Focused ion beam apparatus
11482398 · 2022-10-25
Assignee
Inventors
Cpc classification
H01J37/3005
ELECTRICITY
H01J37/20
ELECTRICITY
International classification
Abstract
The focused ion beam apparatus includes: an electron beam column; a focused ion beam column; a sample stage; a coordinate acquisition unit configured to acquire, when a plurality of irradiation positions to which the focused ion beam is to be applied are designated on a sample, plane coordinates of each of the irradiation positions; a movement amount calculation unit configured to calculate, based on the plane coordinates, a movement amount by which the sample stage is to be moved to a eucentric height so that the eucentric height matches an intersection position at which the electron beam and the focused ion beam match each other at each of the irradiation positions; and a sample stage movement control unit configured to move, based on the movement amount, the sample stage to the eucentric height at each of the irradiation positions.
Claims
1. A focused ion beam apparatus, comprising: an electron beam column configured to irradiate a sample with an electron beam; a focused ion beam column configured to irradiate the sample with a focused ion beam; a sample stage, on which the sample is to be placed in one of a direct manner and an indirect manner, and which is tiltable about a tilt axis perpendicular to the electron beam and the focused ion beam and movable in a height direction; a coordinate acquisition unit configured to acquire, when a plurality of irradiation positions to which the focused ion beam is to be applied are designated on the sample, plane coordinates of each of the plurality of irradiation positions; a movement amount calculation unit configured to calculate, based on the plane coordinates, a movement amount by which the sample stage is to be moved to a first eucentric height (Zs) so that the first eucentric height (Zs) matches an intersection position at which the electron beam and the focused ion beam match each other at each of the plurality of irradiation positions; a memory configured to store a second eucentric height (Zse) at predetermined plane coordinates on the surface of the sample placed on the sample stage; and a sample stage movement control unit configured to move, based on the movement amount, the sample stage to the eucentric height (Zs) at each of the plurality of irradiation positions, wherein the movement amount calculation unit is configured to estimate the first eucentric height (Zs) at each of the plurality of irradiation positions from the second eucentric height (Zse) stored in the memory based on a difference in coordinate between the predetermined plane coordinates and each of the plurality of irradiation positions.
2. The focused ion beam apparatus according to claim 1, wherein the movement amount calculation unit is configured to estimate the first eucentric height (Zs) at each of the plurality of irradiation positions from the second eucentric height (Zse) stored in the memory, based on an arrangement order in coordinate among the predetermined plane coordinates and each of the plurality of irradiation positions.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DESCRIPTION OF THE EMBODIMENTS
(14) Now, at least one embodiment of the present invention is described with reference to the accompanying drawings. In the following description, like components are denoted by like reference symbols.
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(16) A part or all of the components of the focused ion beam apparatus 100 are arranged in a vacuum chamber 40, and the inside of the vacuum chamber 40 is depressurized to a predetermined vacuum degree.
(17) The sample stage 50 is configured to movably support the sample table 51, and a sample 200 is placed on the sample table 51. The sample stage 50 also has a moving mechanism capable of displacing the sample table 51 on five axes.
(18) Specifically, this moving mechanism includes an XY moving mechanism 50xy for moving the sample table 51 along an X-axis and a Y-axis, which are parallel to a horizontal plane and perpendicular to each other, a Z moving mechanism 50z for moving the sample table 51 along a Z-axis (height direction) perpendicular to the X-axis and the Y-axis, a rotation mechanism 50r for rotating the sample table 51 about the Z-axis, and a tilt mechanism 50t for rotating the sample table 51 about a tilt axis TA parallel to the X-axis. The tilt axis TA is perpendicular to irradiation directions of an electron beam 10A and a focused ion beam 20A.
(19) The above-mentioned moving mechanism can be achieved by a piezo element, a stepping motor, and other various actuators.
(20) The sample stage 50 displaces the sample table 51 on the five axes, to thereby move the sample 200 to a plurality of irradiation positions of the electron beam 10A, the focused ion beam 20A, and a gas ion beam 30A (irradiation points (positions) P1, P2, and P3, at which the irradiation beams 10A to 30A intersect one another, and which are illustrated in
(21) At the irradiation points P1 to P3, the surface (cross section) of the sample 200 is irradiated with the electron beam 10A, the focused ion beam 20A, and the gas ion beam 30A (in
(22) The control unit 6 can be formed of a computer including a CPU serving as a central processing unit, a memory 6M (RAM and ROM) configured to store, for example, data and programs, an input port configured to receive input of a signal from an external apparatus, and an output port configured to output a signal to the external apparatus. The control unit 6 is configured so that the CPU executes various kinds of calculation processing based on the programs stored in the memory 6M to control the components of the focused ion beam apparatus 100. Further, the control unit 6 is electrically connected to, for example, control wirings of the electron beam column 10, the focused ion beam column 20, the gas ion beam column 30, the secondary electron detector 4, and the sample stage 50.
(23) The control unit 6 includes a coordinate acquisition unit 6A, a movement amount calculation unit 6B, and a sample stage movement control unit 6C, which are described later.
(24) The control unit 6 is also configured to drive the sample stage 50 based on a command from software or input performed by an operator to adjust the position and posture of the sample 200, to thereby adjust the irradiation positions and irradiation angles of the electron beam 10A, the focused ion beam 20A, and the gas ion beam 30A for irradiating the surface of the sample 200.
(25) The control unit 6 is connected to the input unit 8, for example, a keyboard, for acquiring an instruction input by the operator, and the display unit 7 configured to display, for example, an image of a sample.
(26) The SEM column 10 includes an electron source (not shown) configured to emit electrons and an electron optical system (not shown) configured to form the electrons emitted from the electron source into a beam shape and to scan the electrons. When the sample 200 is irradiated with the electron beam 10A emitted from the electron beam column 10, secondary electrons are generated from the sample 200. The generated secondary electrons are detected by a secondary electron detector (not shown) inside the column or the secondary electron detector 4 outside the column, to thereby be able to acquire the image of the sample 200. In another case, reflected electrons are detected by a reflected electron detector 14 inside the column, to thereby be able to acquire the image of the sample 200.
(27) The electron optical system includes, for example, a condenser lens configured to focus the electron beam 10A, an aperture configured to narrow down the electron beam 10A, an aligner configured to adjust an optical axis of the electron beam 10A, an objective lens configured to focus the electron beam 10A onto the sample 200, and a deflector configured to scan the electron beam 10A on the sample 200.
(28) The FIB column 20 includes an ion source (not shown) configured to generate ions and an ion optical system (not shown) configured to form the ions emitted from the ion source into a focused ion beam shape and to scan the ions. When the sample 200 is irradiated with the focused ion beam 20A being a charged particle beam from the FIB column 20, secondary ions, secondary electrons, and other such secondary charged particles are generated from the sample 200. Those secondary charged particles are detected by the secondary electron detector 4 to acquire the image of the sample 200. The FIB column 20 also increases an irradiation amount of the focused ion beam 20A to perform etching processing (cross-section processing) on the sample 200 within an irradiation range.
(29) The ion optical system has a known configuration, and includes, for example, a condenser lens configured to focus the focused ion beam 20A, an aperture configured to narrow down the focused ion beam 20A, an aligner configured to adjust an optical axis of the focused ion beam 20A, an objective lens configured to focus the focused ion beam 20A on the sample, and a deflector configured to scan the focused ion beam 20A on the sample.
(30) The gas ion beam column 30 includes, for example, an ion source (not shown) configured to generate ions being argon ions, a condenser lens (not shown) configured to focus the ion beam emitted from the ion source, a blanking unit (not shown), an aperture (not shown) configured to narrow down the ion beam, and an objective lens (not shown) configured to focus the ion beam.
(31) The gas gun 5 emits a predetermined gas, for example, an etching gas, to the sample 200. The sample 200 is irradiated with the electron beam 10A, the focused ion beam 20A, or the gas ion beam 30A while the etching gas is being supplied from the gas gun 5, to thereby be able to increase an etching speed of the sample through beam irradiation. In another case, the sample 200 is irradiated with the electron beam 10A, the focused ion beam 20A, or the gas ion beam 30A while a compound gas is being supplied from the gas gun 5, to thereby be able to perform local precipitation (deposition) of gas components in the vicinity of abeam irradiation area.
First Embodiment
(32) Next, with reference to
(33) First, as illustrated in
(34) After acquiring the designated irradiation positions P1 to P3, the control unit 6 (coordinate acquisition unit 6A) acquires plane (XY) coordinates of each of the irradiation positions P1 to P3 (Step S2).
(35) Subsequently, the control unit 6 (movement amount calculation unit 6B) calculates a eucentric height Zs at each of the irradiation positions P1 to P3 and a movement amount in the height direction (Step S4).
(36) This movement amount is an amount by which the sample stage 50 is to be moved in the height direction so as to reach the eucentric height Zs, to thereby cause each of the irradiation positions P1 to P3 of the sample, which are illustrated in
(37) Now, with reference to
(38) In
(39) Subsequently, the control unit 6 tilts the sample about the tilt axis TA by an angle Θ so that the sample is tilted to have a surface S0t. At this time, the Y coordinate of the irradiation position P1 is moved to YΘ0 by ΔY (moved to the left side in
(40) The movement amount obtained at this time is approximated by the following expression:
ΔY=Y0−YΘ0≈Zs×sin Θ Expression 2:
where Y0, YΘ0, and Θ are known. Therefore, Zs can be obtained by the following expression:
Zs=(Y0−YΘ0)/sin Θ Expression 3:
Expression 2 is recorded in the memory 6M or recorded in a program for calculating the eucentric height Zs to be readout by the control unit 6.
(41) Then, the control unit 6 (sample stage movement control unit 6C) controls the Z moving mechanism 50z to move the sample surface S0 in the height direction by a eucentric height (+Zs) to bring a sample surface S1 (irradiation position P1) to the eucentric position (Step S6 of
(42) YΘ0 itself cannot be usually discerned by viewing the SEM image. In view of this, when there is a feature shape (for example, dent that can be distinguished from the surroundings) at the irradiation position P1 itself, the movement amount of the feature shape in the Y-axis direction before and after the tilt may be calculated.
(43) Meanwhile, as illustrated in
(44) In this manner, after the focused ion beam 20A is applied to perform, for example, various kinds of processing and deposition with the irradiation position P1 on the surface of the sample being set to the eucentric position, the irradiation position P1 can be observed by applying the electron beam 10A with the irradiation position P1 being tilted by a predetermined angle.
(45) After the processing and observation at the irradiation position P1 are finished, each of the subsequent irradiation positions P2 and P3 is automatically adjusted to the eucentric height Zs, to thereby improve work efficiency. In addition, as compared to a case in which the eucentric height is manually set, it is possible to inhibit each of the irradiation positions P1 to P3 from falling out of the eucentric height Zs, and it is also possible to inhibit each of the irradiation positions P1 to P3 from falling out of the field of view when the sample is tilted.
(46) In Step S4 of
(47) In addition, as indicated by the arrow (B) in
Second Embodiment
(48) Next, with reference to
(49) The second embodiment is applied when the deviation L in the Y-axis direction occurs at the time of calculation of the eucentric height Zs, and exhibits increased calculation accuracy of the eucentric height Zs than that of the method of
(50) In this case, for example, the deviation L is caused not only by deviations exhibited when the moving mechanism for the sample stage 50 is moved to each of the irradiation positions P1 to P3, due to mounting errors (machine differences) among the sample stages 50 of individual focused ion beam apparatus, and by deviations of actual movement amounts of a piezo element, a stepping motor, and other actuators that form the moving mechanism, but also by a bend from a beam axis of the electron beam 10A for generating the SEM image, which is exhibited when Y0 and YΘ0 described above are determined, and by other such factors.
(51) In addition, the bend from the beam axis of the electron beam 10A is ascribable to measurement conditions including an acceleration voltage and an aperture.
(52)
(53) As illustrated in
(54) Details of those positional relationships are described with reference to
(55) First, on the sample surface S0 before a tilt, the irradiation position of the electron beam 10A is deviated to V1 due to the deviation L, and the Y coordinate of the irradiation position P1 is expressed by the following expression:
Y1=Y0+L Expression 4:
(56) Subsequently, at the irradiation position P1 on a sample surface S0t tilted by the angle Θ, the deviation L also is tilted by the angle Θ, and hence a Y-axis component of the deviation L becomes LxcosΘ. Therefore, the Y coordinate of the irradiation position P1 after the tilt is expressed by the following expression:
YΘ1=YΘ0+L×cos Θ Expression 5:
(57) In this case, when Expression 2 and Expression 4 are substituted into Expression 5, the following expression is obtained.
(58)
(59) In Expression 1, Y1, sin Θ, and cos Θ are known, and Zs and L are unknown.
(60) In view of this, as illustrated in
(61) Therefore, there are two unknowns (Zs and L) in two simultaneous equations, and hence Zs and L can be calculated together.
(62) Then, with Zs and L described above, a highly accurate eucentric height Zs is obtained, and at the same time, the deviation L in the Y-axis direction is found. Thus, the sample stage movement control unit 6C is only required to tilt the sample stage 50 after moving the sample stage 50 by L in the Y-axis direction so as to compensate a deviation amount L.
(63) Therefore, even when the deviation L in the Y-axis direction occurs, it is possible to inhibit a target region from falling out of the field of view when the sample is tilted.
(64) L is sufficiently smaller than Zs, and hence it is possible to easily obtain Zs through use of only one tilt angle Θ in Expression 1 by assigning L as a known value.
(65) In this case, as described above, L is ascribable to the mounting errors (machine differences) among the sample stages 50 of individual focused ion beam apparatus and the measurement conditions (including an acceleration voltage) of the electron beam column 10.
(66) Therefore, for example, as shown in
(67) For example, as shown in
(68) Therefore, Expression 1 is one simultaneous equation with one unknown (Zs), and hence Zs can be calculated.
(69) It is to be understood that Zs may be assigned as a known value in place of L to calculate unknown L.
(70) Next, with reference to
(71) As described above, it is possible to specifically calculate the eucentric height Zs at each of the irradiation positions P1 to P3 through use of, for example, Expression 3 in the first embodiment or Expression 1 in the second embodiment. However, for example, as the number of irradiation positions increases, the calculation requires more time, and the work efficiency may decrease.
(72) In addition, when the FIB processing and the SEM observation or another such operation are performed at the plurality of irradiation positions P1 to P3, it is required to perform processing with the irradiation position P1 being adjusted to the eucentric height, and then move the sample stage 50 to readjust the irradiation position P2 to the eucentric height for processing. Thus, it is difficult to automate continuous processing and observation at the plurality of irradiation positions P1 to P3.
(73) In view of this, a eucentric height Zse is calculated in advance for predetermined plane coordinates of the sample 200 placed on (the sample table 51 on) the sample stage 50 and stored in, for example, a mapping (table), and when the actual eucentric height Zs at each of the irradiation positions P1 to P3 can be estimated from the eucentric height Zse, the work efficiency is improved. In addition, it is not required to calculate the eucentric height Zs at each of the plurality of irradiation positions P1 to P3 every time processing is performed, and it is possible to automate continuous processing and observation at the plurality of irradiation positions P1 to P3.
(74) Only the eucentric height Zs may be estimated, but when the deviation amount L occurs, it is preferred to estimate the deviation amount L together, and hence a case in which both the eucentric height Zs and the deviation amount L are estimated is described below.
(75)
(76) As illustrated in
(77) Subsequently, the movement amount calculation unit 6B refers to the eucentric heights Zse and the deviation amounts Le, which are stored in the memory 6M, to estimate the eucentric height Zs and the deviation amount L at the actual irradiation position P1.
(78) In regard to this estimation, for example, as illustrated in
(79) Other irradiation positions P2, P3 . . . can be estimated in the same manner.
(80) Thus, as illustrated in
(81) Each time the sample 200 is replaced, the eucentric height Zse is measured again, and the table 6T is also generated for each sample.
(82) Incidentally, in the FIB processing and the SEM observation at the irradiation positions P1 . . . , there is a demand to perform processing by irradiating the sample 200 with the focused ion beam 20A with the sample 200 being tilted on the XY plane in order to facilitate the viewing in some cases. In this case, the sample 200 is rotated on an XY plane through use of the rotation mechanism 50r for rotating the sample table 51 about the Z-axis.
(83) However, as illustrated in
(84) Then, in such a case, when the deviation amount Le measured with a rotation angle of 0 in the table 6T is referred to, the estimation accuracy of the deviation amount L at the actual irradiation position P1 decreases.
(85) In view of this, in the table 6T of
(86) For example, Eu2 and Eu7 have the same XY coordinates, but are different in R value. Therefore, the estimation may be performed through use of the eucentric height Zse and the deviation amount Le at one of Eu2 and Eu7, which is closer to the R value of the actual irradiation position P1.
(87) In addition, it has already been described that the two plane coordinates Eu3 and Eu4 are extracted from the table 6T in the ascending order of the distance from the irradiation position P1 in the XY direction, but data to be extracted may be determined by comprehensively estimating the distance in the XY direction and a similarity degree between the R values.
(88) It is to be understood that the present invention is not limited to the above-mentioned embodiments, and covers various modifications and equivalents included in the spirit and scope of the present invention.
(89) For example, the method of calculating a eucentric height is not limited to the above-mentioned method.