METHOD FOR THE PRODUCTION OF A HOLLOW FIBER MODULE, AND HOLLOW FIBER MODULE
20170136415 ยท 2017-05-18
Inventors
- Wilhelm Requate (Heiligenstadt, DE)
- Gerid Hellwig (Niemetal, DE)
- Johannes Wortmeyer (Goettingen, DE)
- Ulrich Apelt (Ebergoetzen, DE)
Cpc classification
B01D63/033
PERFORMING OPERATIONS; TRANSPORTING
International classification
Abstract
A hollow fiber module (1, 1) is made by inserting a bundle of hollow fibers (3) into a housing (2, 2) that has an end closed by a cap (17). A fluid first component (27) that can assume a solid state is introduced into a space adjacent the cap (17) and forms a spacer into which ends of the hollow fibers (6, 7) project. A fluid curable second component (4) is introduced before the first component (27) via a second inflow (28) and is cured to form a sealing layer (9) that embeds the bundle of hollow fibers (3) and seals it with respect to the adjacent housing wall (29, 29). The cap (17) is removed from the module housing (2, 2) along with the first component (27) and ends of the hollow fibers (6) embedded in the first component (27).
Claims
1. A method for producing a hollow fiber module (1, 1), comprising: a first step of inserting a hollow fiber bundle (3) into a module housing (2, 2), that has at least one end closed by a cap (17), a second step of filling a fluid first component (27) via a first inflow (26) and into an intermediate space arranged between the hollow fiber ends (6, 7) and the cap (17), to form a spacer, the fluid first component (27) being formed from a material that can assume a solid state and being filled so that the hollow fiber ends (6, 7) project into the first component (27), and a third step of introducing a fluid curable second component (4) upstream of the first component (27), directed away from the cap (17), via a second inflow (28), wherein the second component (4), when in a cured state forms a sealing layer (9) that embeds the hollow fiber bundle (3) and seals the hollow fiber bundle (3) with respect to an adjacent module housing wall (29, 29), wherein the cap (17) is a removable sprue cover (18, 18, 18), and, after the curing of the second component (4), the cap (17), the first component (27) that has been solidified to form a plug (30), and the hollow fiber ends (6) embedded in the plug (30) and projecting out of the end face (10) of the layer (9) formed by the second component (4) are removed from the module housing (2, 2).
2. The method of claim 1, wherein the step of removing the sprue cover (18, 18, 18) includes severing the hollow fibers (5) in a boundary layer formed by the first component (27) and the second component (4).
3. The method of claim 2, wherein the step of removing the sprue cover (18, 18, 18) includes a rotary, pulling movement.
4. The method of claim 3, further comprising centrifuging the module housing (2, 2) in a centrifuge between the second and the third step.
5. The method of claim 4, further comprising centrifuging the module housing (2, 2) again after solidification of the first component (27) and before the curing of the second component (4).
6. The method of claim 1, further comprising providing the hollow fiber bundle (3) with a supporting fabric before the first step.
7. The method of claim 5, further comprising cutting the hollow fiber bundle (3) to a prespecified length before the first step.
8. The method of claim 7, wherein silicone is filled into the module housing (2, 2) as the first fluid component (27), and polyurethane is filled into the module housing (2, 2) as the second fluid component (4).
9. A hollow fiber module (1, 1), comprising: a module housing (2, 2), a hollow fiber bundle (3) arranged in a module housing (2, 2), at least one sealing layer (9).sub.7 made of a cured second component (4) disposed on an end of the hollow fiber bundle (3) and extending transverse to a longitudinal direction of the hollow fiber bundle (3), wherein the sealing layer (9) embeds the hollow fiber bundle (3) and seals the hollow fiber bundle (3) with respect to an adjacent module housing wall (29, 29), wherein hollow fiber ends (7), and an end face (10) of the sealing layer (9) facing the hollow fiber ends (7), form a common plane in which lumens (11) of the hollow fibers (5) is freely accessible, and the end face (10) of the sealing layer (9) is recessed by a prespecifiable distance (14) with respect to an end face (12) of an adjacent free end (13, 13) of the module housing (2, 2).
10. The hollow fiber module of claim 9, wherein the module housing (2) is a rigid plastic housing.
11. The hollow fiber module of claim 9, wherein the module housing (2) is a flexible tube.
12. The hollow fiber module of claim 11, wherein the free end (13) of the module housing (2) is configured to be directly connected to a tube connector (16).
13. A cap (17) defining a sprue cover (18, 18, 18) for producing the hollow fiber module (1, 1) of claim 9, wherein the sprue cover (18, 18, 18) has a circumferential collar (19, 19, 19) that can be inserted into the free end (13, 13) of the module housing (2 2), and when inserted receives the free hollow fiber ends (6) of the hollow fiber bundle (3), an end of the collar (19, 19, 19) that faces away from the hollow fiber bundle (3) is closed by an end wall (25), and the sprue cover (18, 18, 18) has a first inflow (26) for a first fluid component (27).
14. The cap of claim 13, wherein the circumferential collar (19, 19, 19) has a profiling (21) or resistive elements (22, 23) on its inner surface (20, 20, 20) facing the hollow fiber bundle (3).
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0024]
[0025]
[0026]
[0027]
[0028]
[0029]
[0030]
[0031]
[0032]
[0033]
DETAILED DESCRIPTION
[0034] A hollow fiber module 1 substantially comprises a module housing 2, a hollow fiber bundle 3 and a second component 4.
[0035] In the embodiments shown in
[0036] The hollow fiber bundle consists of a plurality of hollow fibers 5 with hollow fiber ends 6 in the initial state, and the hollow fiber ends 7 in the finished state.
[0037] The second component 4 forms a layer 9 transverse to the longitudinal axis 8 of the hollow fiber module 1, which when cured embeds the hollow fiber ends 7, and seals the hollow fiber bundle 3 with respect to the module housing 2. In the finished state, the layer 9 has an end face 10 which forms, together with the hollow fiber ends 7, a common plane in which the lumen 11 of the hollow fibers 5 is freely accessible. The end face 10 of the sealing layer 9 is recessed relative to the end face 12 of the free end 13 of the module housing 2 by a prespecifiable distance 14.
[0038] In the embodiment shown in
[0039] To produce a hollow fiber module 1, 1, in a first step the hollow fiber bundle 3 is inserted into the module housing 2, 2. For ease of insertion, the hollow fiber bundle 3 can be provided with a supporting fabric, which is not shown. On its free end 13, 13, the module housing 2, 2 is closed by a cap 17 which is designed as a removable sprue cover 18. The sprue cover 18 comprises a circumferential collar 19, which can be inserted into the free end 13 of the module housing 2 in such a manner that it receives the free hollow fiber ends 6 and encloses the hollow fiber bundle 3 with its inner surface 20. The collar 19 of the sprue cover 18 can have on its inner surface 20, enclosing an internal space 24, a profiling 21 (see
[0040] After the module housing 2 has been sealed on its free end by the cap 17, in a second step the fluid first component 27 is filled into an intermediate space arranged between the hollow fiber ends 6 and the cap 17, via the first inflow 26 of the cap 17 and/or the sprue cover 18, wherein the hollow fiber ends 6 project into the first component 27 (see
[0041] After the curing of the second component 4, the sprue cover 18, including the first component 27 which forms the solidified plug 30, together with the hollow fiber ends 6 embedded in the plug 30, the same protruding from the end face 10 of the layer 9 formed by the second component 4, is removed. The sprue cover is removed in a rotating, pulling motion. Due to the rotating motion, the hollow fiber ends 6 are sheared off and the sprue cover 18 can be pulled out, with the plug 30 and the embedded hollow fiber ends 6.
[0042] According to the embodiments, silicone is filled into the module housing 2 as the first fluid component 27, and polyurethane is filled into the module housing 2 as the second fluid component 4. In another embodiment of the invention which is not illustrated, silicone is filled into the module housing as the first fluid component, and as the second fluid component, an epoxy adhesive is filled into the module housing. Alternatively, a mixture of silicone and polyurethane in a ratio of 1:1, 1:2 or 1:3 can be used as the first fluid component, and polyurethane can be used as the second fluid component.
[0043] Of course, the embodiments discussed in the specific description and shown in the figures only represent illustrative embodiments of the present invention. The present disclosure provides a person skilled in the art with a wide spectrum of variation options.
LIST OF REFERENCE NUMBERS
[0044] 1, 1 hollow fiber module
[0045] 2, 2 module housing
[0046] 3 hollow fiber bundle
[0047] 4 second component
[0048] 5 hollow fiber module
[0049] 6 hollow fiber end (initial state)
[0050] 7 hollow fiber end (finished state)
[0051] 8 longitudinal axis of 1
[0052] 9 layer of 4
[0053] 10 end face of 9
[0054] 11 lumen of 5
[0055] 12 end face of 2
[0056] 13, 13 free end of 2/15
[0057] 14 distance
[0058] 15 tube of 2
[0059] 16 tube connection
[0060] 17 cap
[0061] 18, 18, 18 sprue cover
[0062] 19, 19, 19 collar of 18
[0063] 20, 20, 20 inner surface of 19
[0064] 21 profiling
[0065] 22 resistive elements
[0066] 23 resistive elements
[0067] 24, 24, 24 internal space
[0068] 25 end wall
[0069] 26 first inflow
[0070] 27 first component
[0071] 28 second inflow of 2
[0072] 29 module housing wall of 2
[0073] 30 plug of 27