INTEGRATED HOLLOW-CORE OPTICAL FIBER PREFORM, OPTICAL FIBER AND FABRICATION METHOD THEREOF

20250326678 ยท 2025-10-23

    Inventors

    Cpc classification

    International classification

    Abstract

    The disclosure relates to an integrated hollow-core optical fiber preform, an optical fiber and a fabrication method thereof. Initially, holes are drilled to obtain a preform which is then subjected to a drawing process with gas fed into the drilled holes for pressurization control, resulting in an optical fiber with an anti-resonant ring structure. This method employs mechanical drilling to achieve precise positioning of the azimuth angle of the anti-resonant unit, ensuring axial uniformity and preventing any azimuthal shift during the drawing process. Furthermore, no additional materials are introduced for positioning the anti-resonant unit, thereby minimizing contamination from impurities and enhancing properties such as attenuation and strength of the optical fiber. Additionally, gas pressure control expands the anti-resonant unit during the drawing process, reducing its wall thickness and consequently lowering attenuation in this hollow-core optical fiber.

    Claims

    1. An integrated hollow-core optical fiber preform, comprising a jacket tube with multiple circumferentially distributed axial holes formed in a wall of the jacket tube, an internal surface of each of the axial holes at a position closest to a center of the jacket tube having a minimum distance t.sub.1 from an internal surface of the jacket tube, and a ratio of the minimum distance t.sub.1 to a diameter of the axial hole being less than or equal to 0.35.

    2. The integrated hollow-core optical fiber preform according to claim 1, wherein the axial holes are uniformly distributed along a circle, with a number 4.

    3. The integrated hollow-core optical fiber preform according to claim 1, wherein a ratio of an inner diameter of the jacket tube and an outer diameter ranges from 0.2 to 0.8.

    4. The integrated hollow-core optical fiber preform according to claim 1, wherein a capillary tube is inserted into each of the axial holes to form an optical fiber preform with a nested structure.

    5. The integrated hollow-core optical fiber preform according to claim 1, wherein a quartz sheet is inserted into each of the axial holes to form an optical fiber preform with a connecting sheet structure.

    6. A fabrication method of a hollow-core micro-structured optical fiber, comprising steps of: i) selecting a jacket tube and performing drilling from an end of the jacket tube to prepare the integrated hollow-core optical fiber preform according to claim 1; and ii) performing hot-drawing on the integrated hollow-core optical fiber preform obtained in step i), and during such a drawing process, feeding a gas into the axial holes to create a gas pressure in each of the axial holes higher than that in a center hole of the jacket tube, so that a pressure difference between each of the axial holes and the center hole of the jacket tube along with surface tension causes the drawn axial holes to protrude towards the center hole of the jacket tube to form anti-resonant rings with a negative curvature, all of which constitute a ring-shaped anti-resonant layer, with an area enclosed by the anti-resonant layer constituting a hollow fiber core, thereby forming the hollow-core micro-structured optical fiber with the negative-curvature anti-resonant rings.

    7. The fabrication method of the hollow-core micro-structured optical fiber according to claim 6, wherein in step i), after drilling, an acid liquid is fed to corrode the axial holes, such that a ratio of the minimum distance t.sub.1 between the internal surface of each of the axial holes and the internal surface of the jacket tube to the diameter of each of the axial holes is less than or equal to 0.1.

    8. The fabrication method of the hollow-core micro-structured optical fiber according to claim 7, wherein in step i), the acid liquid is hydrofluoric acid.

    9. The fabrication method of the hollow-core micro-structured optical fiber according to claim 6, wherein in step i), when each of the axial holes is embedded with a capillary tube, which is further fed with a gas, gas pressures inside the capillary tubes, the axial holes and the center hole of the jacket tube are controlled to be reduced in gradient.

    10. The fabrication method of the hollow-core micro-structured optical fiber according to claim 9, wherein in step i), the gas fed into the axial holes or the capillary tubes is selected from any one or more of compressed air, nitrogen, helium and argon.

    11. The fabrication method of the hollow-core micro-structured optical fiber according to claim 6, wherein in step ii), the anti-resonant layer and the drawn jacket tube constitute a cladding, wherein the cladding has an outer diameter ranging from 100 to 300 m, and the fiber core has a diameter ranging from 10 to 50 m.

    12. The fabrication method of the hollow-core micro-structured optical fiber according to claim 6, wherein in step ii), each of the anti-resonant rings has a minimum wall thickness less than or equal to 2 m.

    13. A hollow-core micro-structured optical fiber, prepared by the fabrication method according to claim 6.

    Description

    BRIEF DESCRIPTION OF THE DRAWINGS

    [0026] FIG. 1 is a schematic structural diagram of an optical fiber preform with a hollow-core micro-structure provided by Embodiment I of the disclosure;

    [0027] FIG. 2 is a schematic structural diagram of a hollow-core micro-structured optical fiber provided by Embodiment I of the disclosure;

    [0028] FIG. 3 is a schematic structural diagram of an optical fiber preform with a hollow-core micro-structure provided by Embodiment II of the disclosure;

    [0029] FIG. 4 is a schematic structural diagram of a hollow-core micro-structured optical fiber provided by Embodiment II of the disclosure;

    [0030] FIG. 5 is a schematic structural diagram of an optical fiber preform with a nested structure provided by Embodiment III of the disclosure;

    [0031] FIG. 6 is a schematic structural diagram of a hollow-core micro-structured optical fiber provided by Embodiment III of the disclosure;

    [0032] FIG. 7 is a schematic structural diagram of an optical fiber preform with a connecting sheet structure provided by Embodiment IV of the disclosure; and

    [0033] FIG. 8 is a schematic structural diagram of a hollow-core micro-structured optical fiber provided by Embodiment IV of the disclosure.

    LIST OF REFERENCE NUMBERS

    [0034] 1 optical fiber preform [0035] 2 jacket tube [0036] 3 axial hole [0037] 4 hollow-core micro-structured optical fiber [0038] 5 optical fiber cladding [0039] 6 anti-resonant ring [0040] 7 optical fiber hollow-core fiber core, [0041] 10 capillary tube [0042] 11 first layer of anti-resonant rings [0043] 12 second layer of anti-resonant rings [0044] 13 quartz sheet [0045] 14 anti-resonant ring [0046] 15 anti-resonant sheet [0047] 16 axial hole [0048] 17 internal surface of 2 [0049] 18 large circular hole

    DETAILED DESCRIPTION

    [0050] The technical problems to be solved, technical solutions and advantages of the disclosure will become apparent from the following detailed description with reference to the embodiments. It should be understood that the specific embodiments described here are only intended to explain the disclosure, but not to construct limitation to the disclosure. Furthermore, the technical features involved in various implementations of the disclosure described below may be combined with each other as long as they do not constitute a conflict with each other.

    [0051] The disclosure provides a fabrication method of a hollow-core micro-structured optical fiber, comprising the following steps.

    [0052] At step i), a jacket tube is selected and drilling is performed from an end of the jacket tube to prepare an integrated hollow-core optical fiber preform.

    [0053] The integrated hollow-core optical fiber preform comprises a jacket tube with multiple circumferentially distributed axial holes formed in a wall of the jacket tube, an internal surface of each of the axial holes at a position closest to a center of the jacket tube having a minimum distance t.sub.1 from an internal surface of the jacket tube, and a ratio of the minimum distance t.sub.1 to a diameter of the axial hole being less than or equal to 0.35.

    [0054] At step ii), hot-drawing is performed on the integrated hollow-core optical fiber preform obtained in step i), and during such a drawing process, a gas is fed into the axial holes to create a gas pressure in each of the axial holes higher than that in a center hole of the jacket tube, so that a pressure difference between each of the axial holes and the center hole of the jacket tube along with surface tension causes the drawn axial holes to protrude towards the center hole of the jacket tube to form anti-resonant rings with a negative curvature, all of which constitute a ring-shaped anti-resonant layer, with an area enclosed by the anti-resonant layer constituting a hollow fiber core, thereby forming the hollow-core micro-structured optical fiber with the negative-curvature anti-resonant rings.

    Embodiment I

    Fabrication of Hollow Core Fiber Preform

    [0055] As shown in FIG. 1, a jacket tube 2 made from a material of pure silicon dioxide is selected, which has an inner diameter d.sub.0 of 30 mm, an outer diameter D.sub.0 of 50 mm and a length of 1000 mm. Five axial holes 3 are formed in the jacket tube by drilling, where the axial holes are arranged in an isoazimuth mode (with an azimuth angle of) 72, each of the axial holes 3 has a diameter di of 6.5 mm, and a ratio of a minimum distance t.sub.1 between an internal surface of each of the axial holes 3 and an internal surface 17 of the jacket tube to the diameter d.sub.1 of the axial hole is 0.08. Then, an optical fiber preform 1 with a hollow-core micro-structure is prepared.

    Fabrication of Hollow-Core Micro-Structured Optical Fiber

    [0056] The optical fiber preform 1 with the hollow-core micro-structure is placed into a hot-drawing furnace for drawing at a furnace temperature of 1710 C., a hollow-core portion in the middle of the preform maintains a pressure value equal to the atmospheric pressure, and a gas of equal pressure is fed into the five axial holes at a pressure of 2.9 KPa. The pressure difference between the inside and outside of the axial holes leads to the expansion of the axial holes after drawing, which results in formation of anti-resonant rings 6, finally forming a hollow-core micro-structured optical fiber 4 as shown in FIG. 3. An optical fiber cladding 5 has an outer diameter of 124.7 m, an optical fiber hollow-core fiber core 7 has a diameter of 27.4 m, and each of the anti-resonant rings has a minimum wall thickness of 637 nm. The attenuation of the optical fiber at 1550 nm is 12.7 dB/km.

    Embodiment II

    Fabrication of Optical Fiber Preform

    [0057] As shown in FIG. 3, a jacket tube made from a material of pure silicon dioxide is selected, which has an inner diameter of 40 mm, an outer diameter of 80 mm and a length of 900 mm. Six axial holes 3 are formed in the jacket tube by drilling, where the axial holes 3 are arranged in an isoazimuth mode (with an azimuth angle of) 60, each of the axial holes 3 has a diameter of 8.2 mm, and a ratio of a minimum distance 8 between an internal surface of each of the axial holes 3 and an internal surface 17 of the jacket tube to the diameter of the axial hole 3 is 0.21. The drilled jacket tube is placed into an acid liquid for corroding, and a ratio of a minimum distance 9 between an internal surface of each of corroded axial holes 16 and the internal surface 17 of the jacket tube to the diameter of the axial hole 16 is 0.06. Then, an optical fiber preform 1 with a hollow-core micro-structure is prepared.

    Fabrication of Hollow-Core Micro-Structured Optical Fiber

    [0058] The optical fiber preform 1 with the hollow-core micro-structure is placed into a hot-drawing furnace for drawing at a furnace temperature of 1760 C., a gas is fed into a hollow-core portion in the middle of the preform to maintain a gas pressure near 0.56 Kpa, and a gas of equal pressure is fed into the six axial holes 16 at a pressure of 1.9 KPa. The pressure difference between the inside and outside of the axial holes 16 leads to the expansion of the axial holes after drawing, which results in formation of anti-resonant rings 6, finally forming a hollow-core micro-structured optical fiber 4 as shown in FIG. 4. An optical fiber cladding 5 has an outer diameter of 243 m, an optical fiber hollow-core fiber core 7 has a diameter of 42.7 m, and each of the anti-resonant rings 6 has a minimum wall thickness of 336 nm. The attenuation of the optical fiber at 1550 nm is 1.45 dB/km.

    Embodiment III

    Fabrication of Optical Fiber Preform

    [0059] As shown in FIG. 5, a jacket tube 2 made from a material of pure silicon dioxide is selected, which has an inner diameter of 13 mm, an outer diameter of 28 mm and a length of 700 mm. Six axial holes 3 are formed in the jacket tube by drilling, where the axial holes 3 are arranged in an isoazimuth mode (with an azimuth angle of) 60, each of the axial holes has a diameter of 2.4 mm, and a ratio of a minimum distance between an internal surface of each of the axial holes and an internal surface 17 of the jacket tube to the diameter of the axial hole is 0.13. The drilled jacket tube is placed into an acid liquid for corroding, and a ratio of a minimum distance between an internal surface of each of corroded axial holes 3 and the internal surface 17 of the jacket tube to the diameter of the axial hole is 0.06. Then, each of the axial holes is inserted with a capillary tube 10 with an outer diameter of 1.1 mm and a wall thickness of 0.12 mm. Then, an optical fiber preform 1 with a nested structure is prepared.

    Fabrication of Hollow-Core Micro-Structured Optical Fiber

    [0060] The optical fiber preform 1 with the nested structure is placed into a hot-drawing furnace for drawing, at a furnace temperature of 1770 C., a hollow-core portion in the middle of the preform maintains a pressure value equal to the atmospheric pressure, a gas of equal pressure is fed into the six axial holes 3 at a pressure of 3.7 KPa, and a gas of equal pressure is fed into the six nested capillary tubes at a pressure of 4.6 KPa. The pressure difference between the inside and outside of the axial holes as well as the pressure difference between the inside and outside of the nested capillary tubes result in formation of anti-resonant rings with a nested structure, and finally a hollow-core micro-structured optical fiber 4 with a nested structure as shown in FIG. 6 is formed. An optical fiber cladding 5 has an outer diameter of 153 m, an optical fiber hollow-core fiber core has a diameter of 33.2 m, a first layer of anti-resonant rings 11 has a minimum wall thickness of 217 nm, and a second layer of anti-resonant rings 12 has a minimum wall thickness of 265 nm. The attenuation of the optical fiber at 1550 nm is 0.78 dB/km.

    Embodiment IV

    Fabrication of Optical Fiber Preform

    [0061] As shown in FIG. 7, a solid-core rod made from a material of pure silicon dioxide is selected, which has an outer diameter of 63 mm and a length of 1000 mm. Six small circular holes are formed in the solid-core rod as axial holes 3 by drilling, where the axial holes 3 are arranged in an isoazimuth mode (with an azimuth angle of) 60, and each of the axial holes has a diameter of 7.4 mm; and then a large circular hole 18 is drilled in the center of the solid-core rod as a center hole of the jacket tube, where a ratio of a minimum distance between an internal surface of each of the axial holes 3 and an internal surface of a center hole of the jacket tube (large circular hole 18) to the diameter of the axial hole is 0.16. The drilled jacket tube is placed into an acid liquid for corroding, and a ratio of a minimum distance between an internal surface of each of corroded axial holes and the internal surface of the center hole of the jacket tube to the diameter of the axial hole is 0.07. Then, each of the axial holes is inserted with a quartz sheet 13 with a wall thickness of 0.19 mm, whose perpendicular bisector passes through a circle center of the solid-core rod. Then, an optical fiber preform 1 with a connecting sheet structure is prepared.

    Fabrication of Hollow-Core Micro-Structured Optical Fiber

    [0062] The optical fiber preform 1 with the connecting sheet structure is placed into a hot-drawing furnace for drawing at a furnace temperature of 1735 C., a hollow-core portion in the middle of the preform maintains a pressure value equal to the atmospheric pressure, and a gas of equal pressure is fed into the six axial holes at a pressure of 2.6 KPa. The pressure difference between the inside and outside of the axial holes leads to the expansion of the axial holes after drawing, which results in formation of anti-resonant rings 14, the quartz sheets 13 inserted into the axial holes 3 form anti-resonant sheets 15, all of which constitutes a second anti-resonant layer, and finally a hollow-core micro-structured optical fiber 4 as shown in FIG. 8 is formed. An optical fiber cladding 5 has an outer diameter of 201 m, an optical fiber hollow-core fiber core 7 has a diameter of 53.2 m, each of the anti-resonant rings 14 has a minimum wall thickness of 616 nm, and each of the anti-resonant sheets 15 has a minimum wall thickness of 543 nm. The attenuation of the optical fiber at 1550 nm is 1.54 dB/km.

    [0063] Those skilled in the art will understand that the above description only involves embodiments of the disclosure, but is not intended to limit the invention. Any modification, substitution and improvement within the spirit and the principle of the disclosure shall fall into the protection scope of the disclosure.