DEVICE AND METHOD FOR PRECIPITATING SOLIDS FROM A SUSPENSION INCLUDING DISSOLVED GASES
20170088802 ยท 2017-03-30
Assignee
Inventors
Cpc classification
B01D29/117
PERFORMING OPERATIONS; TRANSPORTING
B01D29/6476
PERFORMING OPERATIONS; TRANSPORTING
C12C11/11
CHEMISTRY; METALLURGY
B01D29/76
PERFORMING OPERATIONS; TRANSPORTING
B30B9/128
PERFORMING OPERATIONS; TRANSPORTING
International classification
B30B9/12
PERFORMING OPERATIONS; TRANSPORTING
B01D29/64
PERFORMING OPERATIONS; TRANSPORTING
B01D29/11
PERFORMING OPERATIONS; TRANSPORTING
B01D29/94
PERFORMING OPERATIONS; TRANSPORTING
Abstract
A device for a precipitating solid material particles from a suspension of a brew liquid including dissolved CO.sub.2 and plant based aroma hearer solid material particles, the device including a filter surface which separates a non-filtrate space from a filtrate space wherein the non-filtrate space receives the suspension; a suspension inlet leading into the non-filtrate space, a filtrate outlet opening into the filtrate space; a mechanical compressor that is provided in the non-filtrate space and configured to feed the suspension under a separation of the brew liquid through the filter surface within the non-filtrate space along the filter surface to a compression portion of the non-filtrate space and to compress the remaining solid materials: and a solid material output opening provided in a wall of the non-filtrate space in the compression portion of the non-filtrate space wherein the solid material output opening is closeable tight relative to an ambient atmosphere.
Claims
1. A device for a precipitating solid material particles from a suspension of a brew liquid including dissolved CO.sub.2 and plant based aroma bearer solid material particles, the device comprising: a filter surface which separates a non-filtrate space from a filtrate space wherein the non-filtrate space receives the suspension; a suspension inlet leading into the non-filtrate space, a filtrate outlet opening into the filtrate space; a mechanical compressor device that is provided in the non-filtrate space and configured to feed the suspension under a separation of the brew liquid through the filter surface within the non-filtrate space along the filter surface to a compression portion of the non-filtrate space and to compress the remaining solid materials; and a solid material output opening provided in a wail of the non-filtrate space in the compression portion of the non-filtrate space wherein the solid material output opening is closeable gas tight and pressure tight relative to an ambient atmosphere.
2. The device according to claim 1, wherein the mechanical compressor device is formed by a compressor screw which is arranged rotatable in a sieve tube including the filter surface.
3. The device according to claim 2, wherein the compressor screw includes a feed section and a compressor section, and wherein the feed section transitions into the compressor section continuously.
4. The device according to clam 2, wherein a helical radially outer edge of the compressor screw is arranged directly adjacent to the filter surface.
5. The device according to claim 4, wherein the compressor screw is provided with at least one scraping device at the helical radially outer edge of the compressor screw, and wherein the scraping device contacts the filter surface.
6. The device according to claim 1, wherein the mechanical compressor device includes a piston that is axially movable between a decompression position and a compression position in a cylinder including the filter surface and radially defining the non-filtrate space, wherein bypass devices are provided which facilitate a flow of suspension into the compression portion of the non-filtrate space when the cylinder is moved into the decompression position.
7. The device according to claim 6, wherein the bypass devices are formed by openings in the piston that are provided with check valves.
8. The device according to claim 1, wherein the solid material output opening is provided with a closure element which is preloaded by a preload force into a closed position where the solid material output opening is closed by the closure element gas tight and pressure tight.
9. The device according to claim 8, wherein the closure element is preloaded by a spring into the closed position against a sealing seat of the solid material output opening.
10. The device according to claim 1, wherein the solid material output opening is connected with a solid material output conduit which leads into a pressurized solid material collecting container.
11. The device according to claim 10, wherein the solid material collecting container includes a pressurized gas feed through which pressurized gas is introducible into an interior of the solid material collecting container.
12. The device according to claim 1, wherein at least one fluid inlet opening for a washing fluid for solid material cake washing is provided in front or in the compression portion of the non-filtrate space.
13. A method for precipitating solid material particles from a suspension including a brew liquid including dissolved CO.sub.2 and plant based aroma bearer solid material particles using a device according to one of the preceding claims and comprising the steps: continuously feeding the suspension from a brew liquid including solid material particles into the non-filtrate space; feeding the suspension in the non-filtrate space along the filter surface while precipitating the brew liquid through the filter surface and compressing the solid materials into a compressed solid materials cake; and continuously outputting the said material cake from the non-filtrate space through the solid material output opening while maintaining a positive pressure in the non-filtrate space relative to the ambient atmosphere.
14. The method according to claim 13, wherein the solid material output opening from a start-up of the device until a compressed filter cake is built up is either closed by a closure element, or is in fluid connection with an external pressure cavity in which a pressure is provided which corresponds to a positive pressure in the non-filtrate space.
15. The method according to claim 13, wherein a washing liquid, for example water is added to the solid material cake shortly before reaching a maximum compression of the solid material cake.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
[0042] Advantageous embodiment of the invention with additional configurative details and additional advantages are subsequently described with reference to the appended drawing figures wherein:
[0043]
[0044]
[0045]
[0046]
[0047]
[0048]
[0049]
[0050]
DETAILED DESCRIPTION OF THE INVENTION
[0051]
[0052] The device 1 includes a housing 10 with an inlet portion 10, a cylindrical center portion 10 and an outlet portion 10. The inlet portion 10 is provided with a suspension inlet 11 through which a suspension including brew liquid and solid material particles forming a non-filtrate, for example made from young beer and plant based aroma bearer solid materials like e.g. hops pellets is introducible.
[0053] In the cylindrical center portion 10 of the housing 10 a cylindrical sieve element 12 is internally arranged, wherein a cylindrical circumferential wall 12 of the sieve element is provided with sieve openings 12 so that a filter surface 13 is formed. The sieve element 12 can be provided as gap sieve, hole sieve or it can be provided from fabric material wherein a gap width or a hole diameter is between 5 m and 100 m, advantageously between 20 m and 50 m.
[0054] An outer wall 14 of the center portion 10 of the housing 10 is arranged about the circumferential wall 12 of the sieve element 12 that is provided with the sieve openings 12 wherein the outer wall 14 is arranged at a radial distance from the circumferential wall 12. Thus, an annular cavity 14 is formed between the circumferential wail 12 of the sieve element 12 that is provided with the sieve openings 12 and the outer wall 14 of the center portion 10.
[0055] The interior of the cylindrical sieve element 12 forms an non-filtrate cavity 16 together with the inlet portion 10 and the annular space 14 enveloping the sieve element 12 forms a filtrate space between the sieve surface 13 and the cylindrical wail 14 of the center portion 10 of the housing 10.
[0056] The cylindrical center portion 10 of the housing 10 is provided with a filtrate outlet 15 at its end oriented away from the inlet portion 10, wherein the filtrate outlet opens into the annular cavity 14 and facilitates draining liquid that has passed through the filter surface 13.
[0057] The outlet portion 10 is provided on a side of the housing 10 that is oriented away from the inlet portion 10 wherein the outlet portion is fluid connected with an interior of the cylindrical sieve element 12, thus with the non-filtrate space 16 and wherein the outlet portion is configured adjacent to the cylindrical sieve wall 13 as a closed wall 18 which tapers cone shaped. At a free end of the outlet portion 10 a solid material outlet opening 19 is provided which is provided with a sealing surface 19.
[0058] A closure device 2 is provided in front of the solid material outlet opening 19 wherein the closure device includes a closure element 20 which is movable or also preloadable with a cone shaped sealing surface 20 against the sealing seat 19 of the solid material outlet opening 19 using an actuator 22. The closure element 20 is thus preloaded by a compression spring 21 in a direction towards the sealing seat 19 of the solid material outlet opening 19 so that the solid material outlet opening 19 is closed gas tight and pressure tight by the closure element 20 in an idle position of the closure device 2 (
[0059] A compressor device 3 is arranged in the interior of the cylindrical sieve element 12 coaxial with the cylinder axis X. The compressor device 3 is provided as a compressor screw 30 and includes a screw shaft 32 that is drivable by a motor 31 wherein a screw helix 34 that is only stylized in the figures is arranged at an outer circumference of the screw shaft along an axial extension of the screw shaft and provided as a feed device. The radial outer edge 34 of the screw helix 34 is directly adjacent to the filter surface 13 and is provided with at least one scraping device 34 which contacts the filter surface 13 as illustrated in
[0060] The screw helix 34 forms a feed section of the compressor screw 30 with its upper portion oriented towards its inlet portion 10, wherein the feed section extends over a largest portion of an axial extension of the filter surface 13, thus approximately 75%-80% of the axial extension of the filter surface 18, and which then transitions into a compressor section 30. A pitch of the screw helix 34 is flatter in the compressor section 30 than in the feed section 30 so that an axial feed per revolution of the compression screw in the feed section 30 is greater than in the compressor section 30. The compressor screw 30 extends with its compressor section 30 beyond an end of the filter surface 13 oriented towards the outlet portion 10 into the cone shaped compression space 18 of the outlet portion 10. Thus, a radius of the screw helix 34 in the portion of the compressor section 30 is slightly reduced in order to be able to engage in the conically tapering outlet portion 10.
[0061] In a starting condition, thus when no suspension has been filled into the device the closure device 2 is closed as illustrated in
[0062] In this condition with a closed solid material output opening 19 the suspension U including a brew liquid including dissolved carbon monoxide and plant based aroma bearer solid material particles, wherein the suspension is also referred to as non filtrate, is continuously introduced through the suspension inlet 11 into the non-filtrate space 16 under a positive pressure relative to ambient atmosphere. This positive pressure can be measured in the suspension inlet 11 with a manometer 11. The suspension flows through the inlet portion 10 into the cylindrical center portion 10 to the circumferential wall 12 of the sieve element 12 that is provided with the sieve openings 12. At this location the brew liquid included in the suspension passes through the sieve opening 12 into the annular space 14 while the solid material particles P accumulate on the filter surface 13 at a radially inner side of the circumferential wall 12 of the sieve element 12. The brew liquid designated herein as filtrate F which has flowed through the filter surface 13 into an annular cavity 14 forming a filtrate space 17, is drained through the filtrate outlet 15 from the device 1 according to the invention towards a subsequent process step. A positive pressure relative to the ambient atmosphere is also provided in the filtrate outlet 15 wherein the positive pressure can be measured by a manometer 15.
[0063] The solid material particles P precipitating on the filter surface 13 are fed by the rotating compressor screw 30 to the outlet portion 10 of the housing 10. Thus, the scraping devices 34 clean the filter surface 13 and the screw helix 34 moves the solid material particles P with the feed section 30 of the compressor screw 30 along a feed portion 16 of the non-filtrate space 16 to a compression portion 16 of the non-filtrate space 16 proximal to the conically shaped outlet portion 10 where the compressor screw 30 includes the compressor section 30.
[0064] The lower pitch of the screw helix 34 in the portion of the compressor section 30 an axial feed of the fed solid material particles P is less than in the feed section 30 so that the solid material particles P in the compressor section 30 are pressed into a solid material cake, wherein the remaining brew liquid is pressed out of the solid material cake and flows through the filter surface 13 in outward direction into the filtrate space 17. The solid material particles P that are compressed into a solid material cake are compressed even further by a conically tapering profile of the outlet portion 10. This compressed solid material cake is pressed against the closure element 20 of the closure device 2 by a force of the rotating compressor screw 30 and displaces the closure element 20 against the force of the compression spring 21. The solid materials output opening 19 is thus opened and the solid material cake can exit from the device in an outward direction The strong compression of the solid material cake in the outlet portion 10 compresses the solid material cake into a solid gas tight mass which contacts an inner wall of the outlet portion 10 closely so that no positive pressure can exit from the device 1, in particular not from the non-filtrate space 15 through the open solid material output opening 19. Maintaining the positive pressure in the device 1 is thus also provided for an open closure device 2.
[0065] A variation of the device illustrated in
[0066] The cylindrical center portion 10 of the device 1 is provided with a second lower annular space 14 that is arranged below the annular space 14 forming the filtrate space 17 and sealed relative to the annular space 14. The circumferential wail 12 of the sieve element 12 that is provided with the sieve openings 12 thus extends in the axial direction over a length of the first annular space 14 and the second annular space 14 arranged thereunder. The compressor section 30 of the compressor screw 30 is enveloped by the second annular space 14. The first annular space 14 is provided with the filtrate outlet 15 already described in conjunction with
[0067] The screw shaft 32 in the variant of
[0068] There the washing liquid tube 40 is provided with radially arranged outlet openings 44 through which washing liquid can enter into the non-filtrate space 16 and thus into the solid material cake forming at this location shortly before its maximum compression as indicated by the arrows 46.
[0069] The washing entering the solid material cake that is also designated as filter cake displaces the brew liquid stored in the capillaries when the solid material cake is compressed and releases the brew liquid so that the brew liquid together with the optionally overdosed washing liquid can flow in the compression portion 16 through the portion of the sieve element 12 formed at this location into the second annular space 14. This mixture WF made from washing liquid and brew liquid is drained through the outlet 15 to a subsequent process step where the brew liquid can be separated from the washing liquid mixed therewith.
[0070]
[0071] Whereas in the embodiment of
[0072] The solid material outlet opening 119 of the outlet portion 110 in the embodiment according to
[0073] Furthermore a cleaning device 58 is provided in an upper portion of the solid material collecting container 52 wherein a cleaning fluid R is provided to the cleaning device through a cleaning fluid conduit 58 which is block able by a cut off valve 58 wherein the cleaning fluid can be introduced into the solid material collecting container 52. The volume of the solid material collecting container 52 is sized so that the solid material collecting container 52 can receive all solid materials which are precipitated in a pre-determined time period during continuous operation of the device 101 for precipitating solid material particles.
[0074] Before the device 101 according to the invention is started up compressed gas G is introduced through the compressed gas inlet 56 into the solid material collecting container 52 and thus also into an interior or the device 101, in particular into its non-filtrate space 116 and its filtrate space 117. The device 101 is thus preloaded relative to the atmosphere with a predetermined positive pressure which prevents that CO.sub.2 that is dissolved in the brew liquid suspension subsequently introduced through the suspension inlet 111 gases out.
[0075] After the continuous operation of the device 101 has been completed the outlet valve 54 of the solid material outlet opening 54 of the solid material collecting container 52 is opened and the cleaning fluid R is introduced through the cleaning fluid inlet 58 into the solid material collecting container 52. Thus, the solid material stored in the solid material collecting container 52 is washed out and the solid material collecting container 52 is emptied and cleaned.
[0076]
[0077] The device 1 illustrated in
[0078] The piston arrangement 6 includes a piston 60 which is connected with a co-axial and axially moveable piston rod 62 that is arranged in the sieve element 212. The piston rod 62 is supported axially moveable in an inlet portion 210 of the housing 210 and run out of the inlet portion 210 gas tight and pressure tight. A non illustrated drive of the piston rod is configured so that it can move the piston rod 62 with the piston 60 arranged thereon back and forth according to the double arrow H illustrated in
[0079] The piston is advantageously provided at its outer circumference with a piston ring shaped scraping device 61 (
[0080] In order for suspension U to be able to flow into a space in front of the piston (in
[0081] Solid material output is provided like in the embodiment of
[0082]
[0083] An inert gas conduit 74 is connected to the feed conduit 72 by a cut off valve 74. The filtrate outlet 15 of the device 1 according to the invention is connected with an outlet conduit 75 which leads to a downstream non-illustrated storage tank for the filtered brew liquid F and which is blockable by a cut off valve 75 Furthermore a cleaning outlet 76 that is lockable by a cut off valve 76 is connected to the outlet conduit 75.
[0084] Now before the non-filtrate U is provided to the device 1 according to the invention the valves 71, 75 and 76 are closed. Also the solid material outlet opening 19 of the device according to the invention as described in conjunction with
[0085] In analogy to filling and flushing the device 1 with inert gas the filling and flushing can be performed in the same manner by degassed water. The inflow of degassed water is then arranged behind the cut off valve 71 like the inert gas conduit 74 and the inert gas valve 74.
[0086] The positive pressure from the preloading with the inert gas I has the effect that the suspension U can exit into an environment, namely into the feed conduit 72 which has the same positive pressure after opening the cut off valve 71 at the outlet 71 of the storage container 70 which is also under the same positive pressure, so that a release of carbon dioxide from the brew liquid in the suspension does not occur and a foaming of the suspension is prevented. The suspension is then fed by the feed pump 73 through the feed conduit 72 to the suspension inlet 11 of the device 1 according to the invention and is processed there as is described supra so that the solid material particles are precipitated from the suspension and the essentially particle free brew liquid can be reclaimed wherein the brew liquid then flows through the filtrate outlet 15 and the outlet conduit 75 to the downstream storage tank.
[0087] The invention is not limited to the embodiment recited supra which only describes the core idea of the invention in broad strokes. Within the spirit and scope of the invention the device according to the invention can also have embodiments that differ from the embodiments described supra. Thus, the device can in particular have features which are a combination from the respective individual features of the claims.
[0088] Reference numerals in the claims, the description and in the drawing figures help to better understand the invention and do not limit the spirit and scope of the invention.
REFERENCE NUMERALS AND DESIGNATIONS
[0089] 1 device
[0090] 1 device
[0091] 2 closure device
[0092] 3 compressor device
[0093] 4 solid material washing arrangement
[0094] 5 solid material collecting device
[0095] 6 piston arrangement
[0096] 7 brewing plant
[0097] 10 housing
[0098] 10 inlet portion
[0099] 10 cylindrical center portion
[0100] 10 outlet portion
[0101] 11 suspension net
[0102] 11 manometer
[0103] 12 sieve element
[0104] 12 circumferential wall
[0105] 12 sieve openings
[0106] 13 filter surface
[0107] 14 outer wail
[0108] 14 first annular cavity
[0109] 14 second annular cavity
[0110] 15 filtrate outlet/washing liquid outlet
[0111] 15 manometer
[0112] 15 outlet
[0113] 16 non-filtrate space
[0114] 16 feed portion
[0115] 16 compression portion
[0116] 17 filtrate space
[0117] 18 closed wall
[0118] 18 compressor space
[0119] 19 solid material output opening
[0120] 19 sealing surface/sealing seat
[0121] 20 closure element
[0122] 20 cone shaped sealing surface
[0123] 21 compression spring
[0124] 22 actuator
[0125] 30 compressor screw
[0126] 30 feed section
[0127] 30 compressor section
[0128] 31 motor
[0129] 32 screw shaft
[0130] 34 screw helix
[0131] 34 radially outer edge
[0132] 34 scraping device
[0133] 40 washing liquid tube
[0134] 41 washing liquid annular space
[0135] 42 washing liquid inlet
[0136] 44 outlet openings
[0137] 46 arrow
[0138] 50 solid material output conduit
[0139] 52 solid material collecting container
[0140] 52 cover of solid material collecting container
[0141] 53 solid material feed opening
[0142] 54 closeable output opening/solid material output opening
[0143] 54 output valve
[0144] 55 valve
[0145] 56 compressed gas inlet
[0146] 57 manometer
[0147] 58 cleaning device/cleaning fluid inlet
[0148] 58 cleaning fluid conduit
[0149] 58 cut off valve
[0150] 60 piston
[0151] 60 face of piston 60
[0152] 61 scraping device
[0153] 62 piston rod
[0154] 66 bypass device
[0155] 66 bypass device
[0156] 67 bore hole
[0157] 67 bore hole
[0158] 68 valve flap
[0159] 68 valve Sap
[0160] 70 storage tank
[0161] 71 outlet of storage tank 70
[0162] 71 cutoff valve
[0163] 72 feed conduit
[0164] 73 feed pump
[0165] 74 inert gas conduit
[0166] 74 inert gas cutoff valve
[0167] 75 outlet conduit
[0168] 75 cutoff valve
[0169] 76 cleaning outlet
[0170] 76 cutoff valve
[0171] 101 device
[0172] 110 housing
[0173] 110 inlet portion
[0174] 110 cylindrical center portion
[0175] 110 outlet portion
[0176] 111 suspension inlet
[0177] 112 sieve element
[0178] 115 filtrate outlet
[0179] 116 non-filtrate outlet
[0180] 117 filtrate space
[0181] 119 solid material output opening
[0182] 203 compressor device
[0183] 210 housing
[0184] 210 inlet portion
[0185] 210 outlet portion
[0186] 212 sieve element
[0187] 212 circumferential wall
[0188] 212 sieve opening
[0189] 213 filter surface
[0190] 216 non-filtrate space
[0191] 216feed portion
[0192] 216 compression portion
[0193] 219 solid material output opening
[0194] 220 closure element
[0195] F filtrate
[0196] F filtrate space
[0197] G compressed gas
[0198] H double arrow
[0199] I inert gas
[0200] P solid material particles
[0201] R cleaning
[0202] U suspension
[0203] W washing liquid
[0204] WF mix of washing liquid and brew liquid
[0205] X cylinder axis