HIGH-STRENGTH CONCRETE AND PREPARATION METHOD THEREOF
20230159391 ยท 2023-05-25
Inventors
- Ke Wu (Jinan, CN)
- Tao YANG (Jinan, CN)
- Cao Wang (Jinan, CN)
- Guodong Li (Jinan, CN)
- Rong Chen (Jinan, CN)
- Jiahui Zhao (Jinan, CN)
- Dongxue Hao (Jinan, CN)
- Mingyue Ma (Jinan, CN)
- Hongna Yang (Jinan, CN)
Cpc classification
C04B18/167
CHEMISTRY; METALLURGY
C04B20/026
CHEMISTRY; METALLURGY
C04B18/167
CHEMISTRY; METALLURGY
C04B28/02
CHEMISTRY; METALLURGY
C04B20/026
CHEMISTRY; METALLURGY
C04B28/02
CHEMISTRY; METALLURGY
C04B40/0028
CHEMISTRY; METALLURGY
C04B40/0028
CHEMISTRY; METALLURGY
Y02W30/91
GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
International classification
Abstract
The present disclosure relates to a high-strength concrete and a preparation method thereof. The high-strength concrete includes lignin, recycled fine powder, cement, water, sand, gravels and a water reducing agent. The recycled fine powder is recycled fine powder of discarded concrete, and is prepared by separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm. The lignin is discarded wood lignin, which is prepared by crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering.
Claims
1. A high-strength concrete, comprising lignin, recycled fine powder, cement, water, sand, gravels and a water reducing agent, wherein: the recycled fine powder is recycled fine powder of discarded concrete, and is specifically prepared by: separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm; the lignin is discarded wood lignin, which is extracted by: crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering; the weight ratio of the cement, water, sand, gravels and water reducing agent in the high-strength concrete is 1:0.3:1.2:2.8:0.01; the weight ratio of the lignin to the recycled fine powder is 0.1:5-10; the weight ratio of the lignin to the cement is 0.1-0.3:20; P.Math.042.5 grade cement is adopted, gravels with a particle size of 6 mm to 10 mm are adopted, and a polycarboxylic acid water reducing agent is adopted; and a preparation method of the high-strength concrete mentioned above, comprising the following steps: (1) preparation of recycled fine powder: separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm; (2) preparation of lignin: crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering to obtain the lignin; (3) pouring the lignin and the recycled fine powder into part of the water for uniform mixing; (4) pouring the cement into the remaining water for uniform stirring with a cement mixer; (5) pouring the mixed solution of the lignin and the recycled fine powder into the cement uniformly stirred in step (4), and then adding the water reducing agent for uniform mixing to obtain a mixed solution A; and (6) pouring the gravels and sand into the mixed solution A in step (5) for full stirring to obtain the high-strength concrete.
2. The high-strength concrete of claim 1, wherein the ratio of water in the step (3) and step (4) is 1:2.
Description
DETAILED DESCRIPTION
[0028] The present disclosure will be further described below with reference to specific embodiments, and the advantages and characteristics of the present disclosure will become clear from the description. However, the embodiments are only exemplary and do not constitute any limitation to the scope of the present disclosure. It should be understood by those skilled in the art that modifications and replacements may be made to the details and forms of the technical solutions of the present disclosure without departing from the spirit and scope of the present disclosure, and all these modifications and replacements shall fall within the protection scope of the present disclosure.
[0029] Embodiment one: a high-strength concrete and a preparation method thereof.
[0030] At step 1, P 042.5 grade cement is adopted, gravels with a particle size of 6 m to 10 m are adopted, and a polycarboxylic acid water reducing agent is adopted;
[0031] preparation of recycled fine powder: separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 m; and
[0032] preparation of lignin: crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with a mass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering to obtain the lignin.
[0033] At step 2, 20 kg of cement, 6 kg of water, 24 kg of sand, 56 kg of gravels, and 0.2 kg of water reducing agent are weighted using a meter.
[0034] At step 3, 0.1 kg of lignin and 10 kg of recycled fine powder are poured into 2 kg of water for uniform mixing.
[0035] At step 4, 20 kg of cement is poured into 4 kg of water for full stirring with a cement mixer.
[0036] At step 5, the mixed solution of lignin and recycled fine powder is poured into the cement stirred uniformly in step 4, then 0.2 kg of water reducing agent is added for uniform mixing to obtain a mixed solution A.
[0037] At step 6, 56 kg of gravels and 24 kg of sand are poured into the mixed solution A in step 5 for full stirring to obtain the high-strength concrete.
[0038] Embodiment two: a high-strength concrete and a preparation method thereof
[0039] At step 1, P 042.5 grade cement is adopted, gravels with a particle size of 6 mm to 10 mm are adopted, and a polycarboxylic acid water reducing agent is adopted;
[0040] preparation of recycled fine powder: separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm; and
[0041] preparation of lignin: crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with amass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering to obtain the lignin.
[0042] At step 2, 20 kg of cement, 6 kg of water, 24 kg of sand, 56 kg of gravels, and 0.2 kg of water reducing agent are weighted using.
[0043] At step 3, 0.2 kg of lignin and 12 kg of recycled fine powder are poured into 1.5 kg of water for uniform mixing.
[0044] At step 4, 20 kg of cement is poured into 4.5 kg of water for full stirring with a cement mixer.
[0045] At step 5, the mixed solution of lignin and recycled fine powder is poured into the cement stirred uniformly in step 4, and then 0.2 kg of water reducing agent is added for uniform mixing to obtain a mixed solution A.
[0046] At step 6, 56 kg of gravels and 24 kg of sand are poured into the mixed solution A in step 5 for full stirring to obtain the high-strength concrete.
[0047] Embodiment three: a high-strength concrete and a preparation method thereof
[0048] At step 1, P.Math.042.5 grade cement is adopted, gravels with a particle size of 6 mm to 10 mm are adopted, and a polycarboxylic acid water reducing agent is adopted;
[0049] preparation of recycled fine powder: separating solid waste of discarded buildings, then performing impurity removal and crushing processing, and grinding same by a ball mill into dust with a particle size of less than 0.16 mm; and
[0050] preparation of lignin: crushing the wood, stirring and extracting a sodium hydroxide aqueous solution with a mass concentration of 5% for 1 to 2 hours at the temperature of 80 DEG C. to obtain a black lignin alkali solution, adding a hydrochloric acid solution with amass concentration of 30% into the alkali solution for stirring, and making the pH reduced to 7.0 for standing and layering to obtain the lignin.
[0051] At step 2, 20 kg of cement, 6 kg of water, 24 kg of sand, 56 kg of gravels, and 0.2 kg of water reducing agent are weighted using a meter.
[0052] At step 3, 0.3 kg of lignin and 15 kg of recycled fine powder are poured into 2 kg of water for uniform mixing.
[0053] At step 4, 20 kg of cement is poured into 4 kg of water for full stirring with a cement mixer.
[0054] At step 5, the mixed solution of lignin and recycled fine powder is poured into the cement stirred uniformly in step 4), and then 0.2 kg of water reducing agent is added for uniform mixing to obtain a mixed solution A.
[0055] At step 6, 56 kg of gravels and 24 kg of sand are poured into the mixed solution A in step 5 for full stirring to obtain the high-strength concrete.
Experimental Example One: Axial Compression Experiment
[0056] Experimental Steps:
[0057] In the axial compressive strength experiment, a 150 mm*150 mm*300 mm prismatic specimen is used and standardly cured to a specified age. The specimen is placed upright, with the axis of the specimen aligned with the center of a lower platen of a testing machine, and load is applied at a specified speed until a failure, so as to measure its axial compressive strength. The experimental results are shown in Table 1:
TABLE-US-00001 TABLE 1 Specimen Group Number Compressive Strength (MPa) Plain concrete 33.10 High-strength concrete obtained in 37.62 Embodiment one High-strength concrete obtained in 37.79 Embodiment two High-strength concrete obtained in 38.29 Embodiment three
[0058] Experimental Results:
[0059] By means of the axial compressive strength experiment of plain concrete and the concrete obtained by the present disclosure respectively, the experimental results show that the high-strength concrete obtained by the present disclosure has a significant increase in the compressive strength.