METHOD FOR MAKING XUAN FLANNELETTE

Abstract

The present invention discloses a method for making Xuan flannelette, which includes the following steps: firstly, drying and setting polyester fiber-chemical fiber gray fabric; secondly, coating the set gray fabric with a first sizing and drying the gray fabric, and finally, coating the dried gray fabric with a second sizing and drying the gray fabric. By designing a double-layer coating on the polyester fiber-chemical fiber gray fabric, the present invention makes the Xuan flannelette made according to the present invention suitable for diamond painting, and the yield is improved and the cost is reduced.

Claims

1. A method for making Xuan flannelette, comprising the following steps: step 1, drying and setting polyester fiber-chemical fiber gray fabric; step 2, coating the gray fabric set in step 1 with a first sizing which has the following components by mass: 8-12 parts of styrene-acrylate emulsion, 30-50 parts of polyvinyl acetate emulsion, 4-6 parts of polysiloxane, 10-16 parts of calcium carbonate, 1-3 parts of silicon dioxide, 1-3 parts of magnesium oxide and 0.3-0.7 part of titanium dioxide, and drying the gray fabric; and step 3, coating the gray fabric dried in step 2 with a second sizing which has the following components by mass: 50-65 parts of acrylic emulsion, 10-15 parts of polyvinyl acetate emulsion, 0.08-0.2 parts of a thickening agent, 0.3-0.8 part of a crosslinking agent and 0.5-1.2 parts of a co-crosslinking agent, and drying the gray fabric.

2. The method according to claim 1, wherein in step 2, the first sizing has the following components: 9-10 parts of styrene-acrylate emulsion, 40-45 parts of polyvinyl acetate emulsion, 5-6 parts of polysiloxane, 12-14 parts of calcium carbonate, 1-2 parts of silicon dioxide, 2-2.5 parts of magnesium oxide, and 0.4-0.5 parts of titanium dioxide.

3. The method according to claim 2, wherein in step 2, the first sizing has the following components: 10 parts of styrene-acrylate emulsion, 44 parts of polyvinyl acetate emulsion, 5.5 parts of polysiloxane, 13 parts of calcium carbonate, 2 parts of silicon dioxide, 2.3 parts of magnesium oxide, and 0.5 parts of titanium dioxide.

4. The method according to claim 1, wherein in step 3, the second sizing has the following components: 58 parts of acrylic emulsion, 13 parts of polyvinyl acetate emulsion, 0.1 part of a thickening agent, 0.5 part of a crosslinking agent and 0.8 part of a co-crosslinking agent.

5. The method according to claim 1, wherein the calcium carbonate and the titanium dioxide are coupling modified.

6. The method according to claim 1, wherein the thickening agent is polyvinyl alcohol, the crosslinking agent is one or more of 2,5-dimethyl-2,5-di(tert-butylperoxy)hexane and 2,5-dimethyl-2,5-di(benzoylperoxy)hexane, and the co-crosslinking agent is one or more of trimethylolpropane triallyl ester, trimethylolpropane trimethacrylate, ethylene glycol diacrylate and diethylene glycol dimethacrylate.

7. The method according to claim 1, wherein a drying temperature in step 2 is 80-170 C., and a drying temperature in step 3 is 70-130 C.

8. The method according to claim 1, wherein a first coating layer in step 2 is - 1/10 of a weight of the gray fabric, and a second coating layer in step 3 is 1/20- 1/10 of the weight of the gray fabric.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

[0015] In order to illustrate the technical solution of the embodiments of the present invention more clearly, the accompanying drawings required for the description of the embodiments will be briefly introduced below. Apparently, the accompanying drawings in the following description are merely some rather than all embodiments of the present invention, and a person of ordinary skill in the art may still derive other drawings from these accompanying drawings without creative efforts.

[0016] FIG. 1 is a prior art diamond painting.

DESCRIPTION OF THE EMBODIMENTS

[0017] The present invention will be further described below in conjunction with specific embodiments.

[0018] In the following embodiments, styrene-acrylate emulsion was type 816; polyvinyl acetate emulsion was type SD-40; silicone oil was used as polysiloxane; calcium carbonate and titanium dioxide were modified by a coupling agent, for example, 550 coupling agent solution was sprayed for modification to improve dispersibility; pure acrylic emulsion was used as acrylic emulsion; 2,5-dimethyl-2,5-di(tert-butylperoxy)hexane was used as a crosslinking agent; ethylene glycol diacrylate was used as a co-crosslinking agent; and polyvinyl alcohol was used as a thickening agent.

Embodiment 1

[0019] A method for making Xuan flannelette, included the following steps:

[0020] First step, polyester fiber-chemical fiber gray fabric was dried and set.

[0021] Second step, the gray fabric set in the first step was coated with a first sizing and dried, and the sizing was scraped by a scraper, the first sizing had the following components by mass: 8 parts of styrene-acrylate emulsion, 30 parts of polyvinyl acetate emulsion, 4 parts of polysiloxane, 10 parts of calcium carbonate, 1 part of silicon dioxide, 1 part of magnesium oxide and 0.3 part of titanium dioxide, and the components were added to a stirring mechanism successively to stir uniformly to form the first sizing; and the coating layer was dried at 110 C., and a weight of the coating layer accounted for of a weight of the gray fabric.

[0022] Third step, the gray fabric dried in the second step was coated with a second sizing and dried, the second sizing had the following components by mass: 50 parts of acrylic emulsion, 10 parts of polyvinyl acetate emulsion, 0.08 part of a thickening agent, 0.3 part of a crosslinking agent and 0.5 part of a co-crosslinking agent; and the coating layer was dried at 100 C., and a weight of the coating layer accounted for 1/15 of a weight of the gray fabric.

Embodiment 2

[0023] A method for making Xuan flannelette, included the following steps:

[0024] First step, polyester fiber-chemical fiber gray fabric was dried and set.

[0025] Second step, the gray fabric set in the first step was coated with a first sizing and dried, and the sizing was scraped by a scraper, the first sizing had the following components by mass: 9.5 parts of styrene-acrylate emulsion, 42 parts of polyvinyl acetate emulsion, 5 parts of polysiloxane, 12 parts of calcium carbonate, 1.2 parts of silicon dioxide, 2.2 parts of magnesium oxide and 0.4 part of titanium dioxide, and the components were added to a stirring mechanism successively to stir uniformly to form the first sizing; and the coating layer was dried at 130 C., and a weight of the coating layer accounted for 1/10 of a weight of the gray fabric.

[0026] Third step, the gray fabric dried in the second step was coated with a second sizing and dried, the second sizing had the following components by mass: 55 parts of acrylic emulsion, 12 parts of polyvinyl acetate emulsion, 0.1 part of a thickening agent, 0.4 part of a crosslinking agent and 0.6 part of a co-crosslinking agent; and the coating layer was dried at 100 C., and a weight of the coating layer accounted for 1/10 of a weight of the gray fabric.

Embodiment 3

[0027] A method for making Xuan flannelette, included the following steps:

[0028] First step, polyester fiber-chemical fiber gray fabric was dried and set.

[0029] Second step, the gray fabric set in the first step was coated with a first sizing and dried, and the sizing was scraped by a scraper, the first sizing had the following components by mass: 10 parts of styrene-acrylate emulsion, 44 parts of polyvinyl acetate emulsion, 5.5 parts of polysiloxane, 13 parts of calcium carbonate, 2 parts of silicon dioxide, 2.3 parts of magnesium oxide and 0.5 part of titanium dioxide, and the components were added to a stirring mechanism successively to stir uniformly to form the first sizing; and the coating layer was dried at 110 C., and a weight of the coating layer accounted for 1/9 of a weight of the gray fabric.

[0030] Third step, the gray fabric dried in the second step was coated with a second sizing and dried, the second sizing had the following components by mass: 58 parts of acrylic emulsion, 13 parts of polyvinyl acetate emulsion, 0.1 part of a thickening agent, 0.5 part of a crosslinking agent and 0.8 part of a co-crosslinking agent; and the coating layer was dried at 90 C., and a weight of the coating layer accounted for 1/12 of a weight of the gray fabric.

Embodiment 4

[0031] A method for making Xuan flannelette, included the following steps:

[0032] First step, polyester fiber-chemical fiber gray fabric was dried and set.

[0033] Second step, the gray fabric set in the first step was coated with a first sizing and dried, and the sizing was scraped by a scraper, the first sizing had the following components by mass: 12 parts of styrene-acrylate emulsion, 50 parts of polyvinyl acetate emulsion, 6 parts of polysiloxane, 15 parts of calcium carbonate, 3 parts of silicon dioxide, 2.6 parts of magnesium oxide and 0.6 part of titanium dioxide, and the components were added to a stirring mechanism successively to stir uniformly to form the first sizing; and the coating layer was dried at 110 C., and a weight of the coating layer accounted for 1/10 of a weight of the gray fabric.

[0034] Third step, the gray fabric dried in the second step was coated with a second sizing and dried, the second sizing had the following components by mass: 63 parts of acrylic emulsion, 13 parts of polyvinyl acetate emulsion, 0.1 part of a thickening agent, 0.7 part of a crosslinking agent and 1.1 part of a co-crosslinking agent; and the coating layer was dried at 120 C., and a weight of the coating layer accounted for 1/13 of a weight of the gray fabric.

Comparative Example 1

[0035] Compared to Embodiment 1, there was only a coating of the second sizing in this comparative example.

[0036] The prepared Xuan flannelette was subjected to diamond painting preparation, where background patterns were directly jet printed without thermal transfer printing process, and the prepared diamond painting was detected to have the following properties:

[0037] Under the same conditions and standing for the same time, compared with Comparative Example 1, diamond paintings on the Xuan flannelette prepared according to Embodiments 1-4 had substantially no deformation, and the diamond painting on the Xuan flannelette prepared according to Comparative Example 1 had significant deformation.

[0038] Compared with Comparative Example 1, diamonds on the diamond paintings on the Xuan flannelette prepared according to Embodiments 1-4 had fallen off by 2-3%, diamonds on the diamond paintings on the Xuan flannelette prepared according to Embodiments 2 and 3 had substantially no fall-off (less than 1%), and diamonds on the diamond painting on the Xuan flannelette prepared according to Comparative Example 1 had fallen off by about 15%.

[0039] Compared with Comparative Example 1, the diamond paintings on the Xuan flannelette prepared according to Embodiments 1-4 had dark and bright colors, and clear patterns, but the diamond painting on the Xuan flannelette prepared according to Comparative Example 1 had light and less bright color (visible to the naked eye), and blurry patterns.

[0040] In addition, the diamond paintings on the Xuan flannelette prepared according to Embodiments 1-4 had the advantages of being resistant to high temperature, moisture and freezing, and the like.