METHOD FOR FOCUSING AND OPERATING A PARTICLE BEAM MICROSCOPE
20230078510 · 2023-03-16
Inventors
Cpc classification
H01J37/1471
ELECTRICITY
H01J37/04
ELECTRICITY
International classification
Abstract
A method for operating a particle beam microscope comprises setting a distance of an object from an objective lens, setting an excitation of the objective lens, setting an excitation of a double deflector to a first setting such that a particle beam is incident on the object at a first orientation, and recording a first particle-microscopic image at these settings. The method also comprises setting the excitation of the double deflector to a second setting such that the particle beam is incident on the object at a second orientation which differs from the first orientation; and recording a second particle-microscopic image at the second setting of the double deflector. Thereupon, a new distance of the object from the objective lens is determined based on an analysis of the first and second particle-microscopic images, and the distance of the object from the objective lens is set to the new distance.
Claims
1. A method for operating a particle beam microscope, the particle beam microscope comprising a particle beam source configured to generate a particle beam an objective lens configured to focus the particle beam on an object, and a double deflector a beam path of the particle beam between the particle beam source and the objective lens, the method comprising: when an object is set to a first distance from the objective lens, the objective lens is set to a first excitation, and the double deflector is set to a first excitation so that the particle beam is incident on the object at a first orientation, obtaining first particle-microscopic data at the first setting of the double deflector; setting the excitation of the double deflector to a second setting so that the particle beam is incident on the object at a second orientation different from the first orientation; obtaining second particle-microscopic data at the second setting of the double deflector; and based on an analysis of the first and second particle-microscopic data, performing at least one of the following: i) determining a second distance of the object from the objective lens, and setting the distance of the object from the objective lens to the second distance; and ii) determining a second excitation of the objective lens, and setting the excitation of the objective lens to second new excitation.
2. The method of claim 1, wherein the first particle-microscopic data comprise a first particle-microscopic image, and the second particle-microscopic data comprise a second particle-microscopic image.
3. The method of claim 1, wherein the particle beam microscope further comprises a deflection device configured to scan the particle beam over a surface of the object, and obtaining the first and the second particle-microscopic data each comprises scanning the particle beam over a two-dimensionally extended region on the surface of the object.
4. The method of claim 1, wherein the particle beam microscope further comprises a deflection device configured to scan the particle beam over a surface of the object, and obtaining the first and the second particle-microscopic data each comprises scanning the particle beam along a line on the surface of the object.
5. The method of claim 4, further comprising at least one of the following: determining an orientation of the line in the surface of the object based on an azimuth angle of the orientation with which the particle beam is incident on the object; and determining the azimuth angle of the orientation with which the particle beam is incident on the object based on the orientation of the line in the surface of the object.
6. The method of claim 1, wherein the first and second settings of the double deflector are determined so that substantially no image offset occurs between the first and the second particle-microscopic data.
7. The method of claim 6, wherein the first and second settings of the double deflector are determined on the basis of a computational model of the particle beam microscope.
8. The method of claim 1, wherein the first orientation differs from the second orientation by at least 0.01°.
9. The method of claim 1, wherein, relative to a principal axis of the objective lens, the first and second orientations differ with regard to their elevation and are the same with regard to their azimuth.
10. The method of claim 1, further comprising one of the following: obtaining third particle-microscopic data at the first excitation of the objective lens and at the second distance of the object from the objective lens; obtaining third particle-microscopic data at the second excitation of the objective lens and at the first distance of the object from the objective lens; and obtaining third particle-microscopic data at the second excitation of the objective lens and at the second distance of the object from the objective lens.
11. The method of claim 10, wherein the third particle-microscopic data comprise a third particle-microscopic image.
12. The method of claim 11, wherein the first, second and third settings of the double deflector are determined based on a computational model of the particle beam microscope.
13. The method of claim 1, wherein the particle beam microscope further comprises a stigmator in the beam path of the particle beam between the particle beam source and the objective lens, and the method further comprises: setting an excitation of the stigmator to a first setting; setting the excitation of the double deflector to a third setting so that the particle beam is incident on the object at a third orientation which differs from both the first and second orientations; obtaining fourth particle-microscopic data at the given setting of the stigmator; determining a second setting of the excitation of the stigmator based on an analysis of the first, second and fourth particle-microscopic data; and setting the excitation of the stigmator to the second excitation, wherein the first and the second particle-microscopic data are obtained at the first setting of the stigmator, and the third particle-microscopic data are obtained at the second setting of the excitation of the stigmator.
14. The method of claim 13, wherein the fourth particle-microscopic data are obtained at the first excitation of the objective lens and at the first distance of the object from the objective lens.
15. The method of claim 13, wherein the first, the second and the third settings of the double deflector are determined so that no image offset occurs between the first and fourth particle-microscopic data at the first of the distance of the object from the objective lens and the first excitation of the objective lens.
16. The method of claim 13, wherein, relative to a principal axis of the objective lens, the second and third orientations differ with regard to their azimuth.
17. The method of claim 13, wherein, relative to a principal axis of the objective lens, the second and third orientations are the same with regard to their elevation.
18. The method of claim 13, wherein: obtaining the second particle-microscopic data comprises scanning the particle beam along a first line on the surface of the object; obtaining the third particle-microscopic data comprises scanning the particle beam along a second line on the surface of the object; and a smallest angle between the first and second lines is greater than 10°.
19. The method of claim 1, wherein the first and second particle-microscopic data are recorded at the first excitation of the objective lens and at the first distance of the object from the objective lens.
20. The method of claim 1, wherein the double deflector comprises two individual deflectors at a distance from each other in the beam path of the particle beam.
21. The method of claim 1, wherein the individual deflector comprises four or eight deflection elements distributed in a circumferential direction around the particle beam.
22. The method of claim 21, wherein the deflection elements comprise electrodes and/or coils.
23. One or more machine-readable hardware storage devices comprising instructions that are executable by one or more processing devices to perform operations comprising the method of claim 1.
24. A system comprising: one or more processing devices; and one or more machine-readable hardware storage devices comprising instructions that are executable by the one or more processing devices to perform operations comprising the method of claim 1.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0027] Embodiments of the disclosure are explained in more detail below with reference to figures, in which:
[0028]
[0029]
[0030]
[0031]
[0032]
[0033]
DETAILED DESCRIPTION
[0034]
[0035] The particle beam 13 passes through a condenser lens 27 which collimates the particle beam 13. In the illustrated example, the condenser lens 27 is a magnetic lens with a coil 29, which is excited by a current generated by a settable current source 31 controlled by the controller 15 by way of a control line 33.
[0036] The particle beam 13 thereupon passes through an objective lens 35, which is intended to focus the particle beam 13 at a surface of an object 37 to be examined. In the illustrated example, the objective lens 35 comprises a magnetic lens, the magnetic field of which is generated by a coil 39 which is excited by a current source 41 controlled by the controller 15 by way of a control line 43. The objective lens 35 further comprises an electrostatic lens, the electrostatic field of which is generated between a lower end 45 of the beam tube 12 and an electrode 49. The beam tube 12 is electrically connected to the anode 11, and the electrode 49 can be electrically connected to the ground potential or be set to a potential different from ground by way of a further voltage source (not illustrated in
[0037] The object 37 is held at an object stage 51, the electrical potential of which is set by way of a voltage source 53 controlled by the controller 15 by way of a control line 55. The object 37 is electrically connected to the object stage 51 so that the object 37 also has the electrical potential of the object stage 51. A difference between the electrical potential of the particle emitter 5 and the electrical potential of the object 37 defines the kinetic energy of the particles of the beam 13 when incident on the object 37. In comparison therewith, the particles may have greater kinetic energy within the beam tube 12 and when passing through the condenser lens 27 and the objective lens 35 if they are decelerated by the electrostatic field between the end 45 of the beam tube 12 and the electrode 49 and/or by an electric field between the electrode 49 and the object 37.
[0038] However, it is also possible to embody the particle beam microscope 1 without beam tube 12 and electrode 49, and so the particles are decelerated or accelerated by an electric field between the anode 11 and the object 37 prior to being incident on the object 37. Independently of the embodiment of the particle beam microscope 1 with or without a beam tube 12 and independently of the embodiment and arrangement of the electrode 49, the kinetic energy of the particles when incident on the object 37 is dependent only on the difference between the potentials of the particle beam source 3 and of the object 37.
[0039] The particle beam microscope 1 furthermore comprises a deflection device 57 which is controlled by the controller 15 by way of a control line 59 and which deflects the particle beam 13 such that the particle beam 13 can scan a region 61 on the object 37 under control of the controller 15. The particle beam microscope 1 further comprises a detector 63, which is positioned in such a way that signals which are generated by the particle beam 13 directed at the object 37 and which leave the object are able to be incident on the detector 63 in order to be detected by the latter. These signals can comprise particles such as, for instance, backscattered electrons and secondary electrons or radiation such as, for instance, cathodoluminescence radiation.
[0040] In the particle beam microscope 1 illustrated in
[0041] The particles emanating from the object 37 are caused by the particle beam 13 being incident on the object 37. For example, these detected particles can be particles of the particle beam 13 itself, which are scattered or reflected at the object 37, such as, e.g., backscattered electrons, or they can be particles which are separated from the object 37 by the incident particle beam 13, such as e.g. secondary electrons. However, the detector 63 can also be embodied in such a way that it detects radiation, such as e.g. X-ray radiation, which is generated by the particle beam 13 incident on the object 37. Detection signals from the detector 63 are received by the controller 15 by way of a signal line 65. The controller 15 stores data, derived from the detection signals, depending on the current setting of the deflection device 57 during a scanning process, and so these data represent a particle beam-microscopic image of the region 61 of the object 37. This image can be presented by a display apparatus 67 connected to the controller 15 and be observed by a user of the particle beam microscope 1.
[0042] The particle beam microscope 1 further comprises a double deflector 75, which is arranged in the beam path of the particle beam 13 between the particle beam source 3 and the objective lens 35. In the example shown in
[0043] The double deflector 75 can be used to adjust the particle beam 13; i.e., before the beam passes through the objective lens 35, it is aligned in such a way that the beam can be focused to the best possible extent at the object 37 by the objective lens 35. By way of example, the excitation of the double deflector 75 can be set in such a way that the particle beam 13 passes through a principal plane of the objective lens 35 along an optical axis in the objective lens 35. Further, the double deflector 75 can be used in a method for focusing the particle beam 13 at the object 37, as is described below.
[0044] The particle beam microscope 1 further comprises a stigmator 85, which comprises a plurality of stigmator elements 86 arranged in distributed fashion in the circumferential direction about the particle beam 13, the excitation of the stigmator elements being provided by a driver circuit 87, which is controlled by the controller 15 by way of a control line 88. The stigmator 85 is configured to provide an electric or magnetic quadrupole field, the magnitude and orientation of which are settable.
[0045] A method for focusing the particle beam microscope 1 is explained below with reference to
[0046] The assumption is made that the particle beam 13 is focused in the focal plane 91 at a given excitation of the objective lens 35 and a given setting of the voltage applied to the anode 11 and the setting of the potential of the particle beam source 3. The distance of the focal plane 91 from the objective lens 35 can be calculated with a certain accuracy on the basis of these settings and a computational model of the particle beam microscope 1. Then, an attempt is made to arrange in the calculated focal plane 91 the surface of the object 37 to be examined. However, this is generally possible only with a limited accuracy. In the illustration of
[0047] If the surface of the object 37 is not arranged exactly in the focal plane 91, the generated particle-microscopic images exhibit unnecessary blurring. Thereupon, a method is started for focusing the particle beam microscope 1. To this end, for example, the distance of the object 37 from the objective lens 35 is changed in order to bring the plane 92, in which the surface of the object 37 is arranged, closer to the focal plane 91, or the excitation of the objective lens 35 is changed in order to bring the focal plane 91 closer to the plane 92, in which the surface of the object 37 is arranged. In order to determine a new distance of the object 37 from the objective lens 35 and/or a new excitation of the objective lens 35, used for this purpose, two or more particle-optical images are recorded at two or more different excitations of the double deflector 75 in the performed method.
[0048]
[0049] Since the focal plane 92 of a particle beam microscope 1 is the plane into which the particle emitter 5 is imaged, the line 103 intersects the optical axis 6 in the focal plane 91. However, the line 103 intersects the plane 92, in which the surface of the object 37 is actually arranged, at a distance w1 from the optical axis 6.
[0050] A respective particle-microscopic image of the object is recorded in the two settings of the excitations of the double deflector 75, in which the particle beam 13 runs along the lines 101 and 103, respectively. These two images each show substantially the same structures of the surface of the object 37. However, there is an image offset, which corresponds to the distance w1, between the two recorded images. Therefore, the distance w1 can be determined from an analysis and a comparison of the two recorded particle-optical images. From the distance w1, it is then possible to determine the magnitude of the defocus, i.e., the distance ΔF between the focal plane 91 and the plane 92, in which the surface of the object is arranged, as a measure of the defocus of the particle beam at the surface of the object. It is evident from
[0051] The determination of the distance w1 from the analysis of the two images will now be explained with reference to
[0052] In
[0053] On the basis of the calculated value of ΔF, it is then possible to determine the new distance of the object 37 from the objective lens 35 at which a sharp particle-microscopic image of the object can be recorded at an unchanged excitation of the objective lens 35, or it is possible to determine the new excitation of the objective lens 35 at which a sharp particle-microscopic image of the object 37 can be recorded at an unchanged distance of the object 37 from the objective lens 35, or it is possible to determine a new distance of the object from the objective lens and a new excitation of the objective lens at which it is likewise possible to record a sharp particle-microscopic image of the object.
[0054] The method for focusing the particle beam microscope 1 is explained again below with reference to the flowchart in
[0055] Then, two different excitations of the double deflector are determined in a step 113. By way of example, determining each excitation of the double deflector includes the determination of two deflection angles by which the two individual deflectors deflect the particle beam and which are dimensioned in such a way that the particle beam appears to come from the particle emitter 5 after passing through the double deflector. Then, the first excitation of the double deflector is set in a step 115, whereupon a first particle-microscopic image of the object is recorded in a step 117. Thereupon, the second excitation of the double deflector is set in a step 119, and a second particle-microscopic image is recorded in a step 121. The two recorded particle-microscopic images are analyzed in a step 123 and an image offset between these two images is determined. The defocus ΔF is then further determined in step 123 from the determined image offset and with the additional help of a computational model of the particle beam microscope. Then, a new excitation of the objective lens and/or a new distance of the object from the objective lens are set in a step 125 on the basis of the defocus ΔF. Thereupon, one or more sharp particle-microscopic images of the object can be recorded in a step 127.
[0056] In the example explained with reference to
[0057] It is then possible to implement a third setting of the excitation of the double deflector 75 at which the particle beam 13 is once again deflected by angles α1 and α2 by the individual deflectors 77 and 79, but wherein these deflections are oriented in such a way that they lie in a plane which is oriented orthogonally to the plane of the drawing of
[0058] If the imaging of the particle emitter 5 into the focal plane 91 is astigmatism-free, the two image offsets w1 and w2, measured in the x-direction and y-direction, respectively, will have the same absolute values. Conversely, if the image offset in the x-direction w1 and the image offset in the y-direction w2 have different absolute values, a corresponding defocus ΔFx in the x-direction can be assigned to the image offset in the x-direction and a corresponding defocus ΔFy in the y-direction can be assigned to the image offset in the y-direction. An astigmatism of the imaging of the particle emitter 5 into the focal plane 91 can be determined from the difference between the defocus ΔFx in the x-direction and the defocus ΔFy in the y-direction. Then, an excitation of the stigmator 85 can be changed on the basis of this determined value of the astigmatism in order to compensate for the astigmatism. Consequently, besides determining the defocus ΔF and subsequently improving the focusing of the particle beam microscope, it is also possible to determine the astigmatism and thereafter to compensate for the latter.
[0059] This method is explained again below with reference to the flowchart in
[0060] The offset between the first image and the second image is determined in a step 223 and the defocus ΔF is determined therefrom. The offset between the first and the third image is determined in a step 235, and this offset is compared with the offset between the first image and the second image in order to determine an astigmatism therefrom. Then, a new excitation of the stigmator and a new excitation of the objective lens and/or a new working distance are determined and set in a step 225 such that one or more sharp particle-microscopic images of the object can be recorded in a step 227.
[0061] These images can be presented on a screen 76 of the particle beam microscope 1. The user of the particle beam microscope 1 can control the latter and, for example, the start of the focusing method by way of operating elements, for instance a keyboard 69 and a mouse 71, and a user interface, which is displayed on the screen.
[0062] In the examples explained with reference to
[0063] For this purpose, the particle beam 13 is moved along a line 135 on the surface of the object 37 at the first setting of the excitation of the double deflector 75 by actuating the deflection device 57. The line 135 extends along a straight line and has a starting point 135.sub.s and an ending point 135.sub.e. While the particle beam is scanned from the starting point 135.sub.s along the line 135 to the ending point 135.sub.e, the intensity of secondary particles detected with, for example, the detector 63 is recorded. The result is shown in the graph of
[0064] At the second setting of the excitation of the double deflector 75, the particle beam 13 is scanned along a line 136 with a starting point 136.sub.s and an ending point 136.sub.e on the surface of the object 37. The line 136 is chosen to coincide with or be close to the line 135 on the object. For example, the two lines 135 and 136 extend at a small distance from one another and at a small angle to one another, so that they extend almost parallel to one another. For example, the maximum distance between the two lines 135 and 136 on the object 37 is less than a few tens of nanometers. A curve 138 shows the intensities recorded when scanning along the line 136 at the second setting of the excitation of the double deflector 75.
[0065] The offset w1 can be determined from the comparison of the two curves 137 and 138. In comparison with the determination of the offset from two images, for the recording of which the particle beam is scanned over a two-dimensionally extended region, the offset can be determined much more quickly from the scans along a line.
[0066] For this it is desirable that the orientation of the lines 135 and 136 on the surface of the object 37 is suitably selected. The orientation can be chosen such that the difference between the first and the second orientation with which the particle beam 13 is incident on the surface of the object at the first and second settings of the double deflector 75 causes a maximum offset w1 between the curves 137 and 138. For this purpose, the orientation of the two lines 135 and 136 is determined using a computational model of the particle beam microscope 1. The computational model takes into account here for example the azimuth angles of the first orientation and the second orientation with which the particle beam 13 is incident on the surface of the object 37 at the first and second settings of the double deflector 75. In order to excite the deflection device 57 in such a way that the scans are carried out along the lines 135 and 136, for example the Larmor rotation of the particle beam 13 in the magnetic field of the objective lens 35 is taken into account. However, it is also possible to determine the two orientations with which the particle beam 13 is incident on the surface of the object 37 at the first and second settings of the double deflector 75 in a corresponding manner, based on the previously specified orientation of the lines 135 and 136 on the object.
[0067] The method according to
[0068] The method according to
[0069] For this purpose, in step 217, the first image is not recorded but rather a scan along the line 135, which is oriented in the x-direction, and a scan along a line 141, which is oriented at an angle to the line 135, are performed at the first setting of the double deflector 75. In the example of
[0070] The particle beam device is an electron microscope in the above-described embodiments. However, the disclosure is also applicable to other particle beam devices. Examples thereof include: an ion beam device and a combination of an ion beam device and an electron beam device, in which a location on an object can be irradiated both by an ion beam generated by the ion beam device and by one generated by the electron beam device. Further, the particle beam device can also be a multibeam particle beam device, in which a plurality of particle beams are directed in parallel next to one another at an obj ect.