABLE-US-00149 CY-3-O2 12.00% Clearing point [ C.]: 85.4 CY-5-O2 12.00% n [589 nm, 20 C.]: 0.1039 CCY-3-O3 5.00% CCY-4-O2 5.00% CPY-2-O2 10.00% CPY-3-O2 10.00% CCY-2-1 4.00% CC-3-V 16.00% CCH-23 10.00% CCH-34 4.00% CCP-V-1 4.00% PGP-2-5 2.00% CPGP-5-2 3.00% CPGP-5-3 3.00%

Example 144

(321) TABLE-US-00150 CC-3-V 41.50% Clearing point [ C.]: 74.5 CCY-3-O1 2.50% n [589 nm, 20 C.]: 0.0984 CCY-3-O2 11.50% [1 kHz, 20 C.]: 3.3 CCY-3-O3 5.00% .sub.|| [1 kHz, 20 C.]: 3.5 CPY-2-O2 5.00% .sub. [1 kHz, 20 C.]: 6.7 CPY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 89 CY-3-O2 9.50% K.sub.1 [pN, 20 C.]: 13.2 PY-3-O2 7.00% K.sub.3 [pN, 20 C.]: 15.2 PY-4-O2 3.00% V.sub.0 [20 C., V]: 2.29 PYP-2-3 3.00%

Example 144a

(322) The mixture from Example 144 is additionally mixed with 0.001% of Irganox 1076 (octadecyl 3-(3,5-di-tert-butyl-4-hydroxyphenyl)propionate, BASF) and additionally with

(323) 0.4% of

(324) ##STR00435##

Example 145

(325) TABLE-US-00151 CC-3-V 30.50% Clearing point [ C.]: 80.1 CC-3-V1 4.50% n [589 nm, 20 C.]: 0.1033 CCY-3-O1 6.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 8.00% .sub.|| [1 kHz, 20 C.]: 3.6 CLY-3-O2 8.00% .sub. [1 kHz, 20 C.]: 7.6 CPY-2-O2 8.00% .sub.1 [mPa .Math. s, 20 C.]: 113 CPY-3-O2 12.00% K.sub.1 [pN, 20 C.]: 14.4 CY-3-O2 15.00% K.sub.3 [pN, 20 C.]: 17.0 PY-3-O2 8.00% V.sub.0 [20 C., V]: 2.16

Example 146

(326) TABLE-US-00152 CC-3-V 41.50% Clearing point [ C.]: 74.5 CCY-3-O1 2.50% [1 kHz, 20 C.]: 3.3 CCY-3-O2 11.50% K.sub.1 [pN, 20 C.]: 13.2 CCY-3-O3 5.00% K.sub.3 [pN, 20 C.]: 15.2 CPY-2-O2 5.00% V.sub.0 [20 C., V]: 2.29 CPY-3-O2 12.00% CY-3-O2 9.50% PY-3-O2 7.00% PY-4-O2 3.00% PYP-2-3 3.00%

Example 147

(327) TABLE-US-00153 CC-3-V 26.00% Clearing point [ C.]: 80.5 CCY-3-O2 6.00% n [589 nm, 20 C.]: 0.1040 CCY-3-O3 6.00% [1 kHz, 20 C.]: 4.0 CCY-4-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-5-O2 6.00% .sub. [1 kHz, 20 C.]: 7.7 CPY-2-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 133 CPY-3-O2 6.00% K.sub.1 [pN, 20 C.]: 13.6 PYP-2-3 7.00% K.sub.3 [pN, 20 C.]: 15.4 CY-3-O2 15.00% V.sub.0 [20 C., V]: 2.07 CY-5-O2 12.00% LTS (bulk) [20 C.] >1000 h BCH-32 4.00%

Example 147a

(328) The mixture from Example 147 is additionally mixed with

(329) 0.3% of

(330) ##STR00436##

Example 148

(331) TABLE-US-00154 CC-3-V 26.50% Clearing point [ C.]: 84.6 CC-3-V1 2.00% n [589 nm, 20 C.]: 0.1076 CCH-34 2.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O3 5.00% .sub. [1 kHz, 20 C.]: 7.7 CCY-4-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 129 CPY-2-O2 10.00% K.sub.1 [pN, 20 C.]: 13.9 CPY-3-O2 10.00% K.sub.3 [pN, 20 C.]: 15.4 CY-3-O2 10.50% V.sub.0 [20 C., V]: 2.06 PYP-2-3 9.00% Y-4O-O4 5.00%

Example 148a

(332) The mixture from Example 148 is additionally stabilised with

(333) 0.04% of

(334) ##STR00437##
and
0.015% of

(335) ##STR00438##

Example 149

(336) TABLE-US-00155 APUQU-3-F 1.50% Clearing point [ C.]: 110.1 CC-3-V 34.00% n [589 nm, 20 C.]: 0.1208 CC-3-V1 5.00% [1 kHz, 20 C.]: 6.2 CCP-30CF.sub.3 4.50% .sub.|| [1 kHz, 20 C.]: 9.2 CCP-V-1 10.50% .sub. [1 kHz, 20 C.]: 3.0 CCP-V2-1 6.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CCVC-3-V 3.50% K.sub.1 [pN, 20 C.]: 16.3 CPGP-5-2 4.50% K.sub.3 [pN, 20 C.]: 18.9 CPGP-5-3 4.50% V.sub.0 [20 C., V]: 1.70 DGUQU-4-F 3.00% PGP-2-3 4.00% PGP-2-4 2.00% PGUQU-3-F 5.00% PGUQU-4-F 3.50% PGUQU-5-F 3.00% PPGU-3-F 0.50% PUQU-3-F 5.00%

Example 150

(337) TABLE-US-00156 APUQU-3-F 1.50% Clearing point [ C.]: 110 CC-3-V 35.50% n [589 nm, 20 C.]: 0.1257 CCP-30CF.sub.3 4.00% [1 kHz, 20 C.]: 6.3 CCP-V-1 12.00% .sub.|| [1 kHz, 20 C.]: 9.3 CCP-V2-1 4.50% .sub. [1 kHz, 20 C.]: 3.0 CCVC-3-V 4.00% .sub.1 [mPa .Math. s, 20 C.]: 104 CPGP-5-2 5.00% K.sub.1 [pN, 20 C.]: 16.1 CPGP-5-3 5.00% K.sub.3 [pN, 20 C.]: 18.7 DGUQU-4-F 3.00% V.sub.0 [20 C., V]: 1.69 PGP-2-3 4.00% PGP-2-4 2.00% PGUQU-3-F 5.00% PGUQU-4-F 3.50% PGUQU-5-F 3.00% PPGU-3-F 0.50% PUQU-3-F 5.00% PP-1-2V1 2.50%

Example 151

(338) TABLE-US-00157 CY-3-O2 5.00% Clearing point [ C.]: 102 CY-3-O4 15.00% n [589 nm, 20 C.]: 0.2503 CCY-3-O2 6.00% [1 kHz, 20 C.]: 4.0 CCY-3-O3 6.00% .sub.|| [1 kHz, 20 C.]: 4.3 CPY-2-O2 3.00% .sub. [1 kHz, 20 C.]: 8.3 PTP-102 5.00% .sub.1 [mPa .Math. s, 20 C.]: 392 PPTUI-3-2 15.00% K.sub.1 [pN, 20 C.]: 19.5 PPTUI-3-4 11.00% K.sub.3 [pN, 20 C.]: 24.0 PTP-302FF 12.00% V.sub.0 [20 C., V]: 2.57 PTP-502FF 12.00% CPTP-302FF 5.00% CPTP-502FF 5.00%

Example 152

(339) TABLE-US-00158 CC-3-V 35.00% Clearing point [ C.]: 79.6 CCP-3-1 7.50% n [589 nm, 20 C.]: 0.1095 CCPC-33 2.00% [1 kHz, 20 C.]: 2.6 CCY-3-O2 7.00% .sub.|| [1 kHz, 20 C.]: 3.5 CCY-4-O2 7.50% .sub. [1 kHz, 20 C.]: 6.1 CPY-2-O2 8.50% .sub.1 [mPa .Math. s, 20 C.]: 92 CPY-3-O2 9.00% K.sub.1 [pN, 20 C.]: 14.5 PP-1-2V1 5.50% PY-3-O2 8.00% PYP-2-3 5.00% Y-4O-O4 5.00%

Example 152a

(340) The mixture from Example 152 is additionally stabilised with

(341) 0.04% of

(342) ##STR00439##
and
0.02% of

(343) ##STR00440##

Example 153

(344) TABLE-US-00159 CY-3-O4 25.00% Clearing point [ C.]: 81.2 CY-5-O2 9.00% n [589 nm, 20 C.]: 0.1531 CCY-3-O2 7.00% [1 kHz, 20 C.]: 5.0 CCY-3-O3 4.50% .sub.|| [1 kHz, 20 C.]: 4.1 CPY-2-O2 10.00% .sub. [1 kHz, 20 C.]: 9.1 CPY-3-O2 10.00% .sub.1 [mPa .Math. s, 20 C.]: 298 PYP-2-3 14.00% K.sub.1 [pN, 20 C.]: 13.1 PYP-2-4 10.00% K.sub.3 [pN, 20 C.]: 15.9 CCP-V-1 3.00% V.sub.0 [20 C., V]: 1.89 BCH-32 2.00% PP-1-2V1 3.50% PGP-2-3 2.00%

Example 153a

(345) The mixture from Example 153 is additionally mixed with

(346) 10% of

(347) ##STR00441##

Example 154

(348) TABLE-US-00160 CC-3-V 29.00% Clearing point [ C.]: 80.1 CCY-3-O1 8.00% n [589 nm, 20 C.]: 0.1033 CCY-3-O2 6.00% [1 kHz, 20 C.]: 4.5 CCY-4-O2 2.00% .sub.|| [1 kHz, 20 C.]: 4.0 CLY-3-O2 8.50% .sub. [1 kHz, 20 C.]: 8.4 CLY-3-O3 7.50% .sub.1 [mPa .Math. s, 20 C.]: 98 CPY-2-O2 10.00% K.sub.1 [pN, 20 C.]: 13.2 CPY-3-O2 7.50% K.sub.3 [pN, 20 C.]: 14.6 CY-3-O2 6.50% V.sub.0 [20 C., V]: 1.91 PY-3-O2 10.00% Y-4O-O4 5.00%

Example 154a

(349) The mixture from Example 154 is additionally stabilised with

(350) 0.04% of

(351) ##STR00442##
and
0.02% of

(352) ##STR00443##

Example 155

(353) TABLE-US-00161 CC-3-V 34.00% Clearing point [ C.]: 79.7 CCPC-33 1.00% n [589 nm, 20 C.]: 0.1095 CCY-3-1 4.00% [1 kHz, 20 C.]: 3.5 CCY-3-O2 10.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-4-O2 9.50% .sub. [1 kHz, 20 C.]: 7.2 CPY-2-O2 9.00% .sub.1 [mPa .Math. s, 20 C.]: 105 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 14.0 PP-1-2V1 1.50% PY-3-O2 10.00% PYP-2-3 6.00% Y-4O-O4 5.00%

Example 155a

(354) The mixture from Example 155 is additionally stabilised with

(355) 0.04% of

(356) ##STR00444##
and
0.02% of

(357) ##STR00445##

Example 156

(358) TABLE-US-00162 CC-3-V 19.00% Clearing point [ C.]: 80.2 CCY-3-O1 5.00% n [589 nm, 20 C.]: 0.1104 CCY-3-O2 7.00% [1 kHz, 20 C.]: 3.7 CCY-3-O3 12.00% .sub.|| [1 kHz, 20 C.]: 3.6 CCY-4-O2 8.00% .sub. [1 kHz, 20 C.]: 7.3 CPY-2-O2 9.50% .sub.1 [mPa .Math. s, 20 C.]: 143 CPY-3-O2 10.00% K.sub.1 [pN, 20 C.]: 12.9 CY-3-O2 12.00% K.sub.3 [pN, 20 C.]: 14.5 CY-3-O4 3.50% V.sub.0 [20 C., V]: 2.09 PP-1-3 7.00% PP-1-4 7.00%

Example 157

(359) TABLE-US-00163 CY-3-O2 15.00% Clearing point [ C.]: 79.1 CY-5-O2 9.50% n [589 nm, 20 C.]: 0.0944 CCY-3-O1 4.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O3 4.50% .sub. [1 kHz, 20 C.]: 7.7 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 120 CCY-5-O2 4.00% K.sub.1 [pN, 20 C.]: 13.4 CPY-2-O2 8.00% K.sub.3 [pN, 20 C.]: 15.4 CPY-3-O2 9.00% V.sub.0 [20 C., V]: 2.06 PYP-2-4 2.00% CC-3-V 32.00%

Example 157a

(360) The mixture from Example 157 is additionally stabilised with

(361) 0.015% of

(362) ##STR00446##

Example 158

(363) TABLE-US-00164 CY-3-O2 15.00% Clearing point [ C.]: 79.1 CY-5-O2 9.50% n [589 nm, 20 C.]: 0.0944 CCY-3-O1 4.00% [1 kHz, 20 C.]: 4.0 CCY-3-O2 6.00% .sub.|| [1 kHz, 20 C.]: 3.7 CCY-3-O3 4.50% .sub. [1 kHz, 20 C.]: 7.7 CCY-4-O2 6.00% .sub.1 [mPa .Math. s, 20 C.]: 120 CCY-5-O2 4.00% K.sub.1 [pN, 20 C.]: 13.4 CPY-2-O2 8.00% K.sub.3 [pN, 20 C.]: 15.4 CPY-3-O2 9.00% V.sub.0 [20 C., V]: 2.06 PYP-2-4 2.00% CC-3-V 32.00%

Example 158a

(364) The mixture from Example 158 is additionally stabilised with

(365) 0.015% of

(366) ##STR00447##

Example 159

(367) TABLE-US-00165 APUQU-3-F 4.00% Clearing point [ C.]: 85.7 CC-3-V 41.00% n [589 nm, 20 C.]: 0.1004 CC-3-V1 6.50% [1 kHz, 20 C.]: 6.8 CCP-V-1 12.00% .sub.|| [1 kHz, 20 C.]: 9.8 CCP-V2-1 11.00% .sub. [1 kHz, 20 C.]: 3.0 CPGP-5-3 2.50% .sub.1 [mPa .Math. s, 20 C.]: 69 PGUQU-3-F 5.00% K.sub.1 [pN, 20 C.]: 13.0 PGUQU-4-F 4.00% K.sub.3 [pN, 20 C.]: 16.6 PGUQU-5-F 3.50% V.sub.0 [20 C., V]: 1.47 PUQU-3-F 10.50%

Example 160

(368) TABLE-US-00166 CC-3-V 32.50% Clearing point [ C.]: 74.7 CC-3-V1 1.50% n [589 nm, 20 C.]: 0.1090 CCY-3-O1 8.50% [1 kHz, 20 C.]: 3.8 CCY-3-O2 5.50% .sub.|| [1 kHz, 20 C.]: 3.7 CLY-3-O2 10.00% .sub. [1 kHz, 20 C.]: 7.5 CPY-3-O2 9.50% .sub.1 [mPa .Math. 20 C.]: 102 PY-3-O2 10.50% K.sub.1 [pN, 20 C.]: 13.8 CY-3-O2 14.00% K.sub.3 [pN, 20 C.]: 15.7 PYP-2-3 8.00% V.sub.0 [20 C., V]: 2.15

Example 161

(369) TABLE-US-00167 CC-3-V 33.00% Clearing point [ C.]: 80.2 CCY-3-O1 6.00% n [589 nm, 20 C.]: 0.1116 CCY-3-O2 8.00% [1 kHz, 20 C.]: 4.1 CCY-4-O2 2.50% .sub.|| [1 kHz, 20 C.]: 3.7 CPY-2-O2 8.00% .sub. [1 kHz, 20 C.]: 7.8 CPY-3-O2 12.00% .sub.1 [mPa .Math. s, 20 C.]: 119 CLY-3-O2 8.00% K.sub.1 [pN, 20 C.]: 14.5 PY-1-O4 1.50% K.sub.3 [pN, 20 C.]: 16.1 PY-3-O2 10.00% V.sub.0 [20 C.,]: 2.09 PY-4-O2 8.00% CY-3-O2 3.00%

Example 161a

(370) The mixture from Example 161 is additionally stabilised with

(371) 0.008% of

(372) ##STR00448##

Example 162

(373) TABLE-US-00168 BCH-3F.F 5.00% Clearing point [ C.]: 101 BCH-3F.F.F 8.50% n [589 nm, 20 C.]: 0.0925 CC-3-V1 10.00% [1 kHz, 20 C.]: 5.3 CC-4-V 12.50% .sub.|| [1 kHz, 20 C.]: 8.3 CCG-V-F 9.00% .sub.1 [mPa .Math. s, 20 C.]: 119 CCP-2F.F.F 3.50% K.sub.1 [pN, 20 C.]: 14.2 CCP-3-1 4.50% K.sub.3 [pN, 20 C.]: 19.9 CCP-3F.F.F 10.00% V.sub.0 [20 C., V]: 1.73 CCP-V-1 12.00% CCP-V2-1 7.00% ECCP-5F.F 13.00% PUQU-3-F 5.00%

Example 163

(374) TABLE-US-00169 APUQU-2-F 4.00% Clearing point [ C.]: 86.4 APUQU-3-F 6.00% n [589 nm, 20 C.]: 0.1030 PUQU-3-F 10.00% [1 kHz, 20 C.]: 7.0 CCQU-3-F 2.00% .sub.|| [1 kHz, 20 C.]: 10.1 CCP-V-1 13.00% .sub.1 [mPa .Math. s, 20 C.]: 71 CCP-V2-1 7.00% K.sub.1 [pN, 20 C.]: 13.2 PGUQU-3-F 6.00% K.sub.3 [pN, 20 C.]: 15.8 CC-3-V 40.00% V.sub.0 [20 C., V]: 1.45 CC-3-V1 5.50% PGP-2-3 3.00% CPGP-5-2 3.00% PPGU-3-F 0.50%

Example 163a

(375) The mixture from Example 163 is additionally mixed with 0.25% of RM-41

(376) ##STR00449##

Example 164

(377) TABLE-US-00170 Y-4O-O4 9.00% Clearing point [ C.]: 96 CY-3-O4 12.00% n [589 nm, 20 C.]: 0.0796 CCY-3-O1 5.00% [1 kHz, 20 C.]: 2.3 CCY-3-O2 5.50% .sub.|| [1 kHz, 20 C.]: 3.4 CCY-3-O3 5.50% .sub. [1 kHz, 20 C.]: 5.7 CC-4-V 15.00% K.sub.1 [pN, 20 C.]: 14.8 CC-5-V 5.50% K.sub.3 [pN, 20 C.]: 16.6 CC-3-V1 6.50% V.sub.0 [20 C., V]: 2.85 CCP-V-1 11.00% CCP-V2-1 10.00% CH-33 3.00% CH-35 3.00% CCPC-33 4.50% CCPC-34 4.50%

Example 165

(378) TABLE-US-00171 Y-4O-O4 11.50% Clearing point [ C.]: 95 CCY-3-O1 4.00% n [589 nm, 20 C.]: 0.1697 CCY-3-O2 5.00% [1 kHz, 20 C.]: 4.4 CCY-3-O3 2.50% .sub.|| [1 kHz, 20 C.]: 4.1 CPY-3-O2 4.00% .sub. [1 kHz, 20 C.]: 8.5 CC-4-V 10.00% .sub.1 [mPa .Math. s, 20 C.]: 193 CCP-V-1 6.00% K.sub.1 [pN, 20 C.]: 16.8 CCP-V2-1 12.00% K.sub.3 [pN, 20 C.]: 19.5 BCH-32 5.00% V.sub.0 [20 C., V]: 2.23 PTP-302FF 12.00% PTP-502FF 12.00% CPTP-302FF 8.00% CPTP-502FF 8.00%

Example 166

(379) TABLE-US-00172 CY-3-O2 10.00% Clearing point [ C.]: 80.7 PY-1-O4 5.00% n [589 nm, 20 C.]: 0.1123 PY-3-O2 6.50% [1 kHz, 20 C.]: 4.2 PY-4-O2 3.00% .sub.|| [1 kHz, 20 C.]: 3.8 CCY-3-O1 5.00% .sub. [1 kHz, 20 C.]: 8.0 CCY-3-O2 5.00% .sub.1 [mPa .Math. s, 20 C.]: 150 CCY-4-O2 3.00% K.sub.1 [pN, 20 C.]: 14.6 CLY-3-O2 8.00% K.sub.3 [pN, 20 C.]: 15.2 CPY-2-O2 10.00% V.sub.0 [20 C., V]: 2.01 CPY-3-O2 10.00% CCH-301 8.50% CCH-23 12.00% CCH-34 4.50% CCH-35 3.00% BCH-32 6.50%

Example 167

(380) TABLE-US-00173 PCH-3N.F.F 7.00% Clearing point [ C.]: 91 CP-1V-N 18.00% n [589 nm, 20 C.]: 0.2003 CP-V2-N 16.00% [1 kHz, 20 C.]: 10.3 CC-4-V 12.00% .sub.|| [1 kHz, 20 C.]: 14.3 CCP-V-1 9.00% .sub. [1 kHz, 20 C.]: 4.0 PPTUI-3-2 18.00% PPTUI-3-4 20.00%

Example 168

(381) TABLE-US-00174 BCH-32 8.00% Clearing point [ C.]: 96 CC-3-V 24.50% n [589 nm, 20 C.]: 0.1195 CCP-V-1 8.00% [1 kHz, 20 C.]: 2.7 CCY-2-1 2.00% .sub.|| [1 kHz, 20 C.]: 3.3 CCY-3-O1 6.00% CCY-3-O3 2.00% CLY-3-O2 5.00% CLY-3-O3 5.00% CPY-2-O2 6.50% CPY-3-O2 6.00% CY-3-O2 6.00% CY-3-O4 3.00% CY-5-O2 5.00% PYP-2-3 6.50% PYP-2-4 6.50%

Example 168a

(382) The mixture from Example 168 is additionally stabilised with

(383) 0.03% of

(384) ##STR00450##
and mixed with
0.4% of

(385) ##STR00451##

Filling device and use thereof for dispensing a fluid

Assignee

Inventors

Cpc classification

Classification Explorer

B65B65/06

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B39/12

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B3/28

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B57/04

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B31/00

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B57/145

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B43/59

PERFORMING OPERATIONS; TRANSPORTING

International classification

Classification Explorer

B65B3/28

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B57/14

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B65/06

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B31/00

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B57/04

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B39/12

PERFORMING OPERATIONS; TRANSPORTING

Classification Explorer

B65B43/59

PERFORMING OPERATIONS; TRANSPORTING

Abstract

Claims

Description