SiC SUBSTRATE SEPARATING METHOD
20170136572 ยท 2017-05-18
Inventors
Cpc classification
B23K26/53
PERFORMING OPERATIONS; TRANSPORTING
B23K26/082
PERFORMING OPERATIONS; TRANSPORTING
B23K26/0823
PERFORMING OPERATIONS; TRANSPORTING
B23K26/0006
PERFORMING OPERATIONS; TRANSPORTING
B23K26/0876
PERFORMING OPERATIONS; TRANSPORTING
B24B9/065
PERFORMING OPERATIONS; TRANSPORTING
International classification
B23K26/00
PERFORMING OPERATIONS; TRANSPORTING
B24B9/06
PERFORMING OPERATIONS; TRANSPORTING
H01L21/02
ELECTRICITY
H01L29/16
ELECTRICITY
Abstract
Disclosed herein is an SiC substrate separating method for separating an SiC substrate into at least two parts in a planar manner. The SiC substrate separating method includes an adhesive tape attaching step of attaching a transparent adhesive tape to a first surface of the SiC substrate, a support member attaching step of attaching a support member to a second, opposite surface of the SiC substrate, and a separation start point forming step of setting the focal point of a laser beam at a predetermined depth from the adhesive tape and next applying the laser beam to the adhesive tape while relatively moving the focal point and the SiC substrate to thereby form a modified layer parallel to the first surface of the SiC substrate and cracks propagating from the modified layer, thus forming a separation start point.
Claims
1. An SiC substrate separating method for separating an SiC substrate into at least two parts in a planar manner, said SiC substrate having a first surface and a second surface opposite to said first surface, said SiC substrate separating method comprising: an adhesive tape attaching step of attaching a transparent adhesive tape to said first surface of said SiC substrate; a support member attaching step of attaching a support member to said second surface of said SiC substrate; a separation start point forming step of setting the focal point of a laser beam having a transmission wavelength to said SiC substrate and said adhesive tape inside said SiC substrate at a predetermined depth from said adhesive tape after performing said adhesive tape attaching step and said support member attaching step, and next applying said laser beam to said adhesive tape as relatively moving said focal point and said SiC substrate to thereby form a modified layer parallel to said first surface of said SiC substrate and cracks propagating from said modified layer, thus forming a separation start point; and a separating step of applying an external force to said SiC substrate after performing said separation start point forming step, thereby separating said SiC substrate into a first SiC substrate having said first surface and a second SiC substrate having said second surface at said separation start point in the condition where said adhesive tape is attached to said first SiC substrate and said support member is attached to said second SiC substrate.
2. The SiC substrate separating method according to claim 1, wherein the refractive index of said adhesive tape is higher than the refractive index of air and lower than the refractive index of said SiC substrate.
3. The SiC substrate separating method according to claim 1, further comprising a flattening step of grinding a separation surface of said first SiC substrate separated from said second SiC substrate at said separation start point and also grinding a separation surface of said second SiC substrate separated from said first SiC substrate at said separation start point, by using an abrasive member, thereby flattening said separation surface of said first SiC substrate and said separation surface of said second SiC substrate.
4. An SiC substrate separating method for separating an SiC substrate into at least two parts in a planar manner, said SiC substrate having a first surface, a second surface opposite to said first surface, a c-axis extending from said first surface to said second surface, and a c-plane perpendicular to said c-axis, said SiC substrate separating method comprising: an adhesive tape attaching step of attaching a transparent adhesive tape to said first surface of said SiC substrate; a support member attaching step of attaching a support member to said second surface of said SiC substrate; a separation start point forming step of setting the focal point of a laser beam having a transmission wavelength to said SiC substrate and said adhesive tape inside said SiC substrate at a predetermined depth from said adhesive tape after performing said adhesive tape attaching step and said support member attaching step, and next applying said laser beam to said adhesive tape as relatively moving said focal point and said SiC substrate to thereby form a modified layer parallel to said first surface of said SiC substrate and cracks propagating from said modified layer, thus forming a separation start point; and a separating step of applying an external force to said SiC substrate after performing said separation start point forming step, thereby separating said SiC substrate into a first SiC substrate having said first surface and a second SiC substrate having said second surface at said separation start point in the condition where said adhesive tape is attached to said first SiC substrate and said support member is attached to said second SiC substrate; said separation start point forming step including a modified layer forming step of relatively moving the focal point of said laser beam in a first direction perpendicular to a second direction where said c-axis is inclined by an off angle with respect to a normal to said first surface of said SiC substrate and said off angle is formed between said c-plane and said first surface, thereby linearly forming said modified layer extending in said first direction inside said SiC substrate, and an indexing step of relatively moving said focal point in said second direction to thereby index said focal point by a predetermined amount in said second direction.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
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DETAILED DESCRIPTION OF THE PREFERRED EMBODIMENT
[0036] A preferred embodiment of the present invention will now be described in detail with reference to the drawings. Referring to
[0037] A second slide block 16 is mounted on the first slide block 6 so as to be movable in the Y direction. The second slide block 16 is moved in an indexing direction, or in the Y direction along a pair of guide rails 24 by an indexing mechanism 22 composed of a ball screw 18 and a pulse motor 20. A chuck table 26 having a suction holding portion 26a is mounted on the second slide block 16. The chuck table 26 is movable in the X direction and the Y direction by the feeding mechanism 12 and the indexing mechanism 22 and also rotatable by a motor stored in the second slide block 16.
[0038] A column 28 is provided on the stationary base 4 so as to project upward therefrom. A laser beam applying mechanism (laser beam applying means) 30 is mounted on the column 28. The laser beam applying mechanism 30 is composed of a casing 32, a laser beam generating unit 34 (see
[0039] As shown in
[0040] Referring to
[0041] The ingot 11 has a c-axis 19 inclined by an off angle toward the second orientation flat 15 with respect to a normal 17 to the upper surface 11a and also has a c-plane 21 perpendicular to the c-axis 19. The c-plane 21 is inclined by the off angle with respect to the upper surface 11a. In general, in a hexagonal single crystal ingot including the SiC ingot 11, the direction perpendicular to the direction of extension of the shorter second orientation flat 15 is the direction of inclination of the c-axis 19. The c-plane 21 is set in the ingot 11 innumerably at the molecular level of the ingot 11. In this preferred embodiment, the off angle is set to 4. However, the off angle is not limited to 4 in the present invention. For example, the off angle may be freely set in the range of 1 to 6 in manufacturing the ingot 11.
[0042] Referring again to
[0043] Referring to
[0044] The SiC substrate 31 has a first orientation flat 37 and a second orientation flat 39 perpendicular to the first orientation flat 37. The length of the first orientation flat 37 is set longer than the length of the second orientation flat 39. Since the SiC substrate 31 is obtained by slicing the SiC ingot 11 shown in
[0045] The SiC substrate 31 has a c-axis 19 inclined by an off angle toward the second orientation flat 39 with respect to a normal 17 to the upper surface 31a and also has a c-plane 21 perpendicular to the c-axis 19 (see
[0046] After attaching the adhesive tape 41 and the support member 43 to the SiC substrate 31, the SiC substrate 31 is placed on the chuck table 26 in the condition where the support member 43 is oriented downward as shown in
[0047] In other words, as shown in
[0048] In the SiC substrate separating method of the present invention, it is important that the scanning direction of the laser beam to be applied from the focusing means 36 is set to the direction of the arrow A perpendicular to the direction of the arrow Y1 where the off angle of the SiC substrate 31 is formed. That is, it was found that by setting the scanning direction of the laser beam to the direction of the arrow A as mentioned above in the SiC substrate separating method of the present invention, cracks propagating from a modified layer formed inside the SiC substrate 31 by the laser beam extend very long along the c-plane 21.
[0049] In performing the SiC substrate separating method according to this preferred embodiment, a separation start point forming step is performed in such a manner that the focal point of the laser beam having a transmission wavelength (e.g., 1064 nm) to the SiC substrate 31 and the adhesive tape 41 is set inside the SiC substrate 31 held through the support member 43 on the chuck table 26 at a predetermined depth Dl from the upper surface of the adhesive tape 41 and the laser beam is then applied to the adhesive tape 41 as relatively moving the focal point and the SiC substrate 31 to thereby form a modified layer 45 parallel to the first surface (upper surface) 31a of the SiC substrate 31 and cracks 47 propagating from the modified layer 45 along the c-plane 21, thus forming a separation start point (see
[0050] This separation start point forming step includes a modified layer forming step of relatively moving the focal point of the laser beam in the direction of the arrow A perpendicular to the direction of the arrow Y1 where the c-axis 19 is inclined by the off angle with respect to the normal 17 to the first surface (upper surface) 31a of the SiC substrate 31 and the off angle is formed between the c-plane 21 and the first surface (upper surface) 31a as shown in
[0051] As shown in
[0052] For example, the separation start point forming step is performed under the following laser processing conditions in the preferred embodiment.
[0053] Light source: Nd:YAG pulsed laser
[0054] Wavelength: 1064 nm
[0055] Repetition frequency: 80 kHz
[0056] Average power: 3.2 W
[0057] Pulse width: 4 ns
[0058] Spot diameter: 10 m
[0059] Numerical aperture (NA) of the focusing lens: 0.45
[0060] Index amount: 400 m
[0061] In the laser processing conditions mentioned above, the width W1 of the cracks 47 propagating from the modified layer 45 along the c-plane 21 in one direction as viewed in
[0062] In the case that the average power was set to 2 W, the width W1 of the cracks 47 was approximately 100 m. In the case that the average power was set to 4.5 W, the width W1 of the cracks 47 was approximately 350 m. In the case that the average power is less than 2 W or greater than 4.5 W, the modified layer 45 cannot be well formed inside the SiC substrate 31. Accordingly, the average power of the laser beam to be applied is preferably set in the range of 2 W to 4.5 W. For example, the average power of the laser beam to be applied to the SiC substrate 31 was set to 3.2 W in this preferred embodiment.
[0063] Referring to
[0064] There will now be considered a Fresnel reflection intensity in the case that a laser beam LB is directly applied to the SiC substrate 31 as shown in
[0065] In the case shown in
[0066] On the other hand, in the case shown in
[0067] First, the Fresnel reflection intensity 12 of reflected light R2 on the upper surface of the adhesive tape 41 is given as I.sub.2=I.sub.0{(n2n1)/(n2+n1)}.sup.2=100{(1.51)/(1.5+1)}.sup.2=4%. Accordingly, the intensity of the laser beam LB transmitted through the adhesive tape 41 is given as 96%.
[0068] Next, the Fresnel reflection intensity I.sub.3 of reflected light R3 on the upper surface 31a of the SiC substrate 31 is given as I.sub.3=I.sub.2{(n3n2)/(n3+n2)}.sup.2=96 {(2.61.5)/(2.6+1.5)}.sup.2=6.9%. Accordingly, the intensity of the laser beam transmitted through the SiC substrate 31 becomes 89.1% of the intensity of the laser beam LB applied to the adhesive tape 41.
[0069] It is apparent from the above consideration that when the transparent adhesive tape 41 is attached to the upper surface 31a of the SiC substrate 31 as shown in
[0070] In this manner, the focal point of the laser beam is sequentially indexed to form a plurality of modified layers 45 and the cracks 47 extending from each modified layer 45 along the c-plane 21 inside the SiC substrate 31 over the whole area thereof. Thereafter, a separating step is performed in such a manner that an external force is applied to the SiC substrate 31 to thereby separate the SiC substrate 31 into two parts in a planar manner at the separation start point composed of the modified layers 45 and the cracks 47. This separating step is performed by using the pressing mechanism 54 shown in
[0071] As shown in
[0072] While the SiC substrate 31 is separated into two parts in a planar manner by using the pressing mechanism 54 in this preferred embodiment, the SiC substrate 31 may be separated into two parts in a planar manner by pulling the adhesive tape 41 and the support member 43 in opposite directions, because the adhesive tape 41 is attached to the first surface (upper surface) 31a of the SiC substrate 31, the support member 43 is attached to the second surface (lower surface) 31b of the SiC substrate 31, and the separation start point composed of the modified layers 45 and the cracks 47 is formed inside the SiC substrate 31 over the whole area thereof.
[0073] As shown in
[0074] This flattening step is performed by using a grinding apparatus including a chuck table 58 and a grinding unit 60 shown in
[0075] In the flattening step, the chuck table 58 is rotated at 300 rpm, for example, in the direction shown by an arrow a in
[0076] In the case of flattening the separation surface 49 of the SiC substrate 31A obtained by the separating step mentioned above, it is only necessary to slightly grind the separation surface 49 of the SiC substrate 31A by an amount of approximately 1 m to 5 m, so that the wear amount of the abrasive members 72 can be suppressed to approximately 4 m to 25 m. Further, the separation surface of the other SiC substrate 31B shown in
[0077] In the above preferred embodiment, the separation start point composed of the modified layers 45 and the cracks 47 is formed along the c-plane 21 in the SiC substrate 31. However, the SiC substrate separating method of the present invention is also applicable to the case that the separation start point composed of the modified layers 45 and the cracks 47 is not formed along the c-plane 21 as in Japanese Patent Laid-open No. 2013-49161, because the SiC substrate 31 is reinforced by the adhesive tape 41 and the support member 43 on the opposite sides.
[0078] The present invention is not limited to the details of the above described preferred embodiment. The scope of the invention is defined by the appended claims and all changes and modifications as fall within the equivalence of the scope of the claims are therefore to be embraced by the invention.