STATIC MIXER
20260042070 ยท 2026-02-12
Assignee
Inventors
Cpc classification
B01J12/00
PERFORMING OPERATIONS; TRANSPORTING
B01F35/514
PERFORMING OPERATIONS; TRANSPORTING
B01J19/30
PERFORMING OPERATIONS; TRANSPORTING
B01F25/431
PERFORMING OPERATIONS; TRANSPORTING
B01J19/2405
PERFORMING OPERATIONS; TRANSPORTING
B01F2101/2204
PERFORMING OPERATIONS; TRANSPORTING
B01F2215/0431
PERFORMING OPERATIONS; TRANSPORTING
B01F2025/916
PERFORMING OPERATIONS; TRANSPORTING
B01F35/513
PERFORMING OPERATIONS; TRANSPORTING
International classification
B01F25/431
PERFORMING OPERATIONS; TRANSPORTING
B01F35/513
PERFORMING OPERATIONS; TRANSPORTING
B01J12/00
PERFORMING OPERATIONS; TRANSPORTING
B01J19/24
PERFORMING OPERATIONS; TRANSPORTING
B01J19/30
PERFORMING OPERATIONS; TRANSPORTING
Abstract
The present disclosure provides a static mixer for mixing two or more fluids together. The static mixer comprises a tubular body defining a mixing chamber in which spheroidal bodies are positioned. The spheroidal bodies are arranged sequentially within the mixing chamber, and their size and shape is selected so that they maintain a staggered formation. The tubular body can receive a flow of the two or more fluids at one end and convey them towards an opposite end where a mixed product can be provided. The arrangement of the spheroidal bodies can induce turbulence in the flow of the two or more fluids to mix them as they meander around the spheroidal bodies. The present disclosure further provides a method for mixing two or more fluids by the static mixer.
Claims
1. A static mixer for mixing two or more fluids to provide a fluid product, the static mixer comprising: a tubular mixer body having a first end and a second end, the tubular mixer body defining a mixing chamber having a chamber surface defining an inner diameter, a first end opening, and a second end opening opposite the first end opening, the mixing chamber being configured to receive a flow of the two or more fluids into the first end opening of the tubular mixer body and convey the flow of the two or more fluids toward the second end opening; and a mixing component comprising a plurality of spheroidal bodies located in the mixing chamber of the tubular mixer body, each of the plurality of spheroidal bodies having an outer diameter more than 50% of the inner diameter of the mixing chamber, wherein each of the plurality of spheroidal bodies is maintained in contact with adjacent spheroidal bodies and with the chamber surface of the mixing chamber, and wherein the plurality of spheroidal bodies is configured to induce turbulence in the flow of the two or more fluids to produce the fluid product when the two or more fluids are conveyed through the mixing chamber.
2. The static mixer of claim 1, wherein the fluid product is a mixture of the two or more fluids.
3. The static mixer of claim 1, wherein the fluid product is a product of a reaction between the two or more fluids.
4. The static mixer of claim 1, wherein the tubular mixer body is made of a transparent material.
5. The static mixer of claim 1, wherein the tubular mixer body is made of a flexible material.
6. The static mixer of claim 1, wherein each spheroidal body of the plurality of spheroidal bodies has a respective shape selected from the group consisting of spheres, polyhedrons, ellipsoids, and ovoids.
7. The static mixer of claim 1, wherein each of the plurality of spheroidal bodies is made of a material selected from the group consisting of glass, quartz, polymer, plastic, metal, rubber, and ceramic.
8. The static mixer of claim 1, wherein the plurality of spheroidal bodies includes a first set of spheroidal bodies having a first average outer diameter and a second set of spheroidal bodies having a second average outer diameter, wherein the first average outer diameter is different from the second average outer diameter.
9. The static mixer of claim 1, wherein: the static mixer further comprises: a first stopper positioned in the tubular mixer body adjacent the first end opening and configured to admit the two or more fluids into the mixing chamber; and a second stopper positioned in the tubular mixer body adjacent the second end opening and configured to discharge the fluid mixture out of the mixing chamber; wherein the first stopper and the second stopper are configured to retain the plurality of spheroidal bodies in the mixing chamber of the tubular mixer body.
10. The static mixer of claim 1, wherein the plurality of spheroidal bodies is arranged sequentially along and alternatingly about a central axis of the tubular mixer body by close packing of the plurality of spheroidal bodies in the mixing chamber.
11. The static mixer of claim 1, wherein the tubular mixer body has a first tapered portion at the first end of the tubular mixer body and a second tapered portion at the second end of the tubular mixer body, the first tapered portion and the second tapered portion being configured to contain the plurality of spheroidal bodies in the mixing chamber.
12. The static mixer of claim 1, wherein the mixing chamber has a length of between about 100 mm and about 2000 mm.
13. The static mixer of claim 1, wherein the inner diameter of the mixing chamber is between 1 and 10 mm.
14. The static mixer of claim 1, wherein the outer diameter of each one of the plurality of spheroidal bodies is between about 55% and about 95% of the inner diameter of the mixing chamber.
15. The static mixer of claim 1, wherein the plurality of spheroidal bodies includes from about 10 to about 2000 spheroidal bodies.
16. The static mixer of claim 1, wherein the two or more fluids include nitric oxide and ozone; and the mixing chamber has a length sufficient to ensure that the nitric oxide and ozone mix, by the turbulence, to produce nitrogen dioxide as the fluid product is conveyed toward the second end opening of the tubular mixer body.
17. The static mixer of claim 1, wherein the two or more fluids include nitric oxide and ozone; and the mixing chamber has a length sufficient to ensure that the nitric oxide and ozone mix, by the turbulence, to produce nitrogen trioxide as the fluid product is conveyed toward the second end opening of the tubular mixer body.
18. A method for mixing two or more fluids to produce a fluid product using the static mixer, as defined in claim 1, the method comprising: receiving, by the first end opening at the first end of the tubular mixer body, a flow of the two or more fluids into in the mixing chamber of the tubular mixer body; passing the flow of the two or more fluids through the mixing chamber toward the second end opening at the second end of the tubular mixer body; inducing, by the plurality of spheroidal bodies positioned in the mixing chamber, turbulence in the flow of the two or more fluids to mix the two or more fluids; and providing, at the second end of the tubular mixer body, a flow of the fluid product.
19. The method of claim 18 wherein the two or more fluids comprises ozone (O.sub.3) andnitric oxide (NO) to produce the fluid product nitrogen dioxide (NO.sub.2).
Description
DESCRIPTION OF SPECIFIC EMBODIMENTS OF THE INVENTION
Definitions
[0025] Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs.
[0026] As used herein, the term UV refers to ultraviolet radiation in the region of electromagnetic spectrum including wavelengths from 40 to 4000 (4 to 400 nm).
[0027] As used herein, the term fluid refers to a substance that can flow and conform to the shape of a container. The term encompasses liquids, gases, gels, and combinations thereof.
[0028] As used herein, the term spheroidalrefers to an approximate resemblance to a sphere.
[0029] As used herein, the term adjacent includes approximately proximal to, nearby or beside.
[0030] As used herein, the term inert includes being chemically inert, non-reactive, and/or non-catalytic.
[0031] As used herein, the term about refers to approximately a +/10% variation from a given value. It is to be understood that such a variation is always included in any given value provided herein, whether or not it is specifically referred to.
[0032] The articles a and an are used herein to refer to one or to more than one (i.e., to at least one) of the grammatical object of the article. By way of example, an element means one element or more than one element.
[0033] A first aspect of the present disclosure provides a static mixer for mixing two or more fluids to form a fluid product.
[0034] The present disclosure relates to a static mixer which is simple to make, and which can achieve an efficient low pressure mixing of fluids with a small footprint. The static mixer of the present application permits a short overall length, minimum usage of materials so that weight is minimized and overall manufactured cost is low. In addition, manufacturing consistency can be very high as the spheroidal bodies can self-stagger.
[0035] The static mixer of the present disclosure comprises a tubular mixer body having a first end and a second end, and defining a mixing chamber that has a chamber surface defining an inner diameter, a first end opening, and a second end opening opposite the first end opening. The mixing chamber is configured to receive a flow of two or more fluids into the first end opening and convey the flow toward the second end opening. The static mixer further comprises a mixing component including a plurality of spheroidal bodies located in the mixing chamber Each of the plurality of spheroidal bodies is maintained in contact with adjacent spheroidal bodies and with the chamber surface of the mixing chamber.
[0036] The outer diameter of each spheroidal body of the plurality of spheroidal bodies can be a dimension of the respective spheroidal body along a direction transverse to the tubular mixer body.
[0037] The outer diameter of each spheroidal body can be selected to be greater than 50% of the inner diameter of the mixing chamber to prevent each spheroidal body from aligning with a neighboring spheroidal body in a direction transverse to the tubular mixer body.
[0038] In some embodiments, each spheroidal body of the plurality of spheroidal bodies can have an outer diameter that is between about 55% and about 95% of the inner diameter of the mixing chamber. In some embodiments, each spheroidal body of the plurality of spheroidal bodies can have an outer diameter that is from about 65% to about 75% of the inner diameter of the mixing chamber.
[0039] The plurality of spheroidal bodies is configured to induce turbulence in the flow of the two or more fluids to produce the fluid mixture when the two or more fluids are conveyed through the mixing chamber.
[0040] The spheroidal bodies can force the turbulence and mixing to occur over the entire length of the mixer. As there are no dead spots in the internal volume of the mixer, the turbulence is forced to occur from the start to the end.
[0041] The plurality of spheroidal bodies can define, in the mixing chamber, a peculiar flow path for the flow of the two or more fluids when the flow is received into the first end opening and conveyed toward the second end opening.
[0042] The flow path can separate and join over and over again which can increase mixing efficiency.
[0043] The fluid product can be a mixture and/or a reaction product of the two or more fluids. In some embodiments, the fluid product is a mixture of the two or more fluids. In some embodiments, the fluid product is a product of a reaction between the two or more fluids. In some embodiments, the fluid product is a solution of the two or more fluids.
[0044] The tubular mixer body can be a cylindrical tube. The tubular mixer body can be straight, flexible, or pre-deformed into a fixed shape.
[0045] The tubular mixer body can be made of a material that is transparent, translucent, or opaque. In some embodiments, the tubular mixer body is made of a material that is transparent to UV light. The tubular mixer body can further be made of a material with any rigidity. In some embodiments, the tubular mixer body is made of a material that is flexible.
[0046] The tubular mixer body can further be made of a material that is inert to the two or more fluids and/or the fluid product.
[0047] In some embodiments, the tubular mixer body can be made of a material selected from the group consisting of glasses, quartz, plastics, polymers, metals, rubbers, and ceramics. Metals includes stainless steel, nickel, and chromium-plated metals. Plastics and polymers includes poly(methyl methacrylate), polytetrafluoroethylene, perfluoroalkoxy alkanes (PFAs), polypropylenes, nylons, polyethylenes, polycarbonates, and polyamide-imides. Rubbers includes fluoroelastomers and silicones. Ceramics includes aluminum oxide, zirconium oxide, silicon nitride, and silicon carbide. The tubular mixer body can further be made of a material that is minimally porous, and/or that the two or more fluids and/or the fluid product do not adhere to.
[0048] The chamber surface of the mixing chamber can have a coating. In some embodiments, the coating of the chamber surface is inert to the two or more fluids and/or the fluid product.
[0049] In some embodiments, the fluid product is a product of a reaction between the two or more fluid products that is catalyzed by the coating of the chamber surface. The chamber surface of the mixing chamber can further have any roughness. In some embodiments, the chamber surface and/or the coating is smooth.
[0050] The plurality of spheroidal bodies can be arranged sequentially along and alternatingly about a central axis of the tubular mixer body. The plurality of spheroidal bodies can be arranged to form a staggered or zig-zag pattern in the mixing chamber. In some embodiments, the plurality of spheroidal bodies are arranged by close packing of the plurality of spheroidal bodies in the mixing chamber.
[0051] In some embodiments, the spheroidal bodies arrange themselves automatically into the staggered pattern.
[0052] The outer diameter of each spheroidal body of the plurality of spheroidal bodies can be a dimension of the respective spheroidal body along a direction transverse to the tubular mixer body. The outer diameter of each spheroidal body can be selected to be greater than 50% of the inner diameter of the mixing chamber to prevent each spheroidal body from aligning with a neighboring spheroidal body in a direction transverse to the tubular mixer body.
[0053] Each spheroidal body of the plurality of spheroidal bodies can have a shape selected from the group consisting of spheres, polyhedrons, ellipsoids, and ovoids. In some embodiments, each spheroidal body has a shape selected from the group consisting of octahedra, dodecahedra, and icosahedra. In some embodiments, each spheroidal body has a shape of a truncated polyhedron, a regular polyhedron, a prolate spheroid, or an oblate spheroid. In some embodiments, the spheroidal bodies are not identically shaped. In some embodiments, each spheroidal body has a same shape.
[0054] Each of the plurality of spheroidal bodies can be made of a material that is inert to the two or more fluids and/or the fluid product. In some embodiments, each of the spheroidal bodies is made of a material selected from the group consisting of glasses, quartz, plastics, polymers, metals, rubbers, and ceramics. Metals include stainless steel, nickel, and chromium-plated metals. Plastics and polymers include poly(methyl methacrylate), polytetrafluoroethylenes, PFAs, polypropylenes, nylons, polyethylenes, polycarbonates, and polyamide-imides. Rubbers include fluoroelastomers and silicones. Ceramics include aluminum oxide, zirconium oxide, silicon nitride, and silicon carbide. Each of the plurality of spheroidal bodies can further be made of a material that is minimally porous, and/or that the two or more fluids and/or the fluid product do not adhere to.
[0055] Each of the plurality of spheroidal bodies can have a coating. In some embodiments, the coating of each spheroidal body is inert to the two or more fluids and/or the fluid product. In some embodiments, the fluid product is a product of a reaction between the two or more fluid products that is catalyzed by the coating of each spheroidal body.
[0056] The plurality of spheroidal bodies can include a first set of spheroidal bodies and a second set of spheroidal bodies. The first set of spheroidal bodies can have a first average outer diameter and the second set of spheroidal bodies can have a second average outer diameter that is different from the first average outer diameter.
[0057] The static mixer can further comprise a first stopper and a second stopper. The first stopper can be positioned in the tubular mixer body adjacent the first end opening and can be configured to admit the two or more fluids into the mixing chamber. The second stopper can be positioned in the tubular mixer body adjacent the second end opening and can be configured to discharge the fluid product out of the mixing chamber. Each of the first stopper and the second stopper can be configured to retain the plurality of spheroidal bodies in the mixing chamber.
[0058] In some embodiments, each of the first stopper and the second stopper have a V-shaped cross section. In some embodiments, each of the first stopper and the second stopper have a prismatic shape. In some embodiments, each of the first stopper and the second stopper have a toroidal shape. In some embodiments, each of the first stopper and the second stopper is made of a material that is inert to the two or more fluids and/or the fluid product. In some embodiments, each of the first stopper and the second stopper is made of a material selected from the group consisting of glasses, quartz, plastics, polymers, metals, rubbers, and ceramics. Metals include stainless steel, nickel, and chromium-plated metals. Plastics and polymers include poly(methyl methacrylate), polytetrafluoroethylenes, PFAs, polypropylenes, nylons, polyethylenes, polycarbonates, and polyamide-imides. Rubbers include fluoroelastomers and silicones. Ceramics include aluminum oxide, zirconium oxide, silicon nitride, and silicon carbide. In some embodiments, the first stopper and the second stopper are maintained in position by tube compression fittings, bonding, swaging, and/or barbed connectors.
[0059] the tubular mixer body has a first tapered portion at the first end of the tubular mixer body and a second tapered portion at the second end of the tubular mixer body. The first tapered portion is designed to contain the first stopper in the tubular mixer body at the first end, and the second tapered portion is designed to contain the second stopper in the tubular mixer body at the second end. In some embodiments, each of the first stopper and the second stopper are designed to prevent the plurality of spheroidal bodies from obstructing the flow of the two or more fluids at the first tapered portion and at the second tapered portion, respectively.
[0060] In some embodiments, the first tapered portion and the second tapered portion have a non-circular cross-section designed to contain the plurality of spheroidal bodies while permitting the flow of the two or more fluids.
[0061] In some embodiments, the static mixer further comprises a first fastener positioned outside the first end of the tubular mixer body and a second fastener positioned outside the second end of the tubular mixer body, wherein the first fastener and the second fastener respectively define the first tapered portion and the second tapered portion. In some embodiments, each of the first fastener and the second fastener is a nut or ferrule. In some embodiments, each of the first fastener and the second fastener provides a connection point to the static mixer. In some embodiments, each of the first fastener and the second fastener is a tube compression fitting.
[0062] The flow of the two or more fluids can be received into the first end opening of the tubular mixer body at a first pressure and the fluid product can be discharged at the second end opening of the tubular mixer body at a second pressure that is lower than the first pressure.
[0063] The mixing chamber can preferably have a length of between about 100 mm and about 2000 mm. The inner diameter of the mixing chamber can preferably be between 1 and 10 mm. The plurality of spheroidal bodies can include from about 10 to about 2000 spheroidal bodies.
[0064] The static mixer of the present disclosure can be used to achieve an efficient mixing of NO and O.sub.3. In some embodiments, the mixing chamber has a length sufficient to ensure that the NO and O.sub.3 mix, by the turbulence, to produce NO.sub.2 as the fluid product is conveyed toward the second end opening of the tubular mixer body.
[0065] In accordance with a second aspect of the present disclosure, there is provided a method for mixing two or more fluids to produce a fluid product using the static mixer, as described in relation to the first aspect. The method comprises: receiving, by the first end opening at the first end of the tubular mixer body, a flow of the two or more fluids into the mixing chamber of the tubular mixer body; passing the flow of two or more fluids through the mixing chamber towards the second end opening at the second end of the tubular mixer body; inducing, by the plurality of spheroidal bodies positioned in the mixing chamber, turbulence in the flow of the two or more fluids to mix the two or more fluids; and providing, at the second end of the tubular mixer body, the flow of the fluid product.
[0066] To gain a better understanding of the invention described herein, the following examples are set forth. It will be understood that these examples are intended to describe illustrative embodiments of the invention and are not intended to limit the scope of the invention in any way.
EXAMPLES
[0067]
[0068] In the embodiment of
[0069] In the embodiment of
[0070] In the embodiment of
[0071] The embodiment of
[0072]
[0073]
[0074]
[0075]
[0076]
[0077]
[0078] The design of the static mixer 100 of the present disclosure has been found to provide efficient mixing of two or more fluids to form a mixed fluid product. In particular, it has been established that the conversion of reactant molecules in a fluid sample (such as a conversion of NO and O.sub.3 to NO.sub.2 in a gas sample) can be achieved by a static mixer 100 having a short length and without increasing the pressure of the fluid sample.
[0079] Without being bound by theory, it is believed that the design of the static mixer 100 of the present disclosure provides a confined flow pathway for the two or more fluids to flow through such that the two or more fluids efficiently mix. It is believed that, as the flow of the two or more fluids meanders around each spheroidal body 120 and passes through areas of the mixing chamber 114 that are alternatively constricted or dilated, turbulence is induced in the flow of the two or more fluids to cause them to mix. With the changes in area of the mixing chamber 114, it is believed that the flow of the two or more fluids will experience local changes in pressure.
[0080] It has been observed that, for achieving a full conversion of NO and O.sub.3 to NO.sub.2 by mixing, a static mixer 100 of the present disclosure can have a length that is 10% of that of a conventional static mixer. It has further been observed that reducing the length of the conventional static mixer to 10% results in only 20% of the NO and O.sub.3 being converted to NO.sub.2.
[0081]
[0082] It is obvious that the foregoing embodiments of the disclosure are examples and can be varied in many ways. Such present or future variations are not to be regarded as a departure from the spirit and scope of the disclosure, and all such modifications as would be obvious to one skilled in the art are intended to be included within the scope of the following claims.
[0083] The scope of the claims should not be limited by the preferred embodiments set forth in the disclosure, but should be given the broadest interpretation consistent with the disclosure as a whole.