Cryostat with magnet arrangement which includes an LTS portion and an HTS portion
09766311 · 2017-09-19
Inventors
Cpc classification
H03K17/92
ELECTRICITY
G01R33/3804
PHYSICS
H01F6/06
ELECTRICITY
International classification
H03K17/80
ELECTRICITY
H03K17/92
ELECTRICITY
G01R33/38
PHYSICS
Abstract
A cryostat includes a magnet arrangement for the generation of a magnetic field B0, the magnet arrangement comprising an LTS portion having at least one LTS section made from a conventional low-temperature superconductor and an HTS portion having at least one HTS section made from a high-temperature superconductor. The HTS portion is arranged radially within the LTS portion, and the cryostat is designed to control the temperature of the LTS portion and the HTS portion independently of one another, wherein the HTS portion is electrically isolated from the LTS portion, and is designed to be superconductingly short-circuited. The invention proposes a cryostat with magnet arrangement which enables a high magnetic field strength in a compact space and, at the same time, can be easily constructed.
Claims
1. A cryostat having a magnet arrangement for the generation of a magnetic field B0, wherein the magnet arrangement comprises: a low-temperature superconductor (LTS) portion having at least one LTS section made from a conventional low-temperature superconductor; and a high-temperature superconductor (HTS) portion having at least one HTS section made from a high-temperature superconductor and being arranged radially within the LTS portion, wherein the cryostat is designed to control the temperature of the LTS portion and the HTS portion independently of each other, and wherein the HTS portion is electrically isolated from the LTS portion and is configured to allow it to be superconductingly short-circuited.
2. The cryostat according to claim 1, wherein the HTS portion has no current feed lines.
3. The cryostat according to claim 1, wherein the LTS portion can be short-circuited by means of one or more superconducting switches.
4. The cryostat according claim 1, wherein the at least one HTS section comprises a closed superconducting cylindrical sleeve or one or more closed superconducting rings in a radial layer.
5. The cryostat according to claim 4, wherein said radial layer is deposited on a cylindrical support body.
6. The cryostat according to claim 1, wherein at least one HTS section comprises a coil section which is wound in the form of a solenoid with a tape conductor and is superconductingly short-circuited.
7. The cryostat according to claim 1, wherein the LTS portion comprises at least two LTS sections, including an LTS main section and an LTS shield section.
8. The cryostat according to claim 7, wherein the magnet arrangement has a plurality of charging connections with which the at least two LTS sections can be charged with electrical current and discharged independently of one another.
9. The cryostat according to claim 7, wherein the at least two LTS sections each generate a different magnetic field characteristic.
10. The cryostat according to claim 1, wherein the cryostat forms a first, outer helium tank for the LTS portion and forms a second, inner helium tank for the HTS portion.
11. The cryostat according to claim 10, further comprising a radiation shield arranged between the first helium tank and the second helium tank.
12. The cryostat according to claim 1, wherein the cryostat forms a helium tank for the LTS portion, wherein the HTS portion is arranged in a vacuum chamber which also contains the helium tank, and wherein the HTS portion can be thermally coupled to and decoupled from the helium tank by means of a heat switch.
13. A method for charging the magnet arrangement of a cryostat according to claim 1, the method comprising: a) cooling the LTS portion below a transition temperature T.sub.c,LTS and holding the HTS portion above a transition temperature T.sub.c,HTS; b) charging at least a first LTS section to an interim current I.sub.IN, wherein the interim current I.sub.IN differs from a first operating current I.sub.B.sub.
14. The method according to claim 13, wherein, during step (b), the LTS portion overall is charged with the same interim current I.sub.IN and, during step (d), the LTS portion overall is changed to the same first operating current I.sub.B.sub.
15. The method according to claim 13, wherein the magnet arrangement has at least two LTS sections and a plurality of charging connections with which the at least two LTS sections can be charged with electrical current and discharged independently of one another, and wherein, in step (b), at least one second LTS section is, in turn, charged to a second operating current I.sub.B.sub.
16. The method according to claim 15, wherein the operating currents I.sub.B.sub.
17. The method according to claim 13, wherein the at least one first LTS section comprises an LTS shield section of the magnet arrangement, and wherein, in step (b), the interim current I.sub.IN has an opposite sign to the first operating current I.sub.B.sub.
18. The method according to claim 13, wherein the magnitude of the interim current I.sub.IN is greater than the first operating current I.sub.B.sub.
19. The method according to claim 13, wherein, after step (c), the LTS portion and the HTS portion are held at substantially the same temperature.
20. The method according to claim 13, wherein the LTS portion is, in turn, superconductingly short-circuited in an additional step (e).
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) The invention is shown in the drawings and is explained in more detail with reference to exemplary embodiments. In the drawings:
(2)
(3)
(4)
(5)
(6)
(7)
(8)
(9)
(10)
(11)
(12)
(13)
DETAILED DESCRIPTION
(14) A basic idea of the present invention is, in the case of a magnet arrangement of a cryostat, in particular in the case of an NMR magnet, to arrange the HTS section or the HTS sections (overall HTS portion, also HTS coil) electrically and thermally insulated from the LTS section or the LTS sections (overall LTS portion, also background magnet or LTS coil). Furthermore, the cryostat is designed to charge the HTS section(s) inductively via the LTS section(s). Means for the inductive charging of the HTS section(s) can be provided for this purpose. To this end, in some embodiments, the facility is provided of charging an LTS shield coil optionally with or in opposition to an LTS main coil.
(15) Furthermore, according to the invention, the HTS coil or HTS section can be made from tape material, or also (preferably) designed as an arrangement of one or more superconducting rings or cylinders in which a current is introduced inductively during the charging process.
(16) In addition, a method for inductively charging the HTS coil is described, in which, on the one hand, the LTS coil or the LTS main section is operated in overcurrent mode at different temperatures of LTS and HTS portion. Alternatively, for the charging process, the LTS shield section for the charging process is charged so that the B0 component of the magnetic field in the bore of the cryostat is intensified and the stray field is increased. Subsequently, the HTS coil is cooled below the transition temperature, and the magnetic field of the outer LTS section(s) is reduced and current is passed through the LTS shield section such that the stray field is reduced.
(17) Within the framework of the invention, the temperature of the HTS coil, which is located, for example, in a separate helium tank from the LTS coil, is generally changed only for the charging process; superconductivity in the HTS is switched off and on by increasing and reducing the temperature above/below the transition temperature (critical temperature) of the HTS. For this reason, the temperature change also takes place in a comparatively large frame. As a rule, the temperature of the HTS coil must be controlled between approx. 4 K (or also 2 K) and approx. 100 K which can make structural differences (e.g. additional radiation shields) compared with conventional cryostats necessary or at least advantageous.
(18) Basic Types of Cryostats and Charging Process
(19)
(20) The magnet arrangement 1 is designed to be substantially rotationally symmetrical with regard to a coil axis SA, wherein, for simplification, only the left-hand part of the section of the magnet arrangement 1 is shown in
(21) The LTS portion 2 radially encompasses the HTS portion 5. In normal operation, by means of the magnet arrangement 1, a homogenous magnetic field B0, in which NMR and/or MRI measurements can take place, is generated in the direction of the coil axis SA in a test volume 7, through which the coil axis SA runs centrally. The test volume 7 lies in the room temperature bore of the cryostat. The homogeneity in the test volume 7 is typically 10 ppm or better.
(22) In the embodiment shown, the two (first) LTS sections 11 or 3, 4 respectively are connected electrically superconductingly in series and current can pass through them collectively via the external current feed lines (charging connections) T1, T2 from a power supply 9, wherein the current flowing through the current feed lines T1, T2 can be controlled and in particular varied with the power supply 9. Between the charging connections T1, T2, the LTS portion 2 as a whole can be superconductingly short-circuited by means of a superconducting switch (main switch) 8.
(23) The HTS portion 5 has no external current feed lines. The closed cylindrical sleeve of the HTS section 6 is always superconductingly short-circuited (assuming an adequately low-temperature) so that circulating currents around the coil axis SA are possible.
(24) As the HTS portion (the HTS coil) 5 has no direct electrical connection to the LTS portion (the background magnet) 2 and also has no persistent switch, the HTS coil 5 must be charged inductively. Such a charging process is described by way of example in the following: The background magnet 2 is cooled and charged while the HTS coil 5 is still held above its transition temperature T.sub.c,HTS. The background magnet 2 is overcharged, i.e. a current which lies above the nominal operating current I.sub.B.sub.
(25) In
(26) In a first phase between t0 and t1 the current I.sub.LTS.sub.
(27) Between t1 and t2 the temperature T.sub.HTS of the HTS portion 5 is then reduced below its transition temperature T.sub.c,HTS here likewise to approximately 4.2 K. In doing so, the current I.sub.LTS.sub.
(28) Finally, between t2 and t3, the current I.sub.LTS.sub.
(29) The superconducting switch 8 can then be closed and the power supply 9 can be switched off and/or removed.
(30) Selective Charging/Discharging of Certain Sections
(31) In the background magnet, one coil section can be charged independently of the remaining magnet. An additional current feed line, an additional power supply and an additional superconducting switch are required for this purpose.
(32) The LTS coil section which can be charged independently can then be chosen such that the coupling with the HTS coil is optimal. It is also possible to design this LTS coil section with a notch and thereby determine the homogeneity of the magnetic field B0 in the test volume at the end of the charging process.
(33) In particular, the LTS shield section (which is usually incorporated to reduce the stray field) is suitable for inductive charging as this couples to the HTS coil with negative coupling inductance.
(34)
(35) Here, the LTS portion 2 comprises the outer LTS shield section (shield coil) 3 as a first LTS section 11, and the inner LTS main section (main coil) 4 as a second LTS section 12; both are connected electrically in series. The first LTS section 11 can be charged via the external current feed lines T1, T2 with the power supply 9, and can be superconductingly short-circuited with the superconducting switch 14a. The second LTS section 12 can be charged via the external current feed lines T2 and T3 with a power supply 13 and can be superconductingly short-circuited by means of a superconducting switch 14b. Here, the HTS portion (HTS coil) 5 is, in turn, designed with a single HTS section 6.
(36) Charging then takes place by way of example in accordance with the following scheme: The background magnet 2 (consisting of main coil 4 and shield coil 3) is cooled while the HTS coil 5 is still held above T.sub.c,HTS. Only the main coil 4 of the background magnet 2 is charged and is held at constant current for the rest of the charging process with the power supply 13. In this step, the other power supply 9 keeps the LTS shield section 3 free from current. The shield coil 3 is charged in the wrong direction, i.e. the stray field increases additionally and the magnetic field B0 in the bore increases slightly (without the field-reducing effect of the shield coil 3, the main coil 4 is overloaded; here, however, the above argument relating to the operating current applies). The temperature THTS of the HTS coil 5 is now reduced until it is superconducting. The LTS shield section 3 is now discharged once more and then charged in the right direction. In doing so, the stray field shrinks to its desired value. As a result of the negative coupling coefficient, the current in the HTS coil 5 also increases during this change of current in the LTS shield section 3. During this process, the power supply 13 maintains the main coil 4 at constant current and the magnetic field B0 in the bore increases further. All superconducting switches 14a, 14b are now closed (persistent mode).
(37) In
(38) In a first phase between t0 and t1 the current I.sub.LTS.sub.
(39) In a second phase between t1 and t2, the current I.sub.LTS.sub.
(40) Between t2 and t3 the temperature T.sub.HTS of the HTS portion 5 is then reduced below its transition temperature T.sub.c,HTS, here likewise to approximately 4.2 K. At the same time, the currents I.sub.LTS.sub.
(41) Finally, between t3 and t4, the current I.sub.LTS.sub.
(42) The superconducting switches 14a, 14b can then be closed and the power supplies 9, 13 can be switched off and/or removed.
(43) Independent Temperature Control of the HTS Coil
(44) Different possibilities exist for the independent temperature control of the HTS coil (at least when charging). In general and in particular, with all the embodiments presented in the following, it is advantageous to attach a heater to the HTS coil (or in the tank in which the HTS coil is arranged) in order to be able to raise the temperature of the HTS coil quickly or to hold it at a higher temperature level with respect to the environment.
(45) As shown in
(46) In the embodiment shown, the LTS coil (the LTS portion) 2 comprises an LTS shield section 3 made from NbTi wire and an LTS main section 4 with three sub-coil sections 23a, 23b, 23c, of which the outermost is made from NbTi wire and the two inner 23b, 23c from Nb.sub.3Sn wire. Here, both helium tanks 21, 22 are in each case designed with a neck tube for filling with helium and, in the case of the first tank 21, also for the external current feed lines (not shown in more detail). The second helium tank 22 is provided with an electrical heater 29. In the state of normal operation shown, both helium tanks 21, 22 are filled with liquid helium at 4.2 K; it is to be noted that, during charging, the second helium tank 22 and the HTS coil 5 respectively must be temporarily brought to a warm state while the helium thereof is in gaseous form (or is not present) in the second helium tank 22.
(47) Both helium tanks 21, 22 are arranged in a vacuum container 24; here the walls 24a thereof simultaneously form the outer wall of the cryostat 20. Furthermore, a radiation shield 25a, which is cooled by liquid nitrogen (LN.sub.2) in an outer tank 25, is provided; the helium tanks 21, 22 are also located inside this radiation shield 25a. For simplification, a boundary of the radiation shield 25a with the room temperature bore 26 is not shown in more detail here.
(48) In the embodiment of
(49) In an alternative embodiment, which is shown in
(50) Furthermore, as shown in
(51) In an embodiment of a cryostat 20 of
(52) HTS Coils
(53) Preferably, HTS materialespecially YBCOis deposited in an annular form on cylindrical substrate material (support body) by means of thin film deposition to produce an HTS coil or HTS section. Hastelloy is preferably used as the substrate material. With the help of laser structuring, an initially continuous, deposited HTS cylindrical sleeve can be divided into a plurality of coaxial adjacent rings. The fabrication of coils (actually a collection of rings) can also be carried out in several layers (i.e., a plurality of coaxial rings or ring layers with increasing radii are produced). At the same time, SrTiO.sub.3 is preferably used as an insulator radially between the rings or ring layers.
(54) A coil produced in this manner can also be used for constructing a high-field NMR magnet. As the HTS rings are continuous, there is no need to produce superconducting connections between HTS conductors. The HTS rings can be formed geometrically such that they are sufficiently thin to not negatively affect the homogeneity of the magnetic field (equivalent to filamentation in NbTi or Nb.sub.3Sn wires).
(55) An HTS coil manufactured as described above is not connected electrically in series with the background magnet (consisting of main and shield coil) made from LTS; there is therefore no need to produce superconducting HTS-LTS connections. Likewise, there is no need to bring out an HTS tape conductor in a complicated manner from the region of the highest magnetic field.
(56)
(57) A further HTS section 6 for the invention, similar to the HTS section of
(58) Alternatively, HTS coils or HTS sections can also be produced based on HTS tape conductors. The HTS tape conductor typically comprises a tape-like, metallic substrate (e.g. a sheet steel tape), on which one or more buffer layers (e.g. made from MgO), an HTS layer (e.g. made from YBCO) and, if necessary, shunt and/or protective layers (usually made of Cu or noble metals such as Ag, Au) are deposited.
(59)
(60)
LIST OF REFERENCES
(61) 1 Magnet arrangement 2 LTS portion (background magnet, LTS coil) 3 LTS shield section (shield coil) 4 LTS main section (main coil) 5 HTS portion (HTS coil) 6 HTS section 7 Test volume 8 Superconducting switch (main switch) 9 Power supply 11 First LTS section 12 Second LTS section 13 Power supply 14a, 14b Superconducting switches 20 Cryostat 21 First helium tank 22 Second helium tank 23a-23c Sub-coil sections 24 Vacuum tank (vacuum container) 24a Wall of vacuum tank 24b Vacuum chamber 25 Outer tank for liquid nitrogen (LN.sub.2) 25a Radiation shield of outer tank for liquid nitrogen 26 Room temperature bore 27 Radiation shield between helium tanks 28 Valve 29 Electrical heater 30 Heat switch 31 Cylindrical support body (coil support) 32 Ring made from HTS material 33 Inner layer 34 Outer layer 35 End of slotted HTS tape conductor 36 HTS-HTS joint 37 HTS tape conductor 38 HTS cylindrical sleeve 39 Insulation layer 40 End disk 41 Radial layer
(62) B0 Magnetic field in the test volume in the direction of the coil axis I.sub.B.sub.