Microalloyed steel mechanical property prediction method based on globally additive model
11475317 · 2022-10-18
Assignee
Inventors
Cpc classification
G06N7/01
PHYSICS
G06N5/01
PHYSICS
B21B1/22
PERFORMING OPERATIONS; TRANSPORTING
International classification
Abstract
The present invention provides a microalloyed steel mechanical property prediction method based on globally additive model, including the following steps: determining some influencing factors of the microalloyed steel mechanical property prediction model; calculating the components and contents of carbonitride precipitation in a microalloyed steel rolling process; expressing the microalloyed steel mechanical property prediction model as an additive form of several submodels according to generalized additive model; estimating the microalloyed steel mechanical property prediction model; and verifying reliability of the submodels. The microalloyed steel property prediction models obtained in the foregoing solution have advantages such as high prediction precision and a wide adaptation range, and may be used for design of new products and steel grade component optimization, so as to reduce the quantity of physical tests, shorten the product research and development cycle, and reduce costs.
Claims
1. A microalloyed steel mechanical property prediction method based on globally additive model, comprising the following steps: step A, determining, by a processor, influencing factors of a mechanical property prediction model of microalloyed steel, wherein the determined influencing factors include chemical components and microalloyed steel rolling process parameters, the chemical components include carbon, silicon, manganese, phosphorus and niobium in steel, and the microalloyed steel rolling process parameters include a reheating temperature, a roughing rolling temperature, a finishing entry temperature, a finishing rolling delivery temperature, a coiling temperature and a finishing rolling delivery thickness; step B, calculating, by the processor, components and contents of carbonitride precipitation in the microalloyed steel rolling process; step C, expressing, by the processor, the mechanical property prediction model of microalloyed steel as an additive form of several submodels according to generalized additive model; step D, estimating, by the processor, the mechanical property prediction model of microalloyed steel; step E, verifying, by the processor, reliability of the submodels; and step F, designing microalloyed steel products and optimizing steel grade by the processor using the mechanical property prediction model of microalloyed steel; wherein the step B comprises the following steps: step B-1, developing a thermodynamic model in which the components and the contents of the carbonitride precipitation in hot rolling process are capable of being quantitatively calculated based on a multivariate second-phase solid solution and precipitation theory, and considering interactions between the carbonitrides and AlN(aluminum nitride); and step B-2, solving the thermodynamic model, wherein numerical solution is performed by using the Newton-Raphson algorithm, to determine beginning precipitation temperatures and the precipitation order of the carbonitrides and AlN for the steel with different components by using an iterative solving process, so that the components and the contents of the carbonitride precipitation are obtained in the microalloyed steel rolling process, wherein the thermodynamic model comprises:
K.sub.MX=[M.sub.a][X.sub.a]=C×10.sup.A−B/T wherein
2. The microalloyed steel mechanical property prediction method based on globally additive model according to claim 1, wherein the step A comprises: step A-1, classifying influencing factors into three categories of chemical components, process parameters, and detection parameters, according to metallurgical mechanism, data collection process, and priori knowledge, wherein the detection parameters include sampling unit, sampling time, sampling direction, sample specification, yield type, or a combination thereof; and step A-2, searching for the influencing factors in each of the categories, wherein the step A-2 comprises the following steps: step A-2-1, selecting some recognized influencing factors; and step A-2-2, searching for the influencing factors by using random forests algorithm.
3. The microalloyed steel mechanical property prediction method based on globally additive model according to claim 1, wherein the interstitial element is the carbon element.
4. The microalloyed steel mechanical property prediction method based on globally additive model according to claim 1, wherein the interstitial element is the nitrogen element.
5. The microalloyed steel mechanical property prediction method based on globally additive model according to claim 1, wherein the submodels comprise component submodels and process submodels.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
(1) The accompanying drawings are included to provide a further understanding of the invention, and are incorporated in and constitute a part of this specification. The drawings illustrate embodiments of the invention and, together with the description, serve to explain the principles of the invention.
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DESCRIPTION OF THE EMBODIMENTS
(19) Reference will now be made in detail to the present preferred embodiments of the invention, examples of which are illustrated in the accompanying drawings. Wherever possible, the same reference numbers are used in the drawings and the description to refer to the same or like parts.
(20) It will be apparent to those skilled in the art that various modifications and variations can be made to the structure of the present invention without departing from the scope or spirit of the invention. In view of the foregoing, it is intended that the present invention cover modifications and variations of this invention provided they fall within the scope of the following claims and their equivalents.
(21) With reference to the accompanying drawings and the embodiments, a microalloyed steel mechanical property prediction method based on globally additive model provided in the present invention is described in detail below.
(22) In the following, a mechanical property prediction model is established by using hot continuous rolled microalloyed steel containing Nb as an example.
(23) As shown in
(24) Industrial big data analysis is performed on the parameters in a mechanical property prediction process, to search for the proper influencing factors. The influencing factor has diversity and complexity, and therefore a process of searching for the influencing factor is a repeated correction process. By means of an analysis method such as the random forests algorithm or the Bayesian method and with reference to the metallurgical mechanism and priori knowledge, chemical components such as carbon, silicon, manganese, phosphorus, and niobium in strip steel, and rolling process parameters such as reheating temperature T.sub.F, roughing rolling temperature T.sub.R, finishing entry temperature T.sub.FE, finishing rolling delivery temperature T.sub.FD, coiling temperature T.sub.C, and finishing rolling delivery thickness H.sub.FD are selected as influencing factors (that is, independent variables) of the model. Mechanical property parameters such as tensile strength and yield strength are selected as response variables of the model.
(25) There are many factors that affect the mechanical property, and there are interactions between some variables. This requires a combination of the metallurgical mechanism, statistical method, and the priori knowledge when influencing factors are being looked for.
(26) Step A-1: Classify influencing factors: classify the influencing factors into four categories according to the metallurgical mechanism, the data collection process, and priori knowledge: chemical components, process parameters, detection parameters, and abnormal markers. The detection-related variables are used to describe “how data comes”, for example, sampling unit, sampling time, sampling direction, sample specification, and yield type. When model research reaches an extent, such factors become main factors that limit improvement of precision and reliability of a model. Step A-2 is performed.
(27) Step A-2: Search for the influencing factors in each category, where this step comprises the following steps:
(28) Step A-2-1: Select some recognized influencing factors, for example, components such as C, Si, Mn, N, Nb, V, and Ti, and process parameters such as reheating temperature, finishing rolling temperature, coiling temperature, and finishing rolling delivery thickness. Then, influencing factors that possibly play a significant role are looked for.
(29) Step B: Calculate the components and contents of carbonitride precipitation in the microalloyed steel rolling process, and perform step C.
(30) Step B-1: Based on the multivariate second-phase solid solution and precipitation theory, develop a thermodynamic model in which the component and the content of the carbonitride precipitation in the hot rolling process can be quantitatively calculated, and consider interactions between the carbonitride and AlN. A thermodynamic model for an Fe—M—C—N alloy system is as follows:
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(32) In the foregoing formula, K.sub.MC and K.sub.MN are respectively solubility products of pure carbide and nitride, [M.sub.a], [C.sub.a], and [N.sub.a] are mole fractions of solid-soluted elements, L.sub.CN=−4260 J/mol is the interaction coefficient, R=8.314 J/(K.Math.mol) is the gas constant, T is the absolute temperature, M.sub.0, C.sub.0, and N.sub.0 are mole fractions of the microalloyed element, carbon element, and nitrogen element in steel, and f.sub.p is the mole fraction of precipitated niobium carbonitride.
(33) When there is AlN precipitated, because AlN has a hexagonal lattice structure, AlN is insoluble in carbonitride with a NaCl structure and independently exists. For the Fe—Al—Nb—C—N thermodynamic equilibrium system, the formulas (3) to (5) need to be replaced with the following formulas:
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(35) In the foregoing formulas, K.sub.AlN is the mole fraction of solid-soluted Al in austenite, K.sub.AlN is the solubility product of AlN, f.sub.AlN is the mole fraction of the precipitated AlN, and Al.sub.0 is the mole fraction of Al in the steel. In addition, K.sub.MC, K.sub.MN, and K.sub.AlN are all binary second-phase equilibrium solubility products, and generally may both be represented as:
K.sub.MX=[M.sub.a][X.sub.a]=C×10.sup.A−B/T (11)
(36) In the formula,
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A.sub.Fe, A.sub.M, and A.sub.X are respectively relative atomic masses of iron, the alloy element, and the interstitial element (carbon element or nitrogen element), and A and B are coefficients of the solubility product formula.
(38) Step B-2: Solve the thermodynamic model above. The thermodynamic model is a group of very complex nonlinear equations. Therefore, numerical solution is performed by using the Newton-Raphson algorithm to determine beginning precipitation temperatures and the precipitation order of the carbonitride and AlN for strips with different components by using an iterative solving process, so as to finally obtain the component and the content of the carbonitride precipitation in the microalloyed steel rolling process. The calculation procedure is shown in
(39) Research shows that Nb, C, and N in strip steel precipitate in an austenite phase to form the niobium carbonitride compound. Therefore, contents of NbC and NbN precipitated from each roll of strip steel in the rolling process need to be calculated by using the thermodynamic model, and are represented by mass fractions.
(40) For example,
(41) The model can be used to automatically calculate, according to the component and temperature of the strip, whether there is AlN precipitated. For convenience of comparison, the solid solution mass fraction of each element is represented by using a ratio relative to the original component.
(42) It can be learned from
(43) Step C: Express the microalloyed steel mechanical property prediction model as an additive form of several submodels according to generalized additive model, and perform step D.
(44) First, a theory related to the generalized additive model is briefly described. The generalized additive model is non-parametric extension of generalized linear model. The independent variable is fitted by using a non-parametric function, to estimate the relationship between the dependent variable and the independent variable. Each additive item in the model is estimated by using a single smooth function, and in each additive item, that how the dependent variable varies with the independent variable may be explained. The advantage of the model is that a nonlinear relationship between the dependent variable and the independent variable in high-dimensional data can be processed, and it is suitable for performing an exploratory analysis on data or searching for whether there is a dependence relationship between the dependent variable and the independent variable. The generalized additive model is widely used in many academic fields due to its advantages of simple structure and good flexibility and stability, and its mathematical expression may be written as:
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(46) In the formula, μ is a conditional expectation of the dependent variable Y, μ=E(Y|X.sub.1, X.sub.2, . . . , X.sub.P), g(.Math.) is a link function, α is an intercept, f.sub.j(.Math.) is the single variable function of the independent variable X.sub.j, and p is the number of independent variables.
(47) For the steel mechanical property prediction model, the identity function may be selected as the link function; an estimation method for the single variable smooth function of each independent variable is selected according to the scatter plot of each independent variable and dependent variable. Because the cubic smooth spline has advantages such as simple calculation, good stability, guaranteed astringency, the cubic smooth spline estimation method is selected.
(48) Based on the above, a basic form of the steel mechanical property prediction model may be written as:
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where T.sub.S represents the mechanical property parameter of steel, such as tensile strength, yield strength, or extensibility; α is an intercept; S.sub.j(.Math.) is the cubic smooth spline function of each independent variable X.sub.j, and additionally represents submodels of the mechanical property prediction model; and p is the number of independent variables.
(50) The submodels generally include two categories: submodels for chemical components such as C, Mn, Si, P, Nb, Ti, V, Mo, Cr, and carbonitrides which are generated by the interactions, and submodels for process parameters such as reheating temperature, roughing rolling temperature, finishing rolling entry temperature, coiling temperature, and finishing rolling delivery thickness.
(51) A single variable smooth function of each independent variable is estimated by using the cubic smooth spline, and the form of the model is set as:
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(53) In the formula, S.sub.i(X.sub.i) is a cubic smooth spline function of each independent variable, and mainly comprises influencing factors such as T.sub.F, T.sub.R, T.sub.FE, T.sub.FD, T.sub.C, H.sub.FD, Cs (residual carbon), Si, Mn, P, NbC, and NbN.
(54) Step D: Estimate the microalloyed steel mechanical property prediction model, and perform step E.
(55) After the basic form of the steel mechanical property prediction model is determined, the microalloyed steel mechanical property prediction model is estimated according to a large amount of hot rolling process data collected onsite, that is, a parametric form or a non-parametric form of each submodel is obtained by using an estimation algorithm.
(56) Each single variable smooth function S.sub.j(X.sub.j) is estimated by using the Back-fitting algorithm, and the specific implementation process of the estimation is as follows:
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and
(58) end: until
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is less than a predetermined positive constant or the number of iterations reaches the preset number.
(60) The number of cycles of the Back-fitting algorithm is set to 10, and when cyclic iteration calculation ends, α=539.16 is obtained.
(61) The following provides diagrams of smooth functions of main influencing factors of the tensile strength. As shown in
(62) Step E: Verify reliability of the submodels.
(63) After the mechanical property prediction model is established, reliability of the submodels needs to be verified according to the metallurgical mechanism and production data, that is, authenticity of a law obtained by the submodel needs to be verified. An authentic law often has repeatability. Therefore, when the reliability of the submodels is verified, importance should be attached to the repeatability of the law, and whether the law can be reproduced by data should be verified in different dimensions, thereby preventing generation of some false laws. If a law obtained by a submodel can be reproduced by data or no clear evidence can be found to prove falsehood of the law in most cases, the submodel is considered reliable. Otherwise, the cause of submodel failure needs to be analyzed, and the submodel needs to be revised again.
(64) As shown in
(65) A tensile strength prediction model of hot rolled Nb microalloyed steel can be obtained according to the formula (14) and each single variable smooth function obtained in
(66) Tensile strength and yield strength of 7740 rolls of Nb microalloyed strips (including multiple steel grades) produced by a hot continuous rolling production line are calculated by using the foregoing models. Comparison between predicted values and measured values for the model is shown in
(67) TABLE-US-00001 TABLE 1 Prediction error of the model. Model Tensile strength Yield strength RMSE/MPa 21.6 24.6 ME/% 2.54 3.34
(68) TABLE-US-00002 TABLE 2 Intermediate calculation results of tensile strength for several rolls of strips. Strip steel sequence number Parameter 1 2 3 4 5 6 7 8 9 S.sub.1(T.sub.F) −3.2795 2.4219 3.6200 4.9995 5.6934 6.0414 6.9145 7.2649 7.9679 S.sub.2(T.sub.R) −0.1244 3.1508 6.5596 3.2660 4.2984 2.9198 2.2243 3.4963 6.6715 S.sub.3(T.sub.FE) 1.2963 2.2378 0.9874 2.1188 2.4368 2.4767 2.1981 2.5967 1.3739 S.sub.4(T.sub.FD) −8.2952 −2.6317 0.1411 −7.6808 −1.4386 −1.0425 −7.4764 −2.4324 −1.8355 S.sub.5(T.sub.C) −0.1550 1.4211 0.7026 2.5783 0.4162 1.7096 6.1059 1.9986 5.5121 S.sub.6(H.sub.FD) −5.9162 2.1314 5.6170 17.848 2.0221 2.0028 17.822 2.0221 15.714 S.sub.7(Cs) −4.8975 −5.0430 −3.2161 6.3459 −5.4361 −5.4900 6.0207 −4.9135 −4.2815 S.sub.8(Si) −22.322 −22.600 −13.670 12.143 −18.891 18.5810 12.891 −18.453 24.381 S.sub.8 (Mn) 8.0385 7.6830 6.6687 7.2230 4.0278 3.7995 6.6687 3.8449 7.8596 S.sub.10(P) −17.967 −13.777 −6.1483 −15.339 −21.255 −15.859 −12.920 −17.322 −6.1531 S.sub.11(Nbc) 9.9839 7.1897 18.559 21.117 1.2532 −1.5389 20.931 −2.7791 25.876 S.sub.12(NbN) −9.2894 −5.1192 −9.3244 5.8124 −0.7447 −0.1989 3.0863 −7.8254 −1.0669 T.sub.s predicted 486.236 516.228 549.659 599.595 511.546 515.402 603.629 506.661 621.182 value/MPa T.sub.s measured 483 511 547 605 507 521 602 511 616 value/MPa Error rate/% 0.67 1.02 0.49 0.89 0.90 1.07 0.27 0.85 0.84
(69) It can be learned that, all obtained submodels comply with existing experience and mechanism knowledge, and new models have relatively high prediction precision. In addition, no manual revision is required in the calculation process. In the model, deviations between the predicted values and the measured values are all within a small range. The model has relatively strong adaptability.
Functions and Effects of the Embodiments
(70) According to the microalloyed steel mechanical property prediction method based on globally additive model provided in the embodiments, “globally” means that modeling is performed by collecting production data of multiple steel grades, but not for only a specific steel grade; “additive” means that the model is additive in form. The mechanical property prediction model is divided into multiple submodels by using the generalized additive model.
(71) In addition, impact of carbonitride precipitation of the microalloyed elements on mechanical property needs to be considered. The thermodynamic model is developed based on the multivariate second-phase solid solution and precipitation theory, the components and contents of carbonitride precipitation including different components in the microalloyed steel rolling process at different temperatures are quantitatively calculated, and the calculated component and the content of the carbonitride precipitations are combined with actual production data of microalloyed steel, to establish the mechanical property prediction models that have high reliability, strong extensionality, and wide practicability.
(72) The microalloyed steel mechanical property prediction models obtained in the foregoing technical solution have advantages such as high calculation precision and a wide adaptation range, and may be used for design of new microalloyed steel products and steel grade optimization, so as to reduce a quantity of conventional physical tests, shorten the product research and development cycle, and reduce research and development costs.
(73) The foregoing implementations are exemplary cases of the present invention, and are not intended to limit the protection scope of the present invention.