NOZZLE FOR SPRAYING LIQUID IN THE FORM OF MIST
20230069992 · 2023-03-09
Assignee
Inventors
Cpc classification
B05B1/3478
PERFORMING OPERATIONS; TRANSPORTING
A61M11/00
HUMAN NECESSITIES
B05B1/3436
PERFORMING OPERATIONS; TRANSPORTING
International classification
Abstract
The invention relates to a fluid spray nozzle which is intended to be mounted on a distribution receptacle, the nozzle comprising at least one fluid inlet capillary extending longitudinally along an axis, a supply means to receive the fluid from the at least one inlet capillary in order to supply it to a pillar comprising at least two pipes, the pipes extending longitudinally along the axis A1 and being radially offset relative to the axis, at least two turbulence channels in fluid connection with the at least two pipes, a turbulence chamber for receiving the fluid coming tangentially from the at least two turbulence channels in order to supply at least one spray opening having axial symmetry and a constant cross-section s, the chamber having a cross-section decreasing towards the opening and having a maximum cross-section S and a maximum diameter, the ratio of the cross-section s of the spray opening to the maximum cross-section S of the turbulence chamber is 1%≤s/S≤20%.
Claims
1. A nozzle for spraying a fluid, the nozzle being designed to be mounted on a dispensing container, said nozzle comprising: at least one fluid inlet capillary extending longitudinally along an axis A1, a turbulence chamber for receiving the fluid to be sprayed, said turbulence chamber has a maximum cross-section S and a maximum diameter-D, at least two conduits that extend longitudinally along said axis and being radially offset from said axis, said conduits in fluid connection with the inlet capillary, at least two turbulence channels, in fluid connection with said at least two conduits, and connecting said at least two conduits with the turbulence chamber, said at least two conduits thus connecting the inlet capillary to the at least two turbulence channels, a spray orifice supplied by the turbulence chamber, the spray orifice has axial symmetry and a constant cross-section s, said turbulence chamber has along the axis, a cross-section that decreases towards said spray orifice, wherein the ratio of the cross-sectional area s of the spray orifice to the maximum cross-sectional area S of the turbulence field is such that 1%≤.sup.S/S≤20%, the spray nozzle is operated by means of an actuator independent of the nozzle, and the inlet capillary has a cross-sectional area that allows a fluid shear rate greater than 5000 s.sup.−1.
2. The spray nozzle (1) according to claim 1, wherein 1%≤.sup.S/S≤10%.
3. The spray nozzle according to claim 1, wherein the spray orifice has a cylindrical shape with a diameter d and a height h such that: 40% d≤h≤150% d.
4. The spray nozzle according to claim 1, wherein the at least two turbulence channels each have a right-angled quadrilateral cross-section, said cross-section being between 0.001 and 0.06 mm.sup.2.
5. The spray nozzle according to claim 4, wherein the quadrilateral is a square.
6. The spray nozzle according to claim 1, wherein the supply means comprises either a hollow section chamber of generally cylindrical shape, the base of which extends along a plane perpendicular to the axis, or several supply channels that extend radially on a plane perpendicular to the axis, in order to supply said at least two conduits.
7. The spray nozzle according to claim 1, wherein the turbulence chamber has a truncated cone shape whose angle α between the axis and the generatrix is such that 25°≤α≤55°.
8. The spray nozzle according to claim 1, wherein the at least two conduits are provided in a pillar, said pillar comprising an enveloping cylinder and having an inner surface Sc, said enveloping cylinder comprising a coaxial spacer whose outer surface is polygonal such that the edges of the spacer are in contact with the inner surface of the enveloping cylinder thereby forming at least three conduits in the pillar.
9. The spray nozzle according to claim 1, wherein the at least one inlet capillary comprises at least two portions each with a constant diameter along its length, each portion with a diameter D equal to or greater than the diameter of at least one downstream portion and each portion with a diameter equal to or less than the diameter of at least one upstream portion.
10. A medical device suitable for dispensing a fluid and comprising a nozzle according to claim 1.
11. A method of dispensing a rheofluidifying viscous fluid by spraying, wherein the method comprises using the nozzle according to claim 1.
12. The method according to claim 11, wherein the distribution is carried out in the form of a mist with homogeneous drops, at least 90% of the drops of the mist having a diameter of less than 100 μm.
13. The method according to claim 12, wherein the distribution is carried out in the form of a mist with homogeneous drops whose median diameter is between 10 μm and 50 μm.
14. The method according to claim 12, wherein the distribution is carried out in the form of a mist with homogeneous drops of which less than 12% of the drops have a diameter of less than 10 μm.
15. The method according to claim 11, wherein the distribution is carried out in the form of a homogeneous mist, the dispersion of the drops of which, characterized by the ratio of the deviation of Dv10 and Dv90 from the median, is less than 2.
16. The spray nozzle according to claim 7, wherein the turbulence chamber has a truncated cone shape whose angle α between the axis and the generatrix is such that 30°≤α≤45°.
Description
BRIEF DESCRIPTION OF THE FIGURES
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DETAILED DESCRIPTION
[0060] The following description will be better understood from the drawings shown above. For the purpose of illustration, the nozzle is shown in preferred embodiments. It should be understood, however, that this application is not limited to the specific arrangements, structures, characteristics, embodiments, and appearances indicated. The drawings are not drawn to scale and are not intended to limit the scope of the claims to the embodiments shown therein.
[0061] In general, the invention relates to a spray nozzle 1 for fluid, more specifically for a viscous, rheofluidifying fluid, to be mounted upon a dispensing container.
[0062] The fluid considered may not be a rheofluidizing fluid if its viscosity is of the order of 20 mPa.Math.s, preferably less than 20 mPa.Math.s, i.e., if the viscosity of the fluid is low.
[0063] Therefore, nozzle 1 according to the invention is designed to be attached to a fluid reservoir, specifically, a rheofluidifying viscous fluid.
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[0065] In
[0066] In
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[0068] Length L and the cross-sectional area D of inlet capillary 7 are variables that may be acted upon in the context of the invention in order to modulate the shear rate of the fluid passing through inlet capillary 7. In the particular case where cross-section D of inlet capillary 7 is a disk (the capillary being cylindrical), then the cross-section becomes diameter D, such that S=pi*(D/2).sup.2, where S denotes the cross-section.
[0069] As is well known, the shear rate increases as the cross-sectional area S decreases. At a given flow rate, increasing length L increases the time the fluid is sheared at a given shear rate. This makes it possible to ensure that length L is greater than the flow establishment length and that the viscosity to be achieved at this shear rate is attained. However, the objective is to also reduce the inlet pressure of nozzle 1 and thus to reduce the pressure losses within it. Pressure losses increase as the cross-sections decrease and the lengths increase. It is therefore a question of finding a functional balance, which is achieved by this invention.
[0070] In the embodiment shown in
[0071] Those skilled in the art know that reducing cross-section D of inlet capillary 7 increases the shear rate of the fluid to be propelled, since the shear rate is equal to the fluid velocity divided by the air gap. This leads to a decrease in the viscosity of said fluid within inlet capillary 7 and in nozzle 1 in general.
[0072] Since the viscosity is lower, it is possible to increase the flow rate and thus achieve higher flow velocities while remaining at relatively low pressures. Indeed, at constant viscosity, if we increase the flow rate, we increase the pressure, and this is all the more important as the viscosity is high. In other words, increasing the shear rate reduces the viscosity and thus allows higher flow velocities to be achieved without increasing (very significantly) the pressure. Increasing the speed makes it possible to reach the critical speed which permits generation of an atomization of the fluid and thus create a spray (or mist).
[0073] In other words, by significantly shearing the fluid as soon as it enters nozzle 1 and thus as soon as it enters inlet capillary 7, a low viscosity is achieved along the entire fluid path. This makes it possible to achieve a high flow rate and velocity of the fluid, allowing the atomization of the fluid at the nozzle outlet, i.e., the formation of a spray (mist), without very significantly increasing the pressure at nozzle inlet 1. In other words, it makes it possible to produce a spray (mist) from a rheofluidizing viscous fluid at low pressure, thus facilitating the design of a medical device and limiting risks for its user.
[0074] The small cross-sections make high velocity possible, however a very small cross-section induces a great drop in pressure, and thus requires that very high pressure be applied at the inlet of nozzle 1 to attain the spray.
[0075] In the embodiment shown in
[0078] In other words, the closer a portion 71, 72, 73, 74 of inlet capillary 7 is located to turbulence chamber 3, the smaller its cross-sectional area D is. The different positions 71, 72, 73, 74 may be separated from each other by trays. These plates make a better alignment between the different portions 71, 72, 73, 74 possible.
[0079] The three variants 6a, 6b and 6c in
[0080] Variant 6b, has three portions 71, 72 and 73, each with a constant diameter D along its entire length. Diameter D of the upstream portion 73 is larger than that of central portion 72, itself larger than that of downstream portion 71. This is the embodiment shown in
[0081] Variant 6c, on the other hand, has four portions 71, 72, 73 and 74, each with a constant diameter D. Diameters D are decreasing towards supply means 6 and the two central portions 72 and 73 have similar surface sections. This increases the length of the central portion 72, 73 of the intermediate section. The advantage of this design is to increase length L of inlet capillary 7 when there is only one capillary diameter (flow establishment length at this shear). It is also preferable to increase the length on the intermediate section rather than on the smallest section in order to not increase the pressure losses too much.
[0082] In the three embodiments shown in
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[0084] Generally speaking, the fluid inlet capillary(ies) 7 have a diameter D to generate a fluid shear rate greater than 5000 s.sup.−1. In the case of the embodiments with an inlet capillary 7 with variable portions 71, 72, 73, and 74, it is the upstream portion 74 that makes it possible to attain a shear rate greater than 5000 s.sup.−1. The following sections 71, 72, 73 allow even higher shear rates to be attained.
[0085] The section along axis 2a of
[0086] More generally, inlet capillary 7 is connected to the truncated cone-shaped turbulence chamber 3 by means of conduits 512. These conduits 512 may be obtained in various ways. One way to obtain these conduits 512 is to stack machined parts, thus forming a pillar 5 in which said conduits 512 are provided. However, this method is long and tedious, and industrially unattractive. Alternatively, in the embodiment shown in
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[0090] The advantage of height H1 compared to height H2 is that the shorter lengths induce a lower pressure drop and therefore a lower pressure at nozzle inlet 1. The advantage of height H2 over height H1 is that the length over which the fluid is sheared is greater and therefore induces better shear. Here again, a compromise must be made, which is the subject-matter of this invention.
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[0092] The connection between conduits 512 of pillar 5 and inlet capillary 7 may be provided by a supply means 6 typically taking the form of a hollow tray of a generally flat cylindrical shape. This is illustrated in
[0093] The section along axis 2c of
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[0095] A circular ring, visible in
[0099] As with inlet capillary 7, reducing the cross-section of turbulence channels 41, 42 and 43 increases the shear of the fluid and thus its speed. This increase in speed allows for better turbulence generation and therefore better spraying.
[0100] The length of turbulence channels 41, 42 and 43, i.e., the distance to be covered by the fluid to be sprayed between the circular ring and the tangential inlet of turbulence chamber 3 is ideally between 0.2 and 0.71 mm.
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[0102] Preferably, angle α between axis A1 and the generatrix of the truncated cone-shaped chamber is such that 25°≤α≤55°, preferably: 30°≤α≤45°.
[0103] The height L3 of the truncated cone-shaped chamber is ideally between 0.4 and 0.7 mm.
[0104] Finally, in
[0105] The height h of the spray orifice 2 is ideally between 0.1 mm and 0.15 mm.
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[0108] According to some embodiments, nozzle 1 according to the invention may be considered entirely as a consumable and is therefore made of disposable and/or very short-lived materials. Nozzle 1 according to this invention is thus adaptable to many applications in cosmetics, food processing, and is therefore not limited to the medical field.
[0109] Nozzle 1 is used in combination with an independent actuator. Spray nozzle 1 is thus actuated by means of an actuator that is independent of the nozzle. “Nozzle actuation” means “circulation of the fluid to be dispensed through nozzle 1”.
[0110] This independent actuator can take many different forms, but in all cases it includes a means of circulating the fluid to be sprayed. The actuator may be manual or automated using a mechanical system (pump, syringe pump, spring) or electromechanical (using a motor). The choice of the actuator and the means of circulation of the fluid to be sprayed depends on the desired properties of the spray: size of the cone, flow rate, duration of the spray, for example.
[0111] From the foregoing, it is apparent that nozzle 1 according to the invention makes a high shear of a rheofluidifying viscous fluid possible so as to be able to spray this type of fluid effectively and safely. The diameter of the turbulence channels 41, 42, and 43 is small enough to spray a low flow rate mist, but large enough not to induce excessive pressure drops so as to minimize inlet pressure of nozzle 1.
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[0113] Nozzle 1 according to the invention thus allows the implementation of a process for dispensing a rheofluidifying viscous fluid by spraying. More specifically, this distribution is performed in the form of a mist with homogeneous drops whose characterization by Laser Diffraction (Spraytec/MAL10332887/Malvern/UK) makes it possible to establish the following characteristics: [0114] at least 90% of the drops in the mist have a diameter of less than 100 μm, preferably less than 90 μm, more preferably less than 80 μm, even more preferably 70 μm. In a last preferred mode, less than 60 μm, in other words, that the mist has a Dv90 less than 100 μm, [0115] the median diameter of the mist drops, also referred to as the Dv50 of the mist is between 10 and 50 μm, preferably between 10 and 45 μm, more preferably between 15 and 40 μm, [0116] 12% of the drops have a diameter of less than 10 μm, preferably less than 10 μm, [0117] a distribution of the different drop sizes of a mist concentrated around its median value (Dv50), such that the ratio between the difference between Dv90 and Dv10, and Dv50 is less than 2, preferably less than 1.8, more preferably less than 1.6. In other words, the “SPAN” distribution is less than 2, preferably less than 1.8, more preferably less than 1.6.
REFERENCED NUMBERS
[0118] 1: Spray nozzle [0119] 2: Spray orifice [0120] 3: Turbulence chamber [0121] 4, 41, 42, 43: Turbulence channels [0122] 5: Pillar 51, 511, 512, 513: conduits [0123] 52: enveloping cylinder [0124] 53: Spacer [0125] 6: Supply means, [0126] 61,62,63: supply channels [0127] 7: inlet capillary(ies) [0128] 8: Support [0129] 81: First release of the support capable of receiving the container of liquid to be dispensed, [0130] 81: second release of the support capable of receiving the grooves forming inlet capillaries, [0131] 71,72, 73, 74: portions of constant section of inlet capillary 7 [0132] A1: axis of the spray orifice [0133] H1, H2: height of the pillar [0134] D7: diameter of the fluid inlet capillary [0135] h7: radial distance between the axis of the spray orifice and the axis of the fluid inlet capillary. [0136] L: length of the fluid inlet capillary [0137] d: diameter of the spray orifice [0138] h: height of the spray orifice [0139] L3: Height of the vortex chamber (according to the axis A1) [0140] α: angle between the axis A1 and the generatrix of the turbulence chamber.