EXTRACTION FREEZE DRYING SYSTEM WITH REMOVABLE CONDENSER

Abstract

An extraction freeze drying system. The freeze dryer has a cold collector, heating elements, and a vacuum chamber. A first removable collector vessel is operatively and removably connected to the freeze dryer. A second removable collector vessel is provided for replacing the first removable collector vessel upon removal thereof from the freeze dryer. The first and second removable collectors are jacketed vessels. Fluid is allowed to pass through the jacket to maintain proper temperatures. A sealable lid is attached to the first removable collector vessel immediately upon or prior to removal from the freeze dryer. The sealable lid comprises a drain valve and spout to aid in pouring off water or terpenes during the separation process.

Claims

1. An extraction freeze drying system comprising: a) a freeze dryer having a cold collector, heating elements, and a vacuum chamber; and b) a first removable collector vessel operatively and removably connected to the freeze dryer.

2. The extraction freeze drying system in accordance with claim 1, further comprising a second removable collector vessel for replacing the first removable collector vessel upon removal thereof from the freeze dryer.

3. The extraction freeze drying system in accordance with claim 2, wherein the first and second removable collectors are jacketed vessels.

4. The extraction freeze drying system in accordance with claim 3, further comprising means for allowing fluid to pass through the jacket to maintain proper temperatures.

5. The extraction freeze drying system in accordance with claim 4, further comprising quick disconnect fittings operatively connected to the jacketed vessels to allow removal thereof without leaking fluid.

6. The extraction freeze drying system in accordance with claim 1, further comprising a sealable lid attached to the first removable collector vessel immediately upon or prior to removal from the freeze dryer.

7. The extraction freeze drying system in accordance with claim 6, wherein the sealable lid comprises a drain valve and spout to aid in pouring off water or terpenes during the separation process.

8. The extraction freeze drying system in accordance with claim 1, wherein the first removable collector vessel further comprises a sight glass for allowing a user to monitor condensate collection during a drying process.

Description

BRIEF DESCRIPTION OF THE DRAWING

[0013] A complete understanding of the present invention may be obtained by reference to the accompanying drawing, when considered in conjunction with the subsequent detailed description, in which:

[0014] FIG. 1 is a perspective view of a removable condenser in accordance with the present invention;

[0015] FIG. 2 is a cut-away schematic view of an alternative embodiment of the removable condenser and refrigeration system of FIG. 1;

[0016] FIG. 3 is a cut-away schematic view of another alternative embodiment of the removable condenser and refrigeration system of FIG. 1 showing a refrigerator coil;

[0017] FIG. 4 is a perspective view of the inventive removable condenser as shown in FIG. 1, mounted on a conventional freeze dryer, showing external refrigeration fittings;

[0018] FIG. 5 is a perspective view of an alternate embodiment of the inventive removable condenser as shown in FIG. 4, mounted on a conventional freeze dryer, with internal refrigeration fittings;

[0019] FIG. 6 is a cut-away view of the inventive removable condenser as shown in FIG. 5, illustrating a vacuum chamber and a plurality of shelves;

[0020] FIG. 7 is a perspective view of an extraction freeze dryer of the prior art; and

[0021] FIG. 8 is an exploded view of the extraction freeze dryer of the prior art shown in FIG. 7.

DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENT

[0022] Although the following detailed description contains specific details for the purposes of illustration, those of ordinary skill in the art will appreciate that variations and alterations to the following details are within the scope of the invention. Accordingly, the exemplary embodiments of the invention described below are set forth without any loss of generality to, and without imposing limitations upon, the claimed invention.

[0023] Referring now to FIG. 7, there is shown a perspective view of an extraction freeze dryer of the prior art. Specifically, an extraction freeze dryer manufactured by the Labconco Corporation of Kansas City, Mo. is depicted. It should be understood that other extraction freeze dryers can be used equally well with the present invention, but for simplicity, only the Labconco freeze dryer is described hereinbelow.

[0024] A housing A-1 contains components, not shown, for freeze drying material. Housing A-1 supports a plurality of stainless steel trays supported by shelves A-2, preferably heated, for collecting ice and water that are produced during the freeze drying process. Mounted to the exterior of housing A-1 is a control panel assembly A-9 that includes a touch screen display.

[0025] Referring now also to FIG. 8, there is shown an exploded view of the extraction freeze dryer of the prior art shown in FIG. 7. Instructions for operating the prior art extraction freeze dryer are provided by the Labconco Corporation.

[0026] Housing A-1 encases a 9-Watt motorized fan A-3, which can be a 115V or a 230V model and a compressor A-4, which can be a 115V, 60 Hz, a 230V, 50 Hz, or a 230V, 60 Hz model. Control panel assembly A-9, including display assembly A-5, display gasket A-6, control panel A-7, and control panel label A-8, is mounted to the exterior of housing A-1, as hereinbefore described. A drain fitting or coupling body A-10 is disposed at a lowermost portion of housing A-1 and a coupling insert A-11 is inserted therein. A retaining ring A-12 and drain fitting lanyard A-13 are likewise disposed at a lowermost portion of housing A-1, fastened by a machine screw A-14. A moisture sensor A-15 is operatively connected to the exterior of housing A-1. A vacuum hose A-16 is mounted on housing A-1. A female luer-lok filter A-17, a male luer A-18, a vacuum control/bleed valve A-19, and a vacuum sensor A-20 are all connected to one another and mounted on housing A-1, as shown. An electrical panel assembly A-21, which can be a 115V or a 230V model, is inserted in a cavity in housing A-1. A temperature sensor A-22 is also mounted on housing A-1.

[0027] Now referring to the present invention, a freeze drying system is provided with a first removable collector or condenser that can be capped, sealed, and processed offline to collect terpenes from an ice/water mixture. Another collector or condenser, not shown, is ready and staged to be placed into the freeze dryer immediately after the full first collector is removed, thus reducing the down time between cycles, and realizing a greater overall efficiency.

[0028] The inventive removable collector 1 may be a jacketed vessel 15 with fluid 5 passing through the jacket to maintain proper temperatures (FIGS. 1 and 2). Quick disconnect fittings 6 allow the jacketed vessel 15 to be removed without leaking fluid.

[0029] In an alternate embodiment (FIGS. 3 and 4), a removable vessel 1 is provided with a refrigeration coil inside the housing thereof. Quick disconnect fittings 6 allow the coil 8 to be disconnected without leaking fluid.

[0030] In another alternate embodiment (FIGS. 5 and 6), a removable vessel 1 fits inside of a fixed coil 8 which transfers chilled air from coil 8 to the inner wall of removable vessel 1. The thermal transfer occurs via fitment, or a medium may aid the thermal transfer.

[0031] In all embodiments, a sealable lid 2 attaches to the vessel 1 immediately upon or prior to removal from the freeze dryer. It may encompass a drain valve 11 and spout to aid in pouring off water or terpenes during the separation process. A sight glass or view port 4 on vessel 1 allows the user to monitor condensate collection during the drying process. A proper gasket/seal 9 and insulation ensures that the condensate collects only within the vessel and not on the flange or the exterior thereof.

[0032] The location of the removable collector or condenser 1 may be oriented for easy access and removal. Locating the collector 1 on the side of a tray-style freeze dryer allows for a short, unobstructed path from the tray to the collector.

[0033] Referring now again to FIG. 1, there is shown a perspective view of a removable condenser 1 in accordance with the present invention. Removable condenser 1 is mounted to a housing A-1 (FIG. 7) of a conventional freeze dryer. Condenser 1 has an airtight lid 2 at the uppermost portion thereof. Two vessel cooling entry/exit ports 3 extend from a lower portion and an upper portion, respectively, of condenser 1, as shown. A vessel site glass 4 is optionally and suitably positioned at the periphery of condenser 1 for observation of the extraction process. A drain port 11 extends from the lowermost surface of condenser 1.

[0034] Referring now again to FIG. 2, there is shown a cut-away schematic view of an alternative embodiment of removable condenser and refrigeration system 1 of FIG. 1. Two connect/disconnect fittings 6 are connected to respective vessel cooling entry/exist ports 3, as shown, at the termination of respective refrigeration supply/return tubes 7, both of which are connected to a refrigeration system 14.

[0035] Referring now again to FIG. 3, there is shown a cut-away schematic view of an alternative embodiment of the removable condenser and refrigeration system 1 of FIG. 1. Disposed along the inner surface of the housing of condenser 1 and surrounding components therein is a layer of thermal insulation 5 as is well known in the art. Thermal insulation 5 acts as a jacket and may be hollow to accommodate fluid passing through the jacket to maintain proper temperatures. A refrigeration coil 8 connects the two portions of refrigeration supply/return tubes 7 also in a manner well known in the art.

[0036] Referring now again to FIG. 4, there is shown a perspective view of the inventive removable condenser 1 (alternate embodiments shown in FIGS. 1-3) mounted on the enclosure of conventional freeze dryer 13 with refrigeration supply/return tubes 7 and connect/disconnect fittings 6 disposed on the outside of both condenser 1 and freeze dryer enclosure 13. A vacuum chamber 10 and vacuum seal 9 are components of a freeze dryer.

[0037] Referring now again to FIG. 5, there is shown a perspective view of an alternate embodiment of the inventive removable condenser 1 mounted to the enclosure 13 of a conventional freeze dryer with a fixed refrigeration system, not shown, disposed within the housing of condenser 1. The refrigeration system transfers thermally to removable condenser 1 without the need for connect/disconnect fittings.

[0038] Referring now again to FIG. 6, there is shown a cut-away view of an alternative embodiment of the inventive removable condenser 1, showing vacuum chamber 10 and a plurality of trays supported by shelves 12, preferably heated. Condenser 1 is operatively connected to vacuum chamber 10 in freeze dryer. A vessel site glass 4 allows a user to view into the collector 1 during the drying process. Thermally conductive interface 5 facilitates the transfer of heat from removable condenser 1 to refrigeration coil 8.

[0039] In operation, after each run, an operator removes samples from shelves 12 and turns on a hot gas defrost to melt the ice and allow it to drain from drain port 11. Once all moisture is removed, the freeze dryer may be cleaned and prepped for the next run. Removable condenser 1 allows an operator to trap terpenes and remove them from the freeze dryer to be processed offline, so a new cycle can be started immediately with a separate condenser 1. The system also allows ice to slowly melt in a sealed container that can be refrigerated during the melt process, minimizing lost terpenes.

[0040] All references throughout this application, for example patent documents including issued or granted patents or equivalents; patent application publications; and non-patent literature documents or other source material; are hereby incorporated by reference herein in their entireties, as though individually incorporated by reference, to the extent each reference is at least partially not inconsistent with the disclosure in this application (for example, a reference that is partially inconsistent is incorporated by reference except for the partially inconsistent portion of the reference).

[0041] The terms and expressions which have been employed herein are used as terms of description and not of limitation, and there is no intention in the use of such terms and expressions of excluding any equivalents of the features shown and described or portions thereof, but it is recognized that various modifications are possible within the scope of the invention claimed. Thus, it should be understood that although the present invention has been specifically disclosed by preferred embodiments, exemplary embodiments and optional features, modification and variation of the concepts herein disclosed may be resorted to by those skilled in the art, and that such modifications and variations are considered to be within the scope of this invention as defined by the appended claims. The specific embodiments provided herein are examples of useful embodiments of the present invention and it will be apparent to one skilled in the art that the present invention may be carried out using a great number of variations of the devices, device components, and method steps set forth in the present description. As will be obvious to one of skill in the art, methods and devices useful for the present methods can include a great number of optional composition and processing elements and steps.

[0042] Whenever a range is given in the specification, for example, a temperature range, a time range, or a composition or concentration range, all intermediate ranges and subranges, as well as all individual values included in the ranges given are intended to be included in the disclosure. It will be understood that any subranges or individual values in a range or subrange that are included in the description herein can be excluded from the claims herein.

[0043] All patents and publications mentioned in the specification are indicative of the levels of skill of those skilled in the art to which the invention pertains. References cited herein are incorporated by reference herein in their entirety to indicate the state of the art as of their publication or filing date and it is intended that this information can be employed herein, if needed, to exclude specific embodiments that are in the prior art. For example, when compositions of matter are claimed, it should be understood that compounds known and available in the art prior to Applicant's invention, including compounds for which an enabling disclosure is provided in the references cited herein, are not intended to be included in any composition of matter claims herein.

[0044] As used herein, “comprising” is synonymous with “including,” “containing,” or “characterized by,” and is inclusive or open-ended and does not exclude additional, unrecited elements or method steps. As used herein, “consisting of” excludes any element, step, or ingredient not specified in the claim element. As used herein, “consisting essentially of” does not exclude materials or steps that do not materially affect the basic and novel characteristics of the claim. In each instance herein any of the terms “comprising”, “consisting essentially of,” and “consisting of” may be replaced with either of the other two terms. The invention illustratively described herein suitably may be practiced in the absence of any element or elements, limitation or limitations which is not specifically disclosed herein.

[0045] One of ordinary skill in the art will appreciate that starting materials, biological materials, reagents, synthetic methods, purification methods, analytical methods, assay methods, and biological methods other than those specifically exemplified can be employed in the practice of the invention without resort to undue experimentation. All art-known functional equivalents, of any such materials and methods are intended to be included in this invention. The terms and expressions which have been employed are used as terms of description and not of limitation, and there is no intention that in the use of such terms and expressions of excluding any equivalents of the features shown and described or portions thereof, but it is recognized that various modifications are possible within the scope of the invention claimed. Thus, it should be understood that although the present invention has been specifically disclosed by preferred embodiments and optional features, modification and variation of the concepts herein disclosed may be resorted to by those skilled in the art, and that such modifications and variations are considered to be within the scope of this invention as defined by the appended claims.

[0046] Since other modifications and changes varied to fit particular operating requirements and environments will be apparent to those skilled in the art, the invention is not considered limited to the example chosen for purposes of disclosure and covers all changes and modifications which do not constitute departures from the true spirit and scope of this invention.

[0047] Having thus described the invention, what is desired to be protected by Letters Patent is presented in the subsequently appended claims.