LIQUID-CRYSTAL MEDIUM
20250075129 ยท 2025-03-06
Assignee
Inventors
Cpc classification
C09K2019/3422
CHEMISTRY; METALLURGY
C09K2019/3027
CHEMISTRY; METALLURGY
C09K19/065
CHEMISTRY; METALLURGY
C09K19/3066
CHEMISTRY; METALLURGY
C09K19/3003
CHEMISTRY; METALLURGY
C09K2019/3408
CHEMISTRY; METALLURGY
C09K19/3098
CHEMISTRY; METALLURGY
C09K19/3028
CHEMISTRY; METALLURGY
C09K19/3405
CHEMISTRY; METALLURGY
International classification
Abstract
The invention relates to a liquid-crystalline medium, in particular based on a mixture of polar compounds, and to the use thereof for an active-matrix display, in particular based on the VA, SA-VA, IPS, PS-IPS, FFS, PS-FFS, UB-FFS or PS-UB-FFS effect.
Claims
1-11. (canceled)
12. A method for reducing white flicker, comprising bringing together into a composition one or more compounds of formula G with one or more compounds of formula B and/or C to form a liquid crystal (LC) medium having negative dielectric anisotropy, wherein the reduction of white flicker is achieved compared to an otherwise identical composition, but which does not include either (i) a compound of formula G or (ii) a compound of formula B and/or C ##STR00626## in which the individual radicals, on each occurrence identically or differently, and each, independently of one another, have the following meanings: ##STR00627## denotes ##STR00628## R.sup.0, R.sup.1, R.sup.2 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by ##STR00629## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen, L.sup.1, L.sup.2 denote F or Cl, X.sup.0 denotes F, Cl, CN, SF.sub.5, SCN, NCS, a halogenated alkyl radical, a halogenated alkenyl radical, a halogenated alkoxy radical or a halogenated alkenyloxy radical having 1 to 6 C atoms, Y.sup.1 denotes O, S or CH.sub.2O, and Z.sup.0 denotes a single bond, C.sub.2H.sub.4, CH.sub.2O, CF.sub.2O, or CHCH; and wherein the LC medium is not the following medium TABLE-US-00082 CCP-3-1 3.0% CCP-V-1 2.5% CLY-3-O2 8.0% CLY-4-O2 8.0% CLY-5-O2 7.0% CPY-3-O2 6.5% B(S)-2O-O4 4.0% B(S)-2O-O5 6.0% B(S)-2O-O6 3.0% CC-3-V1 8.0% CC-4-V1 20.0% CC-3-V 6.0% Y-4O-O4 10.0% CCG-V-F 8.0% 100.0%.
13. The method according to claim 12, which comprises adding the one or more compounds of formula G into a composition comprising the one or more compounds of formula B and/or C to form the liquid crystal (LC) medium having negative dielectric anisotropy, wherein the reduction of white flicker is achieved after the addition of the one or more compounds of formula G into said composition; and wherein the LC medium is not the following medium TABLE-US-00083 CCP-3-1 3.0% CCP-V-1 2.5% CLY-3-O2 8.0% CLY-4-O2 8.0% CLY-5-O2 7.0% CPY-3-O2 6.5% B(S)-2O-O4 4.0% B(S)-2O-O5 6.0% B(S)-2O-O6 3.0% CC-3-V1 8.0% CC-4-V1 20.0% CC-3-V 6.0% Y-4O-O4 10.0% CCG-V-F 8.0% 100.0%.
14. The method according to claim 12, which comprises adding the one or more compounds of formula B and/or C into a composition comprising the one or more compounds of formula G to form the liquid crystal (LC) medium having negative dielectric anisotropy, wherein the reduction of white flicker is achieved after the addition of the one or more compounds of formula B and/or C into said composition; and wherein the LC medium is not the following medium TABLE-US-00084 CCP-3-1 3.0% CCP-V-1 2.5% CLY-3-O2 8.0% CLY-4-O2 8.0% CLY-5-O2 7.0% CPY-3-O2 6.5% B(S)-2O-O4 4.0% B(S)-2O-O5 6.0% B(S)-2O-O6 3.0% CC-3-V1 8.0% CC-4-V1 20.0% CC-3-V 6.0% Y-4O-O4 10.0% CCG-V-F 8.0% 100.0%.
15. The method according to claim 12, wherein the compounds of formula B are selected from the following formulae ##STR00630## wherein R.sup.1 and R.sup.2 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by ##STR00631## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen.
16. The method according to claim 12, wherein the compounds of formula C are selected from the following formulae ##STR00632## wherein R.sup.1 and R.sup.2 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by ##STR00633## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen.
17. The method according to claim 12, wherein the compounds of formula G are selected from the following formulae ##STR00634## wherein R.sup.0 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by ##STR00635## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen.
18. The method according to claim 12, wherein the LC medium additionally comprises one or more compounds selected from formulae CY and PY: ##STR00636## in which the individual radicals have the following meanings: a denotes 1 or 2, b denotes 0 or 1, ##STR00637## denotes ##STR00638## R.sup.1 and R.sup.2 each, independently of one another, denote alkyl having 1 to 12 C atoms, in which one or two non-adjacent CH.sub.2 groups may be replaced by O, CHCH, CO, OCO or COO in such a way that O atoms are not linked directly to one another, Z.sup.x and Z.sup.y each, independently of one another, denotes CHCH, CH.sub.2O, OCH.sub.2, CF.sub.2O, OCF.sub.2, O, CH.sub.2, CH.sub.2CH.sub.2 or a single bond, L.sup.1-4 each, independently of one another, denote F, Cl, OCF.sub.3, CF.sub.3, CH.sub.3, CH.sub.2F, or CHF.sub.2, and L.sup.5 denotes H or CH.sub.3.
19. The method according to claim 12, wherein the LC medium additionally comprises one or more compounds selected from formula ZK and one or more compounds selected from formula DK ##STR00639## in which the individual radicals on each occurrence, identically or differently, have the following meanings: ##STR00640## denotes ##STR00641## ##STR00642## denotes ##STR00643## ##STR00644## denotes ##STR00645## and R.sup.3 and R.sup.4 each, independently of one another, denote alkyl having 1 to 12 C atoms, in which one or two non-adjacent CH.sub.2 groups may be replaced by O, CHCH, CO, OCO or COO in such a way that O atoms are not linked directly to one another, Z.sup.y denotes CH.sub.2CH.sub.2, CHCH, CF.sub.2O, OCF.sub.2, CH.sub.2O, OCH.sub.2, COO, OCO, C.sub.2F.sub.4, CFCF or a single bond, R.sup.5 and R.sup.6 each, independently of one another, denote alkyl having 1 to 12 C atoms, in which one or two non-adjacent CH.sub.2 groups may be replaced by O, CHCH, CO, OCO or COO in such a way that O atoms are not linked directly to one another, and e denotes 1 or 2.
20. The method according to claim 12, wherein the LC medium additionally comprises one or more compounds selected from the following formulae ##STR00646## in which alkyl and alkyl* each, independently of one another, denote a straight-chain alkyl radical having 1-6 C atoms, and alkenyl and alkenyl* each, independently of one another, denote a straight-chain alkenyl radical having 2-6 C atoms.
21. The method according to claim 12, wherein the LC medium additionally comprises s one or more compounds of the following formula ##STR00647## in which the individual radicals, on each occurrence identically or differently, and each, independently of one another, have the following meaning R.sup.1, R.sup.2 each, independently of one another, denote alkyl having 1 to 12 C atoms, in which one or two non-adjacent CH.sub.2 groups may be replaced by O, CHCH, CO, OCO or COO in such a way that O atoms are not linked directly to one another, and L.sup.T1-L.sup.T6 denote H, F or Cl, with at least one of L.sup.T1 to L.sup.T6 being F or Cl,
22. The method according to claim 12, wherein the LC medium comprises one or more compounds of formula Cl ##STR00648## wherein R.sup.1 and R.sup.2 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by ##STR00649## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen.
23. The method according to claim 12, wherein the LC medium additionally comprises one or more compounds of formula B ##STR00650## in which the individual radicals, on each occurrence identically or differently, and each, independently of one another, have the following meanings: R.sup.1, R.sup.2 denote a straight chain alkyl or alkoxy radical having 1 to 15 C atoms or a branched alkyl or alkoxy radical having 3 to 15 C atoms, in which one or more CH.sub.2 groups may each be replaced, independently of one another, by, ##STR00651## CC, CF.sub.2O, OCF.sub.2, CHCH, O, COO or OCO in such a way that O atoms are not linked directly to one another, and in which one or more H atoms may be replaced by halogen, L.sup.1, L.sup.2 denote F or Cl, and Y.sup.1 denotes O, S or CH.sub.2O.
24. The method according to claim 12, wherein the LC medium contains 2 to 20% by weight the one or more compounds of formula G.
25. The method according to claim 12, wherein the LC medium contains 4 to 10% by weight the one or more compounds of formula G.
26. The method according to claim 12, wherein the LC medium contains 2 to 20% by weight the one or more compounds of formula B.
27. The method according to claim 12, wherein the LC medium contains 7 to 14% by weight the one or more compounds of formula B.
28. The method according to claim 12, wherein the LC medium contains 2 to 20% by weight the one or more compounds of formula C.
29. The method according to claim 12, wherein the LC medium contains 8 to 12% by weight the one or more compounds of formula C.
30. The method according to claim 12, wherein the LC medium contains 4 to 10% by weight the one or more compounds of formula G and 7 to 14% by weight the one or more compounds of formula B and 8 to 12% by weight the one or more compounds of formula C.
Description
COMPARISON EXAMPLE 1.1
[0354] The nematic LC host mixture C11 is formulated as follows.
TABLE-US-00009 B(S)-2O-O4 2.00% cl. p. 74.0 B(S)-2O-O5 4.00% n 0.1092 CC-3-V 35.00% 3.4 CC-3-V1 3.00% .sub. 3.6 CCP-V-1 2.00% .sub.1 89 CCY-3-O2 7.50% K.sub.1 13.9 CPY-2-O2 6.50% K.sub.3 16.1 CPY-3-O2 18.00% V.sub.0 2.30 CY-3-O2 15.50% |PP-1-2V1 6.50%
COMPARISON EXAMPLE 1.2
[0355] The nematic LC host mixture C12 is formulated as follows.
TABLE-US-00010 B(S)-2O-O4 4.00% cl. p. 75.0 B(S)-2O-O5 4.00% n 0.1097 CC-3-V 40.00% 3.4 CCP-3F.F.F 3.00% .sub. 4.1 CPY-2-O2 18.50% .sub.1 89 CPY-3-O2 15.00% K.sub.1 13.1 CY-3-O2 14.50% K.sub.3 14.3 PP-1-2V1 2.00% V.sub.0 2.16
COMPARISON EXAMPLE 1.3
[0356] The nematic LC host mixture C13 is formulated as follows.
TABLE-US-00011 B(S)-2O-O4 4.00% cl. p. 74.0 B(S)-2O-O5 4.00% n 0.1093 CC-3-V 39.00% 3.5 CCP-3OCF.sub.3 3.50% .sub. 4.0 CPY-2-O2 18.00% .sub.1 87 CPY-3-O2 15.00% K.sub.1 13.2 CY-3-O2 14.50% K.sub.3 14.3 PP-1-2V1 2.00% V.sub.0 2.13
COMPARISON EXAMPLE 1.4
[0357] The nematic LC host mixture C14 is formulated as follows.
TABLE-US-00012 B(S)-2O-O4 4.00% cl. p. 74.5 B(S)-2O-O5 4.00% n 0.1099 CC-3-V 41.50% 3.5 DLGU-3-F 1.00% .sub. 4.0 CPY-2-O2 20.00% .sub.1 89 CPY-3-O2 15.00% K.sub.1 12.9 CY-3-O2 13.50% K.sub.3 14.3 PP-1-2V1 1.00% V.sub.0 2.12
EXAMPLE 1.1
[0358] The nematic LC host mixture N11 is formulated as follows.
TABLE-US-00013 B(S)-2O-O4 4.00% cl. p. 74.0 B(S)-2O-O5 4.00% cl. p. 0.1097 CC-3-V 34.50% n 3.5 CCP-V-1 1.50% 4.0 CCG-V-F 5.00% .sub. 89 CCY-3-O2 10.00% .sub.1 13.7 CPY-2-O2 10.00% K.sub.1 15.1 CPY-3-O2 10.00% K.sub.3 2.20 CY-3-O2 15.50% PP-1-2V1 5.50%
[0359] The mixture contains compound CCG-V-F of formula G.
EXAMPLE 1.2
[0360] The nematic LC host mixture N12 is formulated as follows.
TABLE-US-00014 B(S)-2O-O4 4.00% cl. p. 75.0 B(S)-2O-O5 4.00% cl. p. 0.1097 CC-3-V 37.50% n 3.5 CCG-3-F 5.00% 4.2 CPY-2-O2 20.00% .sub. 91 CPY-3-O2 13.50% .sub.1 13.0 CY-3-O2 14.50% K.sub.1 14.2 PP-1-2V1 1.50% K.sub.3 2.12
[0361] The mixture contains compound CCG-3-F of formula G.
EXAMPLE 1.3
[0362] The nematic LC host mixture N13 is formulated as follows.
TABLE-US-00015 B(S)-2O-O4 4.00% cl. p. 74.5 B(S)-2O-O5 4.00% cl. p. 0.1102 CC-3-V 37.00% n 3.5 CCQG-3-F 5.00% 4.1 CPY-2-O2 19.00% .sub. 92 CPY-3-O2 14.00% .sub.1 13.1 CY-3-O2 15.00% K.sub.1 14.2 PP-1-2V1 2.00% K.sub.3 2.11
[0363] The mixture contains compound CCQG-3-F of formula G.
COMPARISON EXAMPLE 2.1
[0364] The nematic LC host mixture C21 is formulated as follows.
TABLE-US-00016 B(S)-2O-O4 4.00% Clearing point [ C.]: 75.0 B(S)-2O-O5 4.00% n [589 nm, 20 C.]: 0.1249 B(S)-2O-O6 1.00% [1 kHz, 20 C.]: 2.2 CC-3-V 43.50% .sub. [1 kHz, 20 C.]: 3.3 CC-3-V1 7.50% .sub.1 [mPa s, 20 C.]: 71 CCP-V-1 1.75% K.sub.1 [pN, 20 C.]: 14.4 COB(S)-2-O4 6.00% K.sub.3 [pN, 20 C.]: 13.6 CPY-3-O2 6.25% V.sub.0 [V, 20 C.]: 2.65 PGIY-2-O4 6.00% PP-1-2V1 4.25% PYP-2-3 10.00% PYP-2-4 5.75%
EXAMPLE 2.1
[0365] The nematic LC host mixture N21 is formulated as follows.
TABLE-US-00017 B(S)-2O-O4 4.00% Clearing point [ C.]: 76.0 B(S)-2O-O5 4.00% n [589 nm, 20 C.]: 0.1248 B(S)-2O-O6 1.00% [1 kHz, 20 C.]: 2.1 CC-3-V 45.00% .sub. [1 kHz, 20 C.]: 3.7 CCG-V-F 5.50% .sub.1 [mPa s, 20 C.]: 73 CCP-V-1 1.00% K.sub.1 [pN, 20 C.]: 14.5 COB(S)-2-O4 6.00% K.sub.3 [pN, 20 C.]: 13.7 CPY-3-O2 10.00% V.sub.0 [V, 20 C.]: 2.72 PGIY-2-O4 6.00% LTS [bulk; 20 C.]: >1000 h PP-1-2V1 7.50% PYP-2-3 10.00%
The mixture contains compound CCG-V-F of formula G.
[0366] The mixtures N11 to N13 and N21 according to the present invention contain a positive polar compound of formula G having a terminal 3,4-difluorophenyl group. In contrast thereto, the reference mixtures C11 to C14 and C21 do not contain a compound of formula G. Instead these reference mixtures do either not contain any positive polar compound at all (C11, C21), or contain a positive polar compound CCP-3F.F.F or DLGU-3-F with a terminal 3,4,5-trifluorophenyl group (C12, C14), or a positive polar compound CCP-3OCF.sub.3 with a terminal 4-trifluoromethoxyphenyl group (C13).
White Flicker
[0367] The white flicker values of the above mixtures were measured at 25 C., 10 Hz in UB-FFS test cells. The flicker level was determined for voltages at grey levels 64, 127 and in the fully switched state V100 (corresponding to grey level 255).
[0368] Table 1 shows the results for mixtures C11 to C14 and N11 to N13, which were formulated to achieve the physical parameter target values cl.p.75 C., n0.11, 3.4.
TABLE-US-00018 TABLE 1 Mixture Positive polar Flicker at Flicker at Flicker at No. compound GL64 [%] GL127 [%] V100 [%] C11 None 2.9 1.6 3.8 C12 CCP-3F.F.F 3.0 2.0 3.6 C13 CCP-3OCF.sub.3 3.4 1.9 3.7 C14 DLGU-3-F 3.2 1.6 4.4 N11 CCG-V-F 2.7 1.5 2.6 N12 CCG-3-F 2.9 1.7 2.7 N13 CCQG-3-F 3.0 1.7 2.9
[0369] From Table 1 it can be seen that the mixtures N11 to N13 according to the present invention which contain a compound of formula G show significantly reduced flicker at V100, compared to the reference mixtures C11 to C14 which do not contain a compound of formula G.
[0370] Table 2 shows the results for the mixtures C21 and N21, which were formulated to achieve the physical parameter target values cl.p.75 C., n0.125, 2.2.
TABLE-US-00019 TABLE 2 Mixture Positive polar Flicker at Flicker at Flicker at No. compound GL64 [%] GL127 [%] V100 [%] C21 None 8.2 4.8 12.4 N21 CCG-V-F 6.3 3.3 8.2
[0371] From Table 2 it can be seen that the mixture N21 according to the present invention which contains a compound of formula G shows significantly reduced flicker at all grey levels, compared to the reference mixture C21 which does not contain a compound of formula G.
[0372] The results demonstrate that the use of compounds of formula B and/or C in combination with compounds of formula G in dielectrically negative LC mixtures allows to reduce the flicker level while maintaining low viscosities and thus enabling short response times.
EXAMPLE 3
TABLE-US-00020 B(S)-2O-O4 4.0% Clearing point [ C.]: 75 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1098 CC-3-V 34.5% .sub. [1 kHz, 20 C.]: 4.1 CCP-V-1 1.5% .sub. [1 kHz, 20 C.]: 7.5 CCG-4-OT 4.0% [1 kHz, 20 C.]: 3.4 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 14.0 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 14.9 CPY-3-O2 10.5% V.sub.0 [V, 20 C.]: 2.19 CY-3-O2 16.0% .sub.1 [mPa s, 20 C.]: 91 PP-1-2V1 5.5% 100.0%
EXAMPLE 4
TABLE-US-00021 B(S)-2O-O4 4.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1103 CC-3-V 35.5% .sub. [1 kHz, 20 C.]: 4.2 CCP-V-1 1.0% .sub. [1 kHz, 20 C.]: 7.6 BCH-30CF3.F 4.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 13.7 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 14.9 CPY-3-O2 11.0% V.sub.0 [V, 20 C.]: 2.19 CY-3-O2 16.5% .sub.1 [mPa s, 20 C.]: 90 PP-1-2V1 4.0% 100.0%
EXAMPLE 5
TABLE-US-00022 B(S)-2O-O4 4.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1101 CC-3-V 34.5% .sub. [1 kHz, 20 C.]: 4.0 CCP-V-1 1.5% .sub. [1 kHz, 20 C.]: 7.6 CCG-V-OT 4.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 13.9 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 14.9 CPY-3-O2 10.5% V.sub.0 [V, 20 C.]: 2.17 CY-3-O2 16.0% .sub.1 [mPa s, 20 C.]: 90 PP-1-2V1 5.5% 100.0%
EXAMPLE 6
TABLE-US-00023 B(S)-2O-O4 4.0% Clearing point [ C.]: 75 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1091 CC-3-V 35.5% .sub. [1 kHz, 20 C.]: 4.1 CCP-V-1 1.0% .sub. [1 kHz, 20 C.]: 7.6 CLG-3-OT 4.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 14.0 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 15.0 CPY-3-O2 11.0% V.sub.0 [V, 20 C.]: 2.18 CY-3-O2 16.5% .sub.1 [mPa s, 20 C.]: 92 PP-1-2V1 4.0% LTS [bulk; 20 C.]: >1000 h 100.0%
EXAMPLE 7
TABLE-US-00024 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1105 CC-3-V 34.0% .sub. [1 kHz, 20 C.]: 4.2 CCP-V-1 2.0% .sub. [1 kHz, 20 C.]: 7.7 CCG-V-T 4.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 14.1 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 15.1 CPY-3-O2 11.0% V.sub.0 [V, 20 C.]: 2.18 CY-3-O2 16.5% .sub.1 [mPa s, 20 C.]: 95 PP-1-2V1 4.5% 100.0%
EXAMPLE 8
TABLE-US-00025 CC-3-V 34.0% Clearing point [ C.]: 82.9 CY-3-O2 14.0% n [589 nm, 20 C.]: CCY-3-O1 5.0% .sub. [1 kHz, 20 C.]: 4.0 CCY-3-O2 6.0% .sub. [1 kHz, 20 C.]: 8.3 CLY-3-O2 7.0% [1 kHz, 20 C.]: 4.4 CPY-2-O2 8.0% K.sub.1 [pN, 20 C.]: 14.4 CPY-3-O2 8.0% K.sub.3 [pN, 20 C.]: 15.7 PGIY-2-O4 2.0% V.sub.0 [V, 20 C.]: 2.01 PYP-2-3 4.0% .sub.1 [mPa s, 20 C.]: 111 B(S)-2O-O4 5.0% .sub.1 [mPa s, 20 C.]: B(S)-2O-O5 4.0% LTS bulk [h, 10 C.]: CCG-V-F 3.0% LTS bulk [h, 20 C.]: 100.0% LTS bulk [h, 30 C.]:
EXAMPLE 9
TABLE-US-00026 B(S)-2O-O4 3.0% Clearing point [ C.]: 80.5 B(S)-2O-O5 3.0% n [589 nm, 20 C.]: 0.1052 CC-3-V 37.5% .sub. [1 kHz, 20 C.]: 3.9 CCG-V-F 3.0% .sub. [1 kHz, 20 C.]: 7.8 CCY-3-O1 3.5% [1 kHz, 20 C.]: 3.9 CCY-3-O2 4.0% K.sub.1 [pN, 20 C.]: 14.5 CCY-4-O2 2.0% K.sub.3 [pN, 20 C.]: 15.0 CLY-2-O4 5.0% V.sub.0 [V, 20 C.]: 2.07 CLY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 102 CLY-3-O3 6.0% CLY-4-O2 5.0% CY-3-O2 6.0% PGIY-2-O4 4.0% PY-1-O2 9.0% PYP-2-3 2.0% 100.0%
EXAMPLE 10
TABLE-US-00027 B(S)-2O-O4 4.0% Clearing point [ C.]: 80.6 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1043 CC-3-V 35.0% .sub. [1 kHz, 20 C.]: 4.1 CCG-V-F 5.0% .sub. [1 kHz, 20 C.]: 8.1 CCY-3-O1 3.5% [1 kHz, 20 C.]: 4.0 CCY-3-O2 4.0% K.sub.1 [pN, 20 C.]: 14.6 CCY-4-O2 2.0% K.sub.3 [pN, 20 C.]: 14.8 CLY-2-O4 5.0% V.sub.0 [V, 20 C.]: 2.02 CLY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 105 CLY-3-O3 6.0% CLY-4-O2 5.0% CY-3-O2 7.0% PGIY-2-O4 2.0% PY-3-O2 9.0% PYP-2-3 1.5% 100.0%
EXAMPLE 11
TABLE-US-00028 CC-3-V 32.0% Clearing point [ C.]: 81.6 CC-3-V1 5.0% n [589 nm, 20 C.]: 0.1086 CY-3-O2 15.0% .sub. [1 kHz, 20 C.]: 4.0 CCY-3-O1 2.0% .sub. [1 kHz, 20 C.]: 8.5 CCY-3-O2 8.0% [1 kHz, 20 C.]: 4.5 CLY-3-O2 8.0% K.sub.1 [pN, 20 C.]: 14.9 CPY-3-O2 10.0% K.sub.3 [pN, 20 C.]: 16.4 PGIY-2-O4 6.0% V.sub.0 [V, 20 C.]: 2.02 B(S)-2O-O4 4.0% .sub.1 [mPa s, 20 C.]: 112 B(S)-2O-O5 4.0% B(S)-2O-O6 3.0% CCG-V-F 3.0% 100.0%
EXAMPLE 12
TABLE-US-00029 B(S)-2O-O4 3.0% Clearing point [ C.]: 80.7 B(S)-2O-O5 3.0% n [589 nm, 20 C.]: 0.1050 CC-3-V 37.0% .sub. [1 kHz, 20 C.]: 3.9 CCG-V-F 2.0% .sub. [1 kHz, 20 C.]: 7.9 CCY-3-O1 3.5% [1 kHz, 20 C.]: 4.0 CCY-3-O2 4.0% K.sub.1 [pN, 20 C.]: 14.6 CCY-4-O2 2.0% K.sub.3 [pN, 20 C.]: 14.6 CLY-2-O4 5.0% V.sub.0 [V, 20 C.]: 2.03 CLY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 100 CLY-3-O3 6.0% CLY-4-O2 5.0% CY-3-O2 7.0% PGIY-2-O4 4.0% PY-2-O2 3.5% PY-3-O2 5.0% PYP-2-3 2.0% LB(S)-3-OT 1.0% 100.0%
EXAMPLE 13
TABLE-US-00030 CCY-3-O1 4.0% Clearing point [ C.]: 81.9 CCY-3-O2 4.0% n [589 nm, 20 C.]: 0.1047 CCY-4-O2 4.0% .sub. [1 kHz, 20 C.]: 4.0 CLY-2-O4 4.0% .sub. [1 kHz, 20 C.]: 7.9 CLY-4-O2 4.0% [1 kHz, 20 C.]: 3.9 CLY-3-O2 6.0% K.sub.1 [pN, 20 C.]: 14.7 CLY-3-O3 6.0% K.sub.3 [pN, 20 C.]: 14.9 PGIY-2-O4 4.5% V.sub.0 [V, 20 C.]: 2.06 CC-3-V 36.0% .sub.1 [mPa s, 20 C.]: 104 CY-3-O2 8.5% PY-3-O2 7.0% B(S)-2O-O4 3.0% B(S)-2O-O5 3.0% CCG-V-F 3.0% LB(S)-3-OT 1.0% PYP-2-3 2.0% 100.0%
EXAMPLE 14
TABLE-US-00031 B(S)-2O-O4 4.0% Clearing point [ C.]: 73.2 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1040 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.8 CC-3-V 46.0% .sub. [1 kHz, 20 C.]: 6.7 CC-3-V1 3.0% [1 kHz, 20 C.]: 2.9 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 13.5 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.0 CLY-5-O2 4.0% V.sub.0 [V, 20 C.]: 2.32 CPY-2-O2 5.0% .sub.1 [mPa s, 20 C.]: 72 CPY-3-O2 10.0% PY-3-O2 10.0% 100.0%
EXAMPLE 15
TABLE-US-00032 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.4 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1045 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 46.5% .sub. [1 kHz, 20 C.]: 7.0 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.1 CLY-3-O2 9.0% K.sub.1 [pN, 20 C.]: 14.2 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.3 CLY-5-O2 1.5% V.sub.0 [V, 20 C.]: 2.24 CPY-2-O2 1.5% .sub.1 [mPa s, 20 C.]: 74 CPY-3-O2 8.0% PY-3-O2 11.5% 100.0%
EXAMPLE 16
TABLE-US-00033 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.2 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1053 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.7 CC-3-V 51.0% .sub. [1 kHz, 20 C.]: 6.8 CCG-V-F 3.0% [1 kHz, 20 C.]: 3.1 CLY-3-O2 8.0% K.sub.1 [pN, 20 C.]: 13.8 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.2 CPY-2-O2 1.5% V.sub.0 [V, 20 C.]: 2.28 CPY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 72 PGIY-2-O4 5.0% PY-1-O2 7.5% 100.0%
EXAMPLE 17
TABLE-US-00034 B(S)-2O-O4 4.0% Clearing point [ C.]: 73.9 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1054 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 48.5% .sub. [1 kHz, 20 C.]: 6.9 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.0 CLY-3-O2 8.0% K.sub.1 [pN, 20 C.]: 13.9 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.3 CPY-2-O2 2.0% V.sub.0 [V, 20 C.]: 2.28 CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 18
TABLE-US-00035 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.3 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1050 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.1 CC-3-V 46.0% .sub. [1 kHz, 20 C.]: 7.1 CCG-V-F 7.0% [1 kHz, 20 C.]: 3.0 CLY-3-O2 8.0% K.sub.1 [pN, 20 C.]: 13.8 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.2 CPY-2-O2 3.5% V.sub.0 [V, 20 C.]: 2.28 CPY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 73 PY-1-O2 7.0% PY-3-O2 3.5% 100.0%
EXAMPLE 19
TABLE-US-00036 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.9 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1098 B(S)-2O-O6 3.0% .sub. [1 kHz, 20 C.]: 3.8 BCH-32 3.5% .sub. [1 kHz, 20 C.]: 6.5 CC-3-V 48.5% [1 kHz, 20 C.]: 2.6 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 13.5 CLY-3-O2 8.0% K.sub.3 [pN, 20 C.]: 14.3 CPY-3-O2 10.0% V.sub.0 [V, 20 C.]: 2.45 PGIY-2-O4 6.0% PY-1-O2 8.0% 100.0%
EXAMPLE 20
TABLE-US-00037 B(S)-2O-O4 4.0% Clearing point [ C.]: 76.3 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1291 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.0 BCH-32 2.0% .sub. [1 kHz, 20 C.]: 7.0 CC-3-V 40.5% [1 kHz, 20 C.]: 3.0 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 14.1 CLY-3-O2 5.5% K.sub.3 [pN, 20 C.]: 14.0 CPY-3-O2 10.0% V.sub.0 [V, 20 C.]: 2.27 PGIY-2-O4 5.0% PY-1-O2 8.0% PYP-2-3 10.0% PYP-2-4 2.0% 100.0% LTS bulk [h, 30 C.]:
EXAMPLE 21
TABLE-US-00038 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.2 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1494 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.1 BCH-32 3.5% .sub. [1 kHz, 20 C.]: 7.0 CC-3-V 28.5% [1 kHz, 20 C.]: 3.0 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 14.5 CCP-V-1 1.5% K.sub.3 [pN, 20 C.]: 14.0 CPY-2-O2 4.5% V.sub.0 [V, 20 C.]: 2.29 CPY-3-O2 10.0% .sub.1 [mPa s, 20 C.]: 100 PGIY-2-O4 5.0% PP-1-2V1 8.0% PY-1-O2 8.0% PYP-2-3 7.0% PYP-2-4 7.0% 100.0%
EXAMPLE 22
TABLE-US-00039 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.2 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1495 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.3 BCH-32 3.0% .sub. [1 kHz, 20 C.]: 7.2 CC-3-V 23.0% [1 kHz, 20 C.]: 3.0 CCG-V-F 7.0% K.sub.1 [pN, 20 C.]: 14.7 CCP-V-1 6.5% K.sub.3 [pN, 20 C.]: 14.7 CPY-2-O2 3.0% V.sub.0 [V, 20 C.]: 2.34 CPY-3-O2 10.0% .sub.1 [mPa s, 20 C.]: 101 PGIY-2-O4 5.0% .sub.1 [mPa s, 20 C.]: PP-1-2V1 10.0% LTS bulk [h, 10 C.]: PY-1-O2 10.0% LTS bulk [h, 20 C.]: PY-3-O2 1.5% LTS bulk [h, 30 C.]: PYP-2-3 7.0% PYP-2-4 2.0% 100.0%
EXAMPLE 23
TABLE-US-00040 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.7 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1507 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.4 BCH-32 6.5% .sub. [1 kHz, 20 C.]: 7.4 CC-3-V 24.0% [1 kHz, 20 C.]: 2.9 CCG-V-F 9.0% K.sub.1 [pN, 20 C.]: 14.7 CPY-2-O2 5.5% K.sub.3 [pN, 20 C.]: 14.2 CPY-3-O2 9.5% V.sub.0 [V, 20 C.]: 2.31 PGIY-2-O4 5.0% .sub.1 [mPa s, 20 C.]: 104 PP-1-2V1 9.0% PY-1-O2 9.0% PY-3-O2 2.0% PYP-2-3 7.0% PYP-2-4 1.5% 100.0%
EXAMPLE 24
TABLE-US-00041 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.1 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1048 B(S)-2O-O6 3.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 44.5% .sub. [1 kHz, 20 C.]: 7.4 CCG-V-F 3.0% [1 kHz, 20 C.]: 3.5 CLY-2-O4 1.0% K.sub.1 [pN, 20 C.]: 14.0 CLY-3-O2 6.0% K.sub.3 [pN, 20 C.]: 13.8 CLY-3-O3 2.0% V.sub.0 [V, 20 C.]: 2.09 CLY-4-O2 3.0% .sub.1 [mPa s, 20 C.]: 81 CPY-2-O2 1.5% CPY-3-O2 9.5% CY-3-O2 10.5% CY-5-O2 1.0% PGIY-2-O4 7.0% 100.0%
EXAMPLE 25
TABLE-US-00042 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.3 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1019 B(S)-2O-O6 3.5% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 44.5% .sub. [1 kHz, 20 C.]: 7.4 CCG-V-F 4.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 7.0% K.sub.1 [pN, 20 C.]: 13.8 CLY-3-O3 5.0% K.sub.3 [pN, 20 C.]: 13.9 CLY-4-O2 4.0% V.sub.0 [V, 20 C.]: 2.10 CPY-3-O2 5.5% .sub.1 [mPa s, 20 C.]: 80 CY-3-O2 10.5% CY-5-O2 1.0% PGIY-2-O4 7.0% 100.0%
EXAMPLE 26
TABLE-US-00043 CCP-3-1 3.0% Clearing point [ C.]: 88.5 CCP-V-1 2.5% n [589 nm, 20 C.]: 0.1061 CLY-3-O2 8.0% .sub. [1 kHz, 20 C.]: 4.3 CLY-4-O2 8.0% .sub. [1 kHz, 20 C.]: 8.4 CLY-5-O2 7.0% [1 kHz, 20 C.]: 4.1 CPY-3-O2 6.5% K.sub.1 [pN, 20 C.]: 17.4 B(S)-2O-O4 4.0% K.sub.3 [pN, 20 C.]: 15.9 B(S)-2O-O5 6.0% V.sub.0 [V, 20 C.]: 2.08 B(S)-2O-O6 3.0% .sub.1 [mPa s, 20 C.]: 115 CC-3-V1 8.0% CC-4-V1 20.0% CC-3-V 6.0% Y-4O-O4 10.0% CCG-V-F 8.0% 100.0%
EXAMPLE 27
TABLE-US-00044 B(S)-2O-O4 2.0% Clearing point [ C.]: 61 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1071 CC-3-V 28.0% .sub. [1 kHz, 20 C.]: 4.6 CLY-3-O2 0.5% .sub. [1 kHz, 20 C.]: 7.8 CPY-2-O2 12.0% [1 kHz, 20 C.]: 3.3 CPY-3-O2 12.0% K.sub.1 [pN, 20 C.]: 11.2 CY-3-O2 25.0% K.sub.3 [pN, 20 C.]: 12.6 PP-1-2V1 6.5% V.sub.0 [V, 20 C.]: 2.07 CCG-V-F 10.0% .sub.1 [mPa s, 20 C.]: 81 100.0%
EXAMPLE 28
TABLE-US-00045 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1090 CC-3-V 34.5% .sub. [1 kHz, 20 C.]: 4.0 CCG-V-F 5.0% .sub. [1 kHz, 20 C.]: 7.4 CLY-3-O2 9.0% [1 kHz, 20 C.]: 3.5 CPY-2-O2 12.0% K.sub.1 [pN, 20 C.]: 13.5 CPY-3-O2 12.0% K.sub.3 [pN, 20 C.]: 15.0 CY-3-O2 16.5% V.sub.0 [V, 20 C.]: 2.20 PP-1-2V1 5.0% .sub.1 [mPa s, 20 C.]: 91 100.0% .sub.1 [mPa s, 20 C.]:
EXAMPLE 29
TABLE-US-00046 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1096 CC-3-V 36.0% .sub. [1 kHz, 20 C.]: 3.8 CCG-V-F 2.5% .sub. [1 kHz, 20 C.]: 7.2 CCP-V-1 1.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 9.0% K.sub.1 [pN, 20 C.]: 13.6 CPY-2-O2 12.0% K.sub.3 [pN, 20 C.]: 15.1 CPY-3-O2 12.0% V.sub.0 [V, 20 C.]: 2.20 CY-3-O2 16.0% .sub.1 [mPa s, 20 C.]: 90 PP-1-2V1 5.5% 100.0%
EXAMPLE 30
TABLE-US-00047 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1098 CC-3-V 37.0% .sub. [1 kHz, 20 C.]: 3.7 CCG-V-F 1.0% .sub. [1 kHz, 20 C.]: 7.1 CCP-V-1 2.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 9.0% K.sub.1 [pN, 20 C.]: 13.8 CPY-2-O2 12.0% K.sub.3 [pN, 20 C.]: 15.3 CPY-3-O2 12.0% V.sub.0 [V, 20 C.]: 2.21 CY-3-O2 15.5% .sub.1 [mPa s, 20 C.]: 89 PP-1-2V1 5.5% 100.0%
EXAMPLE 31
TABLE-US-00048 B(S)-2O-O4 4.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1097 CC-3-V 34.5% .sub. [1 kHz, 20 C.]: 4.0 CCP-V-1 1.5% .sub. [1 kHz, 20 C.]: 7.4 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 13.7 CPY-2-O2 10.0% K.sub.3 [pN, 20 C.]: 15.0 CPY-3-O2 10.0% V.sub.0 [V, 20 C.]: 2.20 CY-3-O2 15.5% .sub.1 [mPa s, 20 C.]: 89 PP-1-2V1 5.5% 100.0%
EXAMPLE 32
TABLE-US-00049 B(S)-2O-O4 4.0% Clearing point [ C.]: 76 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1248 B(S)-2O-O6 1.0% .sub. [1 kHz, 20 C.]: 3.7 CC-3-V 45.0% .sub. [1 kHz, 20 C.]: 5.8 CCG-V-F 5.5% [1 kHz, 20 C.]: 2.1 CCP-V-1 1.0% K.sub.1 [pN, 20 C.]: 14.5 COB(S)-2-O4 6.0% K.sub.3 [pN, 20 C.]: 13.7 CPY-3-O2 10.0% V.sub.0 [V, 20 C.]: 2.72 PGIY-2-O4 6.0% .sub.1 [mPa s, 20 C.]: 73 PP-1-2V1 7.5% LTS bulk [h, 20 C.]: >1000 PYP-2-3 10.0% 100.0%
EXAMPLE 33
TABLE-US-00050 B(S)-2O-O4 4.0% Clearing point [ C.]: 76 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1099 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 40.0% .sub. [1 kHz, 20 C.]: 7.3 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.4 CLY-3-O2 9.0% K.sub.1 [pN, 20 C.]: 14.2 CPY-2-O2 7.5% K.sub.3 [pN, 20 C.]: 15.1 CPY-3-O2 12.0% V.sub.0 [V, 20 C.]: 2.23 CY-3-O2 10.0% .sub.1 [mPa s, 20 C.]: 84 PP-1-2V1 4.5% 100.0%
EXAMPLE 34
TABLE-US-00051 B(S)-2O-O4 4.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1098 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.1 CC-3-V 37.0% .sub. [1 kHz, 20 C.]: 7.4 CCG-V-F 6.5% [1 kHz, 20 C.]: 3.4 CLY-3-O2 12.0% K.sub.1 [pN, 20 C.]: 14.1 CPY-2-O2 5.5% K.sub.3 [pN, 20 C.]: 15.1 CPY-3-O2 9.0% V.sub.0 [V, 20 C.]: 2.23 CY-3-O2 12.0% .sub.1 [mPa s, 20 C.]: 85 PP-1-2V1 6.0% 100.0%
EXAMPLE 35
TABLE-US-00052 B(S)-2O-O4 4.0% Clearing point [ C.]: 75 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1095 CC-3-V 18.0% .sub. [1 kHz, 20 C.]: 4.0 CC-V-V1 21.5% .sub. [1 kHz, 20 C.]: 7.5 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.5 CLY-3-O2 6.5% K.sub.1 [pN, 20 C.]: 12.9 CPY-2-O2 14.5% K.sub.3 [pN, 20 C.]: 15.3 CPY-3-O2 9.5% V.sub.0 [V, 20 C.]: 2.22 CY-3-O2 15.0% .sub.1 [mPa s, 20 C.]: 87 PP-1-2V1 2.0% 100.0%
EXAMPLE 36
TABLE-US-00053 B(S)-2O-O4 4.0% Clearing point [ C.]: 75 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1095 CC-3-V 17.5% .sub. [1 kHz, 20 C.]: 4.0 CC-V-V1 22.5% .sub. [1 kHz, 20 C.]: 7.5 CCG-V-F 4.5% [1 kHz, 20 C.]: 3.5 CLY-3-O2 6.0% K.sub.1 [pN, 20 C.]: 13.2 CPY-2-O2 7.5% K.sub.3 [pN, 20 C.]: 15.9 CPY-3-O2 16.0% V.sub.0 [V, 20 C.]: 2.25 CY-3-O2 16.0% .sub.1 [mPa s, 20 C.]: 88 PP-1-2V1 2.0% 100.0%
EXAMPLE 37
TABLE-US-00054 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1093 CC-3-V 32.5% .sub. [1 kHz, 20 C.]: 4.2 CCG-V-F 7.5% .sub. [1 kHz, 20 C.]: 7.6 CLY-3-O2 7.0% [1 kHz, 20 C.]: 3.4 CPY-2-O2 7.5% K.sub.1 [pN, 20 C.]: 13.3 CPY-3-O2 17.0% K.sub.3 [pN, 20 C.]: 15.1 CY-3-O2 18.0% V.sub.0 [V, 20 C.]: 2.23 PP-1-2V1 4.5% .sub.1 [mPa s, 20 C.]: 94 100.0% .sub.1 [mPa s, 20 C.]:
EXAMPLE 38
TABLE-US-00055 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1091 CC-3-V 32.5% .sub. [1 kHz, 20 C.]: 4.3 CCG-V-F 8.5% .sub. [1 kHz, 20 C.]: 7.7 CLY-3-O2 2.5% [1 kHz, 20 C.]: 3.4 CPY-2-O2 11.0% K.sub.1 [pN, 20 C.]: 12.8 CPY-3-O2 18.5% K.sub.3 [pN, 20 C.]: 14.5 CY-3-O2 18.5% V.sub.0 [V, 20 C.]: 2.17 PP-1-2V1 2.5% .sub.1 [mPa s, 20 C.]: 95 100.0%
EXAMPLE 39
TABLE-US-00056 B(S)-2O-O4 2.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1093 CC-3-V 29.5% .sub. [1 kHz, 20 C.]: 4.4 CCG-V-F 10.0% .sub. [1 kHz, 20 C.]: 7.8 CLY-3-O2 7.5% [1 kHz, 20 C.]: 3.4 CPY-2-O2 2.5% K.sub.1 [pN, 20 C.]: 13.2 CPY-3-O2 20.0% K.sub.3 [pN, 20 C.]: 15.5 CY-3-O2 20.0% V.sub.0 [V, 20 C.]: 2.25 PP-1-2V1 4.5% 100.0%
EXAMPLE 40
TABLE-US-00057 B(S)-2O-O4 4.0% Clearing point [ C.]: 75 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1248 B(S)-2O-O6 1.0% .sub. [1 kHz, 20 C.]: 4.1 CC-3-V 38.5% .sub. [1 kHz, 20 C.]: 7.1 CC-3-V1 5.0% [1 kHz, 20 C.]: 3.0 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 14.2 CCP-V-1 3.0% K.sub.3 [pN, 20 C.]: 12.9 COB(S)-2-O4 6.0% V.sub.0 [V, 20 C.]: 2.20 CPY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 81 PGIY-2-O4 12.0% PY-2-O2 7.5% PYP-2-3 2.0% PYP-2-4 5.0% 100.0%
EXAMPLE 41
TABLE-US-00058 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1249 B(S)-2O-O6 1.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 44.5% .sub. [1 kHz, 20 C.]: 6.8 CCG-V-F 5.0% [1 kHz, 20 C.]: 2.9 COB(S)-2-O4 6.0% K.sub.1 [pN, 20 C.]: 13.7 CPY-3-O2 12.0% K.sub.3 [pN, 20 C.]: 13.3 PGIY-2-O4 6.0% V.sub.0 [V, 20 C.]: 2.26 PY-3-O2 7.0% .sub.1 [mPa s, 20 C.]: 80 PYP-2-3 10.5% 100.0%
EXAMPLE 42
TABLE-US-00059 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1094 CC-3-V 2.5% .sub. [1 kHz, 20 C.]: 4.0 CC-V-V1 40.0% .sub. [1 kHz, 20 C.]: 7.4 CCG-V-F 5.0% [1 kHz, 20 C.]: 3.4 CLY-3-O2 5.5% K.sub.1 [pN, 20 C.]: 12.5 CPY-2-O2 19.0% K.sub.3 [pN, 20 C.]: 15.6 CPY-3-O2 5.0% V.sub.0 [V, 20 C.]: 2.25 CY-3-O2 15.0% .sub.1 [mPa s, 20 C.]: 85 100.0% .sub.1 [mPa s, 20 C.]:
EXAMPLE 43
TABLE-US-00060 B(S)-2O-O4 4.0% Clearing point [ C.]: 75.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1092 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 4.0 CC-3-V 5.5% .sub. [1 kHz, 20 C.]: 7.3 CC-V-V1 40.5% [1 kHz, 20 C.]: 3.3 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 12.8 CLY-3-O2 5.5% K.sub.3 [pN, 20 C.]: 15.7 CPY-2-O2 14.0% V.sub.0 [V, 20 C.]: 2.29 CPY-3-O2 6.0% .sub.1 [mPa s, 20 C.]: 79 CY-3-O2 11.5% 100.0%
EXAMPLE 44
TABLE-US-00061 B(S)-2O-O4 4.0% Clearing point [ C.]: 94.9 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1047 CC-3-V 39.0% .sub. [1 kHz, 20 C.]: 3.4 CC-3-V1 7.0% .sub. [1 kHz, 20 C.]: 6.3 CCP-3-1 3.0% [1 kHz, 20 C.]: 2.9 CLY-3-O2 6.0% K.sub.1 [pN, 20 C.]: 17.4 CLY-3-O3 6.0% K.sub.3 [pN, 20 C.]: 17.8 CLY-4-O2 6.0% V.sub.0 [V, 20 C.]: 2.62 CLY-5-O2 4.0% .sub.1 [mPa s, 20 C.]: 103 CPY-3-O2 10.0% CY-3-O2 3.0% PGIY-2-O4 4.0% PYP-2-3 1.0% CCG-V-F 3.0% 100.0%
EXAMPLE 45
[0373] Mixture according to Example 44 is stabilized with 0.04% of the compound of formula
##STR00605##
EXAMPLE 46
TABLE-US-00062 CLY-3-O2 6.0% Clearing point [ C.]: 74.8 CLY-3-O3 6.0% n [589 nm, 20 C.]: 0.1023 CLY-4-O2 4.0% .sub. [1 kHz, 20 C.]: 3.9 CY-3-O2 11.5% .sub. [1 kHz, 20 C.]: 7.3 CPY-3-O2 5.5% [1 kHz, 20 C.]: 3.4 B(S)-2O-O4 4.0% K.sub.1 [pN, 20 C.]: 13.7 B(S)-2O-O5 4.0% K.sub.3 [pN, 20 C.]: 13.9 B(S)-2O-O6 3.5% V.sub.0 [V, 20 C.]: 2.10 PGIY-2-O4 7.0% .sub.1 [mPa s, 20 C.]: 81 CC-3-V 44.5% CCG-V-F 4.0% 100.0%
EXAMPLE 47
[0374] Mixture according to Example 48 is stabilized with 0.04% of the compound of formula
##STR00606##
EXAMPLE 48
TABLE-US-00063 CLY-3-O2 6.0% Clearing point [ C.]: 75 CLY-3-O3 2.0% n [589 nm, 20 C.]: 0.1047 CLY-4-O2 4.0% .sub. [1 kHz, 20 C.]: 3.8 CY-3-O2 11.5% .sub. [1 kHz, 20 C.]: 7.3 CPY-2-O2 2.0% [1 kHz, 20 C.]: 3.5 CPY-3-O2 9.0% K.sub.1 [pN, 20 C.]: 13.6 B(S)-2O-O4 4.0% K.sub.3 [pN, 20 C.]: 14.0 B(S)-2O-O5 4.0% V.sub.0 [V, 20 C.]: 2.09 B(S)-2O-O6 3.0% .sub.1 [mPa s, 20 C.]: 80 PGIY-2-O4 7.0% CC-3-V 44.5% CCG-V-F 3.0% 100.0%
EXAMPLE 49
[0375] Mixture according to Example 48 is stabilized with 0.04% of the compound of formula
##STR00607##
EXAMPLE 50
TABLE-US-00064 B(S)-5Cy-O2 4.0% Clearing point [ C.]: 73.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1045 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 3.0 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.9 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.2 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 74 CLY-4-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 51
TABLE-US-00065 B(S)-5Cy-O4 4.0% Clearing point [ C.]: 73.0 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1042 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 2.9 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.8 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.0 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 74 CLY-4-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 52
TABLE-US-00066 B(S)-5Cy-O2 4.0% Clearing point [ C.]: 73.0 B(S)-5Cy-O4 4.0% n [589 nm, 20 C.]: 0.1041 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 2.9 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.9 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.0 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 77 CLY-4-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 53
TABLE-US-00067 B(S)-5Cy-O2 6.0% Clearing point [ C.]: 72.5 B(S)-5Cy-O4 6.0% n [589 nm, 20 C.]: 0.1036 CC-3-V 48.5% [1 kHz, 20 C.]: 2.8 CCG-V-F 5.0% K.sub.1 [pN, 20 C.]: 13.7 CLY-3-O2 8.0% K.sub.3 [pN, 20 C.]: 13.8 CLY-4-O2 5.0% .sub.1 [mPa s, 20 C.]: 79 CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 54
TABLE-US-00068 B(S)-2O-O4 4.0% Clearing point [ C.]: 76.0 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1016 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 3.0 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 15.1 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 15.1 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 82 CLY-4-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% LY-5Cy-O2 9.5% 100.0%
EXAMPLE 55
TABLE-US-00069 B(S)-2O-O4 4.0% Clearing point [ C.]: 74 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1050 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 3.0 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 14.0 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.5 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 77 CLY-5Cy-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 56
TABLE-US-00070 B(S)-2O-O4 4.0% Clearing point [ C.]: 71.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1024 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 3.2 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.4 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.2 CCOY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 75 CLY-4-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 57
TABLE-US-00071 B(S)-2O-O4 4.0% Clearing point [ C.]: 73.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1048 B(S)-2O-O6 4.0% .sub. [1 kHz, 20 C.]: 3.9 CC-3-V 48.5% .sub. [1 kHz, 20 C.]: 6.9 CC1G-V-F 5.0% [1 kHz, 20 C.]: 3.0 CLY-3-O2 8.0% K.sub.1 [pN, 20 C.]: 13.8 CLY-4-O2 5.0% K.sub.3 [pN, 20 C.]: 14.5 CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 58
TABLE-US-00072 CY-5-O2 7.5% Clearing point [ C.]: 80.3 PY-3-O2 5.0% n [589 nm, 20 C.]: 0.1049 CY-3-O2 7.0% [1 kHz, 20 C.]: 3.9 CLY-3-O2 6.0% K.sub.1 [pN, 20 C.]: 14.5 CLY-3-O3 6.0% K.sub.3 [pN, 20 C.]: 15.5 CLY-2-O4 4.0% V.sub.0 [V, 20 C.]: 2.09 CLY-4-O2 3.0% .sub.1 [mPa s, 20 C.]: 110 CPY-2-O2 7.0% CPY-3-O2 9.0% B-2O-O5 5.0% CC-3-V 27.0% CCP-V-1 5.0% CC-3-V1 5.5% CCG-V-F 3.0% 100.0%
EXAMPLE 59
TABLE-US-00073 CC-3-V 32.0% Clearing point [ C.]: 81.6 CC-3-V1 5.0% n [589 nm, 20 C.]: 0.1099 CY-3-O2 15.0% [1 kHz, 20 C.]: 4.4 CCY-3-O1 3.0% K.sub.1 [pN, 20 C.]: 15.0 CCY-3-O2 8.0% K.sub.3 [pN, 20 C.]: 16.5 CLY-3-O2 8.0% V.sub.0 [V, 20 C.]: 2.05 CPY-3-O2 9.0% .sub.1 [mPa s, 20 C.]: 113 PGIY-2-O4 6.0% B(S)-2O-O4 4.0% B(S)-2O-O5 4.0% B(S)-2O-O6 3.0% BCH-3F.F 3.0% 100.0%
EXAMPLE 60
TABLE-US-00074 CC-3-V 30.0% Clearing point [ C.]: 82.7 CC-3-V1 4.0% n [589 nm, 20 C.]: 0.1102 CY-3-O2 16.0% [1 kHz, 20 C.]: 4.2 CCY-3-O1 4.0% K.sub.1 [pN, 20 C.]: 15.0 CCY-3-O2 8.0% K.sub.3 [pN, 20 C.]: 16.6 CLY-3-O2 8.0% V.sub.0 [V, 20 C.]: 2.10 CPY-3-O2 9.0% .sub.1 [mPa s, 20 C.]: 118 PGIY-2-O4 4.0% B(S)-2O-O4 4.0% B(S)-2O-O5 4.0% B(S)-2O-O6 3.0% BCH-3F.F 6.0% 100.0%
EXAMPLE 61
TABLE-US-00075 CC-3-V 30.0% Clearing point [ C.]: 81.8 CC-3-V1 5.0% n [589 nm, 20 C.]: 0.12982 CC-4-V1 4.0% [1 kHz, 20 C.]: 4.0 PY-3-O2 10.0% K.sub.1 [pN, 20 C.]: 15.9 PYP-2-3 6.0% K.sub.3 [pN, 20 C.]: 15.2 CPY-2-O2 8.0% V.sub.0 [V, 20 C.]: 2.06 CPY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 109 CLY-3-O2 6.0% CLY-4-O2 4.0% PGIY-2-O4 4.0% B(S)-2O-O4 4.0% B(S)-2O-O5 5.0% B(S)-2O-O6 4.0% BCH-3F.F 2.0% 100.0%
EXAMPLE 62
[0376] Mixture according to Example 61 is stabilized with 0.04% of the compound of formula
##STR00608##
EXAMPLE 63
[0377] Mixture according to Example 61 is stabilized with 0.04% of the compound of formula
##STR00609##
EXAMPLE 64
TABLE-US-00076 B(S)-2O-O4 4.0% Clearing point [ C.]: 76.1 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1249 B(S)-2O-O6 3.0% [1 kHz, 20 C.]: 2.0 COB(S)-2-O4 3.0% K.sub.1 [pN, 20 C.]: 14.3 CPY-3-O2 8.5% K.sub.3 [pN, 20 C.]: 13.4 PGIY-2-O4 7.5% V.sub.0 [V, 20 C.]: 2.69 PYP-2-3 10.0% .sub.1 [mPa s, 20 C.]: 72 PYP-2-4 3.5% CC-3-V 44.0% CC-3-V1 3.0% PP-1-2V1 3.5% CCG-V-F 6.0% 100.0%
EXAMPLE 65
[0378] Mixture according to Example 64 is stabilized with 0.04% of the compound of formula
##STR00610##
EXAMPLE 66
[0379] Mixture according to Example 64 is stabilized with 0.04% of the compound of formula
##STR00611##
EXAMPLE 67
TABLE-US-00077 B(S)-2O-O4 4.0% Clearing point [ C.]: 94.9 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1047 CC-3-V 39.0% [1 kHz, 20 C.]: 2.9 CC-3-V1 7.0% K.sub.1 [pN, 20 C.]: 17.4 CCP-3-1 3.0% K.sub.3 [pN, 20 C.]: 17.8 CLY-3-O2 6.0% V.sub.0 [V, 20 C.]: 2.62 CLY-3-O3 6.0% .sub.1 [mPa s, 20 C.]: 103 CLY-4-O2 6.0% CLY-5-O2 4.0% CPY-3-O2 10.0% CY-3-O2 3.0% PGIY-2-O4 4.0% PYP-2-3 1.0% CCG-V-F 3.0% 100.0%
EXAMPLE 68
[0380] Mixture according to Example 67 is stabilized with 0.04% of the compound of formula
##STR00612##
EXAMPLE 69
[0381] Mixture according to Example 67 is stabilized with 0.04% of the compound of formula
##STR00613##
EXAMPLE 70
[0382] Mixture according to Example 67 is stabilized with 0.04% of the compound of formula
##STR00614##
EXAMPLE 71
TABLE-US-00078 B(S)-2O-O4 4.0% Clearing point [ C.]: 73.5 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1048 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 3.0 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.5 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 14.3 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 70 CCY-V-O2 5.0% CPY-2-O2 2.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 72
[0383] Mixture according to Example 71 is stabilized with 0.04% of the compound of formula
##STR00615##
EXAMPLE 73
[0384] Mixture according to Example 71 is stabilized with 0.04% of the compound of formula
##STR00616##
EXAMPLE 74
[0385] Mixture according to Example 71 is stabilized with 0.04% of the compound of formula
##STR00617##
EXAMPLE 75
TABLE-US-00079 B(S)-2O-O4 4.0% Clearing point [ C.]: 73.0 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1054 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 2.9 CC-3-V 48.5% K.sub.1 [pN, 20 C.]: 13.5 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 13.8 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 69 CLY-4-O2 5.0% CPY-V-O2 5.0% CPY-V-O4 5.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 76
[0386] Mixture according to Example 75 is stabilized with 0.04% of the compound of formula
##STR00618##
EXAMPLE 77
[0387] Mixture according to Example 75 is stabilized with 0.04% of the compound of formula
##STR00619##
EXAMPLE 78
[0388] Mixture according to Example 75 is stabilized with 0.04% of the compound of formula
##STR00620##
EXAMPLE 79
TABLE-US-00080 B(S)-2O-O4 4.0% Clearing point [ C.]: 74.0 B(S)-2O-O5 4.0% n [589 nm, 20 C.]: 0.1048 B(S)-2O-O6 4.0% [1 kHz, 20 C.]: 2.9 CC-3-V 48.5 K.sub.1 [pN, 20 C.]: 13.2 CCG-V-F 5.0% K.sub.3 [pN, 20 C.]: 13.7 CLY-3-O2 8.0% .sub.1 [mPa s, 20 C.]: 67 CCY-V-O2 5.0% CPY-V-O2 5.0% CPY-V-O4 5.0% PGIY-2-O4 2.0% PY-1-O2 4.5% PY-V2-O2 5.0% 100.0
EXAMPLE 80
[0389] Mixture according to Example 79 is stabilized with 0.04% of the compound of formula
##STR00621##
EXAMPLE 81
[0390] Mixture according to Example 79 is stabilized with 0.04% of the compound of formula
##STR00622##
EXAMPLE 82
[0391] Mixture according to Example 79 is stabilized with 0.04% of the compound of formula
##STR00623##
EXAMPLE 83
TABLE-US-00081 B(S)-5Cy1O-O2 5.0% B(S)-5Cy1O-O4 5.0% CC-3-V 49.5% CCG-V-F 5.0% CLY-3-O2 8.0% CLY-4-O2 5.0% CPY-2-O2 3.0% CPY-3-O2 8.0% PGIY-2-O4 2.0% PY-1-O2 9.5% 100.0%
EXAMPLE 84
[0392] Mixture according to Example 83 is stabilized with 0.04% of the compound of formula
##STR00624##
EXAMPLE 85
[0393] Mixture according to Example 83 is stabilized with 0.04% of the compound of formula
##STR00625##
[0394] Mixture examples 3 to 85 show a reduced or even no flicker while maintaining relatively high clearing points, high contrast and low rotational viscosities.
[0395] The preceding examples can be repeated with similar success by substituting the generically or specifically described reactants and/or operating conditions of this invention for those used in the preceding examples.
[0396] From the foregoing description, one skilled in the art can easily ascertain the essential characteristics of this invention and, without departing from the spirit and scope thereof, can make various changes and modifications of the invention to adapt it to various usages and conditions.