SUBSTITUTED ISOPHTHALIC ACID DIAMIDES
20230159472 · 2023-05-25
Inventors
- Christian Waldraff (Bad Vilbel, DE)
- Ralf Braun (Ramberg, DE)
- Arnim KOEHN (Klein-Winternheim, DE)
- Hartmut AHRENS (Langen, DE)
- Uwe Doeller (Rodgau, DE)
- Elisabeth ASMUS (Hoesbach, DE)
- Birgit BOLLENBACH-WAHL (Weiler/Bingen, DE)
- Christopher Hugh Rosinger (Hofheim, DE)
- Jan Dittgen (Frankfurt, DE)
- Anu Bheemaiah Machettira (Frankfurt am Main, DE)
Cpc classification
C07D271/08
CHEMISTRY; METALLURGY
A01N43/713
HUMAN NECESSITIES
C07D403/12
CHEMISTRY; METALLURGY
International classification
C07D257/06
CHEMISTRY; METALLURGY
A01N43/713
HUMAN NECESSITIES
C07D271/08
CHEMISTRY; METALLURGY
Abstract
Isophthalamides of the general formula (I) are described as herbicides.
##STR00001##
In this formula (I), X, Y and Z represent radicals such as hydrogen, alkyl and halogen. Q represents a heterocyclic ring such as tetrazolyl.
Claims
1. An isophthalamide of formula (I) or salt thereof ##STR00025## in which the symbols and indices are defined as follows: Q is Q.sup.1, Q.sup.2, Q.sup.3 or Q.sup.4 ##STR00026## R.sup.1 is (C.sub.1-C.sub.6)-alkyl, halo-(C.sub.1-C.sub.6)-alkyl or (C.sub.3-C.sub.6)-cycloalkyl, R.sup.2 is (C.sub.1-C.sub.6)-alkyl, R.sup.x is (C.sub.1-C.sub.6)-alkyl, (C.sub.1-C.sub.6)-alkyl-O—(C.sub.1-C.sub.6)-alkyl or phenyl, R.sup.y is halogen, (C.sub.1-C.sub.6)-alkyl or halo-(C.sub.1-C.sub.6)-alkyl, R.sup.z is hydrogen, (C.sub.1-C.sub.6)-alkyl or halo-(C.sub.1-C.sub.6)-alkyl, X is halogen, (C.sub.1-C.sub.6)-alkyl, halo-(C.sub.1-C.sub.6)-alkyl, (C.sub.3-C.sub.6)-cycloalkyl, R.sup.1O, R.sup.2(O).sub.nS or R.sup.1O—(C.sub.1-C.sub.6)-alkyl or R.sup.2S(O).sub.n-(C.sub.1-C.sub.6)-alkyl, Y is halogen, (C.sub.1-C.sub.6)-alkyl, halo-(C.sub.1-C.sub.6)-alkyl, R.sup.1O or R(O).sub.nS, Z is hydrogen, one of the following groups, each of which is substituted by s radicals from the group consisting of halogen, cyano, R.sup.1C(O), R.sup.1OC(O), R.sup.1O and R.sup.2(O).sub.nS: (C.sub.1-C.sub.6)-alkyl, (C.sub.3-C.sub.6)-cycloalkyl, (C.sub.3-C.sub.6)-cycloalkyl-(C.sub.1-C.sub.6)-alkyl, (C.sub.1-C.sub.6)-alkyl-O—(C.sub.1-C.sub.6)-alkyl, (C.sub.2-C.sub.6)-alkenyl, (C.sub.2-C.sub.6)-alkenyl-(C.sub.1-C.sub.6)-alkyl, (C.sub.2-C.sub.6)-alkynyl, (C.sub.2-C.sub.6)-alkynyl-(C.sub.1-C.sub.6)-alkyl, (C.sub.1-C.sub.6)-alkoxy, R.sup.2S(O)n-(C.sub.1-C.sub.6)-alkyl, R.sup.1C(O), R.sup.1OC(O), R.sup.1C(O)—(C.sub.1-C.sub.6)-alkyl, R.sup.1OC(O)—(C.sub.1-C.sub.6)-alkyl, R.sup.1NH—(C.sub.1-C.sub.6)-alkyl, R.sup.1.sub.2N—(C.sub.1-C.sub.6)-alkyl, R.sup.1NHC(O)—(C.sub.1-C.sub.6)-alkyl or R.sup.1.sub.2NC(O)—(C.sub.1-C.sub.6)-alkyl, or one of the following groups, each substituted by s radicals from the group consisting of halogen, (C.sub.1-C.sub.6)-alkyl, halo-(C.sub.1-C.sub.6)-alkyl, (C.sub.1-C.sub.6)-alkoxy, halo-(C.sub.1-C.sub.6)-alkoxy, R.sup.1C(O) and R.sup.1OC(O): phenyl, benzyl, phenyl, benzyl, heterocyclyl or heterocyclyl-(C.sub.1-C.sub.6)-alkyl, n is 0, 1 or 2, s is 0, 1, 2 or 3.
2. The isophthalamide as claimed in claim 1, wherein Q is Q.sup.1, Q.sup.2, Q.sup.3 or Q.sup.4 ##STR00027## R.sup.x is Me, Et, Pr, i-Pr, c-Pr, (CH.sub.2).sub.2OMe or Ph, R.sup.y is Cl, Me, Et or CF.sub.3, R.sup.z is hydrogen, Me, Et or CF.sub.3, X is halogen, (C.sub.1-C.sub.6)-alkyl, halo-(C.sub.1-C.sub.6)-alkyl, c-Pr, OMe, OEt, SMe, SEt, SO.sub.2Me, SO.sub.2Et, CH.sub.2OMe, CH.sub.2SMe, CH.sub.2SO.sub.2Me, (CH.sub.2).sub.2SMe or (CH.sub.2).sub.2SO.sub.2Me, Y is halogen, halo-(C.sub.1-C.sub.6)-alkyl, OMe, SMe, S(O)Me, SO.sub.2Me, SEt, S(O)Et or SO.sub.2Et, Z is hydrogen, (C.sub.1-C.sub.6)-alkyl, (C.sub.3-C.sub.6)-cycloalkyl, CH.sub.2c-Pr, halo-(C.sub.1-C.sub.6)-alkyl, (CH.sub.2).sub.2OMe, (CH.sub.2).sub.2OEt, allyl, propynyl, (CH.sub.2).sub.2SMe, (CH.sub.2).sub.2SO.sub.2Me, C(O)Me, C(O)cPr, C(O)OMe, C(O)OEt, CH.sub.2-(tetrahydrofuran-2-yl), oxetan-3-yl, CH.sub.2C(O)Me, CH.sub.2C(O)c-Pr, CH.sub.2C(O)NMe.sub.2, CH.sub.2CN, Ph, CH.sub.2Ph or CH.sub.2-(thien-2-yl), OMe, OEt, OPr, Oi-Pr.
3. The isophthalamide as claimed in claim 1, wherein Q is Q.sup.1 or Q.sup.4, R.sup.x is Me, Et or Pr, R.sup.z is H or Me, X is F, Cl, Br, I, Me, Et, c-Pr, OMe, SMe, SEt, CH.sub.2OMe or CF.sub.3, Y is F, Cl, Br, I, SMe, S(O)Me, SO.sub.2Me, CF.sub.3, CHF.sub.2 or C.sub.2F.sub.5, Z is hydrogen, Me, Et, c-Pr, Pr, i-Pr, c-Bu, CH.sub.2-c-Pr, CH.sub.2CHF.sub.2, CH.sub.2CF.sub.3, CH(Me)-c-Pr, (CH.sub.2).sub.2OMe, (CH.sub.2).sub.2SMe, CH.sub.2CN, CH.sub.2-(tetrahydrofuran-2-yl), CH.sub.2C(O)NMe.sub.2, Ph or CH.sub.2-(thien-2-yl), oxetan-3-yl, OMe, OEt, OPr, Oi-Pr.
4. An herbicidal composition or plant growth-regulating composition, comprising one or more isophthalamides of formula (I) or salts thereof as claimed in claim 1.
5. The herbicidal composition as claimed in claim 4, further comprising a formulation auxiliary.
6. The herbicidal composition as claimed in claim 4, comprising at least one further active ingredient from the group of insecticides, acaricides, herbicides, fungicides, safeners and/or growth regulators.
7. The herbicidal composition as claimed in claim 4, comprising a safener.
8. The herbicidal composition as claimed in claim 7, in which the safener is selected from the group consisting of mefenpyr-diethyl, cyprosulfamide, isoxadifen-ethyl, cloquintocet-mexyl, benoxacor and dichlormid.
9. A method of controlling one or more unwanted plants, comprising applying an effective amount of at least one isophthalamide of formula (I) and/or salt thereof as claimed in claim 1 or an herbicidal composition thereof to the plants and/or to a site of unwanted vegetation.
10. A product comprising one or more compounds of formula (I) and/or salts as claimed in claim 1 or a herbicidal composition thereof for controlling one or more unwanted plants.
11. The product as claimed in claim 10, wherein the isophthalamides of formula (I) and/or salts are used for controlling one or more unwanted plants in one or more crops of one or more useful plants.
12. The product as claimed in claim 11, wherein the useful plants are transgenic useful plants.
Description
A. CHEMICAL EXAMPLES
Synthesis of 4-bromo-2-chloro-N.SUP.3.-ethyl-N.SUP.1.-(1-methyl-1H-tetrazol-5-yl)isophthalamide (Example No. 1-178)
Step 1: Preparation of 6-bromo-2-chloro-3-(methoxycarbonyl)benzoic Acid
[0381] 1.47 g (5.29 mmol) of methyl 4-bromo-2-chloro-3-formylbenzoate was initially charged 100 ml of acetone. A solution of 636 mg (6.35 mmol) of chromium(VI) oxide in dilute sulfuric acid (H.sub.2O:H.sub.2SO.sub.4 3:1) was slowly added dropwise. The mixture was warmed to room temperature and stirred for 12 hours. Thereafter, a little isopropanol was added and the mixture was concentrated under reduced pressure. The residue was taken up in water and extracted with ethyl acetate, and the organic phase was dried and concentrated to dryness. 1.23 g of 6-bromo-2-chloro-3-(methoxycarbonyl)benzoic acid was obtained.
[0382] .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=14.30 (br s, 1H); 7.82 (d, 1H); 7.77 (d, 1H); 3.88 (s, 3H).
Step 2: Preparation of methyl 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoate
[0383] To an initial charge of 753 mg (2.56 mmol) of 6-bromo-2-chloro-3-(methoxycarbonyl)benzoic acid in 30 ml dichloromethane were added catalytic amounts of dimethylformamide. Thereafter, at room temperature, 490 mg (3.84 mmol) of oxalyl chloride was added and the mixture was stirred for a further 1 hour. The mixture was concentrated to dryness, and the residue was coevaporated with toluene. The resulting residue was taken up in 5 ml of dichloromethane. To an initial charge of 1.9 ml (3.84 mmol) of a 2.5M solution of ethylamine in tetrahydrofuran and 663 mg (5.13 mmol) of Hünig's base in 50 ml dichloromethane was added, at 0° C., the acid chloride solution. The mixture was stirred at room temperature for a further 4 hours. Thereafter, 100 ml of dichloromethane was added and the mixture was washed with aqueous 2M hydrochloric acid. The organic phase was dried and concentrated to dryness. 773 mg of methyl 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoate was obtained.
[0384] .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=8.68 (t, 1H); 7.77 (d, 1H); 7.69 (d, 1H); 3.87 (s, 3H); 3.28 (m, 2H); 1.12 (t, 3H).
Step 3: Preparation of 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoic Acid
[0385] To 773 mg (2.41 mmol) of methyl 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoate in 80 ml of methanol was added, at room temperature, 192 mg (4.82 mmol) of aqueous 1M sodium hydroxide solution. The mixture was stirred at 50° C. for 12 hours and then concentrated to dryness. The residue was taken up in a little water, and the solution was acidified by means of aqueous 2M hydrochloric acid and extracted with dichloromethane. The organic phase was dried and concentrated. 582 g of 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoic acid was obtained.
[0386] .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=13.69 (br s, 1H); 8.65 (t, 1H); 7.72 (d, 1H); 7.66 (d, 1H); 3.26 (m, 2H); 1.12 (t, 3H).
Step 4: Preparation of 4-bromo-2-chloro-N.SUP.3.-ethyl-N.SUP.1.-(1-methyl-1H-tetrazol-5-yl)isophthalamide
[0387] To an initial charge of 189 mg (0.61 mmol) of 4-bromo-2-chloro-3-(ethylcarbamoyl)benzoic acid and 93.5 mg (0.92 mmol) of 5-amino-1-methyl-1H-tetrazole in 3 ml of pyridine was added, at room temperature, 155 mg (1.22 mmol) of oxalyl chloride. The mixture was stirred for a further 12 hours. Addition of 10 ml of water was followed by extraction with dichloromethane, and drying and concentration of the organic phases. The residue was purified by column chromatography (HPLC, C18, gradient: acetonitrile/water (++0.05% trifluoroacetic acid), 10/90.fwdarw.100/0 in 30 min). 66 mg of 4-bromo-2-chloro-N.sup.3-ethyl-N.sup.1-(1-methyl-1H-tetrazol-5-yl)isophthalamide was obtained (Example No. 1-178).
[0388] The examples listed in the tables below were prepared analogously to the methods mentioned above or can be obtained analogously to the methods mentioned above. These compounds are very particularly preferred.
[0389] The abbreviations used here mean: [0390] Me=methyl Bu=butyl Et=ethyl Pr=propyl c=cyclo Ph=phenyl
TABLE-US-00001 TABLE 1 Inventive compounds of the general formula (I) in which Q is Q.sup.1 and R.sup.x is methyl, and the other substituents have the definitions given below.
TABLE-US-00002 TABLE 2 Inventive compounds of the general formula (I) in which Q is Q.sup.1 and R.sup.x is ethyl, and the other substituents have the definitions given below.
TABLE-US-00003 TABLE 3 Inventive compounds of the general formula (I) in which Q is Q.sup.1 and R.sup.x is propyl, and the other substituents have the definitions given below.
TABLE-US-00004 TABLE 4 Inventive compounds of the general formula (I) in which Q is Q.sup.2 and R.sup.x is methyl, and the other substituents have the definitions given below.
TABLE-US-00005 TABLE 5 Inventive compounds of the general formula (I) in which Q is Q.sup.4 and R.sup.z is hydrogen, and the other substituents have the definitions given below.
TABLE-US-00006 TABLE 6 Inventive compounds of the general formula (I) in which Q is Q.sup.4 and R.sup.z is methyl, and other substituents have the definitions given below.
[0391] NMR data for numerous inventive compounds of the formula (I) mentioned in tables above are disclosed below for further characterization:
[0392] Ex. no. 1-4: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.63 (br s, 1H); 8.50 (q, 1H); 7.67 (d, 1H); 7.50 (d, 1H); 3.98 (s, 3H); 2.80 (d, 3H); 2.33 (s, 3H);
[0393] Ex. no. 1-19: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.57 (q, 1H); 7.94 (d, 1H); 7.89 (d, 1H); 4.01 (s, 3H); 3.27 (s, 3H); 2.78 (d, 3H); 2.35 (s, 3H);
[0394] Ex. no. 1-20: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.63 (t, 1H); 7.94 (d, 1H); 7.88 (d, 1H); 4.01 (s, 3H); 3.27 (m, 2H); 3.27 (s, 3H); 2.38 (s, 3H); 1.13 (t, 3H);
[0395] Ex. no. 1-21: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 8.70 (d, 1H); 7.93 (d, 1H); 7.88 (d, 1H); 4.00 (s, 3H); 3.27 (s, 3H); 2.78 (m, 1H); 2.35 (s, 3H); 0.69 (m, 2H); 0.62 (m, 1H); 0.51 (m, 1H);
[0396] Ex. no. 1-25: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.51 (q, 1H); 7.83 (d, 1H); 7.76 (d, 1H); 4.00 (s, 3H); 2.79 (d, 3H); 2.34 (s, 3H);
[0397] Ex. no. 1-26: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.49 (t, 1H); 7.83 (d, 1H); 7.75 (d, 1H); 4.00 (s, 3H); 3.28 (m, 2H); 2.36 (s, 3H); 1.11 (t, 3H);
[0398] Ex. no. 1-27: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.75 (br s, 1H); 8.66 (d, 1H); 7.83 (d, 1H); 7.75 (d, 1H); 4.00 (s, 3H); 2.81 (m, 1H); 2.34 (s, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0399] Ex. no. 1-28: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.72 (t, 1H); 7.83 (d, 1H); 7.76 (d, 1H); 4.01 (s, 3H); 3.13 (m, 2H); 2.38 (s, 3H); 1.01 (m, 1H); 0.45 (m, 2H); 0.23 (m, 2H);
[0400] Ex. no. 1-29: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.80 (br s, 1H); 9.38 (t, 1H); 7.88 (d, 1H); 7.80 (d, 1H); 4.13 (m, 2H); 4.01 (s, 3H); 2.35 (s, 3H);
[0401] Ex. no. 1-30: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 9.09 (t, 1H); 7.86 (d, 1H); 7.78 (d, 1H); 6.13 (tt, 1H); 4.01 (s, 3H); 3.71 (2H); 2.36 (s, 3H);
[0402] Ex. no. 1-31: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.62 (t, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 4.01 (s, 3H); 3.40 (m, 1H); 2.39 (d, 3H); 1.20 (dd, 3H); 0.91 (m, 1H); 0.44 (m, 2H); 0.29 (m, 2H);
[0403] Ex. no. 1-32: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 8.81 (t, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.95 (t, 1H); 4.01 (s, 3H); 3.24 (m, 2H); 1.54 (m, 2H); 0.92 (t, 3H);
[0404] Ex. no. 1-33: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 8.51 (d, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 4.08 (m, 1H); 4.00 (s, 3H); 2.37 (s, 3H); 1.16 (d, 3H); 1.12 (d, 3H);
[0405] Ex. no. 1-34: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.70 (d, 1H); 7.83 (d, 1H); 7.75 (d, 1H); 4.00 (s, 3H); 3.52-3.31 (m, 4H); 3.27 (s, 3H); 2.36 (s, 3H);
[0406] Ex. no. 1-36: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 9.42 (t, 1H); 7.89 (d, 1H); 7.81 (d, 1H); 4.49 (m, 2H); 4.01 (s, 3H); 2.35 (s, 3H);
[0407] Ex. no. 1-37: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 8.72 (br s, 1H); 7.83 (d, 1H); 7.75 (d, 1H); 4.00 (s, 3H); 3.97 (m, 1H); 3.77 (m, 1H); 3.63 (m, 1H); 3.35 (m, 1H); 3.27 (m, 1H); 2.36 (s, 3H); 1.92 (m, 1H); 1.83 (m, 2H); 1.60 (m, 1H);
[0408] Ex. no. 1-41: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 9.41 (d, 1H); 7.87 (d, 1H); 7.80 (d, 1H); 4.98 (m, 1H); 4.80 (t, 2H); 4.54 (t, 1H); 4.48 (t, 1H); 4.01 (s, 3H); 2.36 (s, 3H);
[0409] Ex. no. 1-44: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.56 (q, 1H); 7.80 (d, 1H); 7.63 (d, 1H); 6.91 (t, 1H); 4.00 (t, 1H); 2.80 (d, 3H); 2.33 (s, 3H);
[0410] Ex. no. 1-45: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.65 (t, 1H); 7.79 (d, 1H); 7.63 (d, 1H); 6.91 (t, 1H); 4.00 (s, 3H); 3.30 (m, 2H); 2.35 (s, 3H); 1.13 (t, 3H);
[0411] Ex. no. 1-46: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.68 (br s, 1H); 8.71 (d, 1H); 7.79 (d, 1H); 7.62 (d, 1H); 6.90 (t, 1H); 3.99 (s, 3H); 2.85 (m, 1H); 2.33 (s, 3H); 0.71 (m, 1H); 0.54 (m, 2H);
[0412] Ex. no. 1-47: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.79 (t, 1H); 7.80 (d, 1H); 7.64 (d, 1H); 6.92 (t, 1H); 4.00 (s, 3H); 3.15 (m, 2H); 2.38 (s, 3H); 1.04 (m, 1H); 0.46 (m, 2H); 0.24 (m, 2H);
[0413] Ex. no. 1-49: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 9.12 (t, 1H); 7.82 (d, 1H); 7.66 (d, 1H); 6.93 (t, 1H); 6.19 (tt, 1H); 4.00 (s, 3H); 3.72 (m, 2H); 2.36 (s, 3H);
[0414] Ex. no. 1-56: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.66 (br s, 1H); 8.53 (q, 1H); 7.89 (d, 1H); 7.67 (d, 1H); 3.99 (s, 3H); 3.86 (s, 3H); 2.79 (d, 3H);
[0415] Ex. no. 1-57: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.60 (t, 1H); 7.88 (d, 1H); 7.67 (d, 1H); 3.99 (s, 3H); 3.87 (s, 3H); 3.29 (m, 2H); 1.11 (t, 3H);
[0416] Ex. no. 1-58: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.68 (d, 1H); 7.88 (d, 1H); 7.66 (d, 1H); 3.99 (s, 3H); 3.86 (s, 3H); 2.80 (m, 1H); 0.71 (m, 2H); 0.49 (m, 2H);
[0417] Ex. no. 1-72: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.53 (br s, 1H); 8.57 (q, 1H); 7.85 (d, 1H); 7.54 (d, 1H); 6.96 (t, 1H); 3.99 (s, 3H); 3.85 (s, 3H); 2.81 (d, 3H);
[0418] Ex. no. 1-73: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.52 (br s, 1H); 8.65 (t, 1H); 7.84 (d, 1H); 7.54 (d, 1H); 6.96 (t, 1H); 3.99 (s, 3H); 3.86 (s, 3H); 3.20 (m, 2H); 1.13 (t, 3H);
[0419] Ex. no. 1-74: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.51 (br s, 1H); 8.72 (d, 1H); 7.84 (d, 1H); 7.52 (d, 1H); 6.95 (t, 1H); 3.98 (s, 3H); 3.85 (s, 3H); 2.85 (m, 1H); 0.71 (m, 2H); 0.54 (m, 2H);
[0420] Ex. no. 1-81: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.48 (q, 1H); 7.95 (d, 1H); 7.88 (d, 1H); 4.05 (s, 3H); 2.80 (d, 3H); 2.43 (s, 3H);
[0421] Ex. no. 1-82: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.56 (t, 1H); 7.95 (d, 1H); 7.88 (d, 1H); 4.06 (s, 3H); 3.32 (m, 2H); 2.44 (s, 3H); 1.14 (t, 3H);
[0422] Ex. no. 1-83: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.83 (br s, 1H); 8.64 (d, 1H); 7.94 (d, 1H); 7.88 (d, 1H); 4.05 (s, 3H); 2.80 (m, 1H); 2.43 (s, 3H); 0.71 (m, 2H); 0.53 (br s, 2H);
[0423] Ex. no. 1-84: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.83 (br s, 1H); 8.68 (t, 1H); 7.95 (d, 1H); 7.87 (d, 1H); 4.05 (s, 3H); 3.16 (m, 2H); 2.45 (s, 3H); 1.02 (m, 1H); 0.45 (m, 2H); 0.24 (m, 2H);
[0424] Ex. no. 1-86: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.85 (br s, 1H); 9.10 (t, 1H); 7.98 (d, 1H); 7.92 (d, 1H); 6.11 (tt, 1H); 4.05 (s, 3H); 3.71 (m, 2H); 2.43 (s, 3H);
[0425] Ex. no. 1-87: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.54 (q, 1H); 7.81 (s, 2H); 6.90 (t, 1H); 4.04 (s, 3H); 2.82 (d, 3H); 2.42 (s, 3H);
[0426] Ex. no. 1-88: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.62 (t, 1H); 7.82 (s, 2H); 6.91 (t, 1H); 4.05 (s, 3H); 3.33 (m, 2H); 2.43 (s, 3H); 1.16 (t, 3H);
[0427] Ex. no. 1-89: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 8.70 (d, 1H); 7.81 (br s, 2H); 6.90 (t, 1H); 4.05 (s, 3H); 2.85 (m, 1H); 2.41 (s, 3H); 0.71 (m, 2H); 0.58 (m, 2H);
[0428] Ex. no. 1-90: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 8.76 (t, 1H); 7.82 (br s, 1H); 6.91 (t, 1H); 4.05 (s, 3H); 3.18 (m, 2H); 2.44 (s, 3H); 1.06 (m, 1H); 0.46 (m, 2H); 0.26 (m, 2H);
[0429] Ex. no. 1-92: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 9.14 (t, 1H); 7.85 (br s, 2H); 6.92 (t, 1H); 6.18 (tt, 1H); 4.05 (s, 3H); 3.73 (m, 2H); 2.42 (s, 3H);
[0430] Ex. no. 1-123: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.03 (br s, 1H); 8.72 (q, 1); 8.07 (d, 1H); 8.02 (d, 1H); 4.01 (s, 3H); 3.31 (s, 3H); 2.79 (d, 3H);
[0431] Ex. no. 1-125: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.85 (d, 1H); 8.06 (d, 1H); 8.02 (d, 1H); 4.01 (s, 3H); 3.31 (s, 3H); 2.78 (m, 1H); 0.70 (m, 2H); 0.60 (m, 1H); 0.56 (m, 1H);
[0432] Ex. no. 1-129: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.00 (br s, 1H); 8.69 (q, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.01 (s, 3H); 2.79 (d, 3H);
[0433] Ex. no. 1-130: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.76 (t, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.01 (s, 3H); 3.29 (m, 2H); 1.11 (t, 3H);
[0434] Ex. no. 1-131: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.82 (d, 1H); 7.97 (d, 1H); 7.92 (d, 1H); 4.01 (s, 3H); 2.80 (m, 1H); 0.72 (m, 2H); 0.50 (br s, 2H);
[0435] Ex. no. 1-132: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.89 (t, 1H); 7.98 (d, 1H); 7.93 (d, 1H); 4.02 (s, 3H); 3.15 (m, 2H); 1.00 (m, 1H); 0.45 (m, 2H); 0.24 (m, 2H)
[0436] Ex. no. 1-133: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.06 (br s, 1H); 9.56 (t, 1H); 8.04 (d, 1H); 7.98 (d, 1H); 4.16 (m, 2H); 4.02 (s, 3H);
[0437] Ex. no. 1-134: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.05 (br s, 1H); 9.29 (t, 1H); 8.02 (d, 1H); 7.96 (d, 1H); 6.12 (tt, 1H); 4.02 (s, 3H); 3.72 (m, 2H);
[0438] Ex. no. 1-135: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.77 (d, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.02 (s, 3H); 3.44 (m, 1H); 1.20 (m, 3H); 0.90 (m, 1H); 0.43 (m, 2H); 0.29 (m, 2H);
[0439] Ex. no. 1-136: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.78 (t, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.02 (s, 3H); 3.22 (m, 2H); 1.53 (m, 2H); 0.92 (t, 3H);
[0440] Ex. no. 1-137: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.66 (d, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.07 (m, 1H); 4.01 (s, 3H); 1.14 (br s, 6H);
[0441] Ex. no. 1-138: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.00 (br s, 1H); 8.91 (t, 1H); 7.97 (d, 1H); 7.92 (d, 1); 4.01 (s, 3H); 3.43 (m, 4H); 3.27 (s, 3H);
[0442] Ex. no. 1-139: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.99 (t, 1H); 7.98 (d, 1H); 7.94 (d, 1H); 4.01 (s, 3H); 3.45 (m, 2H); 2.63 (t, 2H); 2.11 (s, 3H);
[0443] Ex. no. 1-140: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.05 (br s, 1H); 9.61 (t, 1H); 8.04 (d, 1H); 7.99 (d, 1H); 4.42 (d, 2H); 4.01 (s, 3H);
[0444] Ex. no. 1-141: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.00 (br s, 1H); 8.90 (t, 1H); 7.97 (d, 1H); 7.92 (d, 1H); 4.01 (s, 3H); 3.95 (m, 1H); 3.77 (m, 1H); 3.63 (m, 1H); 3.30 (m, 2H); 1.95 (m, 1H); 1.83 (m, 2H); 1.63 (m, 1H);
[0445] Ex. no. 1-142: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.90 (t, 1H); 7.96 (d, 1H); 7.91 (d, 1H); 4.18 (br d, 2H); 4.01 (s, 3H); 3.00 (s, 3H); 2.86 (s, 3H);
[0446] Ex. no. 1-143: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.08 (br s, 1H); 10.86 (br s, 1H); 8.04 (m, 2H); 7.65 (d, 2H); 7.38 (m, 2H); 7.15 (t, 1H); 4.02 (s, 3H);
[0447] Ex. no. 1-144: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 9.36 (t, 1H); 7.98 (d, 1H); 7.94 (d, 1H); 7.45 (m, 1H); 7.07 (m, 1H); 6.98 (m, 1H); 4.66 (br s, 2H); 4.01 (s, 3H);
[0448] Ex. no. 1-146: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 9.01 (d, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.35 (m, 1H); 4.01 (s, 3H); 2.25 (m, 2H); 1.98 (m, 2H); 1.70 (m, 2H);
[0449] Ex. no. 1-147: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 8.72 (q, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.96 (t, 1H); 4.01 (s, 3H); 2.81 (d, 3H);
[0450] Ex. no. 1-148: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 8.78 (t, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.95 (t, 1H); 4.01 (s, 3H); 3.31 (m, 2H); 1.13 (t, 3H);
[0451] Ex. no. 1-149: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.92 (br s, 1H); 8.85 (d, 1H); 7.90 (d, 1H); 7.77 (d, 1H); 6.95 (t, 1H); 4.00 (s, 3H); 2.83 (m, 1H); 0.72 (m, 2H); 0.55 (m, 2H);
[0452] Ex. no. 1-155: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 8.70 (d, 1H); 7.90 (d, 1H); 7.77 (d, 1H); 6.94 (t, 1H); 4.09 (m, 1H); 4.01 (s, 3H); 1.16 (d, 6H);
[0453] Ex. no. 1-156: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 8.92 (t, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.96 (t, 1H); 4.01 (s, 3H); 3.46 (m, 4H); 3.29 (s, 3H);
[0454] Ex. no. 1-157: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.95 (br s, 1H); 8.99 (t, 1H); 7.92 (d, 1H); 7.80 (d, 1H); 7.05 (t, 1H); 4.01 (s, 3H); 3.49 (m, 2H); 2.67 (m, 2H); 2.12 (s, 3H);
[0455] Ex. no. 1-158: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.98 (br s, 1H); 9.59 (t, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.01 (t, 1H); 4.40 (d, 2H); 4.01 (s, 3H);
[0456] Ex. no. 1-159: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 8.94 (t, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.97 (t, 1H); 4.01 (s, 3H); 3.98 (m, 1H); 3.78 (m, 1H); 3.64 (m, 1H); 3.35 (m, 2H); 1.95 (m, 1H); 1.84 (m, 2H); 1.62 (m, 1H);
[0457] Ex. no. 1-160: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.95 (br s, 1H); 9.12 (t, 1H); 7.94 (d, 1H); 7.83 (d, 1H); 7.58 (t, 1H); 4.17 (d, 2H); 4.01 (t, 3H); 3.02 (s, 3H); 2.89 (s, 3H);
[0458] Ex. no. 1-161: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 10.84 (br s, 1H); 7.99 (d, 1H); 7.85 (d, 1H); 7.69 (m, 2H); 7.38 (m, 2H); 7.15 (m, 1H); 7.12 (t, 1H); 4.02 (s, 3H);
[0459] Ex. no. 1-162: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.95 (br s, 1H); 9.45 (t, 1H); 7.93 (d, 1H); 7.79 (d, 1H); 7.45 (m, 1H); 7.08 (m, 1H); 6.99 (m, 1H); 6.92 (t, 1H); 4.68 (d, 2H); 4.00 (s, 3H);
[0460] Ex. no. 1-164: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 9.05 (d, 1H); 7.91 (d, 1H); 7.78 (d, 1H); 6.93 (t, 1H); 4.37 (m, 1H); 4.01 (s, 3H); 2.26 (m, 2H); 2.01 (m, 2H); 1.72 (m, 2H);
[0461] Ex. no. 1-165: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.61 (q, 1H); 8.00 (d, 1H); 7.85 (d, 1H); 4.01 (s, 3H); 2.78 (d, 3H);
[0462] Ex. no. 1-166: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.67 (t, 1H); 7.99 (d, 1H); 7.85 (d, 1H); 4.01 (s, 3H); 3.29 (m, 1H); 1.11 (t, 3H);
[0463] Ex. no. 1-173: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 8.79 (d, 1H); 7.77 (d, 1H); 7.66 (d, 1H); 3.99 (s, 3H); 2.82 (m, 1H); 0.72 (m, 2H); 0.52 (m, 2H);
[0464] Ex. no. 1-177: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.65 (q, 1H); 7.81 (d, 1H); 7.69 (d, 1H); 3.99 (s, 3H); 2.79 (d, 3H);
[0465] Ex. no. 1-178: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.71 (t, 1H); 7.81 (d, 1H); 7.68 (d, 1H); 3.99 (s, 3H); 3.28 (m, 2H); 1.14 (t, 3H);
[0466] Ex. no. 1-179: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.77 (d, 1H); 7.80 (d, 1H); 7.68 (d, 1H); 3.99 (s, 3H); 2.81 (m, 1H); 0.72 (m, 2H); 0.54 (d, 2H);
[0467] Ex. no. 1-180: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.80 (t, 1H); 7.81 (d, 1H); 7.68 (d, 1H); 3.99 (s, 3H); 3.16 (m, 2H); 1.02 (m, 1H); 0.46 (m, 2H); 0.26 (m, 2H);
[0468] Ex. no. 1-181: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 9.49 (t, 1H); 7.85 (d, 1H); 7.74 (d, 1H); 4.14 (m, 2H); 3.99 (s, 3H);
[0469] Ex. no. 1-182: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 9.23 (t, 1H); 7.83 (d, 1H); 7.72 (d, 1H); 6.14 (tt, 1H); 3.99 (s, 3H); 3.70 (m, 2H);
[0470] Ex. no. 1-183: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.66 (d, 1H); 7.80 (d, 1H); 7.67 (d, 1H); 3.99 (s, 3H); 3.49 (m, 1H); 1.22 (d, 3H); 0.92 (m, 1H); 0.43 (m, 2H); 0.32 (m, 2H);
[0471] Ex. no. 1-184: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.72 (t, 1H); 7.81 (d, 1H); 7.68 (d, 1H); 3.99 (s, 3H); 3.21 (m, 2H); 1.55 (m, 2H); 0.94 (t, 3H);
[0472] Ex. no. 1-185: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.61 (d, 1H); 7.80 (d, 1H); 7.67 (d, 1H); 4.05 (m, 1H); 3.99 (s, 3H); 1.17 (d, 6H);
[0473] Ex. no. 1-186: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.86 (t, 1H); 7.80 (d, 1H); 7.68 (d, 1H); 3.99 (s, 3H); 3.47 (m, 2H); 3.41 (m, 2H); 3.28 (s, 3H);
[0474] Ex. no. 1-187: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.93 (t, 1H); 7.81 (d, 1H); 7.69 (d, 1H); 3.99 (s, 3H); 3.44 (m, 2H); 2.66 (m, 2H); 2.12 (s, 3H);
[0475] Ex. no. 1-195: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.86 (br s, 1H); 8.58 (q, 1H); 7.98 (d, 1H); 7.47 (d, 1H); 3.98 (s, 3H); 2.79 (d, 3H);
[0476] Ex. no. 1-196: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.85 (br s, 1H); 8.64 (t, 1H); 7.98 (d, 1H); 7.47 (d, 1H); 3.99 (s, 3H); 3.27 (m, 2H); 1.15 (t, 3H);
[0477] Ex. no. 1-197: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.86 (br s, 1H); 8.70 (d, 1H); 7.97 (d, 1H); 7.46 (d, 1H); 3.98 (s, 3H); 2.80 (m, 1H); 0.72 (m, 2H); 0.57 (br s, 2H);
[0478] Ex. no. 1-207: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.67 (q, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.03 (s, 3H); 2.79 (d, 3H);
[0479] Ex. no. 1-208: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.72 (t, 1H); 7.91 (d, 1H); 7.96 (d, 1H); 4.03 (s, 3H); 3.29 (m, 2H); 1.12 (t, 3H);
[0480] Ex. no. 1-209: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.00 (br s, 1H); 8.81 (d, 1H); 7.96 (d, 1H); 7.91 (d, 1H); 4.03 (s, 3H); 2.79 (m, 1H); 0.72 (m, 2H); 0.57 (m, 1H); 0.48 (m, 1H);
[0481] Ex. no. 1-210: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.99 (br s, 1H); 8.84 (t, 1H); 7.96 (d, 1H); 7.91 (d, 1H); 4.03 (s, 3H); 3.14 (m, 2H); 1.01 (m, 1H); 0.45 (m, 2H); 0.24 (m, 2H);
[0482] Ex. no. 1-211: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 9.52 (t, 1H); 8.01 (d, 1H); 7.97 (d, 1H); 4.20 (m, 1H); 4.08 (m, 1H); 4.04 (s, 3H);
[0483] Ex. no. 1-212: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 9.26 (t, 1H); 7.99 (d, 1H); 7.95 (d, 1H); 6.12 (tt, 1H); 4.03 (s, 3H); 3.70 (m, 2H);
[0484] Ex. no. 1-225: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.70 (q, 1H); 7.86 (d, 1H); 7.81 (d, 1H); 6.93 (t, 1H); 4.03 (s, 3H); 2.81 (d, 3H);
[0485] Ex. no. 1-226: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.77 (t, 1H); 7.86 (d, 1H); 7.81 (d, 1H); 6.93 (t, 1H); 4.03 (s, 3H); 3.29 (m, 2H); 1.14 (t, 3H);
[0486] Ex. no. 1-227: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.92 (br s, 1H); 8.83 (d, 1H); 7.85 (d, 1H); 7.80 (d, 1H); 6.93 (t, 1H); 4.02 (s, 3H); 2.83 (m, 1H); 0.71 (m, 2H); 0.57 (m, 2H);
[0487] Ex. no. 1-228: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 8.90 (t, 1H); 7.86 (d, 1H); 7.81 (d, 1H); 6.93 (t, 1H); 4.03 (s, 3H); 3.16 (m, 2H); 1.04 (m, 1H); 0.46 (m, 2H); 0.26 (m, 2H);
[0488] Ex. no. 1-229: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.96 (br s, 1H); 9.54 (t, 1H); 7.91 (d, 1H); 7.84 (d, 1H); 6.92 (t, 1H); 4.14 (m, 2H); 4.03 (s, 3H);
[0489] Ex. no. 1-230: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.95 (br s, 1H); 9.28 (t, 1H); 7.90 (d, 1H); 7.83 (d, 1H); 6.94 (t, 1H); 6.18 (tt, 1H); 4.03 (s, 3H); 3.72 (m, 2H);
[0490] Ex. no. 1-271: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 8.52 (q, 1H); 7.85 (d, 1H); 7.78 (d, 1H); 4.01 (s, 3H); 2.79 (d, 3H); 2.72 (m, 2H); 1.17 (t, 3H);
[0491] Ex. no. 1-272: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.80 (br s, 1H); 8.62 (t, 1H); 7.84 (d, 1H); 7.77 (d, 1H); 4.01 (s, 3H); 3.29 (q, 2H); 2.77 (m, 2H); 1.18 (t, 3H); 1.11 (t, 3H);
[0492] Ex. no. 1-273: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.68 (d, 1H); 7.84 (d, 1H); 7.76 (d, 1H); 4.01 (s, 3H); 2.81 (m, 2H) M 2.70 (m, 1H); 1.17 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0493] Ex. no. 1-274: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.80 (br s, 1H); 8.74 (t, 1H); 7.84 (d, 1H); 7.76 (d, 1H); 4.01 (s, 3H); 3.19 (m, 1H); 3.08 (m, 1H); 2.80 (m, 2H); 1.20 (t, 3H); 1.02 (m, 1H); 0.45 (m, 2H); 0.24 (m, 2H);
[0494] Ex. no. 1-276: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 9.10 (t, 1H); 7.88 (d, 1H); 7.79 (d, 1H); 6.13 (tt, 1H); 4.01 (s, 3H); 3.77 (m, 1H); 3.63 (m, 1H); 2.77 (m, 2H); 1.17 (t, 3H);
[0495] Ex. no. 1-277: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.73 (br s, 1H); 8.57 (q, 3H); 7.80 (d, 1H); 7.64 (d, 1H); 6.89 (t, 1H); 4.00 (s, 3H); 2.81 (d, 3H); 2.74 (q, 2H); 1.15 (t, 3H);
[0496] Ex. no. 1-278: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.72 (br s, 1H); 8.67 (t, 1H); 7.80 (d, 1H); 7.64 (d, 1H); 6.90 (t, 1H); 4.00 (s, 3H); 3.21 (m, 2H); 2.76 (q, 2H); 1.15 (2x t, 6H)
[0497] Ex. no. 1-279: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.72 (br s, 1H); 8.75 (d, 1H); 7.80 (d, 1H); 7.63 (d, 1H); 6.89 (t, 1H); 4.00 (s, 3H); 2.86 (m, 1H); 2.75 (m, 2H); 1.15 (t, 3H); 0.71 (m, 2H); 0.53 (m, 2H);
[0498] Ex. no. 1-286: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.44 (q, 1H); 7.77 (br s, 2H); 4.03 (s, 3H); 2.79 (d, 3H); 2.11 (m, 1H); 0.84 (m, 2H); 0.64 (m, 2H);
[0499] Ex. no. 1-287: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.51 (t, 1H); 7.77 (br s, 2H); 4.03 (s, 3H); 3.29 (m, 2H); 2.14 (m, 1H); 1.13 (t, 3H); 0.84 (m, 2H); 0.66 (m, 2H);
[0500] Ex. no. 1-288: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.59 (d, 1H); 7.77 (br s, 2H); 4.03 (s, 3H); 2.79 (m, 1H); 2.11 (m, 1H); 0.85 (m, 2H); 0.70 (m, 2H); 0.66 (m, 2H); 0.51 (m, 2H);
[0501] Ex. no. 1-289: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.63 (t, 1H); 7.77 (br s, 2H); 4.03 (s, 3H); 3.13 (m, 2H); 2.15 (m, 1H); 1.03 (m, 1H); 0.85 (m, 2H); 0.68 (m, 2H); 0.45 (m, 2H); 0.23 (m, 2H);
[0502] Ex. no. 1-291: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.72 (br s, 1H); 9.03 (t, 1H); 7.80 (br s, 2H); 6.13 (tt, 1H); 4.04 (s, 3H); 3.69 (m, 2H); 2.13 (m, 1H); 0.87 (m, 2H); 0.64 (m, 2H);
[0503] Ex. no. 1-292: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.55 (d, 1H); 7.76 (br s, 2H); 4.03 (s, 3H); 3.38 (m, 1H); 2.18 (m, 1H); 1.21 (d, 3H); 0.89 (m, 3H); 0.69 (m, 2H); 0.44 (m, 2H); 0.34 (m, 1H); 0.24 (m, 1H);
[0504] Ex. no. 1-304: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.64 (br s, 1H); 8.52 (q, 1H); 7.73 (d, 1H); 7.66 (d, 1H); 6.94 (t, 1H); 4.03 (s, 3H); 2.81 (d, 3H); 2.17 (m, 1H); 0.83 (m, 2H); 0.58 (m, 2H);
[0505] Ex. no. 1-305: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.62 (br s, 1H); 8.60 (t, 1H); 7.72 (d, 1H); 7.66 (d, 1H); 6.94 (t, 1H); 4.03 (s, 3H); 3.31 (m, 2H); 2.19 (m, 1H); 1.14 (t, 3H); 0.83 (m, 2H); 0.60 (m, 2H);
[0506] Ex. no. 1-306: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.61 (br s, 1H); 8.67 (d, 1H); 7.72 (d, 1H); 7.65 (d, 1H); 6.94 (t, 1H); 4.03 (s, 3H); 2.84 (m, 1H); 2.16 (m, 1H); 0.83 (m, 2H); 0.70 (m, 2H); 0.57 (m, 4H);
[0507] Ex. no. 1-337: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.03 (br s, 1H); 7.98 (br s, 2H); 4.02 (s, 3H); 3.91 (br s, 1H); 2.07 (br s, 3H);
[0508] Ex. no. 1-338: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.22 (s, 1H); 8.00 (s, 1H); 7.97 (d, 1H); 7.94 (d, 1H); 4.03 (s, 3H);
[0509] Ex. no. 1-339: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.70 (d, 1H); 7.79 (d, 1H); 7.64 (d, 1H); 6.90 (t, 1H); 4.00 (s, 3H); 3.45 (m, 1H); 2.38 (s, 3H); 1.22 (d, 3H); 0.93 (m, 1H); 0.46 (m, 2H); 0.35 (m, 1H); 0.28 (m, 1H);
[0510] Ex. no. 1-340: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 8.79 (d, 1H); 7.85 (d, 1H); 7.81 (d, 1H); 6.91 (t, 1H); 4.03 (s, 3H); 3.45 (m, 1H); 1.23 (d, 3H); 0.92 (m, 1H); 0.44 (m, 2H); 0.38 (m, 1H); 0.29 (m, 1H);
[0511] Ex. no. 1-341: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.66 (d, 1H); 7.83 (d, 1H); 7.76 (d, 1H); 4.01 (s, 3H); 3.40 (m, 1H); 2.84 (q, 2H); 2.78 (m, 1H); 1.22 (t, 3H); 1.17 (t, 3H); 0.91 (m, 1H); 0.43 (m, 2H); 0.29 (m, 2H);
[0512] Ex. no. 1-342: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.62 (q, 1H); 7.84 (d, 1H); 7.64 (d, 1H); 4.01 (s, 3H); 2.79 (d, 3H);
[0513] Ex. no. 1-343: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.68 (t, 1H); 7.83 (d, 1H); 7.63 (d, 1H); 4.01 (s, 3H); 3.28 (q, 2H); 1.14 (t, 3H);
[0514] Ex. no. 1-344: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 8.74 (d, 1H); 7.82 (d, 1H); 7.63 (d, 1H); 4.01 (s, 3H); 2.80 (m, 1H); 0.72 (m, 2H); 0.56 (m, 2H);
[0515] Ex. no. 1-345: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.67 (t, 1H); 7.79 (d, 1H); 7.64 (d, 1H); 6.90 (t, 1H); 4.00 (s, 3H); 3.24 (m, 2H); 2.36 (s, 3H); 1.54 (m, 2H); 0.91 (t, 3H);
[0516] Ex. no. 1-346: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.57 (d, 1H); 7.79 (d, 1H); 7.63 (d, 1H); 6.91 (t, 1H); 4.11 (m, 1H); 4.00 (s, 3H); 2.36 (s, 3H); 1.16 (d, 6H);
[0517] Ex. no. 1-347: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.74 (t, 1H); 7.79 (d, 1H); 7.62 (d, 1H); 6.93 (t, 1H); 4.00 (s, 3H); 3.47 (m, 4H); 3.28 (s, 3H); 2.36 (s, 3H);
[0518] Ex. no. 1-348: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.81 (t, 1H); 7.80 (d, 1H); 7.65 (d, 1H); 7.01 (t, 1H); 4.00 (s, 3H); 3.49 (m, 2H); 2.68 (m, 2H); 2.38 (s, 3H); 2.11 (s, 3H);
[0519] Ex. no. 1-349: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.65 (q, 1H); 7.73 (d, 1H); 7.70 (d, 1H); 4.01 (s, 3H); 2.79 (d, 3H);
[0520] Ex. no. 1-350: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.71 (t, 1H); 7.73 (d, 1H); 7.69 (d, 1H); 4.01 (s, 3H); 3.28 (m, 2H); 1.14 (t, 3H);
[0521] Ex. no. 1-351: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 8.77 (d, 1H); 7.72 (d, 1H); 7.68 (d, 1H); 4.01 (s, 3H); 2.80 (m, 1H); 0.72 (m, 2H); 0.55 (m, 2H);
[0522] Ex. no. 1-352: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.56 (d, 1H); 7.94 (d, 1H); 7.86 (d, 1H); 4.06 (s, 3H); 3.47 (m, 1H); 2.45 (s, 3H); 1.21 (d, 3H); 0.91 (m, 1H); 0.41 (m, 2H); 0.33 (m, 2H);
[0523] Ex. no. 1-353: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.65 (d, 1H); 7.82 (br s, 2H); 6.88 (t, 1H); 4.05 (s, 3H); 3.51 (m, 1H); 2.44 (s, 3H); 1.23 (d, 3H); 0.93 (m, 1H); 0.41 (m, 3H); 0.30 (m, 1H);
[0524] Ex. no. 1-354: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.35 (q, 1H); 7.74 (d, 1H); 7.19 (d, 1H); 3.97 (s, 3H); 3.85 (s, 3H); 2.74 (d, 3H);
[0525] Ex. no. 1-355: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.64 (br s, 1H); 8.41 (t, 1H); 7.74 (d, 1H); 7.18 (d, 1H); 3.97 (s, 3H); 3.85 (s, 3H); 3.24 (m, 2H); 1.10 (t, 3H);
[0526] Ex. no. 1-356: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.64 (br s, 1H); 8.48 (d, 1H); 7.73 (d, 1H); 7.18 (d, 1H); 3.97 (s, 3H); 3.85 (s, 3H); 2.79 (m, 1H); 0.68 (m, 2H); 0.49 (m, 2H);
[0527] Ex. no. 1-357: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.05 (br s, 1H); 11.93 (br s, 1H); 8.06 (d, 1H); 7.99 (d, 1H); 4.02 (s, 3H); 3.74 (s, 3H);
[0528] Ex. no. 1-358: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.04 (br s, 1); 11.81 (br s, 1H); 8.05 (d, 1H); 7.99 (d, 1H); 4.02 (s, 3H); 3.97 (m, 2H); 1.23 (t, 3H);
[0529] Ex. no. 1-359: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.04 (br s, 1H); 11.81 (br s, 1H); 8.05 (d, 1H); 7.98 (d, 1H); 4.02 (s, 3H); 3.88 (m, 2H); 1.64 (m, 2H); 0.94 (t, 3H);
[0530] Ex. no. 1-360: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.04 (br s, 1H); 11.65 (br s, 1H); 8.04 (d, 1H); 7.98 (d, 1H); 4.18 (m, 1H); 4.02 (s, 3H); 1.22 (d, 6H);
[0531] Ex. no. 1-361: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.98 (br s, 1H); 11.92 (br s, 1H); 7.98 (d, 1H); 7.81 (d, 1H); 7.04 (t, 1H); 4.01 (s, 3H); 3.76 (s, 3H);
[0532] Ex. no. 1-362: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.98 (br s, 1H); 11.81 (br s, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.02 (t, 1H); 4.01 (s, 3H); 3.99 (q, 2H); 1.23 (t, 3H);
[0533] Ex. no. 1-363: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.97 (br s, 1H); 11.81 (br s, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.02 (t, 1H); 4.01 (s, 3H); 3.90 (t, 2H); 1.64 (m, 2H); 0.94 (t, 3H);
[0534] Ex. no. 1-364: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.97 (br s, 1H); 11.67 (br s, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.01 (t, 1H); 4.21 (m, 1H); 4.01 (s, 3H); 1.23 (d, 6H);
[0535] Ex. no. 2-19: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 8.57 (q, 1H); 7.94 (d, 1H); 7.88 (d, 1H); 4.36 (q, 2H); 3.27 (s, 3H); 2.78 (d, 3H); 2.35 (s, 3H); 1.47 (t, 3H);
[0536] Ex. no. 2-20: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 8.63 (t, 1H); 7.94 (d, 1H); 7.87 (d, 1H); 4.35 (q, 2H); 3.27 (m, 2H); 3.27 (s, 3H); 2.37 (s, 3H); 1.47 (t, 3H); 1.13 (t, 3H);
[0537] Ex. no. 2-21: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.70 (d, 1H); 7.93 (d, 1H); 7.87 (d, 1H); 4.35 (q, 2H); 3.27 (s, 3H); 2.77 (m, 1H); 2.35 (s, 3H); 1.47 (t, 3H); 0.69 (m, 2H); 0.62 (m, 1H); 0.51 (m, 1H);
[0538] Ex. no. 2-25: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.51 (q, 1H) 7.82 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 2.79 (d, 3H); 2.33 (s, 3H); 1.47 (t, 3H);
[0539] Ex. no. 2-26: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.60 (t, 1H); 7.83 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 3.30 (m, 2H); 2.35 (s, 3H); 1.47 (t, 3H); 1.11 (t, 3H);
[0540] Ex. no. 2-27: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.64 (br s, 1H); 8.66 (d, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 4.35 (q, 2H); 2.81 (m, 1H); 2.34 (s, 3H); 1.47 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0541] Ex. no. 2-28: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.68 (br s, 1H); 8.72 (t, 1H); 7.82 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 3.13 (m, 2H); 2.38 (s, 3H); 1.47 (t, 3H); 1.01 (m, 1H); 0.45 (m, 2H); 0.23 (m, 2H);
[0542] Ex. no. 2-29: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 9.38 (t, 1H); 7.87 (d, 1H); 7.80 (d, 1H); 4.35 (q, 2H); 4.13 (m, 2H); 2.35 (s, 3H); 1.47 (t, 3H);
[0543] Ex. no. 2-30: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.68 (br s, 1H); 9.08 (t, 1H); 7.85 (d, 1H); 7.78 (d, 1H); 6.14 (tt, 1H); 4.35 (q, 2H); 3.70 (m, 2H); 2.36 (s, 3H); 1.47 (t, 3H);
[0544] Ex. no. 2-31: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.66 (br s, 1H); 0.62 (t, 1H); 7.81 (d, 1H); 7.75 (d, 1H); 4.35 (q, 2H); 3.40 (m, 1H); 2.39 (d, 3H); 1.48 (t, 3H); 1.20 (dd, 3H); 0.90 (m, 1H); 0.45 (m, 2H); 0.30 (m, 2H);
[0545] Ex. no. 2-32: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.67 (br s, 1H); 8.62 (t, 1H); 7.82 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 3.21 (m, 2H); 2.36 (s, 3H); 1.51 (m, 2H); 1.47 (t, 3H); 0.91 (t, 3H);
[0546] Ex. no. 2-33: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.50 (d, 1H); 7.81 (d, 1H); 7.75 (d, 1H); 4.35 (q, 2H); 4.09 (m, 1H); 2.36 (s, 3H); 1.47 (t, 3H); 1.16 (d, 3H); 1.12 (d, 3H);
[0547] Ex. no. 2-34: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.66 (br s, 1H); 8.70 (d, 1H); 4.35 (q, 2H); 3.52-3.30 (m, 4H); 3.27 (s, 3H); 2.36 (s, 3H); 1.47 (t, 3H);
[0548] Ex. no. 2-35: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.78 (t, 1H); 7.83 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 3.50 (m, 1H); 3.40 (m, 1H); 2.64 (m, 2H); 2.39 (s, 3H); 2.11 (s, 3H); 1.47 (t, 3H);
[0549] Ex. no. 2-36: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 9.42 (t, 1H); 7.89 (d, 1H); 7.81 (d, 1H); 4.49 (m, 2H); 4.36 (q, 2H); 2.35 (s, 3H); 1.47 (t, 3H);
[0550] Ex. no. 2-37: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.67 (br s, 1H); 8.72 (br s, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 4.37 (q, 2H); 3.96 (m, 1H); 3.77 (m, 1H); 3.62 (m, 1H); 3.37 (m, 1H); 3.27 (m, 1H); 2.36 (s, 3H); 1.94 (m, 1H); 1.82 (m, 2H); 1.60 (m, 1H); 1.47 (t, 3H);
[0551] Ex. no. 2-42: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.66 (br s, 1H); 8.85 (d, 1H); 7.82 (d, 1H); 7.76 (d, 1H); 4.37 (m, 1H); 4.35 (q, 2H); 2.34 (s, 3H); 2.24 (m 2H); 1.97 (m, 2H); 1.69 (m, 2H); 1.47 (t, 3H);
[0552] Ex. no. 2-44: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.56 (q, 1H); 7.79 (d, 1H); 7.64 (d, 1H); 6.91 (t, 1H); 4.34 (q, 2H); 2.81 (d, 3H); 2.33 (s, 3H); 1.47 (t, 3H);
[0553] Ex. no. 2-45: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.65 (t, 1H); 7.78 (d, 1H); 7.64 (d, 1H); 6.91 (t, 1H); 4.34 (q, 2H); 3.31 (m, 2H); 2.35 (s, 3H); 1.47 (t, 3H); 1.13 (t, 3H);
[0554] Ex. no. 2-46: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.71 (d, 1H); 7.78 (d, 1H); 7.63 (d, 1H); 6.91 (t, 1H); 4.34 (q, 2H); 2.85 (m, 1H); 2.33 (s, 3H); 1.47 (t, 3H); 0.71 (m, 2H); 0.53 (m, 2H);
[0555] Ex. no. 2-47: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.79 (t, 1H); 7.79 (d, 1H); 7.64 (d, 1H); 6.92 (t, 1H); 4.35 (q, 2H); 3.16 (m, 2H); 2.38 (s, 3H); 1.47 (t, 3H); 1.05 (m, 1H); 0.46 (m, 2H); 0.24 (m, 2H);
[0556] Ex. no. 2-49: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.60 (br s, 1H); 9.12 (t, 1H); 7.82 (d, 1H); 7.66 (d, 1H); 6.93 (t, 1H); 6.19 (tt, 1H); 4.35 (q, 2H); 3.72 (m, 2H); 2.36 (s, 3H); 1.47 (t, 3H);
[0557] Ex. no. 2-56: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.56 (br s, 1H); 8.53 (q, 1H); 7.88 (d, 1H); 7.67 (d, 1H); 4.34 (q, 2H); 3.86 (s, 3H); 2.79 (d, 3H); 1.47 (t, 3H);
[0558] Ex. no. 2-57: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.54 (br s, 1H); 8.61 (t, 1H); 7.88 (d, 1H); 7.67 (d, 1H); 4.34 (q, 2H); 3.88 (s, 3H); 3.28 (m, 2H); 1.47 (t, 3H); 1.11 (t, 3H);
[0559] Ex. no. 2-58: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.54 (br s, 1H); 8.68 (d, 1H); 7.87 (d, 1H); 7.66 (d, 1H); 4.34 (q, 2H); 3.87 (s, 3H); 2.80 (m, 1H); 1.47 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0560] Ex. no. 2-72: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.42 (br s, 1H); 8.58 (q, 1H); 7.84 (d, 1H); 7.54 (d, 1H); 6.96 (t, 1H); 4.34 (q, 2H); 3.85 (s, 3H); 2.81 (d, 3H); 1.47 (t, 3H);
[0561] Ex. no. 2-73: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.42 (br s, 1H); 8.65 (t, 1H); 7.84 (d, 1H); 7.54 (d, 1H); 6.96 (t, 1H); 4.34 (q, 2H); 3.86 (s, 3H); 3.30 (m, 2H); 1.47 (t, 3H); 1.13 (t, 3H);
[0562] Ex. no. 2-74: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.40 (br s, 1H); 8.72 (d, 1H); 7.83 (d, 1H); 7.53 (d, 1H); 6.95 (t, 1H); 4.33 (q, 2H); 3.85 (s, 3H); 2.85 (m, 1H); 1.47 (t, 3H); 0.72 (m, 2H); 0.55 (m, 2H);
[0563] Ex. no. 2-81: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 8.48 (q, 1H); 7.95 (d, 1H); 7.86 (d, 1H); 4.43 (q, 2H); 2.80 (d, 3H); 2.43 (s, 3H); 1.48 (t, 3H);
[0564] Ex. no. 2-82: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.70 (br s, 1H); 8.56 (t, 1H); 7.94 (d, 1H); 7.86 (d, 1H); 4.43 (q, 2H); 3.30 (m, 2H); 2.44 (s, 3H); 1.48 (t, 3H); 1.13 (s, 3H);
[0565] Ex. no. 2-83: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.72 (br s, 1H); 8.64 (d, 1H); 7.94 (d, 1H); 7.86 (d, 1H); 4.43 (q, 2H); 2.80 (m, 1H); 2.43 (s, 3H); 1.48 (t, 3H); 0.71 (m, 2H); 0.53 (br s, 2H);
[0566] Ex. no. 2-84: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 8.68 (t, 1H); 7.95 (d, 1H); 7.86 (d, 1H); 4.44 (q, 2H); 3.16 (m, 2H); 2.45 (s, 3H); 1.47 (t, 3H); 1.02 (m, 1H); 0.45 (m, 2H); 0.25 (m, 2H);
[0567] Ex. no. 2-86: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.73 (br s, 1H); 9.10 (t, 1H); 7.98 (d, 1H); 7.91 (d, 1H); 6.12 (tt, 1H); 4.43 (q, 2H); 3.71 (m, 2H); 2.43 (s, 3H); 1.49 (t, 3H);
[0568] Ex. no. 2-87: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.55 (q, 1H); 7.81 (s, 2H); 6.91 (t, 1H); 4.43 (q, 2H); 2.83 (d, 3H); 2.42 (s. 3H); 1.49 (t 3H);
[0569] Ex. no. 2-88: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.62 (t, 1H); 7.81 (s, 2H); 6.90 (t, 1H); 4.43 (q, 2H); 3.32 (m, 2H); 2.43 (s, 3H); 1.48 (t, 3H); 1.15 (t, 3H);
[0570] Ex. no. 2-89: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.70 (d, 1H); 7.80 (br s, 2H); 6.90 (t, 1H); 4.43 (q, 2H); 2.85 (m, 1H); 2.41 (s, 3H); 1.48 (t, 3H); 0.72 (m, 2H); 0.57 (m, 2H);
[0571] Ex. no. 2-90: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.66 (br s, 1H); 8.76 (t, 1H); 7.83 (m, 2H); 6.91 (t, 1H); 4.43 (q, 2H); 3.19 (m, 2H); 2.44 (s, 3H); 1.49 (t, 3H); 1.06 (m, 1H); 0.46 (m, 2H); 0.26 (m, 2H);
[0572] Ex. no. 2-92: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.68 (br s, 1H); 9.14 (t, 1H); 7.84 (br s, 2H); 6.92 (t, 1H); 6.18 (tt, 1H); 4.43 (q, 2H); 3.73 (m, 2H); 2.42 (s, 3H); 1.48 (t, 3H);
[0573] Ex. no. 2-123: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.92 (br s, 1H); 8.73 (q, 1H); 8.07 (d, 1H); 8.02 (d, 1H); 4.37 (q, 2H); 2.79 (d, 3H); 1.47 (t, 3H);
[0574] Ex. no. 2-125: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.85 (d, 1H); 8.05 (d, 1H); 8.02 (d, 1H); 4.37 (q, 2H); 3.31 (s, 3H); 2.77 (m, 1H); 1.47 (t, 3H); 0.69 (m, 2H); 0.58 (m, 2H);
[0575] Ex. no. 2-129: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.70 (q, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.37 (q, 2H); 2.79 (d, 3H); 1.47 (t, 3H);
[0576] Ex. no. 2-130: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.76 (t, 1H); 7.96 (d, 1H); 7.93 (d, 1H); 4.37 (q, 2H); 3.28 (m, 2H); 1.47 (t, 3H); 1.12 (t, 3H);
[0577] Ex. no. 2-131: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.83 (d, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.37 (q, 2H); 2.80 (m, 1H); 1.47 (t, 3H); 0.72 (m, 2H); 0.50 (br s, 2H);
[0578] Ex. no. 2-132: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.89 (t, 1H); 7.97 (d, 1H); 7.93 (d, 1H); 4.38 (q, 2H); 3.15 (m, 3H); 1.47 (t, 3H); 0.46 (m, 2H); 0.23 (m, 2H);
[0579] Ex. no. 2-133: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.96 (br s, 1H); 9.56 (t, 1H); 8.03 (d, 1H); 7.98 (d, 1H); 4.38 (q, 2H); 4.15 (m, 2H); 1.47 (t, 3H);
[0580] Ex. no. 2-134: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 9.29 (t, 1H); 8.01 (d, 1H); 7.96 (d, 1H); 6.12 (tt, 1H); 4.38 (q, 2H); 3.71 (m, 2H); 1.47 (t, 3H);
[0581] Ex. no. 2-135: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.77 (d, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.38 (q, 2H); 3.43 (m, 1H); 1.48 (t, 3H); 1.20 (m, 3H); 0.90 (m, 1H); 0.43 (m, 2H); 0.30 (m, 2H);
[0582] Ex. no. 2-138: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.91 (t, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.38 (q, 2H); 3.45 (m, 4H); 3.27 (s, 3H); 1.47 (t, 3H);
[0583] Ex. no. 2-139: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.99 (t, 1H); 7.98 (d, 1H); 7.93 (d, 1H); 4.38 (q, 2H); 3.45 (m, 2H); 2.63 (t, 2H); 2.11 (s, 3H); 1.47 (t, 3H);
[0584] Ex. no. 2-141: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.90 (t, 1H); 7.96 (d, 1H); 7.92 (d, 1H); 4.37 (q, 2H); 3.96 (m, 1H); 3.78 (m, 1H); 3.65 (m, 1H); 3.32 (br s, 2H); 1.93 (m, 1H); 1.83 (m, 2H); 1.62 (m, 1H); 1.47 (t, 3H);
[0585] Ex. no. 2-142: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.90 (t, 1H); 7.95 (d, 1H); 7.90 (d, 1H); 4.37 (q, 2H); 4.18 (br d, 2H); 3.00 (s, 3H); 2.86 (s, 3H); 1.47 (t, 3H);
[0586] Ex. no. 2-143: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.98 (br s, 1H); 10.88 (br s, 1H); 8.06 (d, 1H); 8.02 (d, 1H); 7.65 (d, 2H); 7.38 (t, 2H); 7.16 (t, 1H); 4.38 (q, 2H); 1.47 (t, 3H);
[0587] Ex. no. 2-144: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 9.37 (t, 1H); 7.98 (d, 1H); 7.93 (d, 1H); 7.45 (m, 1H); 7.07 (m, 1H); 6.99 (m, 1H); 4.66 (br s, 2H); 4.37 (q, 2H); 1.47 (t, 3H);
[0588] Ex. no. 2-146: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.61 (br s, 1H); 7.74 (d, 1H); 7.71 (d, 1H); 4.62 (m, 1H); 4.57 (q, 2H); 2.46 (m, 2H); 2.19 (m, 2H); 1.82 (m, 2H); 1.62 (t, 3H);
[0589] Ex. no. 2-147: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.83 (br s, 1H); 8.72 (q, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.96 (t, 1H); 4.37 (q, 2H); 2.81 (d, 3H); 1.47 (t, 3H);
[0590] Ex. no. 2-148: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.79 (t, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.96 (t, 1H); 4.37 (q, 2H); 3.31 (m, 2H); 1.47 (t, 3H); 1.13 (t, 3H);
[0591] Ex. no. 2-149: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.85 (d, 1H); 7.89 (d, 1H); 7.77 (d, 1H); 6.95 (t, 1H); 4.37 (q, 2H); 2.84 (m, 1H); 1.47 (t, 3H); 0.72 (m, 2H); 0.55 (m, 2H);
[0592] Ex. no. 2-154: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 8.81 (t, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.95 (t, 1H); 4.37 (q, 2H); 3.24 (m, 2H); 1.54 (m, 2H); 1.47 (t, 3H); 0.92 (t, 3H);
[0593] Ex. no. 2-155: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.83 (br s, 1H); 8.70 (d, 1H); 7.89 (d, 1H); 7.77 (d, 1H); 6.95 (t, 1H); 4.37 (q, 2H); 4.09 (m, 1H); 1.47 (t, 3H); 1.16 (d, 6H);
[0594] Ex. no. 2-156: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 8.93 (t, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.93 (t, 1H); 4.37 (q, 2H); 3.47 (m, 4H); 3.29 (s, 3H); 1.47 (t, 3H);
[0595] Ex. no. 2-157: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.85 (br s, 1H); 8.99 (t, 1H); 7.92 (d, 1H); 7.80 (d, 1H); 7.05 (t, 1H); 4.37 (q, 2H); 3.49 (m, 2H); 2.67 (m, 2H); 2.12 (s, 3H); 1.47 (t, 3H);
[0596] Ex. no. 2-158: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 9.59 (t, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.01 (t, 1H); 4.37 (m, 4H); 1.47 (t, 3H);
[0597] Ex. no. 2-159: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 8.94 (t, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.98 (t, 1H); 4.37 (q, 2H); 3.99 (m, 1H); 3.78 (m, 1H); 3.65 (m, 1H); 3.35 (m, 2H); 1.94 (m, 1H); 1.84 (m, 2H); 1.62 (m, 1H); 1.47 (t, 3H);
[0598] Ex. no. 2-160: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 9.12 (t, 1H); 7.93 (d, 1H); 7.83 (d, 1H); 7.58 (t, 1H); 4.37 (q, 2H); 4.17 (d, 2H); 3.02 (s, 3H); 2.89 (s, 3H); 1.47 (t, 3H);
[0599] Ex. no. 2-161: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 10.84 (br s, 1H); 7.98 (d, 1H); 7.85 (d, 1H); 7.69 (m, 2H); 7.38 (m, 2H); 7.16 (m, 1H); 7.12 (t, 1H); 4.38 (q, 2H); 1.48 (t, 3H);
[0600] Ex. no. 2-162: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.85 (br s, 1H); 9.45 (t, 1H); 7.92 (d, 1H); 7.79 (d, 1H); 7.45 (m, 1H); 7.07 (m, 1H); 6.99 (m, 1H); 6.92 (t, 1H); 4.68 (d, 2H); 4.36 (q, 2H); 1.47 (t, 3H);
[0601] Ex. no. 2-164: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 9.05 (d, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 6.93 (t, 1H); 4.37 (m, 3H); 2.25 (m, 2H); 2.01 (m, 2H); 1.71 (m, 2H); 1.47 (t, 3H);
[0602] Ex. no. 2-173: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.79 (d, 1H); 7.76 (d, 1H); 7.66 (d, 1H); 4.35 (q, 2H); 2.82 (m, 1H); 1.47 (t, 3H); 0.73 (m, 2H); 0.53 (m, 2H);
[0603] Ex. no. 2-177: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.65 (d, 1H); 7.81 (d, 1H); 7.68 (d, 1H); 4.35 (q, 2H); 2.79 (d, 3H); 1.46 (t, 3H);
[0604] Ex. no. 2-178: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.71 (t, 1H); 7.81 (d, 1H); 7.67 (d, 1H); 4.35 (q, 1H); 3.28 (m, 2H); 1.46 (t, 3H); 1.14 (t, 3H);
[0605] Ex. no. 2-179: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.77 (d, 1H); 7.80 (d, 1H); 7.67 (d, 1H); 4.35 (q, 2H); 2.81 (m, 1H); 1.46 (t, 3H); 0.72 (m, 2H); 0.54 (m, 2H);
[0606] Ex. no. 2-180: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.80 (t, 1H); 7.81 (d, 1H); 7.67 (d, 1H); 4.35 (q, 2H); 3.16 (m, 2H); 1.46 (t, 3H); 1.02 (m, 1H); 0.46 (m, 2H); 0.26 (m, 2H);
[0607] Ex. no. 2-181: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 9.50 (t, 1H); 7.85 (d, 1H); 7.73 (d, 1H); 4.35 (q, 2H); 4.13 (m, 2H); 1.46 (t, 3H);
[0608] Ex. no. 2-182: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 9.23 (t, 1H); 7.83 (d, 1H); 7.71 (d, 1H); 6.14 (tt, 1H); 4.35 (q, 2H); 3.70 (m, 2H); 1.46 (t, 3H);
[0609] Ex. no. 2-183: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.79 (br s, 1H); 8.67 (d, 1H); 7.80 (d, 1H); 7.66 (d, 1H); 4.35 (q, 2H); 3.49 (m, 1H); 1.47 (t, 3H); 1.22 (d, 3H); 0.92 (m, 1H); 0.43 (m, 2H); 0.32 (m, 2H);
[0610] Ex. no. 2-184: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.72 (t, 1H); 7.81 (d, 1H); 7.67 (d, 1H); 4.35 (q, 2H); 3.22 (m, 2H); 1.56 (m, 2H); 1.46 (t, 3H); 0.94 (t, 3H);
[0611] Ex. no. 2-185: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 7.80 (d, 1H); 7.66 (d, 1H); 4.35 (q, 2H); 4.06 (m, 1H); 1.46 (t, 3H); 1.17 (d, 6H);
[0612] Ex. no. 2-186: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.78 (br s, 1H); 8.86 (t, 1H); 7.80 (d, 1H); 7.67 (d, 1H); 4.35 (q, 2H); 3.48 (m, 2H); 3.41 (m, 2H); 3.28 (s, 3H); 1.46 (s, 3H);
[0613] Ex. no. 2-187: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.80 (br s, 1H); 8.93 (t, 1H); 7.81 (d, 1H); 7.69 (d, 1H); 4.35 (q, 2H); 3.44 (m, 2H); 2.67 (m, 2H); 2.09 (s, 3H); 1.46 (t, 3H);
[0614] Ex. no. 2-195: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.74 (br s, 1H); 8.58 (q, 1H); 7.98 (d, 1H); 7.46 (d, 1H); 4.34 (q, 2H); 2.79 (d, 3H); 1.45 (t, 3H);
[0615] Ex. no. 2-196: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.75 (br s, 1H); 8.64 (t, 1H); 7.98 (d, 1H); 7.46 (d, 1H); 4.34 (q, 2H); 3.27 (m, 2H); 1.46 (t, 3H); 1.15 (t, 3H);
[0616] Ex. no. 2-197: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.72 (br s, 1H); 8.70 (d, 1H); 7.97 (d, 1H); 7.45 (d, 1H); 4.34 (q, 2H); 2.79 (m, 1H); 1.45 (t, 3H); 0.72 (m, 2H); 0.57 (br s, 2H);
[0617] Ex. no. 2-207: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.67 (q, 1H); 7.96 (d, 1H); 7.91 (d, 1H); 4.39 (q, 2H); 2.79 (d, 3H); 1.48 (t, 3H);
[0618] Ex. no. 2-208: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.73 (t, 1H); 7.95 (d, 1H); 7.90 (d, 1H); 4.39 (q, 2H); 3.29 (m, 2H); 1.48 (t, 3H); 1.12 (t, 3H);
[0619] Ex. no. 2-210: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.84 (t, 1H); 7.96 (d, 1H); 7.90 (d, 1H); 4.40 (q, 2H); 3.14 (m, 2H); 1.48 (t, 3H); 1.01 (m, 1H); 0.46 (m, 2H); 0.24 (m, 2H);
[0620] Ex. no. 2-211: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 9.52 (t, 1H); 8.00 (d, 1H); 7.96 (d, 1H); 4.40 (q, 2H); 4.19 (m, 1H); 4.08 (m, 1H); 1.48 (t, 3H);
[0621] Ex. no. 2-212: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 9.26 (t, 1H); 7.99 (d, 2H); 7.94 (d, 1H); 6.12 (tt, 1H); 4.40 (q, 2H); 3.70 (m, 2H); 1.48 (t, 3H);
[0622] Ex. no. 2-213: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 8.73 (t, 1H); 7.95 (d, 1H); 4.40 (q, 2H); 3.42 (m, 1H); 1.48 (t, 3H); 1.24 and 1.18 (2x d, 3H); 0.90 (m, 1H); 0.33 (m, 4H);
[0623] Ex. no. 2-225: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.70 (q, 1H); 7.85 (d, 1H); 7.81 (d, 1H); 6.94 (t, 1H); 4.39 (q, 2H); 2.81 (d, 3H); 1.47 (t, 3H);
[0624] Ex. no. 2-226: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.77 (t, 1H); 7.85 (d, 1H); 7.81 (d, 1H); 6.93 (t, 1H); 4.39 (q, 2H); 3.30 (m, 2H); 1.48 (t, 3H); 1.14 (t, 3H);
[0625] Ex. no. 2-227: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 8.83 (d, 1H); 7.84 (d, 1H); 7.80 (d, 1H); 6.93 (t, 1H); 4.39 (q, 2H); 2.83 (m, 1H); 1.47 (t, 3H); 0.72 (m, 2H); 0.57 (m, 2H);
[0626] Ex. no. 2-228: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 8.90 t, 1H); 7.85 (d, 1H); 7.81 (d, 1H); 6.93 (t, 1H); 4.39 (q, 2H); 3.16 (t, 2H); 1.48 (t, 3H); 1.04 (m, 1H); 0.48 (m, 2H); 0.25 (m, 2H);
[0627] Ex. no. 2-229: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.84 (br s, 1H); 9.54 (t, 1H); 7.90 (d, 1H); 7.84 (d, 1H); 6.93 (t, 1H); 4.39 (q, 2H); 4.14 (m, 2H); 1.48 (t, 3H);
[0628] Ex. no. 2-230: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.83 (br s, 1H); 9.28 (t, 1H); 7.89 (d, 1H); 7.83 (d, 1H); 6.94 (t, 1H); 6.18 (tt, 1H); 4.39 (q, 2H); 3.72 (m, 2H); 1.48 (t, 3H);
[0629] Ex. no. 2-271: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.53 (q, 1H); 7.84 (d, 1H); 7.77 (d, 1H); 4.36 (q, 2H); 2.79 (d, 3H); 2.69 (m, 2H); 1.48 (t, 3H); 1.17 (t, 3H);
[0630] Ex. no. 2-272: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.69 (br s, 1H); 8.62 (t, 1H); 7.83 (d, 1H); 7.77 (d, 1H); 4.36 (q, 2H); 3.29 (m, 2H); 2.77 (m, 2H); 1.48 (t, 3H); 1.18 (t, 3H); 1.11 (t, 3H);
[0631] Ex. no. 2-273: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.67 (br s, 1H); 8.67 (d, 1H); 7.82 (d, 1H); 7.76 (d, 1H); 4.35 (q, 2H); 2.80 (m, 2H); 2.70 (m, 1H); 1.47 (t, 3H); 1.17 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0632] Ex. no. 2-276: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 9.10 (t, 1H); 7.86 (d, 1H); 7.79 (d, 1H); 6.13 (tt, 1H); 4.36 (q, 2H); 3.78 (m, 1H); 3.63 (m, 1H); 2.77 (m, 2H); 1.48 (t, 3H); 1.17 (t, 3H);
[0633] Ex. no. 2-277: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.62 (br s, 1H); 8.58 (q, 1H); 7.79 (d, 1H); 7.65 (d, 1H); 6.90 (t, 1H); 4.35 (q, 2H); 2.81 (d, 3H); 2.74 (q, 2H); 1.47 (t, 3H); 1.15 (t, 3H);
[0634] Ex. no. 2-278: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.61 (br s, 1H); 8.67 (t, 1H); 7.79 (d, 1H); 7.65 (d, 1H); 6.90 (t, 1H); 4.35 (q, 2H); 3.31 (m, 2H); 2.76 (q, 2H); 1.48 (t, 3H); 1.15 (2x t, 6H);
[0635] Ex. no. 2-279: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.60 (br s, 1H); 8.74 (d, 1H); 7.78 (d, 1H); 7.64 (d, 1H); 6.89 (t, 1H); 4.35 (q, 2H); 2.86 (m, 1H); 2.73 (m, 2H); 1.47 (t, 3H); 1.15 (t, 3H); 0.72 (m, 2H); 0.53 (m, 2H);
[0636] Ex. no. 2-286: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.45 (q, 1H); 7.77 (br s, 2H); 4.38 (q, 2H); 2.79 (d, 3H); 2.11 (m, 1H); 1.48 (t, 3H); 0.84 (m, 2H); 0.64 (m, 2H);
[0637] Ex. no. 2-287: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.51 (t, 1H); 7.77 (br s, 2H); 4.38 (q, 2H); 3.29 (m, 2H); 2.14 (m, 1H); 1.48 (t, 3H); 1.13 (t, 3H); 0.84 (m, 2H); 0.67 (m, 2H);
[0638] Ex. no. 2-288: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.59 (d, 1H); 7.76 (br s, 2H); 4.37 (q, 2H); 2.79 (m, 1H); 2.12 (m, 1H); 1.48 (t, 3H); 0.85 (m, 2H); 0.70 (m, 2H); 0.66 (m, 2H); 0.51 (br s, 2H);
[0639] Ex. no. 2-289: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.64 (t, 1H); 7.77 (br s, 2H); 4.38 (q, 2H); 3.13 (m, 2H); 2.15 (m, 1H); 1.49 (t, 3H); 1.03 (m, 1H); 0.86 (m, 2H); 0.68 (m, 2H); 0.45 (m, 2H); 0.23 (m, 2H);
[0640] Ex. no. 2-291: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.60 (br s, 1H); 9.03 (t, 1H); 7.80 (br s, 2H); 6.13 (tt, 1H); 4.38 (q, 2H); 3.69 (m, 2H); 2.13 (m, 1H); 1.49 (t, 3H); 0.87 (m, 2H); 0.65 (m, 2H);
[0641] Ex. no. 2-292: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.55 (d, 1H); 7.76 (br s, 2H); 4.38 (q, 2H); 3.37 (m, 1H); 2.17 (m, 1H); 1.49 (t, 3H); 1.20 (br s, 3H); 0.89 (m, 3H); 0.70 (br s, 2H); 0.45 (m, 2H); 0.24 (m, 1H);
[0642] Ex. no. 2-304: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.52 (br s, 1H); 8.53 (q, 1H); 7.72 (d, 1H); 7.66 (d, 1H); 6.94 (t, 1H); 4.37 (q, 2H); 2.81 (d, 3H); 2.16 (m, 1H); 1.49 (t, 3H); 0.83 (m, 2H); 0.58 (m, 2H);
[0643] Ex. no. 2-305: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.52 (br s, 1H); 8.61 (t, 1H); 7.72 (d, 1H); 7.66 (d, 1H); 6.95 (t, 1H); 4.38 (q, 2H); 2.32 (q, 2H); 2.19 (m, 1H); 1.49 (t, 3H); 1.14 (3H); 0.83 (m, 2H); 0.61 (m, 2H);
[0644] Ex. no. 2-306: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.51 (br s, 1H); 8.68 (d, 1H); 7.72 (d, 1H); 7.65 (d, 1H); 6.94 (t, 1H); 4.37 (q, 2H); 2.85 (m, 1H); 2.16 (m, 1H); 1.48 (t, 3H); 0.83 (m, 2H); 0.71 (m, 2H); 0.58 (m, 4H);
[0645] Ex. no. 2-337: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 7.98 (br s, 2H); 4.37 (q, 2H); 3.81 (br s, 1H); 2.07 (br s, 3H); 1.47 (t, 3H);
[0646] Ex. no. 2-338: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 8.22 (s, 1H); 8.00 (s, 1H); 7.96 (d, 1H); 7.93 (d, 1); 4.39 (q, 2H); 1.49 (t, 3H);
[0647] Ex. no. 2-339: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.70 (d, 1H); 7.78 (d, 1H); 7.64 (d, 1H); 6.91 (t, 1H); 4.35 (q, 2H); 3.45 (m, 1H); 2.38 (s, 3H); 1.47 (t, 3H); 1.22 (d, 3H); 0.93 (m, 1H); 0.45 (m, 2H); 0.35 (m, 1H); 0.27 (m, 1H);
[0648] Ex. no. 2-340: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.81 (br s, 1H); 8.79 (d, 1H); 7.84 (d, 1H); 7.81 (d, 1H); 6.91 (t, 1H); 4.39 (q, 2H); 3.45 (m, 1H); 1.48 (s, 3H); 1.23 (d, 3H); 0.93 (m, 1H); 0.44 (m, 2H); 0.38 (m, 1H); 0.29 (m, 1H);
[0649] Ex. no. 2-341: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.68 (br s, 1H); 8.67 (d, 1H); 7.82 (d, 1H); 7.76 (d, 1H); 4.36 (q, 2H); 3.40 (m, 1H); 2.82 (q, 2H); 2.78 (m, 1H); 1.48 (t, 3H); 1.22 (t, 3H); 1.19 (t, 3H); 0.91 (m, 1H); 0.45 (m, 2H); 0.29 (m, 2H);
[0650] Ex. no. 2-342: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.68 (t, 1H); 7.83 (d, 1H); 7.62 (d, 1H); 4.37 (q, 2H); 3.28 (m, 2H); 1.47 (s, 3H); 1.14 (t, 3H);
[0651] Ex. no. 2-343: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.75 (br s, 1H); 8.74 (d, 1H); 7.82 (d, 1H); 7.61 (d, 1H); 4.37 (q, 2H); 2.79 (m, 1H); 1.47 (t, 3H); 0.72 (m, 2H); 0.56 (m, 2H);
[0652] Ex. no. 2-344: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.67 (t, 1H); 7.79 (d, 1H); 7.64 (d, 1H); 6.90 (t, 1H); 4.35 (q, 2H); 3.24 (m, 2H); 2.35 (s, 3H); 1.54 (m, 2H); 1.47 (t, 3H); 0.92 (t, 3H);
[0653] Ex. no. 2-345: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.58 (br s, 1H); 8.56 (d, 1H); 7.78 (d, 1H); 7.63 (d, 1H); 6.91 (t, 1H); 4.34 (q, 2H); 4.11 (m, 1H); 2.36 (s, 3H); 1.47 (t, 3H); 1.16 (d, 6H);
[0654] Ex. no. 2-346: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.74 (t, 1H); 7.78 (d, 1H); 7.64 (d, 1H); 6.93 (t, 1H); 4.35 (q, 2H); 3.47 (m, 4H); 3.28 (s, 3H); 2.35 (s, 3H); 1.47 (t, 3H);
[0655] Ex. no. 2-347: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.59 (br s, 1H); 8.81 (t, 1H); 7.79 (d, 1H); 7.65 (d, 1H); 7.01 (t, 1H); 4.35 (q, 2H); 3.49 (m, 2H); 2.68 (m, 2H); 2.38 (s, 3H); 2.11 (s, 3H); 1.47 (t, 3H);
[0656] Ex. no. 2-348: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.77 (br s, 1H); 8.71 (t, 1H); 7.72 (d, 1H); 7.69 (d, 1H); 4.37 (q, 2H); 3.28 (m, 2H); 1.47 (t, 3H); 1.14 (t, 3H);
[0657] Ex. no. 2-349: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.76 (br s, 1H); 8.77 (d, 1H); 7.71 (d, 1H); 7.68 (d, 1H); 4.37 (q, 2H); 2.80 (m, 2H); 1.47 (t, 3H); 0.72 (m, 2H); 0.54 (m, 2H);
[0658] Ex. no. 2-350: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.71 (br s, 1H); 8.57 (d, 1H); 7.94 (d, 1H); 7.85 (d, 1H); 4.44 (q, 2H); 3.47 (m, 1H); 2.46 (s, 3H); 1.49 (t, 3H); 1.21 (d, 3H); 0.91 (m, 1H); 0.42 (m, 2H); 0.33 (m, 2H);
[0659] Ex. no. 2-351: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.66 (d, 1H); 7.83 (d, 1H); 7.79 (d, 1H); 6.89 (t, 1H); 4.44 (q, 2H); 3.51 (m, 1H); 2.45 (s, 3H); 1.49 (t, 3H); 1.23 (d, 3H); 0.93 (m, 1H); 0.30 (m, 2H);
[0660] Ex. no. 2-352: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.54 (br s, 1H); 8.35 (q, 1H); 7.73 (d, 1H); 7.19 (d, 1H); 7.33 (m, 2H); 3.85 (s, 3H); 2.74 (d, 3H); 1.45 (t, 3H);
[0661] Ex. no. 2-353: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.53 (br s, 1H); 8.41 (t, 1H); 7.72 (d, 1H); 7.18 (d, 1H); 4.33 (q, 2H); 3.85 (s, 3H); 3.24 (m, 2H); 1.46 (t, 3H); 1.10 (t, 3H);
[0662] Ex. no. 2-354: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.53 (br s, 1H); 8.48 (d, 1H); 7.72 (d, 1H); 7.18 (d, 1H); 4.33 (q, 2H); 3.85 (s, 3H); 2.80 (m, 1H); 1.47 (t, 3H); 0.69 (m, 2H); 0.48 (m, 2H);
[0663] Ex. no. 2-357: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 11.93 (br s, 1H); 8.05 (d, 1H); 7.99 (d, 1H); 4.38 (q, 2H); 3.74 (s, 3H); 1.47 (t, 3H);
[0664] Ex. no. 2-358: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.94 (br s, 1H); 11.81 (br s, 1H); 8.04 (d, 1H); 7.98 (d, 1H); 4.38 (q, 2H); 3.97 (m, 2H); 1.48 (t, 3H); 1.23 (t, 3H);
[0665] Ex. no. 2-359: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 11.81 (br s, 1H); 8.04 (d, 1H); 7.98 (d, 1H); 4.38 (q, 2H); 3.88 (m, 2H); 1.64 (m, 2H); 1.47 (t, 3H); 0.94 (t, 3H);
[0666] Ex. no. 2-360: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.93 (br s, 1H); 11.65 (br s, 1H); 8.04 (d, 1H); 7.98 (d, 1H); 4.38 (q, 2H); 4.18 (m, 2H); 1.47 (t, 3H); 1.23 (d, 6H);
[0667] Ex. no. 2-361: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.92 (br s, 1H); 11.87 (br s, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.04 (t, 1H); 4.37 (q, 2H); 3.76 (s, 3H); 1.47 (t, 3H);
[0668] Ex. no. 2-362: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 11.81 (br s, 1H); 7.97 (d, 1H); 7.81 (d, 1H); 7.02 (t, 1H); 4.37 (q, 2H); 3.99 (q, 2H); 1.47 (t, 3H); 1.23 (t, 3H);
[0669] Ex. no. 2-363: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 11.81 (br s, 1H); 7.96 (d, 1H); 7.81 (d, 1H); 7.02 (t, 1H); 4.38 (q, 2H); 3.91 (t, 2H); 1.65 (m, 2H); 1.48 (t, 3H); 0.95 (t, 3H);
[0670] Ex. no. 2-364: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.87 (br s, 1H); 11.67 (br s, 1H); 7.96 (d, 1H); 7.81 (d, 1H); 7.01 (t, 1H); 4.37 (q, 2H); 4.21 (m, 1H); 1.47 (t, 3H); 1.23 (d, 6H);
[0671] Ex. no. 3-26: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.63 (br s, 1H); 8.59 (t, 1H); 7.80 (d, 1H); 7.76 (d, 1H); 4.30 (t, 2H); 3.28 (m, 2H); 2.35 (s, 3H); 1.88 (m, 2H); 1.11 (t, 3H); 0.88 (t, 3H);
[0672] Ex. no. 3-27: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.62 (br s, 1H); 8.66 (d, 1H); 7.80 (d, 1H); 7.75 (d, 1H); 4.30 (t, 2H); 2.81 (m, 1H); 2.34 (s, 3H); 1.88 (m, 2H); 0.88 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0673] Ex. no. 3-125: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.90 (br s, 1H); 8.85 (d, 1H); 8.06 (d, 1H); 8.00 (d, 1H); 4.32 (t, 2H); 3.31 (s, 3H); 2.77 (m, 1H); 1.88 (m, 2H); 0.88 (t, 3H); 0.70 (m, 2H); 0.58 (m, 2H);
[0674] Ex. no. 3-129: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.88 (br s, 1H); 8.70 (q, 1 h); 7.96 (d, 1H); 7.93 (d, 1H); 4.32 (t, 2H); 2.80 (d, 3H); 1.88 (m, 2H); 0.88 (t, 3H);
[0675] Ex. no. 3-208: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.85 (br s, 1H); 8.73 (t, 1H); 7.95 (d, 1H); 7.89 (d, 1H); 4.34 (t, 2H); 3.29 (m, 2H); 1.89 (m 2H); 1.12 (t, 3H); 0.89 (t, 3H);
[0676] Ex. no. 3-273: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.65 (br s, 1H); 8.68 (d, 1H); 7.81 (d, 1H); 7.76 (d, 1H); 4.30 (t, 2H); 2.81 (m 2H); 2.70 (m, 1H); 1.89 (m, 2H); 1.17 (t, 3H); 0.89 (t, 3H); 0.71 (m, 2H); 0.49 (m, 2H);
[0677] Ex. no. 3-337: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.91 (br s, 1H); 7.97 (br s, 2H); 4.31 (t, 2H); 3.89 (br s, 1H); 2.07 (br s, 3H); 1.89 (m, 2H); 0.88 (t, 3H);
[0678] Ex. no. 3-338: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.89 (br s, 1H); 8.22 (s, 1H); 8.01 (s, 1H); 7.94 (s, 2H); 4.34 (t, 2H); 1.90 (m, 2H); 0-90 (t, 3H);
[0679] Ex. no. 4-212: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.22 (br s, 1H); 8.66 (d, 1H); 7.91 (s, 1H); 7.77 (d, 1H); 7.72 (d, 1H); 3.77 (s, 3H); 2.80 (m, 2H); 2.71 (m, 1H); 1.17 (t, 3H); 0.71 (m, 2H); 0.48 (m, 2H);
[0680] Ex. no. 5-58: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.45 (br s, 1H); 9.05 (s, 1H); 8.46 (q, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 2.79 (d, 3H); 2.39 (s, 3H);
[0681] Ex. no. 5-59: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.42 (br s, 1H); 9.07 (s, 1H); 8.53 (t, 1H); 7.90 (d, 1H); 7.78 (d, 1H); 3.28 (m, 2H); 2.40 (s, 3H); 1.12 (t, 3H);
[0682] Ex. no. 5-74: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 9.05 (s, 1H); 8.52 (q, 1H); 7.77 (d, 1H); 7.72 (d, 1H); 6.88 (t, 1H); 2.81 (d, 1H); 2.37 (s, 3H);
[0683] Ex. no. 5-75: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.35 (br s, 1H); 9.05 (s, 1H); 8.60 (t, 1H); 7.77 (d, 1H); 7.72 (d, 1H); 6.88 (t, 1H); 3.32 (m, 2H); 2.39 (s, 3H); 1.14 (t, 3H);
[0684] Ex. no. 5-117: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.62 (br s, 1H); 9.07 (s, 1H); 8.74 (t, 1H); 7.89 (s, 2H); 3.31 (m, 2H); 1.11 (t, 3H);
[0685] Ex. no. 5-122: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.55 (br s, 1H); 9.07 (s, 1H); 8.70 (q, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 6.95 (t, 1H); 2.80 (d, 3H);
[0686] Ex. no. 5-123: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.56 (br s, 1H); 9.06 (s, 1H); 8.77 (t, 1H); 7.82 (d, 1H); 7.74 (d, 1H); 3.29 (m, 2H); 1.13 (t, 3H);
[0687] Ex. no. 5-253: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.61 (br s, 1H); 9.07 (s, 1H); 8.19 (s, 1H); 7.96 (s, 1H); 7.89 (d, 1H); 7.86 (d, 1H);
[0688] Ex. no. 5-254: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.67 (br s, 1H); 9.59 (t, 1H); 9.08 (s, 1H); 7.96 (s, 2H); 4.41 (d, 2H);
[0689] Ex. no. 5-255: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.71 (br s, 1H); 10.85 (br s, 1H); 9.08 (s, 1H); 7.98 (m, 2H); 7.65 (m, 2H); 7.38 (m, 2H); 7.15 (m, 1H);
[0690] Ex. no. 6-26: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.18 (br s, 1H); 8.58 (t, 1H); 7.71 (s, 2H); 3.29 (m, 2H); 2.50 (s, 3H); 2.31 (s, 3H); 1.10 (t, 3H);
[0691] Ex. no. 6-32: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.11 (br s, 1H); 8.64 (t, 1H); 7.67 (d, 1H); 7.59 (d, 1); 6.89 (t, 1H); 3.30 (m, 2H); 2.49 (s, 3H); 2.31 (s, 3H); 1.12 (t, 3H);
[0692] Ex. no. 6-33: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.10 (br s, 1H); 8.70 (d, 1H); 7.67 (d, 1H); 7.58 (d, 1H); 6.89 (t, 1H); 2.85 (m, 1H); 2.49 (s, 3H); 2.28 (s, 3H); 0.70 (m, 2H); 0.53 (m, 2H);
[0693] Ex. no. 6-34: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.11 (br s, 1H); 8.78 (t, 1H); 7.68 (d, 1H); 7.60 (d, 1H); 6.90 (t, 1H); 3.15 (m, 2H); 2.49 (s, 3H); 2.33 (s, 3H); 1.04 (m, 1H); 0.46 (m, 2H); 0.23 (m, 2H);
[0694] Ex. no. 6-43: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.19 (br s, 1H); 8.49 (q, 1H); 7.77 (d, 1H); 7.61 (d, 1H); 3.80 (s, 3H); 2.77 (d, 3H); 2.49 (s, 3H);
[0695] Ex. no. 6-44: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.17 (br s, 1H); 8.57 (t, 1H); 7.76 (d, 1H); 7.62 (d, 1H); 3.81 (s, 3H); 3.27 (m, 2H); 2.49 (s, 3H); 1.10 (t, 3H);
[0696] Ex. no. 6-45: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.17 (br s, 1H); 8.64 (d, 1H); 7.76 (d, 1H); 7.61 (d, 1H); 3.80 (s, 3H); 2.79 (m, 1H); 2.49 (s, 3H); 0.70 (m, 2H); 0.47 (m, 2H);
[0697] Ex. no. 6-49: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.53 (q, 1H); 7.72 (d, 1H); 7.49 (d, 1H); 6.93 (t, 1H); 3.79 (s, 3H); 2.79 (d, 3H); 2.49 (s, 3H);
[0698] Ex. no. 6-50: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.61 (t, 1H); 7.72 (d, 1H); 7.49 (d, 1H); 6.94 (t, 1H); 3.81 (s, 3H); 3.29 (m, 2H); 2.49 (s, 3H); 1.12 (t, 3H);
[0699] Ex. no. 6-51: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.02 (br s, 1H); 8.68 (d, 1H); 7.72 (d, 1H); 7.48 (d, 1H); 6.92 (t, 1H); 3.79 (s, 3H); 2.84 (m, 1H); 2.49 (s, 3H); 0.70 (m, 2H); 0.53 (m, 2H);
[0700] Ex. no. 6-58: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.24 (br s, 1H); 8.46 (q, 1H); 7.90 (d, 1H); 7.76 (d, 1H); 2.79 (d, 3H); 2.49 (s, 3H); 2.39 (s, 3H);
[0701] Ex. no. 6-60: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.25 br s, 1H); 8.61 (d, 1H); 7.89 (d, 1H); 7.76 (d, 1H); 2.79 (m, 1H); 2.49 (s, 3H); 2.39 (s, 3H); 0.71 (m, 2H); 0.52 (br s, 1H);
[0702] Ex. no. 6-74: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.18 (br s, 1H); 8.52 (q, 1H); 7.76 (d, 1H); 7.70 (d, 1H); 6.88 (t, 1H); 2.81 (d, 3H); 2.49 (s, 3H); 2.38 (s, 3H);
[0703] Ex. no. 6-75: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.16 (br s, 1H); 8.59 (t, 1H); 7.77 (d, 1H); 7.69 (d, 1H); 6.88 (t, 1H); 3.31 (m, 2H); 2.49 (s, 3H); 2.39 (s, 3H); 1.14 (t, 3H);
[0704] Ex. no. 6-76: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.17 (br s, 1H); 8.67 (d, 1H); 7.76 (d, 1H); 7.69 (d, 1H); 6.88 (t, 1H); 2.84 (m, 1H); 2.49 (s, 3H); 2.37 (s, 3H); 0.71 (m, 2H); 0.57 (m, 2H);
[0705] Ex. no. 6-116: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.44 (br s, 1H); 8.67 (q, 1H); 7.89 (d, 1H); 7.86 (d, 1H); 2.78 (d, 3H); 2.50 (s, 3H);
[0706] Ex. no. 6-117: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.44 (br s, 1H); 8.74 (t, 1H); 7.89 (d, 1H); 7.86 (d, 1H); 3.27 (m, 2H); 2.49 (s, 3H); 1.11 (t, 3H);
[0707] Ex. no. 6-118: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.44 (br s, 1H); 8.81 (d, 1H); 7.88 (d, 1H); 7.85 (d, 1H); 2.79 (m, 1H); 2.49 (s, 3H); 0.72 (m, 2H); 0.50 (br s, 2H);
[0708] Ex. no. 6-120: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.51 (br s, 1H); 9.54 (t, 1H); 7.93 (s, 2H); 4.14 (m, 2H); 2.52 (s, 3H);
[0709] Ex. no. 6-124: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.36 (br s, 1H); 8.83 (d, 1H); 7.80 (d, 1H); 7.72 (d, 1H); 6.93 (t, 1H); 2.83 (m, 1H); 2.48 (s, 3H); 0.71 (m, 2H); 0.54 (m, 2H);
[0710] Ex. no. 6-141: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.31 (br s, 1H); 8.69 (t, 1H); 7.76 (d, 1H); 7.57 (d, 1H); 3.27 (m, 2H); 2.48 (s, 3H); 1.13 (t, 3H);
[0711] Ex. no. 6-143: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.31 (br s, 1H); 8.79 (t, 1H); 7.76 (d, 1H); 7.57 (d, 1H); 3.15 (m, 2H); 2.49 (s, 3H); 1.01 (m, 1H); 0.44 (m, 2H); 0.25 (m, 2H);
[0712] Ex. no. 6-144: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.32 (br s, 1H); 9.48 (t, 1H); 7.80 (d, 1H); 7.63 (d, 1H); 4.12 (m, 2H); 2.49 (s, 3H);
[0713] Ex. no. 6-145: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.31 (br s, 1H); 9.21 (t, 1H); 7.78 (d, 1H); 7.61 (d, 1H); 6.13 (tt, 1H); 3.69 (m, 2H); 2.49 (s, 3H);
[0714] Ex. no. 6-159: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.41 (br s, 1H); 8.72 (t, 1H); 7.92 (d, 1H); 7.80 (d, 1H); 3.28 (m, 2H); 2.50 (s, 3H); 1.11 (t, 3H);
[0715] Ex. no. 6-161: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.42 (br s, 1H); 8.82 (t, 1H); 7.91 (d, 1H); 7.80 (d, 1H); 3.13 (m, 2H); 2.49 (s, 3H); 1.00 (m, 1H); 0.45 (m, 2H); 0.23 (m, 2H);
[0716] Ex. no. 6-165: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.35 (br s, 1H); 8.75 (t, 1H); 7.77 (d, 1H); 7.74 (d, 1H); 6.91 (t, 1H); 3.29 (m, 2H); 2.49 (s, 3H); 1.13 (t, 3H);
[0717] Ex. no. 6-166: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.36 (br s, 1H); 8.81 (d, 1H); 7.76 (d, 1H); 7.73 (d, 1H); 6.91 (t, 1H); 2.80 (m, 1H); 2.49 (s, 3H); 0.71 (m, 2H); 0.56 (m, 2H);
[0718] Ex. no. 6-167: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.35 (br s, 1H); 8.88 (t, 1H); 7.78 (d, 1H); 7.74 (d, 1H); 6.91 (t, 1H); 3.15 (m, 2H); 2.49 (s, 3H); 1.03 (m, 1H); 0.46 (m, 2H); 0.24 (m, 2H);
[0719] Ex. no. 6-168: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 9.52 (t, 1H); 7.80 (s, 2H); 6.90 (t, 1H); 4.13 (m, 2H); 2.49 (s, 3H);
[0720] Ex. no. 6-169: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.37 (br s, 1H) M 9.26 (t, 1H); 7.80 (d, 1H); 7.78 (d, 1H); 6.92 (t, 1H); 6.17 (tt, 1H); 3.71 (m, 2H); 2.49 (s, 3H);
[0721] Ex. no. 6-210: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.22 (br s, 1H); 8.52 (q, 1H); 7.72 (s, 2H); 2.78 (d, 3H); 2.66 (m, 2H); 2.46 (s, 3H); 1.13 (t, 3H);
[0722] Ex. no. 6-211: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.21 (br s, 1H); 8.61 (t, 1H); 7.72 (br s, 2H); 3.28 (m, 2H); 2.78 (m, 1H); 2.69 (m, 1H); 2.49 (s, 3H); 1.15 (t, 3H); 1.10 (t, 3H);
[0723] Ex. no. 6-212: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.19 (br s, 1H); 8.66 (d, 1H); 7.71 (s, 2H); 2.80 (m, 2H); 2.68 (m, 1H); 2.52 (s, 3H); 1.13 (t, 3H); 0.71 (m, 2H); 0.48 (m, 2H);
[0724] Ex. no. 6-228: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.08 (br s, 1H); 8.61 (t, 1H); 7.73 (d, 1H); 7.63 (d, 1H); 3.12 (m, 2H); 2.49 (s, 3H); 2.11 (m, 1H); 1.02 (m, 1H); 0.80 (m, 2H); 0.62 (m, 2H); 0.46 (m, 2H); 0.22 (m, 2H);
[0725] Ex. no. 6-230: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.11 (br s, 1H); 9.01 (t, 1H); 7.76 (d, 1H); 7.67 (d, 1H); 6.12 (tt, 1H); 3.68 (m, 2H); 2.49 (s, 3H); 2.10 (m, 1H); 0.83 (m, 2H); 0.59 (m, 2H);
[0726] Ex. no. 6-231: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.51 (q, 1H); 7.63 (d, 1H); 7.60 (d, 1H); 6.92 (t, 1H); 2.81 (d, 3H); 2.49 (s, 3H); 2.13 (m, 1H); 0.79 (m, 2H); 0.51 (m, 2H);
[0727] Ex. no. 6-233: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.01 (br s, 1H); 8.66 (d, 1H); 7.60 (m, 2H); 6.92 (t, 1H); 2.84 (m, 1H); 2.49 (s, 3H); 2.12 (m, 1H); 0.79 (m, 2H); 0.70 (m, 2H); 0.54 (m, 4H);
[0728] Ex. no. 6-252: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=11.82 (br s, 1H); 7.91 (br s, 2H); 4.30 (br s, 1H); 2.38 (s, 3H); 1.99 (s, 3H);
[0729] Ex. no. 6-253: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.45 (br s, 1H); 8.20 (s, 1H); 7.98 (s, 1H); 7.89 (d, 1H); 7.86 (d, 1H); 2.52 (s, 3H);
[0730] Ex. no. 6-254: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.44 (br s, 1H); 8.73 (d, 1H); 7.85 (d, 1H); 7.88 (d, 1H); 3.43 (m, 1H); 1.19 (m, 3H); 0.89 (m, 1H); 0.42 (m, 2H); 0.29 (m, 2H);
[0731] Ex. no. 6-255: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.19 (br s, 1H); 8.50 (d, 1H); 7.70 (s, 2H); 4.07 (m, 1H); 2.49 (s, 3H); 2.31 (s, 3H); 1.15 (d, 3H); 1.11 (d, 3H);
[0732] Ex. no. 6-256: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.20 (br s, 1H); 8.84 (d, 1H); 7.71 (s, 2H); 4.36 (m, 1H); 2.49 (s, 3H); 2.30 (s, 3H); 2.24 (m, 2H); 1.97 (m, 2H); 1.48 (m, 2H);
[0733] Ex. no. 6-257: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.31 (br s, 1H); 8.65 (d, 1H); 7.75 (d, 1H); 7.57 (d, 1H); 3.48 (m, 1H); 2.49 (s, 3H); 1.21 (d, 3H); 0.91 (m, 1H); 0.42 (m, 2H); 0.34 (m, 2H);
[0734] Ex. no. 6-258: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.11 (br s, 1H); 8.69 (d, 1H); 7.68 (d, 1H); 7.59 (d, 1H); 6.89 (t, 1H); 3.44 (m, 1H); 2.49 (s, 3H); 2.34 (s, 3H); 1.22 (d, 3H); 0.92 (m, 1H); 0.43 (m, 2H); 0.34 (m, 1H); 0.26 (m, 1H);
[0735] Ex. no. 6-259: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 8.79 (t, 1H); 7.80 (d, 1H); 7.74 (d, 1H); 6.92 (t, 1H); 3.23 (m, 2H); 2.49 (s, 3H); 1.54 (m, 2H); 0.92 (t, 3H);
[0736] Ex. no. 6-260: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 8.69 (d, 1H); 7.79 (d, 1H); 7.73 (d, 1H); 6.92 (t, 1H); 4.08 (m, 1H); 2.49 (s, 3H); 1.16 (d, 6H);
[0737] Ex. no. 6-261: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 9.03 (d, 1H); 7.80 (d, 1H); 7.73 (d, 1H); 6.91 (t, 1H); 4.36 (m, 1H); 2.49 (s, 3H); 2.26 (m, 2H); 2.01 (m, 2H); 1.69 (m, 2H);
[0738] Ex. no. 6-262: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 8.90 (t, 1H); 7.80 (d, 1H); 7.74 (d, 1H); 6.94 (t, 1H); 3.45 (m, 4H); 3.28 (s, 3H); 2.49 (s, 3H);
[0739] Ex. no. 6-263: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.35 (br s, 1H); 8.91 (t, 1H); 7.80 (d, 1H); 7.73 (d, 1H); 6.95 (t, 1H); 3.98 (m, 1H); 3.78 (m, 1H); 3.65 (m, 1H); 3.34 (m, 2H); 2.49 (s, 3H); 1.94 (m, 1H); 1.84 (m, 2H); 1.62 (m, 1H);
[0740] Ex. no. 6-264: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.38 (br s, 1H); 9.43 (t, 1H); 7.82 (d, 1H); 7.75 (d, 1H); 7.45 (m, 1H); 7.07 (m, 1H); 6.99 (m, 1H); 6.90 (t, 1H); 4.67 (d, 3H); 2.49 (s, 3H);
[0741] Ex. no. 6-265: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.39 (br s, 1H); 9.10 (t, 1H); 7.83 (d, 1H); 7.79 (d, 1H); 7.57 (t, 1H); 4.16 (d, 2H); 3.01 (s, 3H); 2.88 (s, 3H);
[0742] Ex. no. 6-266: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.41 (br s, 1H); 10.83 (br s, 1H); 7.88 (d, 1H); 7.80 (d, 1H); 7.69 (m, 2H); 7.37 (m, 2H); 7.15 (m, 1H); 7.10 (t, 1H); 2.49 (s, 3H);
[0743] Ex. no. 6-267: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.35 (br s, 1H); 8.77 (d, 1H); 7.75 (m, 2H); 6.89 (t, 1H); 3.45 (m, 1H); 2.49 (s, 3H); 1.22 (d, 3H); 0.92 (m, 1H); 0.41 (m, 3H); 0.28 (m, 1H);
[0744] Ex. no. 6-268: .sup.1H-NMR (400 MHz, DMSO-d.sub.6): δ=12.08 (br s, 1H); 8.53 (d, 1H); 7.73 (d, 1H); 7.62 (d, 1H); 3.36 (m, 1H); 2.49 (s, 3H); 2.21 (m, 1H); 1.20 (d, 3H); 0.89 (m, 1H); 0.83 (m, 2H); 0.63 (br s, 2H); 0.44 (m, 2H); 0.32 (m, 1H); 0.24 (m, 1H).
B. FORMULATION EXAMPLES
[0745] a) A dusting product is obtained by mixing 10 parts by weight of a compound of the formula (I) and/or salts thereof and 90 parts by weight of talc as an inert substance and comminuting the mixture in a hammer mill. [0746] b) A readily water-dispersible, wettable powder is obtained by mixing 25 parts by weight of a compound of the formula (I) and/or salts thereof, 64 parts by weight of kaolin-containing quartz as an inert substance, 10 parts by weight of potassium lignosulfonate and 1 part by weight of sodium oleoylmethyltaurate as a wetting agent and dispersant, and grinding the mixture in a pinned-disk mill. [0747] c) A readily water-dispersible dispersion concentrate is obtained by mixing 20 parts by weight of a compound of the formula (I) and/or salts thereof with 6 parts by weight of alkylphenol polyglycol ether (® Triton X 207), 3 parts by weight of isotridecanol polyglycol ether (8 EO) and 71 parts by weight of paraffinic mineral oil (boiling range for example about 255 to above 277° C.), and grinding the mixture in a friction ball mill to a fineness of below 5 microns. [0748] d) An emulsifiable concentrate is obtained from 15 parts by weight of a compound of the formula (I) and/or salts thereof, 75 parts by weight of cyclohexanone as a solvent and 10 parts by weight of ethoxylated nonylphenol as an emulsifier. [0749] e) Water-dispersible granules are obtained by mixing [0750] 75 parts by weight of a compound of the formula (I) and/or salts thereof, [0751] 10 parts by weight of calcium lignosulfonate, [0752] 5 parts by weight of sodium lauryl sulfate, [0753] 3 parts by weight of polyvinyl alcohol and [0754] 7 parts by weight of kaolin, [0755] grinding the mixture in a pinned-disk mill, and granulating the powder in a fluidized bed by spray application of water as a granulating liquid. [0756] f) Water-dispersible granules are also obtained by homogenizing and precomminuting, in a colloid mill, [0757] 25 parts by weight of a compound of the formula (I) and/or salts thereof, [0758] 5 parts by weight of sodium 2,2′-dinaphthylmethane-6,6′-disulfonate [0759] 2 parts by weight of sodium oleoylmethyltaurate, [0760] 1 part by weight of polyvinyl alcohol, [0761] 17 parts by weight of calcium carbonate and [0762] 50 parts by weight of water, [0763] then grinding the mixture in a bead mill and atomizing and drying the resulting suspension in a spray tower by means of a one-phase nozzle.
C. BIOLOGICAL EXAMPLES
[0764] The abbreviations used for the harmful plants mean:
TABLE-US-00007 ABUTH Abutilon theophrasti ALOMY Alopecurus myosuroides AVEFA Avena fatua AMARE Amaranthus retroflexus CYPES Cyperus esculentus DIGSA Digitaria sanguinalis ECHCG Echinochloa crus-galli HORMU Hordeum murinum LOLMU Lolium multiflorum LOLRI Lolium rigidum MATIN Matricaria inodora PHBPU Pharbitis purpurea POLCO Polygonum convolvulus SETVI Setaria viridis STEME Stellaria media VERPE Veronica persica VIOTR Viola tricolor
[0765] 1. Pre-Emergence Herbicidal Action Against Harmful Plants
[0766] Seeds of monocotyledonous and dicotyledonous weed plants and crop plants are laid out in sandy loam soil in wood-fiber pots and covered with soil. The compounds of the invention, formulated in the form of wettable powders (WP) or as emulsion concentrates (EC), are then applied to the surface of the covering soil in the form of an aqueous suspension or emulsion at a water application rate equivalent to 600 to 800 l/ha, with addition of 0.2% wetting agent. After the treatment, the pots are placed in a greenhouse and kept under good growth conditions for the trial plants. The damage to the test plants is scored visually after a test period of 3 weeks by comparison with untreated controls (herbicidal activity in percent (%): 100% activity=the plants have died, 0% activity=like control plants). Numerous compounds of the invention showed very good action against a multitude of important harmful plants. The tables below illustrate, in an illustrative manner, the post-emergence herbicidal action of the compounds of the invention, the herbicidal activity being stated in percent.
TABLE-US-00008 TABLE 1a Pre-emergence action at 20 g/ha against ABUTH in % Example number Dosage [g/ha] ABUTH 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 80 2-338 20 90 3-338 20 90 2-337 20 100 3-337 20 100 1-26 20 100 2-26 20 100 3-26 20 100 6-26 20 100 1-208 20 100 2-208 20 100 3-208 20 100 6-159 20 100 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 100 6-118 20 100 1-149 20 100 2-149 20 100 6-124 20 100 5-59 20 100 5-58 20 90 5-117 20 100 5-253 20 90 5-75 20 100 5-74 20 80 5-123 20 100 5-122 20 90 1-82 20 100 1-87 20 100 2-87 20 100 1-88 20 100 2-88 20 100 1-209 20 100 2-25 20 100 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 90 2-173 20 90 1-273 20 100 2-273 20 90 3-273 20 90 6-212 20 80 1-44 20 100 2-44 20 100 1-45 20 80 2-45 20 80 1-46 20 90 2-46 20 100 1-30 20 100 1-31 20 100 2-31 20 100 1-28 20 90 2-28 20 100 2-29 20 100 1-304 20 100 2-304 20 100 1-305 20 100 2-305 20 100 1-306 20 100 2-306 20 100 2-177 20 90 1-178 20 90 1-179 20 80 1-132 20 100 2-132 20 100 1-135 20 100 2-135 20 100 6-254 20 100 2-134 20 100 6-120 20 80 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 100 1-279 20 100 2-279 20 80 2-195 20 100 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-226 20 80 2-196 20 100 2-57 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 2-271 20 100 2-32 20 100 1-34 20 80 2-34 20 80 6-255 20 100 2-33 20 100 2-42 20 100 1-146 20 100 1-72 20 100 2-72 20 100 1-73 20 100 2-73 20 100 1-74 20 100 2-74 20 100 1-138 20 100 2-138 20 80 1-137 20 100 1-136 20 90 1-180 20 90 2-180 20 100 6-143 20 100 1-183 20 100 2-183 20 100 1-182 20 100 2-182 20 100 6-145 20 100 1-181 20 90 2-181 20 100 2-36 20 90 1-228 20 100 2-228 20 100 6-167 20 90 1-230 20 90 2-230 20 100 2-286 20 100 1-287 20 100 2-287 20 100 2-288 20 100 1-210 20 100 2-210 20 100 1-212 20 80 2-213 20 100 1-288 20 100 1-289 20 100 2-289 20 100 1-291 20 100 2-291 20 100 2-292 20 100 1-271 20 100 2-47 20 100 1-339 20 90 2-339 20 100 6-258 20 100 1-49 20 80 2-49 20 100 1-229 20 90 2-229 20 80 1-340 20 100 6-267 20 90 2-340 20 100 1-47 20 100 1-33 20 90 1-32 20 100 2-154 20 100 6-259 20 90 1-155 20 100 2-155 20 100 6-260 20 90 1-164 20 80 2-164 20 90 6-261 20 80 1-165 20 90 1-166 20 90 2-156 20 100 1-159 20 80 2-161 20 90 2-211 20 100 2-272 20 100 1-161 20 80 2-276 20 100 1-276 20 100 1-211 20 100 1-274 20 100 1-272 20 90 6-211 20 90 1-341 20 100 1-292 20 100 2-341 20 100 1-83 20 100 2-83 20 100 1-89 20 90 2-89 20 100 6-161 20 100 6-268 20 100 2-342 20 100 1-344 20 90 1-345 20 100 2-344 20 100 1-346 20 90 2-345 20 90 2-346 20 80 1-195 20 90 2-184 20 100 1-185 20 100 2-185 20 100 1-186 20 100 2-186 20 100 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 80 2-354 20 90
TABLE-US-00009 TABLE 1b Pre-emergence action at 80 g/ha against ABUTH in % Example number Dosage [g/ha] ABUTH 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 90 1-337 80 100 2-337 80 100 3-337 80 100 6-252 80 80 1-123 80 100 2-123 80 100 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 2-125 80 100 3-125 80 100 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 100 2-82 80 100 6-58 80 100 1-147 80 90 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 100 5-58 80 100 5-117 80 100 5-253 80 100 5-75 80 100 5-74 80 100 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 1-209 80 100 1-4 80 100 1-25 80 100 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 90 3-273 80 100 6-212 80 90 4-212 80 90 1-44 80 100 2-44 80 100 1-45 80 100 2-45 80 100 6-32 80 80 1-46 80 100 2-46 80 100 6-33 80 90 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 100 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 100 1-134 80 90 2-134 80 100 1-133 80 100 2-133 80 100 6-120 80 100 1-277 80 100 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 80 1-226 80 90 2-226 80 80 6-165 80 100 6-166 80 100 2-196 80 100 1-56 80 90 6-45 80 90 2-57 80 100 6-43 80 100 1-58 80 80 2-58 80 100 2-56 80 100 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 100 2-32 80 100 1-34 80 100 2-34 80 100 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 100 2-146 80 90 1-143 80 100 5-255 80 100 5-254 80 100 1-146 80 100 2-143 80 100 1-72 80 100 2-72 80 100 1-73 80 100 2-73 80 100 6-50 80 90 1-74 80 100 2-74 80 100 6-51 80 100 1-138 80 100 2-138 80 100 1-137 80 100 1-136 80 100 1-180 80 100 2-180 80 100 6-143 80 100 1-183 80 100 2-183 80 100 6-257 80 100 1-182 80 100 2-182 80 100 6-145 80 100 1-181 80 100 2-181 80 100 6-144 80 90 1-36 80 100 2-36 80 100 1-228 80 100 2-228 80 100 6-167 80 100 1-230 80 100 2-230 80 100 6-169 80 90 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 100 2-289 80 100 6-228 80 90 1-291 80 100 2-291 80 100 6-230 80 90 2-292 80 100 1-271 80 100 2-47 80 100 6-34 80 100 1-339 80 100 2-339 80 100 6-258 80 100 1-49 80 100 2-49 80 100 1-41 80 100 1-229 80 100 2-229 80 100 1-340 80 100 6-267 80 100 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 100 6-260 80 100 1-164 80 80 2-164 80 100 6-261 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 100 1-159 80 100 2-159 80 100 1-160 80 80 2-160 80 90 2-161 80 100 6-266 80 80 2-211 80 100 2-272 80 100 1-161 80 90 2-276 80 100 1-276 80 100 1-211 80 100 1-274 80 100 6-168 80 100 1-272 80 100 6-211 80 100 1-341 80 100 1-292 80 100 2-341 80 100 2-158 80 100 1-83 80 100 2-83 80 100 6-60 80 90 1-89 80 100 2-89 80 100 6-161 80 100 6-268 80 100 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 100 1-345 80 100 2-344 80 100 1-346 80 100 2-345 80 100 1-347 80 100 2-346 80 90 2-347 80 100 1-195 80 100 1-184 80 100 2-184 80 100 1-185 80 100 2-185 80 100 1-186 80 100 2-186 80 100 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 1-354 80 100 2-352 80 100 1-355 80 100 2-353 80 100 1-356 80 100 2-354 80 100
TABLE-US-00010 TABLE 1c Pre-emergence action at 3200 g/ha against ABUTH in % Example number Dosage [g/ha] ABUTH 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00011 TABLE 2a Pre-emergence action at 20 g/ha against ALOMY in % Example number Dosage [g/ha] ALOMY 2-129 20 90 1-129 20 90 1-208 20 80 2-208 20 80 1-130 20 100 2-130 20 90 1-131 20 80 2-131 20 90 1-149 20 80 2-149 20 80 1-173 20 80 2-173 20 100 1-177 20 80 2-177 20 90 1-178 20 80 2-178 20 80 1-179 20 80 2-179 20 80 1-132 20 80 1-134 20 80 1-133 20 90 6-120 20 80 2-278 20 80 2-279 20 80 1-197 20 100 2-227 20 80 1-227 20 80 2-196 20 90 2-58 20 90 2-207 20 80 2-32 20 90 1-34 20 80 2-34 20 80 6-255 20 90 2-33 20 90 2-42 20 80 6-256 20 80 1-137 20 90 2-180 20 80 1-182 20 80 2-287 20 80 1-212 20 100 1-32 20 80 2-155 20 80 1-166 20 90 2-276 20 90 1-276 20 90 1-211 20 90 1-274 20 80 1-272 20 90 1-341 20 80 1-292 20 80 2-341 20 80 1-83 20 80 2-83 20 90 1-342 20 90 2-342 20 90 1-344 20 90 2-343 20 80 1-345 20 80 2-344 20 80 1-195 20 90 1-184 20 90 2-184 20 90 1-185 20 90 2-348 20 90 1-351 20 100
TABLE-US-00012 TABLE 2b Pre-emergence action at 80 g/ha against ALOMY in % Example number Dosage [g/ha] ALOMY 3-129 80 80 2-129 80 100 1-129 80 100 6-116 80 100 2-338 80 90 3-338 80 80 2-337 80 90 3-337 80 100 1-26 80 100 2-26 80 100 3-26 80 80 6-26 80 80 1-208 80 100 2-208 80 90 3-208 80 90 6-159 80 80 1-130 80 100 2-130 80 100 1-81 80 80 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 90 2-149 80 90 6-124 80 90 5-117 80 90 5-123 80 80 5-122 80 80 1-82 80 80 1-87 80 90 2-87 80 80 1-88 80 90 2-88 80 90 1-209 80 80 1-4 80 80 1-25 80 90 2-25 80 90 3-27 80 90 1-27 80 90 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 90 2-273 80 90 6-212 80 80 1-44 80 90 2-44 80 80 1-45 80 90 2-45 80 90 1-46 80 90 2-46 80 100 1-30 80 80 2-30 80 100 1-31 80 90 2-31 80 80 1-28 80 90 2-28 80 90 1-29 80 100 2-29 80 80 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 6-141 80 90 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 90 1-135 80 90 2-135 80 90 6-254 80 90 1-134 80 100 2-134 80 90 1-133 80 90 2-133 80 90 6-120 80 90 1-277 80 90 1-278 80 90 2-278 80 90 1-279 80 80 2-279 80 90 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 90 1-225 80 100 1-226 80 90 2-226 80 90 6-165 80 80 2-196 80 100 1-56 80 90 2-57 80 90 1-58 80 90 2-58 80 100 2-56 80 90 1-57 80 80 1-207 80 100 2-207 80 90 2-271 80 80 2-32 80 100 1-34 80 100 2-34 80 90 6-255 80 100 2-33 80 100 2-42 80 90 6-256 80 90 2-146 80 80 1-146 80 90 1-141 80 90 1-37 80 100 2-37 80 90 2-72 80 80 1-73 80 80 2-73 80 100 1-74 80 90 2-74 80 100 1-138 80 90 2-138 80 90 2-141 80 90 1-137 80 90 1-136 80 90 1-180 80 100 2-180 80 100 1-183 80 90 2-183 80 90 1-182 80 100 2-182 80 80 6-145 80 90 1-181 80 100 2-181 80 80 1-228 80 90 2-228 80 80 1-230 80 90 2-286 80 80 2-287 80 90 2-288 80 90 1-210 80 80 2-210 80 100 1-212 80 100 2-212 80 100 1-288 80 90 1-289 80 90 2-289 80 90 1-291 80 80 2-291 80 80 2-292 80 90 1-271 80 90 2-47 80 100 6-34 80 80 1-339 80 90 2-339 80 90 6-258 80 90 1-49 80 80 2-49 80 90 1-229 80 90 2-229 80 90 1-340 80 90 6-267 80 80 1-47 80 90 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 80 1-155 80 90 2-155 80 100 6-260 80 90 1-164 80 100 1-165 80 100 1-166 80 100 1-156 80 90 2-156 80 100 2-159 80 80 1-162 80 90 2-211 80 90 2-272 80 90 2-276 80 90 1-276 80 100 1-211 80 100 1-274 80 90 6-168 80 80 1-272 80 100 6-211 80 90 1-341 80 90 1-292 80 90 2-341 80 90 1-83 80 100 2-83 80 90 1-89 80 90 2-89 80 100 6-161 80 90 1-342 80 100 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 90 1-345 80 90 2-344 80 100 1-346 80 90 2-345 80 80 1-347 80 80 2-346 80 80 1-195 80 90 1-184 80 100 2-184 80 100 1-185 80 100 2-185 80 90 1-186 80 90 2-186 80 100 1-349 80 100 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 90 1-352 80 80 1-86 80 100 2-86 80 90 1-92 80 90 2-92 80 90 1-90 80 80 1-353 80 90 2-351 80 80 1-354 80 80 2-352 80 90 1-355 80 90 2-353 80 90 1-356 80 100 2-354 80 90
TABLE-US-00013 TABLE 2c Pre-emergence action at 320 g/ha against ALOMY in % Example number Dosage [g/ha] ALOMY 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 90 2-337 320 100 6-117 320 90 1-81 320 100 2-81 320 90 2-82 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00014 TABLE 3a Pre-emergence action at 20 g/ha against AMARE in % Example number Dosage [g/ha] AMARE 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 100 2-338 20 90 3-338 20 80 1-337 20 90 2-337 20 90 3-337 20 100 6-252 20 80 1-123 20 80 2-123 20 80 1-26 20 100 2-26 20 100 3-26 20 100 6-26 20 100 1-208 20 100 2-208 20 100 3-208 20 100 6-159 20 100 1-125 20 90 2-125 20 80 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 100 6-118 20 80 1-149 20 100 2-149 20 100 6-124 20 100 5-59 20 100 5-58 20 100 5-117 20 90 5-253 20 100 5-75 20 100 5-74 20 100 5-123 20 100 5-122 20 80 1-82 20 90 1-87 20 90 2-87 20 100 1-88 20 100 2-88 20 100 1-209 20 100 1-4 20 90 1-25 20 100 2-25 20 100 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 100 1-273 20 100 2-273 20 90 3-273 20 100 6-212 20 90 4-212 20 90 1-44 20 100 2-44 20 100 1-45 20 100 2-45 20 100 6-32 20 80 1-46 20 100 2-46 20 100 6-33 20 90 1-30 20 100 2-30 20 100 1-31 20 100 2-31 20 100 1-28 20 100 2-28 20 100 1-29 20 100 2-29 20 100 1-304 20 100 2-304 20 100 1-305 20 100 2-305 20 100 1-306 20 100 2-306 20 90 1-177 20 100 2-177 20 100 1-178 20 100 2-178 20 100 1-179 20 100 2-179 20 100 1-132 20 100 2-132 20 100 1-135 20 100 2-135 20 100 6-254 20 100 1-134 20 100 2-134 20 100 1-133 20 90 2-133 20 90 6-120 20 100 1-277 20 100 2-277 20 100 1-278 20 100 2-278 20 100 1-279 20 100 2-279 20 100 2-195 20 100 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 100 1-225 20 100 1-226 20 100 2-226 20 100 6-165 20 100 6-166 20 90 2-196 20 100 1-56 20 100 6-45 20 80 6-44 20 80 2-57 20 100 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 2-271 20 100 2-32 20 100 1-34 20 100 2-34 20 90 6-255 20 100 2-33 20 100 2-42 20 100 6-256 20 90 2-146 20 100 5-255 20 90 1-146 20 100 1-141 20 100 1-37 20 100 2-37 20 90 1-72 20 100 2-72 20 100 6-49 20 80 1-73 20 100 2-73 20 100 6-50 20 100 1-74 20 100 2-74 20 100 6-51 20 80 1-144 20 90 2-144 20 80 1-138 20 100 2-138 20 100 2-141 20 100 1-137 20 100 1-136 20 100 1-180 20 100 2-180 20 100 6-143 20 100 1-183 20 100 2-183 20 90 1-182 20 100 2-182 20 100 6-145 20 90 1-181 20 100 2-181 20 100 6-144 20 90 1-36 20 100 2-36 20 100 1-228 20 100 2-228 20 100 6-167 20 100 1-230 20 100 2-230 20 100 6-169 20 90 2-286 20 100 1-287 20 100 2-287 20 100 2-288 20 100 1-210 20 100 2-210 20 100 1-212 20 100 2-213 20 100 1-288 20 100 1-289 20 90 2-289 20 100 1-291 20 100 2-291 20 100 6-230 20 100 2-292 20 100 1-271 20 100 2-47 20 100 6-34 20 100 1-339 20 100 2-339 20 100 6-258 20 100 1-49 20 100 2-49 20 100 1-41 20 90 1-229 20 100 2-229 20 100 1-340 20 100 6-267 20 90 2-340 20 100 1-47 20 100 1-33 20 100 1-32 20 100 2-154 20 100 6-259 20 100 1-155 20 100 2-155 20 100 6-260 20 100 2-164 20 100 6-261 20 100 1-165 20 100 1-166 20 100 1-156 20 100 2-156 20 100 6-262 20 90 1-159 20 100 2-159 20 100 1-162 20 90 2-162 20 90 6-264 20 80 1-160 20 100 2-160 20 100 2-161 20 90 6-266 20 90 2-211 20 100 2-272 20 100 1-161 20 100 2-276 20 100 1-276 20 90 1-211 20 100 1-274 20 100 6-168 20 90 1-272 20 100 6-211 20 100 1-341 20 100 1-292 20 100 2-341 20 100 1-158 20 100 2-83 20 100 1-89 20 100 2-89 20 90 6-161 20 100 1-342 20 100 1-343 20 100 2-342 20 90 1-344 20 100 2-343 20 100 1-345 20 100 2-344 20 100 1-346 20 100 2-345 20 100 2-346 20 100 1-195 20 90 1-184 20 100 2-184 20 100 1-185 20 100 2-185 20 100 1-186 20 80 2-186 20 100 1-349 20 100 1-350 20 100 2-348 20 100 1-351 20 100 2-349 20 100 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 100 2-352 20 100 1-355 20 100 2-353 20 100 1-356 20 100 2-354 20 100
TABLE-US-00015 TABLE 3b Pre-emergence action at 80 g/ha against AMARE in % Example number Dosage [g/ha] AMARE 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 80 1-337 80 100 2-337 80 100 3-337 80 100 6-252 80 90 1-123 80 100 2-123 80 100 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 1-125 80 100 2-125 80 100 3-125 80 100 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 100 2-82 80 100 6-58 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 100 5-58 80 100 5-117 80 90 5-253 80 100 5-75 80 100 5-74 80 100 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 1-209 80 100 1-4 80 100 1-25 80 100 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 100 3-273 80 100 6-212 80 90 4-212 80 90 1-44 80 100 2-44 80 100 1-45 80 100 2-45 80 100 6-32 80 100 1-46 80 100 2-46 80 100 6-33 80 100 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 100 6-231 80 100 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 6-233 80 80 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 6-141 80 100 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 100 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 100 6-120 80 100 1-277 80 100 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 100 1-226 80 100 2-226 80 100 6-165 80 100 6-166 80 100 2-196 80 100 1-56 80 100 6-45 80 100 6-44 80 100 2-57 80 100 6-43 80 100 1-58 80 100 2-58 80 100 2-56 80 100 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 100 2-32 80 100 1-34 80 100 2-34 80 100 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 100 2-146 80 100 2-142 80 100 1-143 80 100 5-255 80 100 1-142 80 100 5-254 80 100 1-140 80 100 1-146 80 100 1-141 80 100 1-37 80 100 2-37 80 100 2-143 80 100 1-72 80 100 2-72 80 100 6-49 80 100 1-73 80 100 2-73 80 100 6-50 80 100 1-74 80 100 2-74 80 100 6-51 80 100 2-35 80 90 1-144 80 100 2-144 80 100 1-138 80 100 2-138 80 100 2-141 80 100 1-137 80 100 1-136 80 100 1-180 80 100 2-180 80 100 6-143 80 100 1-183 80 100 2-183 80 100 6-257 80 100 1-182 80 100 2-182 80 100 6-145 80 100 1-181 80 100 2-181 80 100 6-144 80 100 1-36 80 100 2-36 80 100 1-228 80 100 2-228 80 100 6-167 80 100 1-230 80 100 2-230 80 100 6-169 80 100 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 100 2-289 80 100 6-228 80 100 1-291 80 100 2-291 80 100 6-230 80 100 2-292 80 100 1-271 80 100 2-47 80 100 6-34 80 100 1-339 80 100 2-339 80 100 6-258 80 100 1-49 80 100 2-49 80 100 1-41 80 100 1-229 80 100 2-229 80 100 1-340 80 100 6-267 80 100 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 100 6-260 80 100 1-164 80 100 2-164 80 100 6-261 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 100 1-157 80 100 2-157 80 90 1-159 80 100 2-159 80 100 1-162 80 100 2-162 80 100 6-264 80 100 1-160 80 100 2-160 80 100 6-265 80 80 2-161 80 100 6-266 80 100 2-211 80 100 2-272 80 100 1-161 80 100 2-276 80 100 1-276 80 100 1-211 80 100 1-274 80 100 6-168 80 100 1-272 80 100 6-211 80 100 1-341 80 100 1-292 80 100 2-341 80 100 1-158 80 100 2-158 80 100 1-83 80 100 2-83 80 100 6-60 80 100 1-89 80 100 2-89 80 100 6-76 80 100 6-161 80 100 6-268 80 100 1-342 80 100 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 100 1-345 80 100 2-344 80 100 1-346 80 100 2-345 80 100 1-347 80 100 2-346 80 100 1-195 80 100 1-184 80 100 2-184 80 100 1-185 80 100 2-185 80 100 1-186 80 100 2-186 80 100 1-349 80 100 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 1-354 80 100 2-352 80 100 1-355 80 100 2-353 80 100 1-356 80 100 2-354 80 100
TABLE-US-00016 TABLE 3c Pre-emergence action at 320 g/ha against AMARE in % Example number Dosage [g/ha] AMARE 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 90 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00017 TABLE 4a Pre-emergence action at 20 g/ha against AVEFA in % Example number Dosage [g/ha] AVEFA 2-129 20 100 1-129 20 100 2-337 20 90 2-26 20 80 3-26 20 80 1-208 20 80 1-130 20 100 2-130 20 90 1-131 20 80 1-149 20 80 2-149 20 80 2-27 20 80 2-173 20 90 1-29 20 80 1-177 20 80 2-178 20 90 1-135 20 80 1-134 20 80 2-134 20 80 2-197 20 80 1-225 20 80 1-226 20 80 2-196 20 80 1-207 20 80 2-32 20 90 2-33 20 80 2-42 20 80 2-288 20 80 1-212 20 80 2-291 20 80 1-164 20 100 2-276 20 80 1-211 20 80 1-274 20 80 1-341 20 80 1-343 20 80 1-345 20 80 1-346 20 80 2-345 20 80 1-195 20 80 2-349 20 90 2-92 20 80 2-90 20 80
TABLE-US-00018 TABLE 4b Pre-emergence action at 80 g/ha against AVEFA in % Example number Dosage [g/ha] AVEFA 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 90 3-338 80 90 2-337 80 100 3-337 80 100 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 80 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 90 2-125 80 100 3-125 80 80 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 90 2-81 80 80 2-82 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 90 1-149 80 100 2-149 80 100 6-124 80 90 5-59 80 80 5-58 80 80 5-117 80 90 5-74 80 80 1-82 80 90 1-87 80 90 2-87 80 90 1-88 80 90 2-88 80 90 1-209 80 100 1-4 80 90 1-25 80 90 2-25 80 100 3-27 80 90 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 90 3-273 80 90 1-44 80 90 2-44 80 90 1-45 80 90 2-45 80 100 1-46 80 100 2-46 80 100 1-30 80 100 2-30 80 100 1-31 80 90 2-31 80 100 1-28 80 100 2-28 80 90 1-29 80 90 2-29 80 100 1-306 80 80 1-177 80 100 2-177 80 90 1-178 80 100 2-178 80 100 6-141 80 80 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 90 1-135 80 100 2-135 80 90 6-254 80 90 1-134 80 90 2-134 80 90 1-133 80 100 2-133 80 90 6-120 80 90 1-277 80 90 1-278 80 90 2-278 80 90 1-279 80 90 2-279 80 100 2-195 80 80 2-225 80 80 1-197 80 100 2-227 80 90 1-227 80 90 2-197 80 100 1-225 80 80 1-226 80 90 2-226 80 100 2-196 80 100 1-56 80 80 2-57 80 90 1-58 80 80 2-58 80 90 1-57 80 90 1-207 80 90 2-207 80 90 2-32 80 90 2-34 80 90 6-255 80 80 2-33 80 90 2-42 80 90 6-256 80 80 2-73 80 80 2-74 80 80 1-137 80 90 1-136 80 80 1-180 80 80 2-180 80 80 1-183 80 90 2-183 80 80 1-182 80 90 2-182 80 90 1-181 80 80 2-181 80 90 1-228 80 90 2-228 80 80 1-230 80 90 2-230 80 80 2-287 80 80 2-288 80 90 1-210 80 90 2-210 80 90 1-212 80 90 2-212 80 90 1-288 80 90 1-289 80 80 2-291 80 80 2-292 80 90 1-271 80 80 2-47 80 80 1-339 80 100 2-339 80 80 2-49 80 80 1-229 80 80 2-229 80 90 1-340 80 80 1-33 80 100 1-155 80 90 2-155 80 90 1-164 80 100 1-166 80 100 2-211 80 80 2-272 80 80 2-276 80 90 1-276 80 90 1-211 80 90 1-274 80 90 6-168 80 80 1-272 80 90 6-211 80 80 1-341 80 90 2-341 80 90 1-83 80 80 2-83 80 90 1-89 80 90 2-89 80 90 1-342 80 100 1-343 80 80 2-342 80 90 1-344 80 90 2-343 80 100 1-345 80 90 2-344 80 80 1-346 80 80 2-345 80 80 2-346 80 80 1-195 80 90 2-184 80 90 1-185 80 100 2-185 80 100 2-186 80 80 1-349 80 100 1-350 80 90 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 80 1-86 80 100 2-86 80 90 2-92 80 80 2-90 80 90 2-351 80 80 2-352 80 80 2-354 80 90
TABLE-US-00019 TABLE 4c Pre-emergence action at 320 g/ha against AVEFA in % Example number Dosage [g/ha] AVEFA 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 90 2-337 320 100 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00020 TABLE 5a Pre-emergence action at 20 g/ha against CYPES in % Example number Dosage [g/ha] CYPES 2-129 20 100 1-129 20 90 6-116 20 100 6-253 20 80
TABLE-US-00021 TABLE 5b Pre-emergence action at 80 g/ha against CYPES in % Example number Dosage [g/ha] CYPES 3-129 80 100 2-129 80 100 1-129 80 90 6-116 80 100 1-338 80 90 2-338 80 90 3-338 80 90 6-253 80 90
TABLE-US-00022 TABLE 5c Pre-emergence action at 320 g/ha against CYPES in % Example number Dosage [g/ha] CYPES 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 90 6-253 320 100
TABLE-US-00023 TABLE 6a Pre-emergence action at 20 g/ha against ECHCG in % Example number Dosage [g/ha] ECHCG 1-129 20 80 2-337 20 80 1-26 20 80 1-130 20 90 2-130 20 80 6-124 20 80 5-59 20 80 5-117 20 80 5-123 20 90 5-122 20 80 2-87 20 80 1-88 20 90 2-27 20 90 1-273 20 90 1-31 20 90 2-28 20 80 1-305 20 80 2-305 20 80 1-177 20 80 1-178 20 80 1-132 20 90 1-135 20 80 6-254 20 90 2-134 20 80 1-278 20 90 1-227 20 80 1-225 20 90 1-226 20 80 2-226 20 100 2-57 20 90 1-58 20 100 1-57 20 90 2-42 20 90 6-256 20 80 1-137 20 80 1-183 20 90 1-228 20 90 2-287 20 90 2-288 20 90 1-210 20 80 2-210 20 80 1-288 20 80 1-289 20 80 1-271 20 90 1-32 20 80 1-164 20 100 1-166 20 90 1-211 20 90 6-161 20 80 1-345 20 90 2-344 20 90 2-84 20 90 2-350 20 80 1-86 20 90 2-86 20 80 2-90 20 90 1-353 20 90
TABLE-US-00024 TABLE 6b Pre-emergence action at 80 g/ha against ECHCG in % Example number Dosage [g/ha] ECHCG 3-129 80 80 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 90 2-337 80 100 3-337 80 90 1-26 80 100 2-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 80 6-159 80 100 1-130 80 100 2-130 80 100 6-117 80 90 1-81 80 100 2-81 80 100 2-82 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 90 6-124 80 100 5-59 80 100 5-58 80 90 5-117 80 100 5-75 80 100 5-74 80 90 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 1-209 80 90 1-4 80 90 1-25 80 100 2-25 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 90 3-273 80 80 6-212 80 90 4-212 80 80 1-44 80 90 1-45 80 90 2-45 80 100 6-32 80 90 1-46 80 80 2-46 80 90 6-33 80 100 1-30 80 80 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 90 2-29 80 100 1-304 80 100 2-304 80 90 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 1-177 80 100 2-177 80 90 1-178 80 100 2-178 80 100 6-141 80 90 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 100 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 100 6-120 80 100 1-277 80 90 2-277 80 90 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 80 2-225 80 90 1-197 80 90 2-227 80 100 1-227 80 90 2-197 80 100 1-225 80 100 1-226 80 100 2-226 80 100 6-165 80 100 6-166 80 80 1-56 80 90 6-45 80 80 6-44 80 100 2-57 80 100 6-43 80 100 1-58 80 100 2-58 80 100 2-56 80 90 1-57 80 90 1-207 80 90 2-207 80 100 2-271 80 100 6-210 80 90 2-32 80 100 1-34 80 90 2-34 80 90 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 100 1-146 80 100 1-141 80 90 1-37 80 80 2-37 80 80 1-72 80 80 2-72 80 100 1-73 80 100 2-73 80 100 1-74 80 100 2-74 80 100 1-144 80 100 2-144 80 80 1-138 80 100 2-138 80 90 2-141 80 80 1-137 80 100 1-136 80 90 1-180 80 100 2-180 80 100 1-183 80 100 2-183 80 90 6-257 80 80 1-182 80 100 2-182 80 100 6-145 80 90 1-181 80 100 2-181 80 100 6-144 80 100 1-228 80 100 2-228 80 100 6-167 80 100 1-230 80 90 2-230 80 90 6-169 80 90 2-286 80 90 1-287 80 90 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 90 2-213 80 90 1-288 80 100 1-289 80 100 2-289 80 100 6-228 80 90 1-291 80 90 2-291 80 90 6-230 80 80 2-292 80 100 1-271 80 100 2-47 80 100 6-34 80 100 1-339 80 100 2-339 80 100 6-258 80 100 1-49 80 80 2-49 80 90 1-229 80 80 2-229 80 80 1-340 80 100 6-267 80 80 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 100 6-260 80 100 1-164 80 100 2-164 80 80 6-261 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 90 1-159 80 90 2-159 80 90 1-162 80 100 2-162 80 80 2-211 80 90 2-272 80 100 2-276 80 80 1-276 80 100 1-211 80 100 1-274 80 100 6-168 80 90 1-272 80 100 6-211 80 100 1-341 80 90 1-292 80 90 2-341 80 100 1-83 80 90 2-83 80 90 6-60 80 80 1-89 80 100 2-89 80 90 6-161 80 100 1-342 80 100 1-343 80 90 2-342 80 80 1-344 80 90 2-343 80 90 1-345 80 100 2-344 80 100 1-346 80 90 2-345 80 90 2-346 80 90 1-195 80 100 1-184 80 100 2-184 80 100 1-185 80 100 2-185 80 90 1-186 80 80 2-186 80 100 1-349 80 90 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 90 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 2-352 80 80
TABLE-US-00025 TABLE 6c Pre-emergence action at 320 g/ha against ECHCG in % Example number Dosage [g/ha] ECHCG 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00026 TABLE 7a Pre-emergence action at 20 g/ha against HORMU in % Example number Dosage [g/ha] HORMU 2-337 20 90 2-130 20 90
TABLE-US-00027 TABLE 7b Pre-emergence action at 80 g/ha against HORMU in % Example number Dosage [g/ha] HORMU 3-129 80 90 2-129 80 90 1-129 80 90 6-116 80 90 2-338 80 80 3-338 80 80 2-337 80 90 3-337 80 100 1-26 80 80 2-26 80 90 3-26 80 80 6-26 80 80 1-208 80 80 2-208 80 90 6-159 80 80 1-130 80 90 2-130 80 100 1-81 80 80 2-81 80 90 2-82 80 80 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90 1-131 80 80 2-131 80 80 1-149 80 90 2-149 80 90 6-124 80 80 5-117 80 80 2-87 80 80 2-88 80 80 1-209 80 80 1-4 80 80 2-25 80 90 1-27 80 80 2-27 80 90 1-173 80 90 2-173 80 100 1-273 80 80 2-273 80 80 2-46 80 90
TABLE-US-00028 TABLE 7c Pre-emergence action at 320 g/ha against HORMU in % Example number Dosage [g/ha] HORMU 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 90 2-337 320 100 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 90 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00029 TABLE 8a Pre-emergence action at 20 g/ha against LOLRI in % Example number Dosage [g/ha] LOLRI 1-173 20 80 1-164 20 100
TABLE-US-00030 TABLE 8b Pre-emergence action at 80 g/ha against LOLRI in % Example number Dosage [g/ha] LOLRI 1-129 80 90 2-337 80 80 1-26 80 80 2-208 80 80 1-130 80 100 2-130 80 100 1-131 80 80 1-149 80 90 2-149 80 90 5-117 80 80 1-82 80 80 1-87 80 80 2-87 80 80 2-88 80 80 1-25 80 80 2-25 80 80 1-27 80 80 2-27 80 80 1-173 80 90 2-173 80 90 1-273 80 80 2-273 80 80 1-45 80 80 2-45 80 80 1-46 80 90 2-46 80 90 1-177 80 90 2-177 80 90 1-178 80 80 2-178 80 80 1-179 80 90 2-179 80 80 1-132 80 80 2-132 80 90 2-135 80 80 1-134 80 80 2-134 80 80 2-133 80 80 2-279 80 80 2-195 80 90 1-197 80 80 1-227 80 90 2-197 80 90 1-225 80 80 2-196 80 100 2-32 80 90 1-34 80 80 6-255 80 80 2-33 80 80 2-42 80 80 1-138 80 90 1-137 80 90 1-136 80 90 1-182 80 80 2-182 80 80 1-181 80 80 2-288 80 90 1-212 80 80 2-212 80 90 1-288 80 80 1-289 80 80 1-271 80 100 2-47 80 80 1-339 80 100 2-339 80 80 1-47 80 80 1-33 80 80 1-32 80 90 2-154 80 90 1-155 80 90 2-155 80 80 1-164 80 100 1-165 80 80 1-166 80 80 1-159 80 80 2-276 80 80 1-272 80 80 1-83 80 80 1-343 80 80 2-342 80 80 1-344 80 90 2-343 80 90 1-345 80 80 1-195 80 80 2-184 80 80 1-185 80 90 1-349 80 90 1-92 80 90
TABLE-US-00031 TABLE 8c Pre-emergence action at 320 g/ha against LOLRI in % Example number Dosage [g/ha] LOLRI 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 90 2-338 320 100 2-337 320 90 1-81 320 80 2-81 320 90 2-82 320 90 1-147 320 100 2-147 320 90 1-148 320 90 2-148 320 90
TABLE-US-00032 TABLE 9a Pre-emergence action at 20 g/ha against MATIN in % Example number Dosage [g/ha] MATIN 3-129 20 90 2-129 20 100 1-129 20 100 6-116 20 90 2-337 20 80 1-123 20 80 2-123 20 80 1-26 20 100 2-26 20 100 3-26 20 90 6-26 20 80 1-208 20 90 2-208 20 100 3-208 20 100 6-159 20 100 1-125 20 80 2-125 20 80 3-125 20 100 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 90 6-118 20 90 1-149 20 100 2-149 20 90 6-124 20 90 5-59 20 80 5-58 20 90 5-117 20 90 5-75 20 80 5-74 20 80 1-82 20 100 1-87 20 80 2-87 20 90 1-88 20 100 2-88 20 100 1-209 20 80 1-25 20 90 2-25 20 100 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 80 2-173 20 100 1-273 20 100 2-273 20 100 3-273 20 90 6-212 20 80 4-212 20 80 1-44 20 90 2-44 20 90 1-45 20 100 2-45 20 90 1-46 20 90 2-46 20 90 6-33 20 80 1-30 20 100 2-30 20 100 1-31 20 100 2-31 20 100 1-28 20 100 2-28 20 100 1-29 20 100 2-29 20 100 1-304 20 90 2-304 20 90 1-305 20 100 2-305 20 100 1-306 20 100 2-306 20 90 1-177 20 90 2-177 20 90 1-178 20 90 2-178 20 90 1-179 20 90 2-179 20 100 1-132 20 100 2-132 20 100 1-135 20 90 2-135 20 90 6-254 20 80 1-134 20 90 2-134 20 90 1-133 20 90 2-133 20 90 6-120 20 90 1-277 20 90 2-277 20 90 1-278 20 100 2-278 20 100 1-279 20 100 2-279 20 90 2-195 20 100 2-225 20 80 1-197 20 90 2-227 20 100 1-227 20 80 2-197 20 80 1-225 20 90 1-226 20 100 2-226 20 90 6-165 20 80 2-196 20 100 1-56 20 90 2-57 20 90 1-58 20 90 2-58 20 100 2-56 20 90 1-57 20 90 1-207 20 90 2-207 20 90 2-271 20 100 6-210 20 80 2-32 20 100 2-34 20 90 2-33 20 100 2-42 20 100 2-146 20 100 2-142 20 80 1-143 20 80 5-255 20 80 1-146 20 100 2-143 20 90 1-72 20 80 2-72 20 100 1-73 20 90 2-73 20 100 1-74 20 100 2-74 20 100 1-144 20 90 1-138 20 90 2-138 20 90 2-141 20 80 1-137 20 100 1-136 20 90 1-180 20 90 2-180 20 100 1-183 20 90 2-183 20 90 6-257 20 80 1-182 20 90 2-182 20 90 1-181 20 90 2-181 20 90 1-228 20 80 2-228 20 90 1-230 20 90 2-230 20 90 2-286 20 100 1-287 20 100 2-287 20 100 2-288 20 90 1-210 20 100 2-210 20 100 1-212 20 90 2-213 20 100 1-288 20 100 1-289 20 90 2-289 20 90 1-291 20 90 2-291 20 90 2-292 20 90 1-271 20 100 2-47 20 100 2-339 20 100 1-49 20 90 2-49 20 100 1-229 20 100 2-229 20 100 1-340 20 100 6-267 20 90 2-340 20 100 1-47 20 80 1-33 20 100 1-32 20 100 2-154 20 100 6-259 20 90 1-155 20 100 2-155 20 100 6-260 20 100 2-164 20 100 6-261 20 90 1-165 20 100 1-166 20 100 1-156 20 90 2-156 20 100 2-161 20 80 2-211 20 90 2-272 20 100 1-161 20 90 2-276 20 100 1-276 20 90 1-211 20 90 1-274 20 100 6-168 20 80 1-272 20 90 1-341 20 100 1-292 20 100 2-341 20 100 1-83 20 90 2-83 20 100 1-89 20 90 2-89 20 90 6-161 20 100 1-342 20 80 2-342 20 90 1-344 20 90 2-343 20 80 1-345 20 100 2-344 20 100 1-346 20 90 2-345 20 100 2-346 20 90 1-195 20 90 1-184 20 80 2-184 20 90 1-185 20 100 2-185 20 100 2-186 20 80 2-348 20 90 2-349 20 90 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 100 1-354 20 80 2-352 20 90 1-355 20 80 2-353 20 90 2-354 20 100
TABLE-US-00033 TABLE 9b Pre-emergence action at 80 g/ha against MATIN in % Example number Dosage [g/ha] MATIN 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 90 1-338 80 80 2-338 80 90 3-338 80 90 2-337 80 100 3-337 80 100 1-123 80 100 2-123 80 100 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 90 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 1-125 80 100 2-125 80 100 3-125 80 100 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 100 2-82 80 100 6-58 80 80 1-147 80 90 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 90 5-58 80 100 5-117 80 100 5-75 80 100 5-74 80 90 5-122 80 90 1-82 80 100 1-87 80 90 2-87 80 90 1-88 80 100 2-88 80 100 1-209 80 100 1-4 80 100 1-25 80 100 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 100 3-273 80 100 6-212 80 90 4-212 80 80 4-212 80 90 1-44 80 90 2-44 80 100 1-45 80 100 2-45 80 100 6-32 80 90 1-46 80 100 2-46 80 100 6-33 80 90 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 100 6-231 80 80 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 6-141 80 80 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 100 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 100 6-120 80 90 1-277 80 100 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 100 1-226 80 100 2-226 80 100 6-165 80 100 6-166 80 100 2-196 80 100 1-56 80 90 6-45 80 90 6-44 80 80 2-57 80 100 6-43 80 80 1-58 80 100 2-58 80 100 2-56 80 100 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 90 2-32 80 100 1-34 80 90 2-34 80 100 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 90 2-146 80 100 2-142 80 100 1-143 80 100 5-255 80 100 1-142 80 90 1-146 80 100 1-141 80 100 1-37 80 90 2-143 80 100 1-72 80 100 2-72 80 100 1-73 80 100 2-73 80 100 6-50 80 80 1-74 80 100 2-74 80 100 2-35 80 80 1-144 80 90 2-144 80 90 1-138 80 100 2-138 80 100 2-141 80 90 1-137 80 100 1-136 80 100 1-180 80 100 2-180 80 100 1-183 80 100 2-183 80 100 6-257 80 90 1-182 80 100 2-182 80 100 1-181 80 100 2-181 80 100 6-144 80 80 2-36 80 90 1-228 80 100 2-228 80 100 6-167 80 90 1-230 80 100 2-230 80 100 6-169 80 80 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 100 2-289 80 100 6-228 80 80 1-291 80 100 2-291 80 100 6-230 80 80 2-292 80 100 1-271 80 100 2-47 80 100 6-34 80 90 1-339 80 100 2-339 80 100 6-258 80 90 1-49 80 100 2-49 80 100 1-41 80 100 1-229 80 100 2-229 80 100 1-340 80 100 6-267 80 100 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 100 6-260 80 100 1-164 80 100 2-164 80 100 6-261 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 100 1-159 80 90 2-159 80 90 1-162 80 90 2-162 80 90 1-160 80 80 2-160 80 90 2-161 80 90 6-266 80 80 2-211 80 100 2-272 80 100 1-161 80 100 2-276 80 100 1-276 80 100 1-211 80 100 1-274 80 100 6-168 80 90 1-272 80 100 6-211 80 90 1-341 80 100 1-292 80 100 2-341 80 100 2-158 80 90 1-83 80 100 2-83 80 100 6-60 80 90 1-89 80 100 2-89 80 100 6-76 80 90 6-161 80 100 1-342 80 100 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 100 1-345 80 100 2-344 80 100 1-346 80 100 2-345 80 100 1-347 80 90 2-346 80 90 1-195 80 100 1-184 80 100 2-184 80 100 1-185 80 100 2-185 80 100 1-186 80 90 2-186 80 100 1-349 80 90 1-350 80 90 2-348 80 90 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 1-354 80 80 2-352 80 90 1-355 80 100 2-353 80 100 1-356 80 100 2-354 80 100
TABLE-US-00034 TABLE 9c Pre-emergence action at 320 g/ha against MATIN in % Example number Dosage [g/ha] MATIN 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00035 TABLE 10a Pre-emergence action at 20 g/ha against PHBPU in % Example number Dosage [g/ha] PHBPU 3-129 20 80 2-26 20 90 2-27 20 80 2-134 20 80 1-277 20 80 2-279 20 80 2-197 20 80 2-196 20 80 1-56 20 80 1-57 20 80 2-33 20 80 2-42 20 80 1-138 20 80 1-137 20 80 2-287 20 80 2-210 20 80 1-212 20 80 2-213 20 80 2-291 20 80 2-292 20 80 1-271 20 80 1-339 20 100 2-154 20 80 2-86 20 80
TABLE-US-00036 TABLE 10b Pre-emergence action at 80 g/ha against PHBPU in % Example Dosage number [g/ha] PHBPU 3-129 80 90 2-129 80 90 1-129 80 90 3-337 80 90 2-26 80 100 2-131 80 80 2-149 80 80 5-59 80 80 5-117 80 100 1-82 80 80 1-87 80 80 2-87 80 80 1-88 80 90 2-88 80 90 1-209 80 80 1-25 80 90 2-25 80 80 3-27 80 90 1-27 80 100 2-27 80 90 1-173 80 90 2-173 80 90 1-273 80 100 2-273 80 90 3-273 80 90 1-44 80 80 1-45 80 90 2-45 80 80 1-46 80 80 2-46 80 90 1-30 80 100 2-30 80 80 1-31 80 80 2-31 80 80 2-29 80 80 1-304 80 80 2-304 80 90 1-305 80 90 2-305 80 90 1-306 80 90 2-306 80 100 1-177 80 80 2-177 80 80 1-178 80 80 2-179 80 80 1-132 80 80 2-132 80 90 1-135 80 80 2-135 80 80 1-134 80 80 2-134 80 90 2-133 80 80 6-120 80 80 1-277 80 90 2-277 80 80 1-278 80 90 2-278 80 90 1-279 80 90 2-279 80 90 2-225 80 90 2-227 80 90 1-227 80 80 2-197 80 90 1-225 80 100 2-226 80 100 2-196 80 90 1-56 80 80 2-57 80 80 1-58 80 90 2-58 80 90 2-56 80 80 1-57 80 80 1-207 80 80 2-207 80 80 2-271 80 100 2-32 80 90 2-34 80 80 6-255 80 90 2-33 80 80 2-42 80 90 6-256 80 80 2-146 80 90 1-146 80 80 1-141 80 80 2-37 80 80 2-73 80 80 1-74 80 100 2-74 80 90 1-138 80 90 2-138 80 80 2-141 80 80 1-137 80 90 1-136 80 80 2-180 80 100 1-183 80 90 2-183 80 90 1-182 80 90 2-182 80 90 1-181 80 80 2-181 80 80 1-228 80 90 2-228 80 100 1-230 80 90 2-230 80 80 2-286 80 90 1-287 80 100 2-287 80 80 2-288 80 90 1-210 80 80 2-210 80 90 1-212 80 80 2-212 80 80 2-213 80 90 1-288 80 100 1-289 80 80 2-289 80 80 6-228 80 80 1-291 80 80 2-291 80 90 2-292 80 90 1-271 80 90 2-47 80 90 1-339 80 100 2-339 80 80 6-258 80 90 2-49 80 80 1-229 80 90 1-340 80 90 2-340 80 80 1-33 80 100 1-32 80 80 2-154 80 100 6-259 80 80 1-155 80 100 2-155 80 100 1-164 80 100 2-164 80 100 1-165 80 100 1-166 80 80 1-156 80 80 2-159 80 90 2-272 80 80 1-161 80 80 2-276 80 90 1-276 80 90 1-211 80 80 1-274 80 90 1-272 80 80 1-341 80 80 1-292 80 80 2-341 80 80 1-89 80 80 2-344 80 90 2-345 80 80 1-184 80 80 2-184 80 90 1-185 80 80 2-185 80 100 1-186 80 80 2-348 80 80 2-84 80 90 1-86 80 80 2-86 80 90 1-92 80 90 2-92 80 90 2-351 80 80
TABLE-US-00037 TABLE 10c Pre-emergence action at 320 g/ha against PHBPU in % Example Dosage number [g/ha] PHBPU 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 80 1-338 320 80 2-338 320 80 3-338 320 100 2-337 320 90
TABLE-US-00038 TABLE 11a Pre-emergence action at 20 g/ha against POLCO in % Example Dosage number [g/ha] POLCO 2-129 20 100 1-337 20 80 3-26 20 80 1-208 20 80 1-125 20 80 5-74 20 80 2-25 20 100 2-27 20 80 2-173 20 90 2-44 20 80 1-45 20 90 2-30 20 80 2-31 20 80 1-278 20 90 2-278 20 80 1-279 20 80 2-279 20 80 1-58 20 80 2-146 20 80 2-72 20 80 2-144 20 80 1-137 20 80 2-183 20 90 1-166 20 100 1-276 20 80 1-274 20 80 1-272 20 80
TABLE-US-00039 TABLE 11b Pre-emergence action at 80 g/ha against POLCO in % Example Dosage number [g/ha] POLCO 3-129 80 80 2-129 80 100 1-129 80 100 3-338 80 80 1-337 80 80 2-123 80 80 1-26 80 90 2-26 80 80 3-26 80 90 6-26 80 100 1-208 80 90 2-208 80 90 3-208 80 80 6-159 80 80 1-125 80 80 1-131 80 80 2-131 80 90 6-118 80 80 1-149 80 80 2-149 80 100 5-117 80 80 5-74 80 80 5-123 80 80 1-82 80 90 1-87 80 90 1-88 80 80 2-88 80 90 1-25 80 80 2-25 80 100 2-27 80 100 1-173 80 80 2-173 80 100 1-273 80 90 2-44 80 90 1-45 80 90 2-45 80 90 6-32 80 80 1-46 80 80 2-46 80 90 2-30 80 80 2-31 80 80 2-28 80 90 1-304 80 80 2-304 80 80 1-305 80 80 1-306 80 90 2-306 80 80 1-132 80 80 2-132 80 80 1-277 80 90 2-277 80 90 1-278 80 100 2-278 80 80 1-279 80 90 2-279 80 90 2-195 80 80 2-225 80 90 1-227 80 90 2-197 80 100 1-225 80 90 1-226 80 90 2-226 80 80 6-165 80 80 6-166 80 80 2-196 80 90 1-56 80 90 2-57 80 90 1-58 80 90 2-58 80 80 2-56 80 90 1-207 80 90 2-207 80 90 2-271 80 80 2-32 80 90 2-34 80 90 2-42 80 80 2-146 80 80 1-146 80 80 2-72 80 80 2-73 80 80 1-74 80 80 2-74 80 80 2-35 80 80 2-144 80 90 1-138 80 90 2-138 80 90 2-141 80 80 1-137 80 100 1-180 80 100 2-180 80 90 1-183 80 80 2-183 80 90 2-182 80 90 6-169 80 100 2-287 80 80 2-288 80 90 1-212 80 80 2-212 80 80 1-288 80 80 1-289 80 80 2-289 80 80 1-291 80 80 2-291 80 80 2-292 80 100 1-271 80 80 2-47 80 80 1-339 80 80 2-339 80 80 6-258 80 80 1-49 80 90 2-49 80 90 1-229 80 80 1-340 80 90 1-47 80 100 1-33 80 90 1-32 80 100 2-154 80 90 6-259 80 90 1-155 80 90 2-155 80 90 2-164 80 90 1-165 80 90 1-166 80 100 2-156 80 90 2-272 80 80 1-161 80 80 2-276 80 90 1-276 80 90 1-211 80 90 1-274 80 90 1-272 80 90 6-211 80 90 1-341 80 80 1-292 80 90 2-83 80 90 1-89 80 80 2-342 80 80 2-343 80 90 1-345 80 90 2-344 80 90 1-346 80 80 2-345 80 90 1-184 80 80 2-348 80 90 2-350 80 100 1-86 80 80 1-354 80 80 1-355 80 80
TABLE-US-00040 TABLE 11c Pre-emergence action at 320 g/ha against POLCO in % Example Dosage number [g/ha] POLCO 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 90 1-338 320 80 2-338 320 90 3-338 320 80 2-337 320 80 2-81 320 100 2-82 320 90 1-147 320 90 2-147 320 80 1-148 320 80 2-148 320 100
TABLE-US-00041 TABLE 12a Pre-emergence action at 20 g/ha against SETVI in % Example Dosage number [g/ha] SETVI 2-129 20 100 2-337 20 90 1-26 20 80 2-26 20 80 1-208 20 100 2-208 20 80 1-130 20 90 2-130 20 90 1-131 20 80 2-131 20 80 1-149 20 90 6-124 20 80 1-82 20 80 1-209 20 90 1-25 20 80 2-25 20 100 1-27 20 100 1-173 20 90 1-273 20 100 2-273 20 80 1-30 20 90 2-30 20 100 1-304 20 90 1-305 20 80 2-177 20 100 1-179 20 80 1-132 20 80 1-134 20 90 2-134 20 80 2-133 20 100 1-279 20 80 2-279 20 80 2-195 20 80 1-197 20 100 2-227 20 100 2-197 20 90 1-225 20 90 1-226 20 100 2-226 20 80 6-165 20 90 2-196 20 90 1-56 20 90 2-57 20 80 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 90 1-207 20 100 2-207 20 100 2-271 20 100 2-32 20 100 2-34 20 100 6-255 20 100 2-33 20 80 2-42 20 80 6-256 20 80 1-141 20 90 1-37 20 90 1-74 20 100 2-141 20 90 1-182 20 100 2-182 20 90 6-167 20 80 1-230 20 90 2-286 20 80 1-287 20 90 2-287 20 90 2-288 20 90 1-212 20 80 1-288 20 100 1-340 20 90 1-155 20 80 1-166 20 80 1-272 20 80 1-341 20 80 1-89 20 90 1-346 20 100 1-195 20 90 1-349 20 90 1-351 20 100 1-86 20 80 2-92 20 100
TABLE-US-00042 TABLE 12b Pre-emergence action at 80 g/ha against SETVI in % Example Dosage number [g/ha] SETVI 3-129 80 90 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 90 1-337 80 90 2-337 80 100 6-252 80 90 1-26 80 100 2-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 100 2-82 80 100 6-58 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 100 5-58 80 100 5-117 80 90 5-253 80 80 5-75 80 100 5-74 80 90 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 1-209 80 100 1-4 80 100 1-25 80 100 2-25 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 90 3-273 80 100 6-212 80 90 1-44 80 100 2-44 80 100 1-45 80 100 2-45 80 100 1-46 80 100 2-46 80 100 6-33 80 100 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 90 1-305 80 100 2-305 80 80 1-306 80 100 2-306 80 100 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 80 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 100 6-120 80 100 1-277 80 100 2-277 80 80 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 100 1-226 80 100 2-226 80 100 6-165 80 100 6-166 80 100 2-196 80 100 1-56 80 100 6-45 80 100 6-44 80 90 2-57 80 100 6-43 80 90 1-58 80 100 2-58 80 100 2-56 80 100 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 100 2-32 80 100 1-34 80 100 2-34 80 100 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 100 2-146 80 100 1-146 80 80 1-141 80 100 1-37 80 100 2-37 80 100 1-72 80 100 2-72 80 100 1-73 80 100 2-73 80 100 1-74 80 100 2-74 80 100 1-144 80 80 1-138 80 100 2-138 80 80 2-141 80 100 1-137 80 100 1-136 80 80 1-180 80 90 2-180 80 100 1-183 80 100 2-183 80 100 1-182 80 100 2-182 80 100 6-145 80 100 1-181 80 100 2-181 80 100 6-144 80 90 1-228 80 100 2-228 80 90 6-167 80 80 1-230 80 100 2-230 80 90 6-169 80 100 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 80 2-289 80 90 6-228 80 80 1-291 80 100 2-291 80 100 2-292 80 100 1-271 80 100 2-47 80 100 2-339 80 100 6-258 80 80 1-49 80 80 2-49 80 100 1-229 80 100 2-229 80 100 1-340 80 100 6-267 80 80 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 90 6-260 80 100 2-164 80 80 6-261 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 100 1-162 80 80 6-264 80 80 2-211 80 100 2-272 80 100 2-276 80 100 1-276 80 100 1-211 80 100 1-274 80 100 6-168 80 90 1-272 80 100 6-211 80 100 1-341 80 100 1-292 80 100 2-341 80 90 1-83 80 100 2-83 80 100 1-89 80 100 2-89 80 100 6-76 80 80 6-161 80 100 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 100 1-345 80 100 2-344 80 80 1-346 80 100 2-345 80 100 1-195 80 100 1-185 80 100 2-185 80 100 1-186 80 80 1-349 80 100 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 1-354 80 90 2-352 80 100 1-355 80 90
TABLE-US-00043 TABLE 12c Pre-emergence action at 320 g/ha against SETVI in % Example Dosage number [g/ha] SETVI 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00044 TABLE 13a Pre-emergence action at 20 g/ha against STEME in % Example Dosage number [g/ha] STEME 3-129 20 90 2-129 20 80 1-129 20 100 6-116 20 90 2-337 20 90 1-26 20 100 2-26 20 100 3-26 20 80 6-26 20 80 1-208 20 100 2-208 20 100 3-208 20 90 6-159 20 80 2-125 20 80 3-125 20 90 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 100 6-118 20 90 1-149 20 90 2-149 20 100 6-124 20 80 5-59 20 90 5-58 20 100 5-117 20 90 5-75 20 100 5-74 20 90 5-123 20 90 5-122 20 90 1-82 20 100 1-87 20 90 2-87 20 100 1-88 20 100 2-88 20 100 1-25 20 80 2-25 20 90 3-27 20 100 1-27 20 90 2-27 20 100 1-173 20 80 2-173 20 100 1-273 20 100 2-273 20 90 3-273 20 90 6-212 20 80 1-44 20 90 2-44 20 90 1-45 20 90 2-45 20 90 1-46 20 90 2-46 20 90
TABLE-US-00045 TABLE 13b Pre-emergence action at 80 g/ha against STEME in % Example Dosage number [g/ha] STEME 3-129 80 100 2-129 80 80 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 90 3-338 80 90 2-337 80 90 3-337 80 100 1-123 80 90 2-123 80 80 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 1-125 80 100 2-125 80 100 3-125 80 100 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 90 2-82 80 100 6-58 80 90 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 90 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 90 5-59 80 100 5-58 80 100 5-117 80 90 5-253 80 90 5-75 80 100 5-74 80 100 5-123 80 90 5-122 80 90 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 1-209 80 90 1-4 80 90 1-25 80 90 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 90 3-273 80 100 6-212 80 90 4-212 80 90 1-44 80 90 2-44 80 100 1-45 80 90 2-45 80 100 6-32 80 90 1-46 80 100 2-46 80 100
TABLE-US-00046 TABLE 13c Pre-emergence action at 320 g/ha against STEME in % Example number Dosage [g/ha] STEME 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 90 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 90 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00047 TABLE 14a Pre-emergence action at 20 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 2-337 20 80 1-125 20 80 1-209 20 90 1-4 20 80 1-25 20 80 1-27 20 80 2-27 20 80 1-178 20 80 2-56 20 80 2-32 20 90 2-34 20 90 2-33 20 80 6-256 20 80 2-37 20 80 1-73 20 80 2-73 20 90 1-183 20 90 2-286 20 80 2-287 20 90 2-292 20 90 1-271 20 90 1-339 20 100 2-339 20 80 6-258 20 90 1-340 20 100 1-32 20 80 2-155 20 80 1-165 20 80 1-166 20 80 2-156 20 80 1-161 20 80 1-274 20 90 1-341 20 80 1-292 20 100 1-158 20 80 2-158 20 80 2-342 20 80 1-344 20 80 1-349 20 90 1-84 20 80 2-84 20 80 1-352 20 90 1-356 20 100 2-354 20 80
TABLE-US-00048 TABLE 14b Pre-emergence action at 80 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 1-129 80 100 1-338 80 90 2-338 80 100 3-338 80 90 1-337 80 90 2-337 80 90 3-337 80 100 1-26 80 80 1-125 80 80 3-125 80 80 1-130 80 80 2-130 80 80 2-81 80 90 1-148 80 80 2-148 80 80 1-149 80 100 2-149 80 80 5-58 80 80 5-75 80 90 5-122 80 100 1-82 80 90 1-87 80 90 2-87 80 90 1-88 80 100 2-88 80 100 1-209 80 100 1-4 80 90 1-25 80 100 2-25 80 100 3-27 80 90 1-27 80 90 2-27 80 100 2-173 80 80 1-273 80 90 2-273 80 100 3-273 80 100 2-44 80 90 1-45 80 90 2-45 80 90 1-46 80 90 2-46 80 90 1-31 80 100 2-28 80 80 1-304 80 100 2-304 80 100 1-305 80 100 2-305 80 100 1-306 80 90 2-306 80 100 1-177 80 100 2-177 80 80 1-178 80 80 2-178 80 90 2-179 80 90 1-132 80 100 1-135 80 90 2-135 80 100 6-254 80 100 1-277 80 90 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 90 2-279 80 90 2-225 80 100 2-227 80 100 1-227 80 100 2-197 80 90 1-225 80 80 1-226 80 90 2-226 80 100 2-196 80 80 1-56 80 90 2-57 80 90 1-58 80 100 2-56 80 100 1-57 80 80 1-207 80 100 2-207 80 90 2-271 80 100 2-32 80 100 1-34 80 100 2-34 80 90 6-255 80 90 2-33 80 90 2-42 80 90 6-256 80 80 2-146 80 80 2-37 80 80 2-143 80 80 2-72 80 90 1-73 80 100 2-73 80 90 1-74 80 100 2-74 80 90 1-144 80 80 2-144 80 100 1-138 80 90 2-138 80 100 1-137 80 90 1-136 80 90 1-180 80 80 1-183 80 100 2-183 80 90 2-181 80 100 1-36 80 90 1-228 80 90 2-228 80 90 1-230 80 100 2-230 80 100 2-286 80 100 1-287 80 90 2-287 80 100 2-288 80 100 1-210 80 80 2-213 80 90 1-288 80 100 1-289 80 100 2-289 80 100 2-291 80 90 2-292 80 100 1-271 80 100 2-47 80 100 1-339 80 100 2-339 80 100 6-258 80 100 1-49 80 100 2-49 80 100 1-41 80 90 1-229 80 100 2-229 80 80 1-340 80 100 6-267 80 90 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 1-155 80 100 2-155 80 100 6-260 80 90 1-164 80 90 2-164 80 100 1-165 80 100 1-166 80 100 2-156 80 100 1-159 80 80 2-159 80 80 6-264 80 90 2-160 80 80 2-161 80 80 2-272 80 90 1-161 80 90 2-276 80 80 1-211 80 100 1-274 80 90 1-272 80 90 6-211 80 80 1-341 80 90 1-292 80 100 2-341 80 90 1-158 80 80 2-158 80 90 1-83 80 80 1-89 80 90 2-89 80 90 6-268 80 90 1-343 80 80 2-342 80 80 1-344 80 90 1-345 80 80 2-344 80 80 1-346 80 80 2-345 80 100 2-346 80 80 1-184 80 90 2-184 80 100 2-186 80 90 1-349 80 90 1-350 80 80 2-348 80 80 1-351 80 90 2-349 80 80 1-84 80 100 2-84 80 80 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 90 1-92 80 100 2-92 80 100 1-90 80 90 2-90 80 90 1-353 80 100 2-351 80 100 1-355 80 100 1-356 80 100 2-354 80 80
TABLE-US-00049 TABLE 14c Pre-emergence action at 320 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 80 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 90 6-117 320 90 1-81 320 100 2-81 320 90 2-82 320 90 1-147 320 90 2-147 320 90 1-148 320 100 2-148 320 100
TABLE-US-00050 TABLE 15a Pre-emergence action at 20 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 20 100 2-129 20 100 1-129 20 100 1-337 20 80 2-337 20 90 3-337 20 100 1-26 20 90 2-26 20 100 3-26 20 100 1-208 20 100 2-208 20 100 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 100 6-118 20 90 1-149 20 100 2-149 20 100 5-59 20 100 5-58 20 90 5-117 20 100 5-75 20 100 5-123 20 90 5-122 20 80 1-82 20 100 1-87 20 80 2-87 20 90 1-88 20 100 2-88 20 100 1-25 20 80 3-27 20 90 1-27 20 100 2-27 20 100 1-173 20 80 1-273 20 100 2-273 20 90 3-273 20 100 2-44 20 100 1-45 20 80 2-45 20 90 1-46 20 90 2-46 20 100 1-30 20 100 2-30 20 100 1-31 20 100 2-31 20 100 1-28 20 100 2-28 20 100 1-29 20 100 2-29 20 100 1-304 20 100 2-304 20 90 1-305 20 100 2-305 20 90 1-306 20 100 2-306 20 100 2-177 20 100 2-178 20 100 1-179 20 100 2-179 20 100 1-132 20 100 2-132 20 100 2-135 20 100 1-134 20 90 2-134 20 100 1-133 20 100 1-277 20 100 2-277 20 100 1-278 20 100 2-278 20 100 1-279 20 100 2-279 20 100 2-195 20 100 2-225 20 80 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 100 1-226 20 80 2-226 20 100 6-165 20 80 2-196 20 90 1-56 20 100 2-57 20 100 1-58 20 100 2-58 20 100 2-56 20 80 1-57 20 100 1-207 20 100 2-207 20 90 2-271 20 100 2-32 20 100 1-34 20 100 2-34 20 100 6-255 20 80 2-33 20 100 2-42 20 100 6-256 20 90 2-146 20 100 1-141 20 80 2-72 20 100 6-49 20 80 1-73 20 100 2-73 20 90 1-74 20 100 2-74 20 100 1-144 20 80 1-138 20 100 2-138 20 90 1-137 20 90 1-136 20 90 1-180 20 80 2-180 20 100 1-183 20 100 1-182 20 90 2-182 20 100 1-181 20 100 1-228 20 90 2-228 20 100 6-167 20 90 1-230 20 100 2-230 20 90 2-286 20 90 1-287 20 100 2-287 20 100 2-288 20 100 1-210 20 100 2-210 20 100 1-212 20 100 2-213 20 100 1-288 20 100 1-289 20 100 2-289 20 100 1-291 20 100 2-291 20 100 2-292 20 100 1-271 20 100 2-47 20 80 1-339 20 100 2-339 20 100 2-49 20 90 1-340 20 100 2-340 20 100 1-33 20 100 2-155 20 90 1-165 20 90 1-166 20 100 2-272 20 90 2-276 20 100 1-276 20 80 1-274 20 90 1-272 20 90 1-341 20 100 1-292 20 90 2-341 20 90 1-83 20 90 2-89 20 90 2-342 20 90 2-343 20 90 2-344 20 80 1-346 20 80 2-345 20 80 2-346 20 80 1-195 20 100 1-185 20 80 2-185 20 80 1-351 20 100 2-349 20 90 2-84 20 80 1-352 20 100 2-350 20 100 1-86 20 100 2-92 20 90 1-90 20 90 2-90 20 80 1-353 20 100 2-351 20 100 2-352 20 80 2-353 20 90 2-354 20 80
TABLE-US-00051 TABLE 15b Pre-emergence action at 80 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 80 2-338 80 100 3-338 80 90 1-337 80 80 2-337 80 100 3-337 80 100 1-123 80 80 2-123 80 80 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 100 6-159 80 100 1-125 80 100 2-125 80 100 3-125 80 100 1-130 80 100 2-130 80 100 6-117 80 80 1-81 80 90 2-81 80 90 2-82 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 90 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 100 5-58 80 100 5-117 80 100 5-253 80 90 5-75 80 100 5-74 80 100 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 90 1-88 80 100 2-88 80 100 1-209 80 100 1-25 80 100 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 90 2-173 80 100 1-273 80 100 2-273 80 100 3-273 80 100 4-212 80 90 1-44 80 90 2-44 80 100 1-45 80 100 2-45 80 100 1-46 80 100 2-46 80 100 6-33 80 100 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 100 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 90 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 90 6-120 80 90 1-277 80 100 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 100 1-226 80 100 2-226 80 100 6-165 80 90 6-166 80 100 2-196 80 100 1-56 80 100 6-45 80 90 2-57 80 100 1-58 80 100 2-58 80 100 2-56 80 90 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 90 2-32 80 100 1-34 80 100 2-34 80 100 6-255 80 90 2-33 80 100 2-42 80 100 6-256 80 90 2-146 80 100 2-142 80 100 5-255 80 100 1-142 80 90 5-254 80 90 1-140 80 90 1-146 80 100 1-141 80 100 1-37 80 100 2-37 80 100 2-143 80 80 1-72 80 100 2-72 80 100 6-49 80 80 1-73 80 100 2-73 80 100 1-74 80 100 2-74 80 100 1-144 80 100 2-144 80 90 1-138 80 100 2-138 80 100 2-141 80 90 1-137 80 100 1-136 80 100 1-180 80 100 2-180 80 100 1-183 80 100 2-183 80 100 1-182 80 100 2-182 80 100 1-181 80 100 2-181 80 80 2-36 80 100 1-228 80 100 2-228 80 100 6-167 80 100 1-230 80 100 2-230 80 100 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 100 2-289 80 100 1-291 80 100 2-291 80 100 2-292 80 100 1-271 80 100 2-47 80 100 1-339 80 100 2-339 80 100 6-258 80 80 1-49 80 100 2-49 80 100 1-41 80 100 1-229 80 100 2-229 80 100 1-340 80 100 6-267 80 80 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 80 1-155 80 100 2-155 80 100 2-164 80 100 1-165 80 100 1-166 80 100 1-156 80 100 2-156 80 100 6-262 80 90 2-159 80 80 2-162 80 80 1-160 80 80 2-160 80 100 2-161 80 100 2-211 80 80 2-272 80 100 2-276 80 100 1-276 80 100 1-211 80 100 1-274 80 90 1-272 80 100 6-211 80 80 1-341 80 100 1-292 80 100 2-341 80 100 1-158 80 90 2-158 80 100 1-83 80 100 2-83 80 100 1-89 80 100 2-89 80 100 6-161 80 80 1-343 80 100 2-342 80 100 1-344 80 100 2-343 80 100 1-345 80 100 2-344 80 100 1-346 80 100 2-345 80 100 1-347 80 80 2-346 80 80 1-195 80 100 1-184 80 90 2-184 80 100 1-185 80 100 2-185 80 100 2-186 80 90 1-349 80 100 1-350 80 100 2-348 80 100 1-351 80 100 2-349 80 100 1-84 80 100 2-84 80 100 1-352 80 100 2-350 80 100 1-86 80 100 2-86 80 100 1-92 80 100 2-92 80 100 1-90 80 100 2-90 80 100 1-353 80 100 2-351 80 100 2-352 80 80 1-355 80 100 2-353 80 100 1-356 80 100 2-354 80 100
TABLE-US-00052 TABLE 15c Pre-emergence action at 320 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 320 100 2-129 320 100 1-129 320 100 6-116 320 100 1-338 320 100 2-338 320 100 3-338 320 100 6-253 320 100 2-337 320 100 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 90 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
TABLE-US-00053 TABLE 16a Pre-emergence action at 20 g/ha against DIGSA in % Example number Dosage [g/ha] DIGSA 2-337 20 90 3-337 20 90 2-123 20 80 1-26 20 100 2-26 20 100 6-26 20 100 1-208 20 100 2-208 20 90 6-159 20 90 1-130 20 100 2-130 20 100 1-131 20 100 2-131 20 90 6-118 20 90 1-149 20 100 2-149 20 90 5-59 20 100 5-58 20 90 5-117 20 100 5-253 20 80 5-75 20 100 5-74 20 90 5-123 20 100 5-122 20 100 1-82 20 100 1-87 20 100 2-87 20 100 1-88 20 100 2-88 20 100 1-209 20 100 1-25 20 90 2-25 20 100 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 100 1-273 20 100 2-273 20 100 3-273 20 90 6-212 20 100 4-212 20 80 4-212 20 80 1-44 20 90 2-44 20 100 1-45 20 100 2-45 20 90 6-32 20 90 1-46 20 90 2-46 20 100 6-33 20 80 1-30 20 100 2-30 20 100 1-31 20 100 2-31 20 100 1-28 20 100 2-28 20 100 1-29 20 100 2-29 20 90 1-304 20 100 2-304 20 90 6-231 20 80 1-305 20 100 2-305 20 100 1-306 20 100 2-306 20 100 1-177 20 100 2-177 20 100 1-178 20 100 2-178 20 100 6-141 20 90 1-179 20 100 2-179 20 100 1-132 20 100 2-132 20 80 1-135 20 90 2-135 20 100 6-254 20 90 1-134 20 90 2-134 20 80 1-133 20 90 1-277 20 100 2-277 20 90 1-278 20 100 2-278 20 100 1-279 20 100 2-279 20 90 2-195 20 90 2-225 20 100 1-197 20 100 2-227 20 90 1-227 20 100 2-197 20 100 6-165 20 90 6-166 20 80 2-196 20 90 6-45 20 90 2-57 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 90 2-271 20 100 6-210 20 100 2-32 20 100 1-34 20 100 2-34 20 100 6-255 20 100 2-33 20 100 2-42 20 100 6-256 20 90 1-146 20 100 1-141 20 90 1-37 20 80 1-72 20 90 2-72 20 100 1-73 20 90 2-73 20 90 1-74 20 100 2-74 20 100 1-144 20 90 1-138 20 100 2-138 20 100 1-137 20 100 1-136 20 100 1-180 20 100 2-180 20 100 1-183 20 100 2-183 20 90 1-182 20 100 2-182 20 100 6-145 20 90 1-181 20 100 6-144 20 90 1-228 20 100 2-228 20 100 1-230 20 90 2-230 20 100 2-286 20 100 1-287 20 100 2-287 20 100 2-288 20 100 1-210 20 100 2-210 20 100 1-212 20 100 2-213 20 80 1-288 20 100 1-289 20 100 2-289 20 100 6-228 20 90 1-291 20 100 2-291 20 100 2-292 20 100 1-271 20 100 2-47 20 100 6-34 20 100 1-339 20 100 2-339 20 100 6-258 20 100 1-49 20 90 2-49 20 100 1-229 20 100 1-340 20 100 2-340 20 100 1-47 20 100 1-33 20 100 1-32 20 100 2-154 20 100 6-259 20 100 1-155 20 100 2-155 20 100 6-260 20 100 6-261 20 80 1-165 20 100 1-156 20 100 2-156 20 100 6-262 20 100
TABLE-US-00054 TABLE 16b Pre-emergence action at 80 g/ha against DIGSA in % Example Dosage number [g/ha] DIGSA 1-337 80 100 2-337 80 100 3-337 80 100 6-252 80 90 1-123 80 90 2-123 80 90 1-26 80 100 2-26 80 100 3-26 80 100 6-26 80 100 1-208 80 100 2-208 80 100 3-208 80 80 6-159 80 100 1-125 80 90 3-125 80 80 1-130 80 100 2-130 80 100 6-117 80 100 1-81 80 100 2-81 80 100 2-82 80 100 6-58 80 100 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 100 1-131 80 100 2-131 80 100 6-118 80 100 1-149 80 100 2-149 80 100 6-124 80 100 5-59 80 100 5-58 80 100 5-117 80 100 5-253 80 90 5-75 80 100 5-74 80 100 5-123 80 100 5-122 80 100 1-82 80 100 1-87 80 100 2-87 80 100 1-88 80 100 2-88 80 100 6-75 80 80 1-209 80 100 1-4 80 100 1-25 80 100 2-25 80 100 3-27 80 100 1-27 80 100 2-27 80 100 1-173 80 100 2-173 80 100 1-273 80 100 2-273 80 100 3-273 80 100 6-212 80 100 4-212 80 90 4-212 80 90 1-44 80 100 2-44 80 100 1-45 80 100 2-45 80 100 6-32 80 100 1-46 80 100 2-46 80 100 6-33 80 100 1-30 80 100 2-30 80 100 1-31 80 100 2-31 80 100 1-28 80 100 2-28 80 100 1-29 80 100 2-29 80 100 1-304 80 100 2-304 80 100 6-231 80 90 1-305 80 100 2-305 80 100 1-306 80 100 2-306 80 100 6-233 80 90 1-177 80 100 2-177 80 100 1-178 80 100 2-178 80 100 6-141 80 100 1-179 80 100 2-179 80 100 1-132 80 100 2-132 80 100 1-135 80 100 2-135 80 100 6-254 80 100 1-134 80 100 2-134 80 100 1-133 80 100 2-133 80 90 6-120 80 90 1-277 80 100 2-277 80 100 1-278 80 100 2-278 80 100 1-279 80 100 2-279 80 100 2-195 80 100 2-225 80 100 1-197 80 100 2-227 80 100 1-227 80 100 2-197 80 100 1-225 80 90 1-226 80 90 6-165 80 100 6-166 80 100 2-196 80 100 1-56 80 80 6-45 80 100 2-57 80 100 6-43 80 100 1-58 80 80 2-58 80 100 2-56 80 100 1-57 80 100 1-207 80 100 2-207 80 100 2-271 80 100 6-210 80 100 2-32 80 100 1-34 80 100 2-34 80 100 6-255 80 100 2-33 80 100 2-42 80 100 6-256 80 100 2-146 80 100 1-143 80 80 1-146 80 100 1-141 80 100 1-37 80 100 2-37 80 100 1-72 80 100 2-72 80 100 1-73 80 100 2-73 80 100 6-50 80 100 1-74 80 100 2-74 80 100 6-51 80 100 1-144 80 90 2-144 80 100 1-138 80 100 2-138 80 100 2-141 80 90 1-137 80 100 1-136 80 100 1-180 80 100 2-180 80 100 6-143 80 100 1-183 80 100 2-183 80 100 6-257 80 100 1-182 80 100 2-182 80 100 6-145 80 100 1-181 80 100 2-181 80 100 6-144 80 100 2-36 80 90 1-228 80 100 2-228 80 100 6-167 80 90 1-230 80 100 2-230 80 100 6-169 80 90 2-286 80 100 1-287 80 100 2-287 80 100 2-288 80 100 1-210 80 100 2-210 80 100 1-212 80 100 2-212 80 100 2-213 80 100 1-288 80 100 1-289 80 100 2-289 80 100 6-228 80 100 1-291 80 100 2-291 80 100 6-230 80 80 2-292 80 100 1-271 80 100 2-47 80 100 6-34 80 100 1-339 80 100 2-339 80 100 6-258 80 100 1-49 80 100 2-49 80 100 1-41 80 100 1-229 80 100 2-229 80 100 1-340 80 100 2-340 80 100 1-47 80 100 1-33 80 100 1-32 80 100 2-154 80 100 6-259 80 100 1-155 80 100 2-155 80 100 6-260 80 100 1-164 80 80 2-164 80 100 6-261 80 100 1-165 80 100 1-166 80 90 1-156 80 100 2-156 80 100 6-262 80 100
TABLE-US-00055 TABLE 16c Pre-emergence action at 320 g/ha against DIGSA in % Example Dosage number [g/ha] DIGSA 2-337 320 100 6-252 320 90 6-117 320 100 1-81 320 100 2-81 320 100 2-82 320 100 6-58 320 100 1-147 320 100 2-147 320 100 1-148 320 100 2-148 320 100
[0767] 2. Post-Emergence Herbicidal Action Against Harmful Plants
[0768] Seeds of monocotyledonous and dicotyledonous weed and crop plants are laid out in sandy loam soil in wood-fiber pots, covered with soil and cultivated in a greenhouse under good growth conditions. 2 to 3 weeks after sowing, the test plants are treated at the one-leaf stage. The compounds of the invention, formulated in the form of wettable powders (WP) or as emulsion concentrates (EC), are then sprayed onto the green parts of the plants in the form of an aqueous suspension or emulsion at a water application rate equivalent to 600 to 800 l/ha, with addition of 0.2% wetting agent. After the test plants have been left to stand in the greenhouse under optimal growth conditions for about 3 weeks, the action of the preparations is assessed visually in comparison to untreated controls (herbicidal action in percent (%): 100% activity=the plants have died, 0% activity=like control plants). Numerous compounds of the invention showed very good action against a multitude of important harmful plants. The tables below illustrate, in an illustrative manner, the post-emergence herbicidal action of the compounds of the invention, the herbicidal activity being stated in percent.
TABLE-US-00056 TABLE 17a Post-emergence action at 5 g/ha against ABUTH in % Example Dosage number [g/ha] ABUTH 3-129 5 100 2-129 5 100 1-129 5 100 6-116 5 90 1-338 5 90 2-338 5 100 3-338 5 90 6-253 5 100 3-337 5 80 1-26 5 90 2-26 5 100 3-26 5 80 6-26 5 90 1-208 5 80 2-208 5 90 3-208 5 90 6-159 5 90 1-130 5 90 2-130 5 90 1-131 5 90 6-118 5 80 1-149 5 80 2-149 5 80 6-124 5 80 5-59 5 90 5-58 5 90 5-117 5 80 5-253 5 90 5-75 5 90 5-74 5 90 5-123 5 90 5-122 5 80 1-82 5 90 1-87 5 90 2-87 5 90 1-88 5 90 2-88 5 90 1-209 5 90 1-4 5 90 1-25 5 100 2-25 5 100 1-27 5 100 2-27 5 100 2-173 5 90 1-273 5 90 2-273 5 90 3-273 5 80 6-212 5 80 1-44 5 90 2-44 5 80 1-45 5 80 2-45 5 80 6-32 5 80 1-46 5 90 2-46 5 80 1-30 5 80 2-30 5 80 1-31 5 80 1-28 5 80 2-28 5 80 1-304 5 90 2-304 5 90 1-305 5 90 2-305 5 80 1-306 5 80 1-177 5 90 2-177 5 80 1-178 5 80 2-178 5 90 1-277 5 90 2-277 5 80 1-278 5 80 2-278 5 80 1-279 5 80 2-195 5 100 2-225 5 100 2-227 5 100 1-227 5 100 1-225 5 80 1-226 5 90 1-56 5 80 6-45 5 80 2-57 5 90 1-58 5 90 2-58 5 100 2-56 5 100 1-57 5 90 1-207 5 80 2-271 5 100 2-32 5 90 1-34 5 90 2-34 5 90 6-255 5 90 2-33 5 90 2-42 5 80 6-256 5 80 1-72 5 80 2-72 5 80 1-73 5 80 2-73 5 80 1-74 5 80 2-74 5 80 2-286 5 90 1-287 5 90 2-287 5 80 2-288 5 80 1-210 5 80 2-210 5 80 1-288 5 80 1-289 5 80 1-291 5 80 2-291 5 80 1-271 5 80 2-47 5 90 2-47 5 80 6-34 5 80 2-339 5 80 6-258 5 80 1-49 5 90 2-49 5 90 1-41 5 80 1-32 5 90 2-154 5 80 1-155 5 80 2-155 5 80 1-164 5 80 1-165 5 90 1-166 5 90 1-156 5 90 6-262 5 80 2-211 5 80 2-272 5 90 2-276 5 80 1-276 5 80 1-272 5 80 6-211 5 80 1-83 5 90 2-83 5 90 1-89 5 90 2-89 5 90 1-342 5 90 1-343 5 90 2-342 5 80 1-345 5 80 2-344 5 90 1-346 5 80 2-345 5 90 1-347 5 80 2-346 5 90 1-184 5 80 2-184 5 90 1-185 5 80 2-185 5 90 1-186 5 90 2-186 5 80 1-349 5 80 2-348 5 90 1-86 5 100 2-86 5 80 1-92 5 90 2-92 5 80 1-90 5 80 1-354 5 90 1-355 5 80 2-353 5 90 2-354 5 90
TABLE-US-00057 TABLE 17b Post-emergence action at 20 g/ha against ABUTH in % Example Dosage number [g/ha] ABUTH 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 90 2-338 20 100 3-338 20 90 6-253 20 100 1-337 20 80 2-337 20 100 3-337 20 80 6-252 20 80 1-123 20 80 1-26 20 100 2-26 20 100 3-26 20 90 6-26 20 90 1-208 20 90 2-208 20 90 3-208 20 90 6-159 20 100 3-125 20 80 1-130 20 90 2-130 20 90 6-117 20 80 1-81 20 80 2-81 20 90 2-82 20 90 6-58 20 80 1-147 20 90 2-147 20 90 1-148 20 90 2-148 20 90 1-131 20 90 2-131 20 90 6-118 20 90 1-149 20 100 2-149 20 100 6-124 20 80 5-59 20 90 5-58 20 90 5-117 20 90 5-253 20 90 5-75 20 90 5-74 20 90 5-123 20 90 5-122 20 90 1-82 20 90 1-87 20 90 2-87 20 90 1-88 20 90 2-88 20 90 1-209 20 100 1-4 20 90 1-25 20 100 2-25 20 100 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 90 2-173 20 100 1-273 20 90 2-273 20 90 3-273 20 90 6-212 20 90 4-212 20 80 1-44 20 100 2-44 20 90 1-45 20 90 2-45 20 80 6-32 20 80 1-46 20 90 2-46 20 80 6-33 20 80 1-30 20 80 2-30 20 80 1-31 20 80 2-31 20 80 1-28 20 80 2-28 20 80 1-29 20 80 2-29 20 80 1-304 20 90 2-304 20 90 1-305 20 90 2-305 20 90 1-306 20 80 2-306 20 80 1-177 20 90 2-177 20 90 1-178 20 80 2-178 20 90 6-141 20 80 1-179 20 80 2-179 20 90 1-132 20 80 2-132 20 80 1-135 20 80 2-135 20 80 6-254 20 80 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 2-279 20 80 2-195 20 100 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 80 1-225 20 80 1-226 20 90 2-226 20 90 6-165 20 90 6-166 20 80 2-196 20 100 1-56 20 100 6-45 20 90 6-44 20 80 2-57 20 100 1-58 20 90 2-58 20 100 2-56 20 100 1-57 20 90 1-207 20 90 2-207 20 90 2-271 20 100 6-210 20 90 2-32 20 90 1-34 20 100 2-34 20 90 6-255 20 90 2-33 20 90 2-42 20 90 6-256 20 90 2-146 20 80 1-146 20 80 2-143 20 80 1-72 20 90 2-72 20 80 6-49 20 80 1-73 20 80 2-73 20 80 6-50 20 80 1-74 20 80 2-74 20 80 2-230 20 80 2-286 20 90 1-287 20 100 2-287 20 80 2-288 20 80 1-210 20 90 2-210 20 80 1-212 20 80 2-213 20 80 1-288 20 80 1-289 20 80 2-289 20 80 1-291 20 90 2-291 20 80 2-292 20 80 1-271 20 90 2-47 20 90 2-47 20 90 6-34 20 80 2-339 20 80 6-258 20 90 1-49 20 90 2-49 20 90 1-41 20 80 2-229 20 80 1-340 20 80 6-267 20 80 1-47 20 80 1-33 20 90 1-32 20 90 2-154 20 90 6-259 20 80 1-155 20 90 2-155 20 80 6-260 20 90 1-164 20 80 6-261 20 80 1-165 20 90 1-166 20 90 1-156 20 90 2-156 20 90 6-262 20 90 1-159 20 80 2-160 20 90 2-161 20 80 2-211 20 80 2-272 20 90 2-276 20 80 1-276 20 80 1-211 20 80 1-274 20 80 1-272 20 90 6-211 20 90 1-341 20 80 1-292 20 80 2-341 20 80 1-158 20 80 1-83 20 90 2-83 20 90 6-60 20 90 1-89 20 90 2-89 20 90 6-161 20 90 1-342 20 90 1-343 20 90 2-342 20 90 1-344 20 90 2-343 20 80 1-345 20 90 2-344 20 90 1-346 20 100 2-345 20 90 1-347 20 90 2-346 20 90 1-195 20 80 1-184 20 80 2-184 20 90 1-185 20 90 2-185 20 100 1-186 20 90 2-186 20 90 1-349 20 90 2-348 20 90 1-351 20 80 2-349 20 80 2-84 20 90 1-352 20 100 2-350 20 80 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 90 1-90 20 90 2-90 20 90 1-353 20 80 2-351 20 80 1-354 20 100 2-352 20 80 1-355 20 100 2-353 20 100 1-356 20 100 2-354 20 90
TABLE-US-00058 TABLE 17c Post-emergence action at 80 g/ha against ABUTH in % Example Dosage number [g/ha] ABUTH 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 100 2-337 80 100 6-252 80 100 6-117 80 80 1-81 80 90 2-81 80 90 2-82 80 90 6-58 80 80 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90
TABLE-US-00059 TABLE 18a Post-emergence action at 5 g/ha against ALOMY in % Example Dosage number [g/ha] ALOMY 2-129 5 100 1-129 5 90 2-27 5 80 1-273 5 80 2-177 5 80 1-178 5 90 2-178 5 80 1-179 5 90 1-132 5 80 2-195 5 80 1-226 5 80 2-32 5 90 2-33 5 90 2-42 5 90 1-136 5 80 1-182 5 90 2-182 5 80 1-181 5 80 1-210 5 80 1-212 5 80 2-291 5 80 1-271 5 80 2-47 5 80 1-47 5 80 1-32 5 80 1-165 5 90 1-166 5 80 1-342 5 90 1-343 5 90 2-342 5 90 2-343 5 80 1-345 5 80 2-344 5 80 1-346 5 80 2-345 5 80 1-195 5 90 1-184 5 80 2-184 5 80 1-186 5 80 2-348 5 80 1-351 5 90 2-352 5 80
TABLE-US-00060 TABLE 18b Post-emergence action at 20 g/ha against ALOMY in % Example Dosage number [g/ha] ALOMY 3-129 20 80 2-129 20 100 1-129 20 100 6-116 20 80 2-338 20 80 1-26 20 90 2-26 20 80 3-26 20 80 1-208 20 80 2-208 20 80 6-159 20 80 1-130 20 80 2-130 20 80 6-117 20 80 1-81 20 80 2-81 20 80 1-147 20 80 2-147 20 80 1-148 20 80 2-148 20 80 1-131 20 90 2-131 20 80 6-118 20 80 1-149 20 80 2-149 20 80 6-124 20 90 5-59 20 80 5-58 20 80 5-117 20 80 5-75 20 80 5-123 20 80 5-122 20 80 1-82 20 90 1-87 20 80 2-87 20 80 1-88 20 80 2-88 20 80 1-209 20 80 1-4 20 80 1-25 20 100 2-25 20 90 1-27 20 100 2-27 20 90 1-173 20 80 2-173 20 100 1-273 20 100 2-273 20 80 6-212 20 80 1-46 20 90 2-46 20 80 1-30 20 80 2-31 20 80 1-177 20 90 2-177 20 100 1-178 20 100 2-178 20 90 6-141 20 90 1-179 20 90 2-179 20 90 1-132 20 90 1-135 20 90 2-134 20 80 1-133 20 90 2-133 20 80 2-278 20 80 2-195 20 100 2-197 20 90 1-225 20 90 1-226 20 100 2-226 20 90 6-165 20 80 2-196 20 90 2-57 20 90 2-58 20 80 2-56 20 80 1-57 20 80 1-207 20 90 2-207 20 90 2-271 20 100 2-32 20 100 1-34 20 90 2-34 20 100 6-255 20 90 2-33 20 100 2-42 20 100 2-142 20 80 1-142 20 90 2-74 20 80 1-138 20 90 1-137 20 90 1-136 20 90 2-180 20 90 1-183 20 90 2-183 20 80 1-182 20 100 2-182 20 100 6-145 20 80 1-181 20 100 2-181 20 90 2-36 20 90 1-228 20 90 2-228 20 80 1-230 20 90 2-230 20 90 2-287 20 90 2-288 20 90 1-210 20 100 2-210 20 90 1-212 20 90 1-288 20 90 2-289 20 90 1-291 20 90 2-291 20 80 2-292 20 80 1-271 20 90 2-47 20 90 2-47 20 90 1-339 20 80 2-339 20 80 6-258 20 80 2-49 20 80 1-229 20 80 1-340 20 80 1-47 20 90 1-33 20 90 1-32 20 90 2-154 20 80 1-155 20 90 2-155 20 90 1-165 20 100 1-166 20 90 1-156 20 80 2-156 20 90 1-160 20 80 2-160 20 80 2-211 20 80 2-272 20 90 2-276 20 80 1-276 20 80 1-274 20 80 1-272 20 90 1-341 20 80 1-292 20 80 1-83 20 100 2-83 20 100 1-89 20 90 2-89 20 90 6-161 20 90 1-342 20 100 1-343 20 100 2-342 20 90 1-344 20 100 2-343 20 100 1-345 20 90 2-344 20 90 1-346 20 90 2-345 20 80 1-347 20 80 2-346 20 80 1-195 20 100 1-184 20 80 2-184 20 100 1-185 20 90 2-185 20 90 1-186 20 90 2-186 20 80 1-349 20 80 2-348 20 90 1-351 20 90 2-349 20 80 1-84 20 100 2-84 20 90 1-352 20 80 2-350 20 80 1-86 20 100 2-86 20 80 1-92 20 90 2-92 20 80 1-90 20 80 1-353 20 80 2-351 20 80 1-354 20 80 2-352 20 90 1-355 20 80 1-356 20 80 2-354 20 80
TABLE-US-00061 TABLE 18c Post-emergence action at 80 g/ha against ALOMY in % Dosage Example number [g/ha] ALOMY 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 80 2-337 80 90 6-117 80 90 1-81 80 90 2-81 80 90 2-82 80 90 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90
TABLE-US-00062 TABLE 19a Post-emergence action at 5 g/ha against AMARE in % Example Dosage number [g/ha] ALOMY 3-129 5 90 2-129 5 100 1-129 5 100 6-116 5 100 1-338 5 90 2-338 5 80 3-338 5 90 2-337 5 80 3-337 5 90 2-123 5 80 1-26 5 90 2-26 5 100 3-26 5 90 6-26 5 100 1-208 5 100 2-208 5 90 3-208 5 80 6-159 5 90 1-130 5 90 2-130 5 90 1-131 5 100 2-131 5 100 6-118 5 100 1-149 5 90 2-149 5 100 6-124 5 100 5-59 5 90 5-58 5 90 5-117 5 100 5-253 5 80 5-75 5 90 5-74 5 90 5-123 5 90 5-122 5 90 1-82 5 90 1-87 5 90 2-87 5 90 1-88 5 90 2-88 5 90 1-209 5 90 1-4 5 80 1-25 5 100 1-27 5 100 2-27 5 100 1-173 5 100 2-173 5 100 1-273 5 90 6-212 5 80 1-44 5 100 2-44 5 100 1-45 5 90 2-45 5 100 6-32 5 80 1-46 5 100 2-46 5 100 6-33 5 90 1-304 5 90 2-304 5 90 6-231 5 80 1-305 5 90 2-305 5 100 1-306 5 100 2-306 5 90 1-177 5 90 2-177 5 100 1-178 5 90 2-178 5 100 6-141 5 90 1-179 5 100 2-179 5 100 1-132 5 100 2-132 5 80 1-135 5 90 2-135 5 90 6-254 5 80 1-134 5 90 2-134 5 80 1-133 5 90 2-133 5 80 6-120 5 80 1-277 5 100 2-277 5 90 1-278 5 90 2-278 5 90 1-279 5 90 2-195 5 100 2-225 5 100 1-197 5 100 2-227 5 100 1-227 5 100 2-197 5 80 1-225 5 90 1-226 5 90 2-226 5 90 1-56 5 100 2-57 5 100 1-58 5 100 2-58 5 100 2-56 5 100 1-57 5 100 1-207 5 100 2-207 5 100 2-271 5 100 6-210 5 100 2-32 5 100 1-34 5 100 2-34 5 100 6-255 5 100 2-33 5 100 2-42 5 100 6-256 5 80 2-146 5 80 1-141 5 90 1-144 5 80 1-138 5 80 2-138 5 90 2-141 5 80 1-137 5 90 1-136 5 90 1-181 5 100 1-228 5 90 6-167 5 80 2-286 5 90 2-287 5 90 2-288 5 90 1-212 5 90 1-288 5 90 1-289 5 90 2-289 5 90 1-291 5 80 6-230 5 90 2-292 5 80 1-271 5 90 2-47 5 90 2-47 5 100 6-34 5 90 1-339 5 80 2-339 5 80 6-258 5 90 1-49 5 90 2-49 5 90 1-41 5 80 1-229 5 90 2-229 5 80 1-340 5 90 6-267 5 90 2-340 5 90 1-47 5 90 1-33 5 80 1-32 5 90 2-154 5 90 6-259 5 80 1-155 5 90 2-155 5 90 1-164 5 90 2-164 5 80 6-261 5 80 1-165 5 90 1-166 5 80 1-156 5 80 2-156 5 90 1-159 5 90 2-159 5 90 1-162 5 90 2-162 5 80 1-160 5 90 2-160 5 90 2-161 5 90 6-266 5 80 2-211 5 90 2-272 5 90 1-161 5 80 2-276 5 80 1-276 5 100 1-211 5 90 1-274 5 100 6-168 5 80 1-272 5 90 6-211 5 80 1-341 5 80 1-292 5 80 2-341 5 90 1-158 5 80 1-83 5 100 2-83 5 100 6-60 5 80 1-89 5 100 2-89 5 100 6-76 5 100 6-161 5 100 6-268 5 90 1-342 5 100 1-343 5 100 2-342 5 100 1-344 5 100 2-343 5 90 1-345 5 100 2-344 5 100 1-346 5 100 2-345 5 90 1-347 5 100 2-346 5 100 1-195 5 100 1-184 5 100 2-184 5 100 1-185 5 100 2-185 5 100 1-186 5 90 2-186 5 100 1-349 5 100 1-350 5 90 2-348 5 90 1-351 5 100 2-349 5 90 1-84 5 100 2-84 5 100 1-352 5 100 2-350 5 100 1-86 5 100 2-86 5 100 1-92 5 100 2-92 5 100 1-90 5 100 2-90 5 100 1-353 5 100 2-351 5 100 1-354 5 90 2-352 5 100 1-355 5 100 2-353 5 100 1-356 5 100 2-354 5 100
TABLE-US-00063 TABLE 19b Post-emergence action at 20 g/ha against AMARE in % Example Dosage number [g/ha] AMARE 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 90 2-338 20 100 3-338 20 90 2-337 20 100 3-337 20 100 1-123 20 80 2-123 20 80 1-26 20 100 2-26 20 100 3-26 20 90 6-26 20 100 1-208 20 100 2-208 20 100 3-208 20 90 6-159 20 100 1-125 20 80 2-125 20 80 3-125 20 90 1-130 20 90 2-130 20 100 1-81 20 90 2-81 20 90 2-82 20 90 1-147 20 90 2-147 20 90 1-148 20 90 2-148 20 90 1-131 20 100 2-131 20 100 6-118 20 100 1-149 20 100 2-149 20 100 6-124 20 100 5-59 20 90 5-58 20 90 5-117 20 100 5-253 20 80 5-75 20 90 5-74 20 100 5-123 20 90 5-122 20 90 1-82 20 90 1-87 20 100 2-87 20 90 1-88 20 90 2-88 20 90 1-209 20 100 1-4 20 90 1-25 20 100 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 100 1-273 20 100 2-273 20 90 6-212 20 90 4-212 20 80 1-44 20 100 2-44 20 100 1-45 20 90 2-45 20 100 6-32 20 100 1-46 20 100 2-46 20 100 6-33 20 90 2-31 20 80 1-304 20 90 2-304 20 100 6-231 20 90 1-305 20 90 2-305 20 100 1-306 20 100 2-306 20 90 1-177 20 100 2-177 20 100 1-178 20 100 2-178 20 100 6-141 20 100 1-179 20 100 2-179 20 100 1-132 20 100 2-132 20 90 1-135 20 90 2-135 20 90 6-254 20 100 1-134 20 90 2-134 20 100 1-133 20 100 2-133 20 90 6-120 20 90 1-277 20 100 2-277 20 90 1-278 20 90 2-278 20 100 1-279 20 100 2-279 20 100 2-195 20 100 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 90 1-225 20 100 1-226 20 100 2-226 20 100 6-165 20 80 6-166 20 90 1-56 20 100 6-45 20 80 6-44 20 90 2-57 20 100 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 2-271 20 100 6-210 20 100 2-32 20 100 1-34 20 100 2-34 20 100 6-255 20 100 2-33 20 100 2-42 20 100 6-256 20 90 2-146 20 80 2-142 20 100 5-255 20 90 1-142 20 90 5-254 20 80 1-140 20 80 1-146 20 100 1-141 20 100 1-144 20 90 1-138 20 90 2-138 20 90 2-141 20 80 1-137 20 90 1-136 20 90 1-181 20 100 1-36 20 100 2-36 20 90 1-228 20 90 2-228 20 90 6-167 20 100 1-230 20 100 2-230 20 100 6-169 20 90 2-286 20 100 2-287 20 100 2-288 20 100 2-210 20 100 1-212 20 100 1-288 20 100 1-289 20 90 2-289 20 100 6-228 20 90 1-291 20 90 2-291 20 90 6-230 20 90 2-292 20 90 1-271 20 90 2-47 20 90 2-47 20 100 6-34 20 100 1-339 20 90 2-339 20 90 6-258 20 90 1-49 20 90 2-49 20 100 1-41 20 90 1-229 20 90 2-229 20 90 1-340 20 90 6-267 20 90 2-340 20 100 1-47 20 90 1-33 20 100 1-32 20 90 2-154 20 90 6-259 20 100 1-155 20 90 2-155 20 90 6-260 20 80 1-164 20 90 2-164 20 90 6-261 20 90 1-165 20 90 1-166 20 90 1-156 20 90 2-156 20 90 6-262 20 90 2-157 20 90 1-159 20 100 2-159 20 100 1-162 20 90 2-162 20 100 6-264 20 80 1-160 20 100 2-160 20 100 2-161 20 100 6-266 20 100 2-211 20 90 2-272 20 100 1-161 20 90 2-276 20 90 1-276 20 100 1-211 20 90 1-274 20 100 6-168 20 100 1-272 20 100 6-211 20 90 1-341 20 100 1-292 20 100 2-341 20 100 1-158 20 90 1-83 20 100 2-83 20 100 6-60 20 100 1-89 20 100 2-89 20 100 6-76 20 100 6-161 20 100 6-268 20 100 1-342 20 100 1-343 20 100 2-342 20 100 1-344 20 100 2-343 20 100 1-345 20 100 2-344 20 100 1-346 20 100 2-345 20 100 1-347 20 100 2-346 20 100 1-195 20 100 1-184 20 100 2-184 20 100 1-185 20 100 2-185 20 100 1-186 20 100 2-186 20 100 1-349 20 100 1-350 20 100 2-348 20 100 1-351 20 100 2-349 20 100 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 100 1-354 20 100 2-352 20 100 1-355 20 100 2-353 20 100 1-356 20 100 2-354 20 100
TABLE-US-00064 TABLE 19c Post-emergence action at 80 g/ha against AMARE in % Example Dosage number [g/ha] AMARE 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 100 2-337 80 100 6-117 80 80 1-81 80 90 2-81 80 90 2-82 80 90 6-58 80 90 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90
TABLE-US-00065 TABLE 20a Post-emergence action at 5 g/ha against AVEFA in % Example Dosage number [g/ha] AVEFA 2-129 5 100 6-116 5 100 2-208 5 80 2-131 5 80 5-117 5 80 2-27 5 90 1-173 5 90 1-28 5 80 2-28 5 80 1-29 5 80 1-132 5 80 2-32 5 90 2-34 5 80
TABLE-US-00066 TABLE 20b Post-emergence action at 20 g/ha against AVEFA in % Example Dosage number [g/ha] AVEFA 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 80 2-338 20 80 3-337 20 80 2-26 20 80 1-208 20 90 2-208 20 90 3-208 20 80 1-130 20 80 2-130 20 90 2-81 20 90 2-82 20 90 6-58 20 80 1-147 20 90 2-147 20 90 1-148 20 100 2-148 20 90 1-131 20 80 2-131 20 80 1-149 20 100 5-117 20 90 5-75 20 80 5-74 20 80 5-123 20 80 5-122 20 80 1-82 20 90 1-87 20 80 2-87 20 80 1-88 20 80 2-88 20 80 1-4 20 80 2-25 20 100 3-27 20 90 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 100 1-273 20 90 3-273 20 80 1-44 20 80 2-44 20 80 1-46 20 80 1-30 20 80 1-31 20 90 2-31 20 80 1-28 20 80 2-28 20 90 1-29 20 90 2-29 20 80 1-178 20 80 2-178 20 80 1-179 20 90 1-132 20 90 2-135 20 80 1-277 20 80 2-195 20 80 1-227 20 80 1-225 20 80 1-226 20 80 2-226 20 80 2-57 20 80 1-58 20 90 2-58 20 80 2-271 20 80 2-32 20 100 2-34 20 80 2-33 20 100 1-137 20 80 2-182 20 80 1-181 20 90 2-230 20 80 2-288 20 80 1-212 20 80 1-291 20 80 2-291 20 90 2-292 20 80 1-271 20 80 2-47 20 80 1-49 20 80 1-165 20 90 2-272 20 80 2-341 20 90 2-83 20 90 2-89 20 80 1-344 20 80 2-345 20 80 1-349 20 80 1-351 20 80 2-349 20 90 1-84 20 80 2-84 20 100 1-352 20 80 2-350 20 90 1-86 20 100 2-86 20 80 1-92 20 90 2-92 20 80 2-90 20 80 1-353 20 80 2-351 20 80
TABLE-US-00067 TABLE 20c Post-emergence action at 80 g/ha against AVEFA in % Example Dosage number [g/ha] AVEFA 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 100 6-253 80 80 2-337 80 90 6-117 80 90 1-81 80 90 2-81 80 100 2-82 80 90 6-58 80 90 1-147 80 90 2-147 80 100 1-148 80 100 2-148 80 90
TABLE-US-00068 TABLE 21a Post-emergence action at 20 g/ha against CYPES in % Example Dosage number [g/ha] CYPES 1-338 20 80
TABLE-US-00069 TABLE 21b Post-emergence action at 80 g/ha against CYPES in % Example Dosage number [g/ha] CYPES 2-129 80 90 1-129 80 80 1-338 80 90 6-253 80 80
TABLE-US-00070 TABLE 22a Post-emergence action at 5 g/ha against ECHCG in % Example Dosage number [g/ha] ECHCG 1-129 5 100 2-26 5 80 6-26 5 80 6-159 5 80 1-130 5 80 5-59 5 80 5-58 5 80 5-117 5 80 5-75 5 80 5-74 5 80 5-123 5 90 5-122 5 90 1-82 5 80 1-87 5 80 2-87 5 80 1-88 5 80 2-88 5 80 2-27 5 80 2-173 5 80 1-273 5 80 2-273 5 80 3-273 5 80 6-212 5 90 1-45 5 80 1-46 5 80 2-30 5 80 1-31 5 80 2-31 5 80 1-28 5 80 2-28 5 80 2-305 5 90 1-306 5 90 2-306 5 90 1-135 5 80 2-135 5 80 1-278 5 90 1-279 5 80 1-225 5 90 1-226 5 100 6-165 5 90 6-166 5 80 1-56 5 80 2-57 5 100 1-58 5 90 2-58 5 90 1-57 5 80 2-32 5 80 1-34 5 90 2-34 5 90 6-255 5 90 2-33 5 90 2-42 5 90 6-256 5 90 1-37 5 80 2-72 5 80 1-73 5 80 2-73 5 80 1-74 5 80 2-74 5 80 1-138 5 80 2-138 5 80 1-137 5 90 1-136 5 80 6-257 5 80 2-182 5 90 1-181 5 80 2-228 5 80 1-230 5 80 6-169 5 80 2-287 5 80 2-288 5 80 1-212 5 80 2-213 5 80 1-288 5 80 2-289 5 80 1-291 5 80 2-291 5 80 2-292 5 80 1-271 5 80 2-47 5 80 2-47 5 80 6-34 5 80 1-339 5 90 6-258 5 80 1-49 5 80 1-229 5 90 1-47 5 90 1-33 5 80 6-259 5 80 1-155 5 90 6-260 5 90 1-164 5 80 1-156 5 80 2-156 5 90 2-272 5 80 1-211 5 80 1-274 5 80 6-168 5 80 1-272 5 80 1-341 5 80 1-292 5 80 2-341 5 80 6-161 5 90 1-343 5 80 2-344 5 80 1-346 5 80 2-346 5 80 1-185 5 90 2-84 5 100 1-352 5 100 1-86 5 80 2-86 5 100 1-92 5 100 2-92 5 80 1-353 5 100 2-351 5 100
TABLE-US-00071 TABLE 22b Post-emergence action at 20 G/ha against ECHCG in % Example Dosage number [g/ha] ECHCG 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 90 2-338 20 80 1-26 20 80 2-26 20 80 6-26 20 90 2-208 20 80 6-159 20 90 1-130 20 80 2-130 20 80 6-117 20 80 1-81 20 80 2-81 20 90 2-82 20 80 6-58 20 90 1-147 20 90 2-147 20 90 1-148 20 80 2-148 20 80 1-131 20 90 2-131 20 80 6-118 20 90 1-149 20 80 2-149 20 80 6-124 20 80 5-59 20 90 5-58 20 90 5-117 20 80 5-253 20 80 5-75 20 80 5-74 20 80 5-123 20 90 5-122 20 90 1-82 20 90 1-87 20 80 2-87 20 80 1-88 20 90 2-88 20 80 1-209 20 90 1-4 20 100 1-25 20 100 2-25 20 80 1-27 20 80 2-27 20 100 1-173 20 80 2-173 20 90 1-273 20 90 2-273 20 90 3-273 20 80 6-212 20 90 1-44 20 80 2-44 20 80 1-45 20 80 2-45 20 80 1-46 20 80 2-46 20 80 6-33 20 80 1-30 20 80 2-30 20 80 1-31 20 80 2-31 20 90 1-28 20 90 2-28 20 80 1-29 20 80 2-29 20 80 1-304 20 90 2-304 20 80 1-305 20 90 2-305 20 90 1-306 20 90 2-306 20 90 6-233 20 80 1-177 20 90 1-178 20 90 2-178 20 90 6-141 20 80 1-179 20 90 2-179 20 80 1-132 20 90 2-132 20 90 1-135 20 100 2-135 20 90 6-254 20 90 1-134 20 90 2-134 20 90 2-133 20 80 6-120 20 90 1-277 20 90 2-277 20 100 1-278 20 90 2-278 20 90 1-279 20 90 2-279 20 90 2-225 20 100 1-197 20 90 2-227 20 80 2-197 20 90 1-225 20 100 1-226 20 100 2-226 20 90 6-165 20 100 6-166 20 90 2-196 20 80 1-56 20 90 6-45 20 90 6-44 20 90 2-57 20 100 1-58 20 90 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 80 6-210 20 80 2-32 20 90 1-34 20 90 2-34 20 100 6-255 20 100 2-33 20 100 2-42 20 100 6-256 20 90 1-146 20 80 1-37 20 80 2-37 20 80 1-72 20 80 2-72 20 80 1-73 20 80 2-73 20 80 6-50 20 80 1-74 20 80 2-74 20 80 6-51 20 80 1-138 20 90 2-138 20 90 2-141 20 80 1-137 20 90 1-136 20 90 2-180 20 90 1-183 20 100 2-183 20 90 6-257 20 90 1-182 20 80 2-182 20 90 1-181 20 80 2-181 20 90 6-144 20 80 1-228 20 80 2-228 20 90 6-167 20 80 1-230 20 80 6-169 20 90 2-286 20 100 1-287 20 100 2-287 20 80 2-288 20 80 1-210 20 80 2-210 20 90 1-212 20 80 2-212 20 80 2-213 20 80 1-288 20 80 1-289 20 80 2-289 20 90 1-291 20 80 2-291 20 80 2-292 20 80 1-271 20 80 2-47 20 90 2-47 20 80 6-34 20 90 1-339 20 90 2-339 20 90 6-258 20 90 1-49 20 90 2-49 20 90 1-41 20 90 1-229 20 90 2-229 20 90 1-340 20 90 6-267 20 90 2-340 20 90 1-47 20 90 1-33 20 90 1-32 20 90 2-154 20 90 6-259 20 90 1-155 20 90 6-260 20 90 1-164 20 90 2-164 20 80 6-261 20 90 1-165 20 90 1-166 20 90 1-156 20 90 2-156 20 90 6-262 20 80 1-159 20 90 1-162 20 80 2-211 20 80 2-272 20 90 2-276 20 90 1-276 20 80 1-211 20 90 1-274 20 90 6-168 20 80 1-272 20 90 6-211 20 90 1-341 20 90 1-292 20 80 2-341 20 90 1-83 20 90 2-83 20 90 6-60 20 90 2-89 20 90 6-76 20 80 6-161 20 90 1-342 20 80 1-343 20 90 1-345 20 90 2-344 20 90 1-346 20 90 2-345 20 80 1-347 20 90 2-346 20 90 1-195 20 80 1-184 20 100 2-184 20 100 1-185 20 100 2-185 20 100 1-186 20 90 1-350 20 80 2-348 20 80 1-351 20 100 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 100 2-352 20 90 1-355 20 90
TABLE-US-00072 TABLE 22c Post-emergence action at 80 g/ha against ECHCG in % Example Dosage number [g/ha] ECHCG 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 100 3-338 80 80 6-253 80 90 2-337 80 90 6-117 80 80 1-81 80 90 2-81 80 90 2-82 80 80 6-58 80 90 1-147 80 90 2-147 80 90 1-148 80 80 2-148 80 90
TABLE-US-00073 TABLE 23a Post-emergence action at 5 g/ha against HORMU in % Example Dosage number [g/ha] HORMU 2-129 5 80 1-129 5 90 1-273 5 80
TABLE-US-00074 TABLE 23b Post-emergence action at 20 g/ha against HORMU in % Example Dosage number [g/ha] HORMU 3-129 20 90 2-129 20 90 1-129 20 100 6-116 20 90 1-338 20 80 2-26 20 80 6-117 20 80 2-82 20 80 1-147 20 80 2-147 20 80 2-148 20 80 1-131 20 80 2-131 20 100 5-59 20 80 5-117 20 80 5-122 20 80 1-82 20 90 1-87 20 80 2-87 20 80 2-88 20 80 1-25 20 100 2-25 20 80 1-27 20 80 2-27 20 90 1-173 20 90 2-173 20 100 1-273 20 90 2-46 20 80
TABLE-US-00075 TABLE 23c Post-emergence action at 80 g/ha against HORMU in % Example Dosage number [g/ha] HORMU 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 100 3-338 80 100 6-253 80 90 6-117 80 90 1-81 80 80 2-81 80 80 2-82 80 90 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90
TABLE-US-00076 TABLE 24a Post-emergence action at 5 g/ha against LOLRI in % Example Dosage number [g/ha] LOLRI 1-129 5 80
TABLE-US-00077 TABLE 24b Post-emergence action at 20 g/ha against LOLRI in % Example Dosage number [g/ha] LOLRI 2-129 20 100 1-129 20 100 1-26 20 80 2-81 20 80 1-148 20 80 5-123 20 80 5-122 20 80 1-82 20 80 1-209 20 80 2-27 20 80 1-173 20 90 1-273 20 80 1-178 20 80 1-179 20 80 2-32 20 80 1-181 20 80 1-165 20 80 1-351 20 80
TABLE-US-00078 TABLE 24c Post-emergence action at 80 g/ha against LOLRI in % Example Dosage number [g/ha] LOLRI 3-129 80 80 2-129 80 100 1-129 80 100 6-116 80 90 1-338 80 80 2-338 80 90 2-81 80 90 2-82 80 90 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 80
TABLE-US-00079 TABLE 25a Post-emergence action at 5 g/ha against MATIN in % Example Dosage number [g/ha] MATIN 3-129 5 100 2-129 5 80 6-116 5 80 1-26 5 90 2-26 5 80 3-26 5 90 3-208 5 90 1-131 5 90 2-131 5 90 2-149 5 90 5-117 5 80 5-122 5 80 2-87 5 80 1-88 5 80 2-25 5 90 3-27 5 90 1-27 5 80 2-27 5 100 1-273 5 100 2-273 5 80 3-273 5 80 1-44 5 80 2-44 5 80 1-45 5 80 2-31 5 80 1-304 5 90 2-304 5 90 1-305 5 90 2-305 5 80 1-306 5 90 2-306 5 80 2-177 5 90 2-178 5 90 2-179 5 80 2-132 5 80 1-135 5 80 2-135 5 90 1-277 5 90 2-277 5 90 1-278 5 80 2-278 5 90 1-279 5 90 2-195 5 80 2-196 5 80 2-57 5 80 1-58 5 80 2-58 5 80 2-56 5 80 1-57 5 80 2-207 5 80 2-271 5 100 2-32 5 90 2-33 5 90 2-146 5 80 2-73 5 80 1-74 5 80 1-137 5 80 1-183 5 90 2-183 5 80 2-182 5 90 2-181 5 80 2-286 5 90 1-287 5 80 2-287 5 90 2-288 5 80 1-210 5 80 2-213 5 90 1-288 5 90 2-289 5 80 1-291 5 80 2-291 5 80 2-292 5 80 1-271 5 90 2-49 5 80 1-33 5 80 1-32 5 80 1-164 5 80 1-166 5 80 2-272 5 80 1-292 5 80 1-83 5 80 2-83 5 80 2-89 5 90 1-346 5 80 2-345 5 90 2-185 5 80 1-352 5 80 2-350 5 80 2-86 5 80 1-353 5 80
TABLE-US-00080 TABLE 25b Post-emergence action at 20 g/ha against MATIN in % Example Dosage number [g/ha] MATIN 3-129 20 100 2-129 20 100 1-129 20 90 6-116 20 90 3-337 20 80 1-26 20 90 2-26 20 90 3-26 20 90 1-208 20 80 2-208 20 80 3-208 20 90 6-159 20 90 1-130 20 80 2-130 20 80 6-117 20 90 1-81 20 80 2-81 20 100 2-82 20 90 1-147 20 100 2-147 20 100 1-148 20 100 2-148 20 90 1-131 20 90 2-131 20 100 6-118 20 80 1-149 20 100 2-149 20 100 6-124 20 80 5-58 20 80 5-117 20 90 5-75 20 80 5-123 20 80 5-122 20 80 1-82 20 80 1-87 20 80 2-87 20 90 1-88 20 80 2-88 20 80 1-25 20 100 2-25 20 100 3-27 20 100 1-27 20 100 2-27 20 100 2-173 20 100 1-273 20 100 2-273 20 90 3-273 20 90 1-44 20 90 2-44 20 80 1-45 20 80 2-45 20 80 1-46 20 80 2-46 20 80 2-31 20 80 1-28 20 80 2-28 20 80 2-29 20 80 1-304 20 90 2-304 20 90 1-305 20 90 2-305 20 90 1-306 20 90 2-306 20 90 1-177 20 90 2-177 20 90 1-178 20 90 2-178 20 90 1-179 20 80 2-179 20 90 1-132 20 80 2-132 20 80 1-135 20 90 2-135 20 90 6-254 20 80 2-134 20 80 2-133 20 90 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 2-279 20 80 2-195 20 90 2-225 20 80 2-197 20 80 1-226 20 80 2-226 20 80 2-196 20 90 1-56 20 90 2-57 20 90 1-58 20 90 2-58 20 90 2-56 20 90 1-57 20 90 1-207 20 90 2-207 20 90 2-271 20 100 2-32 20 90 2-33 20 90 2-42 20 80 2-146 20 90 5-255 20 80 1-72 20 80 2-72 20 80 1-73 20 80 2-73 20 80 1-74 20 90 2-74 20 80 1-137 20 80 1-136 20 80 2-180 20 80 1-183 20 90 2-183 20 90 2-182 20 90 2-181 20 90 2-228 20 80 2-286 20 90 1-287 20 90 2-287 20 90 2-288 20 90 1-210 20 90 2-210 20 90 2-213 20 100 1-288 20 100 1-289 20 80 2-289 20 90 1-291 20 90 2-291 20 90 2-292 20 90 1-271 20 90 2-47 20 80 1-339 20 80 2-339 20 80 1-49 20 80 2-49 20 80 1-229 20 80 2-229 20 80 1-340 20 80 2-340 20 80 1-33 20 80 1-32 20 90 2-154 20 80 1-155 20 80 2-155 20 90 6-260 20 80 1-164 20 80 2-164 20 80 1-165 20 80 1-166 20 80 2-161 20 80 2-211 20 80 2-272 20 80 2-276 20 90 1-276 20 80 1-274 20 80 1-272 20 90 1-341 20 80 1-292 20 80 2-341 20 80 1-83 20 90 2-83 20 100 1-89 20 80 2-89 20 90 1-345 20 80 2-344 20 80 1-346 20 90 2-345 20 100 1-195 20 80 2-185 20 90 1-84 20 90 2-84 20 80 1-352 20 90 2-350 20 90 1-86 20 80 2-86 20 90 1-92 20 80 2-92 20 80 1-90 20 80 2-90 20 90 1-353 20 90 2-351 20 80 2-352 20 80 2-353 20 80
TABLE-US-00081 TABLE 25c Post-emergence action at 80 g/ha against MATIN in % Example Dosage number [g/ha] MATIN 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 3-338 80 80 6-117 80 90 1-81 80 100 2-81 80 100 2-82 80 90 1-147 80 100 2-147 80 100 1-148 80 100 2-148 80 90
TABLE-US-00082 TABLE 26a Post-emergence action at 5 g/ha against PHBPU in % Example Dosage number [g/ha] PHBPU 1-129 5 80 6-116 5 80 2-26 5 80 3-26 5 80 1-208 5 80 2-208 5 80 3-208 5 80 1-130 5 80 5-59 5 80 5-58 5 80 5-117 5 80 5-75 5 80 1-82 5 80 1-87 5 80 2-87 5 80 1-88 5 80 2-88 5 80 2-25 5 80 3-27 5 90 2-173 5 80 2-44 5 80 1-45 5 80 1-46 5 80 2-31 5 80 2-135 5 80 1-134 5 80 1-277 5 90 2-278 5 80 1-279 5 90 1-227 5 80 2-57 5 80 2-56 5 80 2-32 5 80 1-34 5 90 2-34 5 90 6-255 5 90 2-42 5 90 2-146 5 80 1-138 5 80 1-137 5 80 1-180 5 90 2-182 5 80 1-228 5 80 2-286 5 90 1-287 5 90 2-288 5 80 1-212 5 80 2-213 5 80 1-289 5 80 1-291 5 80 2-291 5 80 2-47 5 80 1-339 5 80 2-339 5 90 1-49 5 80 2-49 5 80 1-47 5 80 2-154 5 90 1-155 5 90 1-164 5 90 1-165 5 90 1-166 5 80 1-159 5 80 2-159 5 80 2-211 5 80 2-272 5 90 2-276 5 80 1-274 5 80 1-292 5 80 1-342 5 80 2-342 5 80 1-345 5 80 1-346 5 80 1-347 5 90 1-195 5 80 1-84 5 90 2-350 5 80 1-86 5 80 2-86 5 80 2-353 5 80
TABLE-US-00083 TABLE 26b Post-emergence action at 20 g/ha against PHBPU in % Example number Dosage [g/ha] PHBPU 3-129 20 90 2-129 20 100 1-129 20 100 6-116 20 80 3-338 20 80 1-26 20 80 2-26 20 80 3-26 20 90 6-26 20 80 1-208 20 90 2-208 20 80 3-208 20 90 6-159 20 80 1-130 20 90 1-147 20 80 1-131 20 90 2-131 20 80 1-149 20 90 2-149 20 90 5-59 20 90 5-58 20 90 5-117 20 90 5-75 20 80 5-74 20 100 5-123 20 80 5-122 20 90 1-82 20 90 1-87 20 90 2-87 20 80 1-88 20 90 2-88 20 90 1-209 20 90 1-25 20 80 2-25 20 90 3-27 20 100 1-27 20 90 2-27 20 90 2-173 20 90 1-273 20 80 3-273 20 80 1-44 20 80 2-44 20 80 1-45 20 80 2-45 20 80 1-46 20 80 2-46 20 80 1-30 20 80 2-30 20 90 1-31 20 80 2-31 20 90 1-28 20 90 2-28 20 80 2-29 20 80 2-304 20 90 1-305 20 90 2-305 20 90 2-306 20 80 1-177 20 80 1-178 20 80 2-178 20 90 2-179 20 80 1-132 20 90 1-135 20 90 2-135 20 80 6-254 20 80 1-134 20 90 2-134 20 90 1-133 20 80 2-133 20 80 6-120 20 90 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 1-197 20 90 1-227 20 90 1-225 20 80 1-226 20 80 2-226 20 80 1-56 20 80 2-57 20 90 1-58 20 90 2-58 20 90 2-56 20 90 1-57 20 90 1-207 20 80 2-207 20 80 2-32 20 90 1-34 20 90 2-34 20 100 6-255 20 90 2-33 20 90 2-42 20 90 6-256 20 90 2-146 20 90 1-37 20 80 2-143 20 80 1-72 20 80 2-72 20 80 2-73 20 80 1-74 20 90 2-74 20 80 2-144 20 80 1-138 20 90 2-138 20 80 2-141 20 80 1-137 20 80 1-180 20 90 2-180 20 90 1-183 20 80 2-183 20 80 2-182 20 90 6-145 20 80 1-181 20 90 2-181 20 90 1-228 20 80 2-228 20 80 2-286 20 90 1-287 20 100 2-288 20 90 1-210 20 100 2-210 20 90 1-212 20 90 2-213 20 80 1-288 20 80 1-289 20 90 2-289 20 90 6-228 20 80 1-291 20 90 2-291 20 90 6-230 20 80 1-271 20 90 2-47 20 90 2-47 20 90 6-34 20 80 1-339 20 90 2-339 20 90 1-49 20 90 2-49 20 90 1-229 20 80 2-229 20 90 1-340 20 90 6-267 20 80 2-340 20 80 1-47 20 90 1-33 20 80 2-154 20 90 1-155 20 90 2-155 20 80 6-260 20 90 1-164 20 90 1-165 20 90 1-166 20 90 1-156 20 90 2-156 20 90 1-159 20 80 2-159 20 90 1-162 20 80 2-161 20 80 6-266 20 80 2-211 20 80 2-272 20 100 2-276 20 90 1-276 20 90 1-274 20 90 1-272 20 90 1-341 20 80 1-292 20 80 2-341 20 80 1-83 20 90 2-83 20 80 2-89 20 80 6-161 20 80 1-342 20 90 1-343 20 80 2-342 20 90 1-345 20 80 2-344 20 80 1-346 20 90 2-345 20 100 1-347 20 90 2-346 20 80 1-195 20 80 1-184 20 80 2-348 20 80 1-84 20 90 2-84 20 80 1-352 20 90 2-350 20 80 1-86 20 90 2-86 20 90 1-92 20 90 2-92 20 90 1-90 20 90 1-353 20 90 2-351 20 90 2-352 20 80 1-355 20 80 2-353 20 80 1-356 20 80 2-354 20 80
TABLE-US-00084 TABLE 26c Post-emergence action at 80 g/ha against PHBPU in % Example number Dosage [g/ha] PHBPU 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 90 1-338 80 90 2-338 80 90 3-338 80 90 2-337 80 80 6-117 80 80 1-81 80 80 2-81 80 90 1-147 80 90 2-147 80 80
TABLE-US-00085 TABLE 27a Post-emergence action at 5 g/ha against POLCO in % Example number Dosage [g/ha] POLCO 1-72 5 100
TABLE-US-00086 TABLE 27b Post-emergence action at 20 g/ha against POLCO in % Example number Dosage [g/ha] POLCO 1-26 20 90 2-26 20 80 6-26 20 80 3-125 20 80 2-130 20 80 1-147 20 90 2-148 20 90 1-149 20 100 2-149 20 80 5-122 20 80 1-88 20 80 1-27 20 90 2-173 20 90 2-30 20 80 1-28 20 80 2-304 20 80 2-305 20 100 1-306 20 80 1-178 20 80 6-141 20 80 1-179 20 80 2-179 20 90 1-207 20 100 1-72 20 100 1-73 20 80 1-74 20 80 2-180 20 100 1-183 20 100 2-287 20 100 1-212 20 100 1-271 20 80
TABLE-US-00087 TABLE 27c Post-emergence action at 80 g/ha against POLCO in % Example number Dosage [g/ha] POLCO 3-129 80 90 2-129 80 100 1-129 80 100 6-116 80 80 1-81 80 90 2-81 80 80 2-82 80 80 6-58 80 100 1-147 80 90 2-147 80 80 1-148 80 80 2-148 80 90
TABLE-US-00088 TABLE 28a Post-emergence action at 5 g/ha against SETVI in % Example number Dosage [g/ha] SETVI 2-129 5 100 1-129 5 100 6-116 5 100 1-26 5 100 2-26 5 80 1-208 5 80 2-208 5 80 2-131 5 90 1-149 5 100 2-149 5 90 6-124 5 80 5-58 5 80 5-117 5 100 5-253 5 80 5-75 5 80 5-74 5 80 5-123 5 80 5-122 5 80 1-82 5 80 1-87 5 80 2-87 5 80 1-88 5 80 2-88 5 90 1-209 5 100 1-27 5 100 2-27 5 80 1-173 5 90 2-173 5 100 1-273 5 80 2-273 5 80 6-33 5 80 1-28 5 80 1-304 5 90 2-304 5 80 2-305 5 90 1-306 5 90 2-306 5 80 1-177 5 90 2-177 5 90 1-179 5 90 2-179 5 90 1-134 5 90 1-133 5 90 2-133 5 80 1-277 5 90 2-277 5 90 2-278 5 80 1-279 5 90 2-195 5 90 2-197 5 80 1-225 5 90 1-226 5 100 2-226 5 100 1-56 5 100 2-57 5 100 1-58 5 100 2-58 5 90 2-56 5 80 1-57 5 100 1-207 5 100 2-207 5 90 2-271 5 100 6-210 5 90 2-32 5 80 1-34 5 80 2-34 5 80 6-255 5 80 2-33 5 80 1-182 5 90 2-182 5 90 6-145 5 80 2-287 5 80 2-288 5 80 1-210 5 80 1-212 5 80 1-288 5 80 1-289 5 80 1-339 5 80 1-49 5 90 1-229 5 80 1-33 5 80 1-166 5 90 2-272 5 90 1-276 5 80 1-272 5 90 2-158 5 90 1-83 5 80 1-89 5 90 2-89 5 90 1-342 5 90 2-342 5 90 1-344 5 80 2-343 5 90 1-346 5 100 2-345 5 80 1-195 5 100 1-185 5 80 1-349 5 90 2-348 5 80 2-349 5 90 1-84 5 100 2-84 5 80 1-352 5 80 2-86 5 100 1-92 5 90 2-92 5 80 2-352 5 80
TABLE-US-00089 TABLE 28b Post-emergence action at 20 g/ha against SETVI in % Example number Dosage [g/ha] SETVI 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 1-338 20 80 2-338 20 80 6-253 20 90 1-26 20 100 2-26 20 100 6-26 20 80 1-208 20 80 2-208 20 80 1-130 20 80 2-81 20 90 1-131 20 100 2-131 20 100 1-149 20 100 2-149 20 100 6-124 20 90 5-59 20 90 5-58 20 100 5-117 20 100 5-253 20 80 5-75 20 80 5-74 20 90 5-123 20 80 5-122 20 90 1-82 20 90 1-87 20 90 2-87 20 80 1-88 20 90 2-88 20 100 1-209 20 100 1-4 20 80 1-25 20 80 2-25 20 80 3-27 20 90 1-27 20 100 2-27 20 100 1-173 20 90 2-173 20 100 1-273 20 100 2-273 20 90 3-273 20 80 6-212 20 80 4-212 20 80 1-44 20 90 1-45 20 80 2-45 20 80 6-32 20 80 1-46 20 80 6-33 20 80 2-30 20 80 1-28 20 80 1-29 20 80 2-29 20 80 1-304 20 90 2-304 20 80 1-305 20 90 2-305 20 90 1-306 20 90 2-306 20 80 1-177 20 90 2-177 20 90 1-178 20 90 2-178 20 90 1-179 20 90 2-179 20 90 1-132 20 90 2-132 20 80 1-135 20 80 6-254 20 80 1-134 20 90 1-133 20 100 2-133 20 90 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 2-195 20 100 2-197 20 100 1-225 20 100 1-226 20 100 2-226 20 100 6-165 20 80 6-166 20 100 2-196 20 100 1-56 20 100 6-45 20 100 6-44 20 80 2-57 20 100 6-43 20 90 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 2-271 20 100 6-210 20 100 2-32 20 100 1-34 20 90 2-34 20 90 6-255 20 90 2-33 20 100 1-72 20 80 2-72 20 80 2-73 20 100 1-74 20 100 2-74 20 90 1-138 20 80 1-137 20 80 1-136 20 80 2-180 20 90 1-182 20 100 2-182 20 100 6-145 20 90 1-181 20 90 2-181 20 90 2-230 20 100 6-169 20 90 2-286 20 80 2-287 20 90 2-288 20 90 1-210 20 90 2-210 20 80 1-212 20 90 1-288 20 100 1-289 20 90 2-289 20 80 1-291 20 80 2-291 20 90 2-292 20 80 1-271 20 80 2-47 20 90 6-34 20 90 1-339 20 90 2-339 20 100 1-49 20 100 2-49 20 90 1-41 20 80 1-229 20 90 2-229 20 80 1-47 20 80 1-33 20 90 6-259 20 90 1-155 20 80 1-165 20 90 1-166 20 90 1-156 20 80 2-156 20 80 6-262 20 80 2-211 20 90 2-272 20 100 2-276 20 80 1-276 20 80 1-274 20 90 1-272 20 90 1-341 20 80 1-292 20 90 2-158 20 90 1-83 20 100 2-83 20 100 1-89 20 90 2-89 20 100 6-76 20 80 6-161 20 90 1-342 20 90 1-343 20 100 2-342 20 90 1-344 20 90 2-343 20 90 1-345 20 90 2-344 20 80 1-346 20 100 2-345 20 100 1-195 20 100 1-185 20 100 2-185 20 80 1-186 20 80 1-349 20 90 1-350 20 80 2-348 20 100 1-351 20 100 2-349 20 100 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 80 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 90 1-353 20 100 1-354 20 100 2-352 20 80 2-354 20 90
TABLE-US-00090 TABLE 28c Post-emergence action at 80 g/ha against SETVI in % Example number Dosage [g/ha] SETVI 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 100 2-338 80 100 3-338 80 90 6-253 80 100 1-81 80 90 2-81 80 90 2-148 80 80
TABLE-US-00091 TABLE 29a Post-emergence action at 5 g/ha against STEME in % Example number Dosage [g/ha] STEME 3-129 5 100 2-129 5 100 1-129 5 100 6-116 5 90 3-338 5 80 1-26 5 90 2-26 5 80 1-208 5 90 2-208 5 80 3-208 5 80 1-130 5 80 2-130 5 80 1-131 5 80 2-131 5 90 1-149 5 90 2-149 5 90 6-124 5 90 5-59 5 90 5-58 5 90 5-117 5 100 5-75 5 90 5-74 5 80 5-123 5 90 5-122 5 90 1-82 5 90 1-87 5 80 2-87 5 80 1-88 5 90 2-88 5 90 1-4 5 80 1-25 5 80 2-25 5 90 1-27 5 100 2-27 5 100 1-173 5 80 2-173 5 100 1-273 5 90 2-273 5 80 3-273 5 80 6-212 5 80 1-44 5 80 2-46 5 80
TABLE-US-00092 TABLE 29b Post-emergence action at 20 g/ha against STEME in % Example number Dosage [g/ha] STEME 3-129 20 100 2-129 20 100 1-129 20 100 6-116 20 100 2-338 20 90 3-338 20 100 2-337 20 90 3-337 20 100 1-26 20 90 2-26 20 90 3-26 20 90 6-26 20 80 1-208 20 90 2-208 20 100 3-208 20 90 6-159 20 90 2-125 20 80 3-125 20 80 1-130 20 80 2-130 20 80 6-117 20 90 1-81 20 90 2-81 20 90 2-82 20 80 6-58 20 80 1-147 20 80 2-147 20 80 1-148 20 90 2-148 20 80 1-131 20 100 2-131 20 90 6-118 20 100 1-149 20 90 2-149 20 90 6-124 20 90 5-59 20 100 5-58 20 90 5-117 20 100 5-253 20 80 5-75 20 100 5-74 20 90 5-123 20 90 5-122 20 100 1-82 20 90 1-87 20 100 2-87 20 90 1-88 20 90 2-88 20 100 1-209 20 90 1-4 20 90 1-25 20 100 2-25 20 100 3-27 20 80 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 100 1-273 20 100 2-273 20 90 3-273 20 90 6-212 20 90 1-44 20 80 2-44 20 80 1-45 20 80 6-32 20 80 1-46 20 80 2-46 20 80 6-33 20 80
TABLE-US-00093 TABLE 29c Post-emergence action at 80 g/ha against STEME in % Example number Dosage [g/ha] STEME 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 100 3-338 80 100 6-253 80 90 2-337 80 90 6-117 80 90 1-81 80 90 2-81 80 100 2-82 80 90 6-58 80 80 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 80
TABLE-US-00094 TABLE 30a Post-emergence action at 5 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 1-129 5 80 2-337 5 80 1-149 5 80 1-87 5 80 1-88 5 80 1-44 5 80 2-46 5 80 1-304 5 80 1-132 5 90 1-135 5 80 2-133 5 80 1-277 5 80 2-277 5 80 1-278 5 80 1-279 5 80 1-57 5 80 2-207 5 80 2-271 5 80 2-32 5 90 1-72 5 80 1-73 5 80 2-73 5 80 1-74 5 80 1-183 5 80 2-286 5 80 2-287 5 80 1-289 5 80 2-289 5 80 1-271 5 80 1-165 5 80 1-166 5 80 1-341 5 80 1-292 5 80 1-89 5 90 2-89 5 80 1-346 5 80 1-353 5 80
TABLE-US-00095 TABLE 30b Post-emergence action at 20 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 2-129 20 80 1-129 20 80 2-338 20 90 3-338 20 90 6-253 20 80 2-337 20 100 3-337 20 90 2-123 20 80 1-26 20 80 1-208 20 80 2-208 20 80 1-81 20 80 2-81 20 80 2-82 20 80 1-147 20 90 2-147 20 80 1-148 20 80 2-148 20 80 1-131 20 90 1-149 20 100 5-59 20 80 5-58 20 80 5-117 20 80 5-122 20 80 1-82 20 80 1-87 20 90 2-87 20 80 1-88 20 90 2-88 20 80 1-209 20 80 1-25 20 80 2-25 20 90 1-27 20 100 2-27 20 80 2-173 20 80 1-273 20 90 3-273 20 80 1-44 20 100 2-44 20 80 1-45 20 80 1-46 20 90 2-46 20 80 1-31 20 80 2-31 20 80 1-304 20 80 2-304 20 90 1-305 20 80 2-305 20 90 1-306 20 90 2-306 20 90 1-177 20 80 2-177 20 80 1-178 20 80 1-179 20 80 1-132 20 90 1-135 20 90 2-135 20 90 6-254 20 80 1-134 20 80 2-134 20 80 1-133 20 90 2-133 20 80 6-120 20 80 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 100 1-279 20 100 2-279 20 90 1-197 20 80 2-227 20 80 1-227 20 80 1-225 20 90 1-226 20 90 2-226 20 90 2-196 20 80 1-56 20 90 2-57 20 90 1-58 20 80 2-56 20 80 1-57 20 90 1-207 20 90 2-207 20 90 2-271 20 90 2-32 20 90 1-34 20 90 2-34 20 80 6-255 20 80 2-42 20 90 2-146 20 80 1-37 20 80 2-37 20 80 1-72 20 90 2-72 20 80 1-73 20 80 2-73 20 90 1-74 20 90 2-74 20 80 1-183 20 90 2-183 20 90 1-181 20 90 1-228 20 90 1-230 20 80 2-230 20 90 2-286 20 80 1-287 20 80 2-287 20 100 2-288 20 80 1-212 20 80 1-289 20 90 2-289 20 100 1-291 20 80 2-291 20 80 2-292 20 80 1-271 20 90 2-47 20 80 1-339 20 90 2-339 20 80 6-258 20 80 1-49 20 90 1-340 20 80 2-340 20 90 1-47 20 80 1-33 20 80 1-32 20 90 1-155 20 80 1-165 20 80 1-166 20 90 1-156 20 80 2-156 20 90 1-276 20 80 1-274 20 80 1-272 20 80 1-341 20 90 1-292 20 90 1-83 20 90 2-83 20 80 1-89 20 90 2-89 20 90 1-342 20 80 1-343 20 80 1-344 20 90 1-345 20 90 2-344 20 80 1-346 20 80 2-345 20 80 1-347 20 90 2-346 20 80 1-195 20 80 1-185 20 80 2-186 20 80 1-349 20 80 1-84 20 90 2-84 20 80 1-352 20 90 2-350 20 80 1-86 20 90 1-92 20 90 2-92 20 90 1-90 20 90 1-353 20 90 2-351 20 90 1-354 20 90 2-352 20 90 1-355 20 90 2-353 20 100 1-356 20 90 2-354 20 90
TABLE-US-00096 TABLE 30c Post-emergence action at 80 g/ha against VERPE in % Example number Dosage [g/ha] VERPE 3-129 80 80 2-129 80 90 1-129 80 100 6-116 80 90 1-338 80 100 2-338 80 100 3-338 80 90 6-253 80 90 2-337 80 100 6-117 80 80 1-81 80 90 2-81 80 90 2-82 80 90 1-147 80 90 2-147 80 90 1-148 80 80 2-148 80 90
TABLE-US-00097 TABLE 31a Post-emergence action at 5 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 5 80 2-129 5 80 1-129 5 80 1-26 5 100 1-208 5 80 2-208 5 100 3-208 5 100 1-125 5 100 2-125 5 100 1-130 5 90 2-130 5 90 1-131 5 100 2-131 5 100 1-149 5 100 2-149 5 100 5-58 5 80 5-117 5 90 5-123 5 80 5-122 5 90 2-88 5 80 1-209 5 100 1-25 5 100 2-25 5 80 3-27 5 80 1-27 5 100 2-27 5 100 1-173 5 90 1-273 5 100 1-45 5 80 2-45 5 80 1-46 5 80 2-46 5 80 1-304 5 80 2-304 5 80 6-231 5 90 1-305 5 90 2-305 5 80 2-306 5 90 1-177 5 90 2-177 5 80 1-178 5 80 1-179 5 80 2-179 5 90 1-132 5 80 1-135 5 80 1-134 5 90 2-134 5 80 1-277 5 80 2-277 5 90 1-278 5 90 2-278 5 90 1-279 5 90 2-279 5 80 2-195 5 100 2-225 5 100 2-227 5 90 1-227 5 100 2-197 5 80 1-226 5 100 2-226 5 90 1-56 5 100 2-57 5 90 1-58 5 90 2-58 5 100 2-56 5 80 1-57 5 100 1-207 5 100 2-207 5 100 2-271 5 80 1-146 5 80 1-73 5 80 1-74 5 80 1-183 5 90 2-183 5 100 1-182 5 100 2-287 5 80 2-288 5 90 1-212 5 80 1-288 5 90 1-289 5 80 1-291 5 90 2-291 5 80 2-47 5 80 1-83 5 90 2-83 5 80 1-89 5 90 2-89 5 90 1-345 5 90 2-344 5 90 1-346 5 90 2-345 5 90 1-347 5 80 2-346 5 80 1-195 5 90 2-185 5 100 1-84 5 100 2-84 5 100 1-352 5 100 2-350 5 100 1-86 5 90 2-86 5 100 2-92 5 100 1-90 5 80 2-90 5 100 1-353 5 100 2-351 5 100
TABLE-US-00098 TABLE 31b Post-emergence action at 20 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 20 90 2-129 20 100 1-129 20 100 6-116 20 80 2-338 20 100 3-338 20 90 6-253 20 80 1-337 20 80 3-337 20 100 1-123 20 100 1-26 20 100 2-26 20 80 3-26 20 90 6-26 20 100 1-208 20 100 2-208 20 100 3-208 20 100 1-125 20 100 2-125 20 100 3-125 20 80 1-130 20 90 2-130 20 100 2-82 20 80 1-148 20 80 1-131 20 100 2-131 20 100 6-118 20 80 1-149 20 100 2-149 20 100 6-124 20 100 5-59 20 80 5-58 20 80 5-117 20 100 5-75 20 80 5-123 20 90 5-122 20 90 1-82 20 90 1-87 20 80 2-87 20 100 1-88 20 80 2-88 20 90 1-209 20 100 1-25 20 100 2-25 20 90 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 90 2-173 20 100 1-273 20 100 1-44 20 80 2-44 20 80 1-45 20 90 2-45 20 100 1-46 20 80 2-46 20 80 1-304 20 90 2-304 20 90 6-231 20 90 1-305 20 90 2-305 20 90 1-306 20 90 2-306 20 90 1-177 20 90 2-177 20 100 1-178 20 80 2-178 20 90 6-141 20 80 1-179 20 90 2-179 20 100 1-132 20 90 2-132 20 90 1-135 20 90 2-135 20 90 1-134 20 90 2-134 20 90 1-133 20 80 2-133 20 80 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 2-279 20 90 2-195 20 100 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 100 1-225 20 80 1-226 20 100 2-226 20 100 6-165 20 80 1-56 20 100 2-57 20 100 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 2-271 20 80 6-210 20 80 1-140 20 80 1-146 20 100 1-37 20 80 1-72 20 90 2-72 20 80 6-49 20 80 1-73 20 80 2-73 20 100 6-50 20 80 1-74 20 90 2-74 20 80 1-180 20 90 2-180 20 100 1-183 20 90 2-183 20 100 1-182 20 100 2-182 20 100 1-228 20 80 2-228 20 80 2-286 20 80 1-287 20 80 2-287 20 90 2-288 20 100 1-210 20 90 2-210 20 90 1-212 20 90 2-213 20 90 1-288 20 90 1-289 20 90 2-289 20 90 1-291 20 100 2-291 20 90 2-292 20 80 1-271 20 90 2-47 20 90 2-47 20 80 2-340 20 80 1-47 20 80 1-33 20 80 1-32 20 80 2-155 20 80 1-165 20 80 1-166 20 80 2-156 20 80 2-272 20 80 2-276 20 80 1-276 20 80 1-274 20 80 1-272 20 90 1-341 20 80 1-292 20 80 1-83 20 90 2-83 20 80 1-89 20 90 2-89 20 90 1-342 20 80 1-343 20 80 2-342 20 80 2-343 20 90 1-345 20 100 2-344 20 100 1-346 20 100 2-345 20 90 1-347 20 100 2-346 20 100 1-195 20 100 1-184 20 90 1-185 20 80 2-185 20 100 2-186 20 80 2-348 20 80 1-351 20 80 2-349 20 80 1-84 20 100 2-84 20 100 1-352 20 100 2-350 20 100 1-86 20 100 2-86 20 100 1-92 20 100 2-92 20 100 1-90 20 100 2-90 20 100 1-353 20 100 2-351 20 100 1-354 20 90 2-352 20 90 1-355 20 100 2-353 20 80 1-356 20 90 2-354 20 100
TABLE-US-00099 TABLE 31c Post-emergence action at 80 g/ha against VIOTR in % Example number Dosage [g/ha] VIOTR 3-129 80 100 2-129 80 100 1-129 80 100 6-116 80 100 1-338 80 90 2-338 80 100 3-338 80 100 6-253 80 80 2-337 80 90 6-117 80 80 1-81 80 80 2-81 80 90 2-82 80 80 1-147 80 80 2-147 80 80 1-148 80 90 2-148 80 80
TABLE-US-00100 TABLE 32a Post-emergence action at 5 g/ha against DIGSA in % Example number Dosage [g/ha] DIGSA 1-26 5 90 2-26 5 90 6-26 5 90 1-208 5 80 2-208 5 80 6-159 5 80 1-130 5 90 2-130 5 80 1-131 5 100 2-131 5 90 6-118 5 100 1-149 5 100 2-149 5 100 5-59 5 90 5-58 5 90 5-117 5 90 5-75 5 90 5-74 5 90 5-123 5 90 5-122 5 90 1-82 5 90 1-87 5 100 2-87 5 90 1-88 5 90 2-88 5 90 1-4 5 80 1-25 5 90 2-25 5 80 1-27 5 90 2-27 5 100 1-173 5 90 1-273 5 90 2-273 5 80 3-273 5 80 6-212 5 80 1-44 5 80 1-45 5 80 6-32 5 80 1-46 5 80 2-305 5 80 1-306 5 90 2-306 5 80 1-177 5 90 1-179 5 90 6-254 5 80 1-133 5 90 1-277 5 90 2-277 5 90 1-278 5 90 2-278 5 90 1-279 5 90 2-279 5 90 2-195 5 80 1-197 5 100 1-227 5 100 1-225 5 90 1-226 5 90 1-56 5 90 6-45 5 90 6-44 5 80 2-57 5 90 6-43 5 90 1-58 5 100 2-58 5 100 2-56 5 90 1-57 5 100 1-207 5 90 2-207 5 80 6-210 5 90 1-34 5 80 2-34 5 80 6-255 5 90 6-256 5 80 1-181 5 90 1-228 5 90 2-228 5 80 2-286 5 90 1-287 5 100 2-287 5 90 2-288 5 90 1-210 5 80 2-210 5 80 1-212 5 90 1-288 5 90 1-289 5 90 2-289 5 90 1-291 5 90 2-291 5 90 2-292 5 90 1-271 5 90 2-47 5 90 1-339 5 90 2-339 5 80 1-49 5 80 2-49 5 90 1-41 5 80 1-229 5 90 2-340 5 80 1-155 5 90 6-260 5 90 1-165 5 90 1-166 5 90 2-272 5 90
TABLE-US-00101 TABLE 32b Post-emergence action at 20 g/ha against DIGSA in % Example number Dosage [g/ha] DIGSA 1-26 20 100 2-26 20 90 6-26 20 90 1-208 20 90 2-208 20 90 6-159 20 90 1-130 20 90 2-130 20 80 6-117 20 80 1-81 20 80 2-81 20 90 2-82 20 90 6-58 20 80 1-147 20 90 2-147 20 90 1-148 20 90 2-148 20 90 1-131 20 100 2-131 20 90 6-118 20 100 1-149 20 100 2-149 20 100 6-124 20 90 5-59 20 90 5-58 20 100 5-117 20 90 5-253 20 80 5-75 20 90 5-74 20 90 5-123 20 90 5-122 20 90 1-82 20 90 1-87 20 100 2-87 20 90 1-88 20 90 2-88 20 90 6-75 20 90 1-209 20 90 1-4 20 90 1-25 20 100 2-25 20 90 3-27 20 100 1-27 20 100 2-27 20 100 1-173 20 100 2-173 20 80 1-273 20 90 2-273 20 90 3-273 20 90 6-212 20 90 1-44 20 90 1-45 20 80 2-45 20 80 6-32 20 80 1-46 20 80 2-31 20 80 2-28 20 80 1-304 20 90 1-305 20 80 2-305 20 90 1-306 20 90 2-306 20 90 1-177 20 90 6-141 20 80 1-179 20 90 1-132 20 90 2-132 20 80 1-135 20 90 2-135 20 80 6-254 20 90 1-134 20 90 2-134 20 80 1-133 20 90 1-277 20 90 2-277 20 90 1-278 20 90 2-278 20 90 1-279 20 90 2-279 20 90 2-195 20 90 2-225 20 100 1-197 20 100 2-227 20 100 1-227 20 100 2-197 20 90 1-225 20 90 1-226 20 100 2-226 20 80 6-165 20 90 2-196 20 90 1-56 20 100 6-45 20 90 6-44 20 90 2-57 20 100 6-43 20 100 1-58 20 100 2-58 20 100 2-56 20 100 1-57 20 100 1-207 20 100 2-207 20 100 6-210 20 90 2-32 20 90 1-34 20 90 2-34 20 100 6-255 20 100 6-256 20 90 1-181 20 90 1-228 20 90 2-228 20 80 1-230 20 90 2-230 20 90 2-286 20 90 1-287 20 100 2-287 20 90 2-288 20 90 1-210 20 90 2-210 20 90 1-212 20 100 2-212 20 100 2-213 20 90 1-288 20 100 1-289 20 90 2-289 20 100 6-228 20 80 1-291 20 100 2-291 20 100 2-292 20 90 1-271 20 100 2-47 20 90 6-34 20 80 1-339 20 90 2-339 20 90 6-258 20 90 1-49 20 90 2-49 20 90 1-41 20 90 1-229 20 90 1-340 20 90 2-340 20 90 1-47 20 90 1-33 20 90 2-154 20 90 6-259 20 90 1-155 20 90 6-260 20 90 1-164 20 80 6-261 20 90 1-165 20 90 1-166 20 90 1-156 20 90 2-156 20 80 6-262 20 90 6-264 20 80 2-211 20 80 2-272 20 90
TABLE-US-00102 TABLE 32c Post-emergence action at 80 g/ha against DIGSA in % Example number Dosage [g/ha] DIGSA 2-337 80 90 6-117 80 90 1-81 80 90 2-81 80 90 2-82 80 90 6-58 80 90 1-147 80 90 2-147 80 90 1-148 80 90 2-148 80 90
Comparative Experiments
[0769] In the experiments that follow, herbicidal action of numerous inventive compounds and the structurally closest compounds known from D1 (WO 2012/028579 A1) were compared under the above-specified conditions by the pre-emergence and post-emergence method. The example numbers given in the tables relate to the compounds disclosed in the respective documents.
TABLE-US-00103 TABLE 5 Herbicidal pre-emergence action Dosage Herbicidal action against Example No.: (g a.i./ha) ALOMY AVEFA ABUTH MATIN STEME VIOTR 1-129, inventive 80 100 100 100 100 100 100 4-251, from Di 80 0 0 50 70 70 0 Dosage Herbicidal action against Example No.: (g a.i./ha) ALOMY AVEFA SETVI AMARE STEME VIOTR 1-147, inventive 80 90 100 100 100 100 100 4-251, from DI 80 0 0 20 70 70 0 Dosage Herbicidal action against Example No.: (g a.i./ha) ALOMY AVEFA SETVI STEME HORMU 2-147, inventive 80 90 100 100 70 90 5-251, from DI 80 0 0 80 40 10 Dosage Herbicidal action against Example No.: (g a.i./ha) AVEFA MATIN ABUTH AMARE STEME VIOTR 1-129, inventive 20 100 100 100 100 100 100 4-251, from DI 20 0 0 40 0 30 80 Dosage Herbicidal action against Example No.: (g a.i./ha) AVEFA SETVI ABUTH MATIN POLCO VIOTR 2-129, inventive 20 100 100 100 100 100 100 5-251, from Di 20 0 30 70 70 40 80
TABLE-US-00104 TABLE 6 Herbicidal post-emergence action Example Dosage Herbicidal action against No.: (g a.i./ha) ALOMY AVEFA MATIN PHBPU POLCO VIOTR 1-147, 20 80 90 100 80 90 70 inventive 4-251, 20 20 0 30 60 30 50 from Di Example Dosage Herbicidal action against No.: (g a.i./ha) ALOMY AVEFA LOLRI MATIN PHBPU HORMU 2-147, 20 80 90 70 100 70 80 inventive 5-251, 20 60 30 30 50 50 30 from DI Example Dosage Herbicidal action against No.: (g a.i./ha) ALOMY ECHCG SETVI ABUTH STEME VIOTR 1-129, 5 90 100 100 100 100 80 inventive 4-251, 5 0 50 0 70 60 20 from DI Example Dosage Herbicidal action against No.: (g a.i./ha) ALOMY AVEFA SETVI AMARE MATIN HORMU 2-129, 5 100 100 100 100 80 80 inventive 5-251, 5 30 20 30 80 30 20 from DI