METHOD FOR PRODUCING A PLANAR LIGHT CIRCUIT AND PLANAR LIGHT CIRCUIT
20250327974 ยท 2025-10-23
Assignee
Inventors
Cpc classification
International classification
Abstract
A method for producing a planar light circuit is specified. The method comprises: providing a substrate free of light producing regions, depositing a waveguide layer, applying a photostructurable mask on the waveguide layer, photostructuring of the photostructurable mask such that the photostructurable mask is removed in regions, etching of the waveguide layer in the regions such that channels are produced in the waveguide layer, wherein the channels confine waveguides, removal of the photostructurable mask layer, and singulating into a planar light circuit. Furthermore, a planar light circuit is specified.
Claims
1. A method for producing a planar light circuit comprising: providing a substrate free of light producing regions, depositing a waveguide layer, applying a photostructurable mask on the waveguide layer, photostructuring of the photostructurable mask such that the photostructurable mask is removed in regions, etching of the waveguide layer in the regions such that channels are produced in the waveguide layer, wherein the channels confine waveguides and wherein a majority of the waveguide layer remains on the substrate, removal of the photostructurable mask, and singulating into a planar light circuit.
2. The method for producing a planar light circuit according to claim 1, wherein the waveguide layer comprises a material selected from the following group: SiN.sub.x, SiO.sub.xN.sub.y, GaN, HfO.sub.2, LiNbO.sub.3, Ta.sub.2O.sub.5, Nb.sub.2O.sub.5, HfO.sub.2, TiO.sub.2, Si and mixtures thereof.
3. The method for producing a planar light circuit according to claim 1, wherein an adhesion layer is deposited on the waveguide layer before applying the photostructurable mask.
4. The method for producing a planar light circuit according to claim 1, wherein an adhesion promoter is applied on the waveguide layer before applying the photostructurable mask.
5. The method for producing a planar light circuit according to claim 1, wherein the waveguide layer is deposited by plasma-enhanced chemical vapor deposition.
6. The method for producing a planar light circuit according to claim 5, wherein a low frequency plasma source is used in the plasma-enhanced chemical vapor deposition.
7. The method for producing a planar light circuit according to claim 1, wherein the waveguide layer is etched by inductively coupled plasma etching.
8. The method for producing a planar light circuit according to claim 7, wherein a reaction chamber for the inductively coupled plasma etching is cleaned before etching the waveguide layer.
9. The method for producing a planar light circuit according to claim 1, wherein a cladding is applied on the waveguide layer after removal of the photostructurable mask.
10. A planar light circuit comprising: a substrate free of light producing regions, and a waveguide layer on the substrate, wherein the waveguide layer comprises channels confining a waveguide and the waveguide layer covers a majority of the substrate.
11. The planar light circuit according to claim 10, wherein the waveguide is a multi-mode waveguide.
12. The planar light circuit according to claim 10, wherein the substrate comprises or consists of a transparent or opaque inorganic material selected from the group consisting of: fused silica, sapphire, YAG, MgF.sub.2, AlN, various glasses, single crystal semiconductor based materials.
13. The planar light circuit according to claim 10, wherein the substrate is opaque, the substrate comprises an interlayer, and the interlayer is transparent.
14. The planar light circuit according to claim 10, wherein an adhesion layer is arranged on the waveguide layer.
15. The planar light circuit according to claim 10, wherein a cladding is arranged on the waveguide layer and a material of the cladding has a lower refractive index than a material of the waveguide layer.
16. The planar light circuit according to claim 15, wherein the cladding comprises a material selected from the following group: SiO.sub.2, Al.sub.2O.sub.3, HfO.sub.2, oxide glass.
17. The planar light circuit according to claim 10, wherein the waveguide layer has a thickness of at least 500 nanometers.
18. The planar light circuit according to claim 10, wherein the waveguide comprises, seen in top view, at least two branches merging together into a single branch in at least one combining region.
Description
BRIEF DESCRIPTION OF THE DRAWINGS
In the figures:
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DETAILED DESCRIPTION
[0081] In the exemplary embodiments and figures, similar or similarly acting constituent parts are provided with the same reference symbols. The elements illustrated in the figures and their size relationships among one another should not be regarded as true to scale. Rather, individual elements may be represented with an exaggerated size for the sake of better representability and/or for the sake of better understanding.
[0082] As shown in
[0083] A waveguide layer 4 is deposited on the substrate 1 as shown in
TABLE-US-00001 TABLE 1 Parameters for PECVD deposition of Si-poor SiN.sub.x. Parameter Value Table Temperature 300 C. Chamber Pressure 650 mTorr N.sub.2 490 sccm NH.sub.3 40 sccm 5% SiH.sub.4 in Ar 160 sccm Low frequency electrode impedance 882 Ohms Low frequency power 20 W Low frequency period 7 s Low frequency pulsed? yes High frequency power 20 W High frequency period 13 s High frequency pulsed? No Estimated deposition rate 13.703 nm/min
[0084] The waveguide layer 4 presently has a thickness of about 3 micrometer. Table 2 shows extinction coefficients for the waveguide layer 4 depending on the wavelength. The extinction coefficient here and in the following is to be understood as the parameter b in the equation I(x)=I.sub.0*exp(b*x) where I is the intensity depending on a distance x along a waveguide.
TABLE-US-00002 TABLE 2 Extinction coefficients of a waveguide layer 4 with Si-poor SiN.sub.x and a thickness of about 3 micrometer. Wavelength (nm) Extinction coefficient (1/mm) 405 (purple) 0.521 450 (blue) 0.105 532 (green) 0.119 650 (red) 0.030
[0085] After the deposition of the waveguide layer 4, an adhesion layer 5 is deposited on the waveguide layer 4, as shown in
TABLE-US-00003 TABLE 3 Parameters for PECVD deposition of an adhesion layer 4 comprising SiO.sub.2. Parameter Value Table Temperature 300 C. Chamber Pressure 1000 mTorr N.sub.2O 710 sccm 5% SiH.sub.4 in Ar 150 sccm High frequency power 20 W Approximate deposition rate 60 nm/min
[0086] In a further step, as shown in
TABLE-US-00004 TABLE 4 HMDS spin coating parameters. Velocity Ramp Time Step (rpm) (rpm/s) (s) 1 500 200 5 2 5000 750 30 3 0 500 0
[0087] After applying the adhesion promoter 6, the waveguide layer 4 is heated for 3 min to 110 C. Then, a photostructurable mask 7 is applied on the adhesion promoter 6 by spin coating using the parameters shown in table 5.
TABLE-US-00005 TABLE 5 Photostructurable mask 7 spin coating parameters. Step Velocity (rpm) Ramp (rpm/s) Time (s) 1 500 200 5 2 6000 750 60 3 0 500 0
[0088] The photostructurable mask 7 is heated for 3 min to 110 C. Presently, the photostructurable mask 7 has a thickness of about 5 micrometer.
[0089] Before photostructuring, the photostructurable mask 7 is allowed to rehydrate. For this the photostructurable mask 7 was left in air for about 30 min.
[0090] As shown in
TABLE-US-00006 TABLE 6 Parameters for exposure to electromagnetic radiation. Parameter Value Exposure dose 6.1 s @ 24.9 mW/cm.sup.2 Wavelength 365 nm Alignment Gap 6 m Expose Type Hard Hard contact wait time 10 s WEC Type Contact WEC Offset Off
[0091] WEC is the abbreviation for wedge error compensation. The WEC type contact means that a structuring mask is in direct contact with the photostructurable mask 7 during exposure to electromagnetic radiation. The exposure type hard brings a structuring mask in direct contact with the photostructurable mask 7. The hard contact wait time represents a delay during which the structuring mask will be in contact with the photostructurable mask 7 before exposure to the electromagnetic radiation.
[0092] After exposure to electromagnetic radiation, the photostructurable mask 7 is developed using a developer. In this way, the photostructurable mask 7 is removed in the regions. Presently, a potassium-based buffered developer mixed with water is used as developer. The ratio of water to developer is 1:4. A development time was about 90 s.
[0093] In a next step of the method for producing a planar light circuit, the waveguide layer 4 is etched in the regions which are free of the photostructurable mask 7 (
[0094] Before the etching of the waveguide layer 4, a reaction chamber for the inductively coupled plasma etching is cleaned. To clean the reaction chamber the parameters described in table 7 are set. A clean time is for example about 10 min.
TABLE-US-00007 TABLE 7 Parameters for reaction chamber cleaning. Parameter Value ICP Power 1500 W Electrode 150 W Chuck Temperature Setpoint 15 C. Backing helium pressure 0 Torr Chamber Pressure 20 mTorr O.sub.2 40 sccm SF.sub.6 10 sccm
[0095] After cleaning of the reaction chamber, the waveguide layer 4 is etched using the parameters listed in table 8. An etching time is about 12.5 minutes.
TABLE-US-00008 TABLE 8 Parameters for etching the waveguide layer 4. Parameter Value ICP Power 1250 W Electrode 15 W Chuck Temperature Setpoint 15 C. Backing helium pressure 5 Torr Chamber Pressure 6 mTorr SF.sub.6 6 sccm CHF.sub.3 26 sccm
[0096] During etching of the waveguide layer 4, the adhesive layer 4 is also removed in the regions free of the photostructurable mask 7.
[0097] As shown in
[0098] As shown in
TABLE-US-00009 TABLE 9 Parameters for applying the cladding 11 by PECVD. Parameter Value Table Temperature 400 C. Chamber Pressure 1500 mTorr N.sub.2O 480 sccm CF.sub.4 800 sccm 5% SiH.sub.4 in Ar 160 sccm High frequency power 20 W High frequency pulsed No Deposition time 20 min
[0099] The cladding 11 covers the waveguide layer 4. In particular, the cladding 11 is in direct physical contact with the adhesion layer 5. The channels 8 are partially filled with the cladding 8. Side faces 21 of the channels 8 and a bottom face 20 of the channels 8 formed by the substrate 1 are covered with the cladding 11.
[0100] To produce a planar light circuit 10, the wafer is singulated. For singulation, cleaving locations 12 are scored into the wafer. The planar light circuit 10 is obtained by cleaving at the cleaving locations 12, 13, 14 using pliers. An order of cleaving is shown in
[0101] Additionally, the wafer is in particular diced, lapped, and polished. However, care must be taken to minimize chipping of facets of the waveguide.
[0102] The planar light circuits 10 shown in
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[0106] Here, n.sub.Si is the refractive index of a waveguide layer 4 consisting of Si, n.sub.Si3N4 is the refractive index of a waveguide layer 4 consisting of stoichiometric SiN.sub.x, that is Si.sub.3N.sub.4, and n.sub.waveguide layer is the refractive index of waveguide layer 4 consisting of non-stoichiometric SiN.sub.x. Presently, n.sub.Si=3.610 and n.sub.Si3N3=2.018.
[0107] Using the plot shown in
[0108] The SEM image shown in
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[0111] In
[0112] The structure of the planar light circuit 10 shown in
[0113] The planar light circuit 10 shown as cross-section in
[0114] The planar light circuit 10 shown in
[0115] Channels 8 run through the waveguide layer 4 such that a waveguide 9 is formed in the waveguide layer 4. Two channels 8 confine the waveguide 9. Thus, seen in cross-section, the channels 8 in the waveguide layer 4 and the waveguide 9 comprise a rectangular shape.
[0116] A cladding 11 is arranged on the waveguide layer 4. The cladding 11 partially fills the channels 8 in the waveguide layer 4. Presently, the cladding 11 comprises or consists of fluorine doped SiO.sub.2. Seen in the cross-section, the waveguide 9 surrounded by the cladding 11 has approximately the shape of a trapezoid with two rounded corners. This shape may be compared to the shape of a toast.
[0117] A bottom face and side faces of the channels 8 are covered by the cladding 11. A thickness of the cladding 11 is smaller at the bottom face 20 of the channels 8 than a top face 22 of the waveguide 9 facing away from the substrate 1. The thickness of the cladding 11 on the side faces 21 of the channels 8 decreases in a direction towards the bottom face 20 of the channels 8. In other words, the cladding 11 comprises an undercut in the region of the channels 8. A distance of the cladding 11 outside of the channels 8 in the waveguide layer 4 is smaller than inside the channels 8.
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[0119] At the bottom face 20 of the channels 8 the cladding 11 comprises a lower thickness than on the top face 22 of the waveguide 9. Presently, the thickness of the cladding 11 at the bottom face 20 is about 1.08 micrometers and the top face 22 of the waveguide 9 about 2.45 micrometers. The thickness of the cladding 11 on the side face 21 is about 844 nanometers in the region of the bottom face 20 of the channels 8. The thickness on the side face 21 increases to reach about 1.09 micrometers in the region of the top face 22 of the waveguide 9. The cladding 11 surrounding the waveguide 9 has a maximum width of about 5.48 micrometers in a region above the top face 22 of the waveguide 9. A distance between the cladding 11 on the waveguide 9 and the cladding 11 on the surrounding waveguide layer 4 is about 550 nanometers at the narrowest point.
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[0121] The branches 15 comprise a curved shape in top view. For example, the branches 15 comprise a Bezir, a sigmoidal shape or the shape of a tangent function. A course of the branches 15, seen in top view, comprises at least one inflection point. A starting point of the two branches 15 is equally distanced to a starting point of the middle branch 16.
[0122] An efficiency of the planar light circuit 10 described herein was measured using both lens coupled laser diodes and butt-coupled laser diodes. The results are shown in table 10. During measurements a high NA microscope objective (NA=0.85) was used.
TABLE-US-00010 TABLE 10 Efficiencies of a planar light circuit 10. efficiency Wavelength Fast left middle right (nm) axis Polarization branch branch branch 450 Horizontal Vertical 0.347 0.371 0.341 450 Vertical Horizontal 0.489 0.485 0.493 532 Round Vertical 0.424 0.460 0.368 532 Round Horizontal 0.350 0.377 0.344 650 Horizontal Vertical 0.342 0.414 0.384 650 Vertical Horizontal 0.455 0.483 0.558 450 Vertical Horizontal 0.302 0.424 0.517 450 Vertical Horizontal 0.499 0.485 0.444 450 Vertical Horizontal 0.483 0.424 0.405
[0123] For 450 nanometer and 650 nanometer laser diodes, the fast axis is perpendicular to the polarization. In case of the 532 nanometer laser diode which is believed to be second harmonic converted, the beam is round, so there is no distinction of beam asymmetry with respect to polarization. The waveguides 9 in particular are taller than wide and have more cladding 11 in the vertical direction. The vertical direction is perpendicular to a main extension plane of the planar light circuit. This suggests that aligning the fast axis with the vertical direction should yield higher efficiency due to greater availability of modes and better confinement. This agrees with the experimental results for the 450 nanometer and 650 nanometer laser diodes. The 532 nanometer laser diode does not have this spatial asymmetry. In this case, the vertical polarized light seems to have increased efficiency.
[0124] Using a green edge emitting laser diode, light was coupled into the middle branch 16 of a planar light circuit 10 and an efficiency of 0.45 was achieved.
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[0126] In the case of in-line or imaging spectroscopy using the radiation emitting device 23, the laser diodes 24 are sequentially (not in any particular order) switch on such that the desired wavelength appears at a source port of the spectroscopy system and the detector detecting the currently applied excitation wavelength. Furthermore, more sophisticated schemes can be employed whereby all laser diodes 24 can be pulsed or modulated at the same time. For example, an orthogonal pulse sequences such as a Hadamard orthogonal set is used for modulation. Alternatively, each laser diode 24 is modulated at a different frequency which can be independently detected via lock-in or down-conversion schemes.
[0127] The features and exemplary embodiments described in connection with the figures can be combined with each other according to further exemplary embodiments, even if not all combinations are explicitly described. Furthermore, the exemplary embodiments described in connection with the figures may have alternative or additional features as described in the general part.
[0128] The invention is not restricted to the exemplary embodiments by the description on the basis of said exemplary embodiments. Rather, the invention encompasses any new feature and also any combination of features, which in particular comprises any combination of features in the patent claims and any combination of features in the exemplary embodiments, even if this feature or this combination itself is not explicitly specified in the patent claims or exemplary embodiments.