High-gravity rotating bed device having new structure and application thereof

Abstract

A high-gravity rotating bed device, including a motor, a rotor and a housing. The rotor and the motor are entirely arranged within the housing. A load-bearing plate is provided within the housing. The load-bearing plate divides the housing into a reaction chamber and a balance chamber. The motor is arranged within the balance chamber. A transmission shaft of the motor passes through the load-bearing plate and is fixedly connected to the rotor arranged within the reaction chamber. A gas inlet, a gas outlet, a liquid inlet and a liquid outlet are arranged on the housing. An externally communicating pipeline is arranged on the balance chamber. Also disclosed is an application of the present high-gravity rotating bed device under high-pressure conditions in operations such as mixing, transferring and reacting.

Claims

1. A high-gravity rotating bed device having a new structure, comprising a motor, a rotor and a housing, wherein both the rotor and the motor are arranged in the housing; a bearing plate is arranged in the housing, and the bearing plate divides the housing into a reaction chamber and a balance chamber; the motor is arranged in the balance chamber, and a transmission shaft of the motor passes through the bearing plate to be fixedly connected to the rotor arranged in the reaction chamber; a gas inlet, a gas outlet, a liquid inlet and a liquid outlet are formed on the housing; and a pipeline communicated with the outside is arranged on the balance chamber.

2. The motor built-in high-gravity rotating bed device according to claim 1, wherein the reaction chamber is positioned above the bearing plate, and the balance chamber is positioned below the bearing plate; the gas inlet is formed on a side wall of the reaction chamber, the gas outlet extends out of the reaction chamber from a center of the rotor, and the liquid inlet is connected to a liquid distributor at a peripheral position of a hollow part of the rotor; and the liquid outlet extends out of the reaction chamber from an upper opening of the bearing plate.

3. The motor built-in high-gravity rotating bed device according to claim 2, wherein a pipeline is arranged at a lower end of the motor to be communicated with the reaction chamber.

4. The motor built-in high-gravity rotating bed device according to claim 1, wherein the reaction chamber is positioned below the bearing plate, and the balance chamber is positioned above the bearing plate; the gas inlet is formed on a side wall of the reaction chamber, the gas outlet extends out of the reaction chamber from a center of the rotor, and the liquid inlet is connected to the liquid distributor at the peripheral position of a hollow part of the rotor; and the liquid outlet is formed at a bottom of the reaction chamber.

5. The motor built-in high-gravity rotating bed device according to claim 1 wherein the motor is a shielding motor.

6. Application of the device according to claim 1 in operation processes of mixing, transfer and reaction in a high-pressure environment, wherein a rotating speed of the motor is 20 to 3,000 rpm, an operation temperature in the reaction chamber is 40 to 400° C., and an operation pressure in the reaction chamber is 0.05 to 50 MPa.

7. The application according to claim 6, wherein when material reaction is performed in the reaction chamber, protective gas is introduced into the balance chamber through an external pipeline, so that the pressures in the reaction chamber and the balance chamber are balanced.

8. The application according to claim 6, wherein the rotating speed of the motor is 500 to 3,000 rpm, the operation temperature in the chambers is 100 to 400° C., and the operation pressures in the chambers are 1 to 50 MPa.

9. The application according to claim 6, wherein the rotating speed of the motor is 2,000 to 3,000 rpm, the operation temperature in the chambers is 300 to 400° C., and the operation pressures in the chambers are 20 to 50 Mpa.

Description

BRIEF DESCRIPTION OF DRAWINGS

(1) FIG. 1 is a structural schematic diagram of a high-gravity rotating bed device of embodiment 1 of the invention;

(2) FIG. 2 is a structural schematic diagram of a high-gravity rotating bed device of embodiment 2 of the invention;

(3) FIG. 3 is a flow schematic diagram of the mixing, transfer and reaction processes of the motor built-in high-gravity rotating bed device of the invention;

(4) wherein:

(5) 10—motor; 20—rotor; 30—housing; 31—bearing plate; 32—reaction chamber; 33—balance chamber; 331—pipeline communicated with outside; 34—gas inlet; 35—gas outlet; 36—liquid inlet; 361—liquid distributor; 37—liquid outlet; 13—steel cylinder; 141, 142, 143—valve; 151, 152, 153—flowmeter; 161, 162—pump; 171, 172, 173—storage tank.

DETAILED DESCRIPTION OF THE EMBODIMENTS

(6) The implementation solution of the invention will be further illustrated below in conjunction with the accompanying drawings and embodiments. However, the invention is not limited to the listed embodiments.

(7) Embodiment 1

(8) With reference to FIG. 1, a high-gravity rotating bed device having a new structure comprises a motor 10, a rotor 20 and a housing 30;

(9) both the rotor 20 and the motor 10 are arranged in the housing 30;

(10) the motor 10 is a shielding motor; motors made of different materials can be selected according to the mixing, transfer and reaction processes of different media to be used as the shielding motor arranged in the housing; members in the motor arranged in the housing cannot react with gas or liquid in chambers;

(11) a bearing plate 31 is arranged in the housing 30, and the bearing plate 31 divides the housing 30 into a reaction chamber 32 and a balance chamber 33;

(12) the motor 10 is arranged in the balance chamber 33 and is fixed on the bearing plate 31, and the weight of the motor 10 is borne by the bearing plate 31; a transmission shaft of the motor 10 passes through the center of the bearing plate 31 to be fixedly connected to the rotor 20 arranged in the reaction chamber 32;

(13) a gas inlet 34, a gas outlet 35, a liquid inlet 36 and a liquid outlet 37 are formed on the housing 30;

(14) the reaction chamber 32 is positioned above the bearing plate 31, and the balance chamber 33 is positioned below the bearing plate 31; the gas inlet 34 is formed on the side wall of the reaction chamber 32, the gas outlet 35 extends out of the reaction chamber 32 from the center of the rotor 20, and the liquid inlet 36 is connected to a liquid distributor 361 at the peripheral position of a hollow part of the rotor 20; the liquid outlet 37 extends out of the reaction chamber 32 from an upper opening of the bearing plate 31;

(15) a pipeline 331 communicated with the outside is arranged on the balance chamber 33; and a pipeline is arranged at the lower end of the motor 10 to be communicated with the reaction chamber 32, so that liquid leaked into a collection tank (not shown in the figure) at the lower end of the motor 10 is returned to the reaction chamber 32 to be discharged.

(16) By arrangement of the two chambers, when rotor packing needs a high temperature and a high pressure, the two chambers also can reach pressure balance in short time, even though little leakage is generated between an output shaft of the motor and the bearing plate, so that tight sealing is not required and the problem of difficulty in sealing in the high-pressure process is solved.

(17) It is more important that protective gas (e.g., inert gas) can be directly introduced into the balance chamber 33 through the pipeline 331 communicated with the outside, and a pressure of the protective gas is matched with a pressure in the reaction chamber, thereby ensuring pressure stability in the reaction chamber and stable material reaction.

(18) Application of the above device in the operation processes of mixing, transfer, reaction and the like in a high-pressure environment adopts the following parameter conditions: a rotating speed of the motor is preferably 20 to 3,000 rpm, an operation temperature in the reaction chamber is preferably −40 to 400° C., and operation pressures in the reaction chamber and in the balance chamber are the same, preferably 0.05 to 50 MPa.

(19) According to a further improved embodiment, the rotating speed of the motor is preferably 500 to 3,000 rpm, the operation temperature in the reaction chamber is preferably 100 to 400° C., and the operation pressures in the reaction chamber and in the balance chamber are the same, preferably 1 to 50 MPa.

(20) According to a much further improved embodiment, the rotating speed of the motor is preferably 2,000 to 3,000 rpm, the operation temperature in the chamber is preferably 300 to 400° C., and the operation pressures in the reaction chamber and in the balance chamber are the same, preferably 20 to 50 MPa.

(21) Embodiment 2

(22) With reference to FIG. 2, a high-gravity rotating bed device having a new structure comprises a motor 10, a rotor 20 and a housing 30;

(23) both the rotor 20 and the motor 10 are arranged in the housing 30;

(24) the motor 10 is a shielding motor; motors made of different materials can be selected according to the mixing, transfer and reaction processes of different media to be used as the shielding motor arranged in the housing; members in the motor arranged in the housing cannot react with gas or liquid in chambers;

(25) a bearing plate 31 is arranged in the housing 30, and the bearing plate 31 divides the housing 30 into a reaction chamber 32 and a balance chamber 33;

(26) the motor 10 is arranged in the balance chamber 33 and is fixed on the bearing plate 31, and the weight of the motor 10 is borne by the bearing plate 31; a transmission shaft of the motor 10 passes through the center of the bearing plate 31 to be fixedly connected to the rotor 20 arranged in the reaction chamber 32;

(27) a gas inlet 34, a gas outlet 35, a liquid inlet 36 and a liquid outlet 37 are formed on the housing 30;

(28) the reaction chamber 32 is positioned below the bearing plate 31, and the balance chamber 33 is positioned above the bearing plate 31; the gas inlet 34 is formed on the side wall of the reaction chamber 32, the gas outlet 35 extends out of the reaction chamber 32 from the center of the rotor 20, and the liquid inlet 36 is connected to a liquid distributor 361 at the peripheral position of a hollow part of the rotor 20; the liquid outlet 37 is formed at the bottom of the reaction chamber 37; and

(29) a pipeline 331 communicated with the outside is arranged at the bottom of the balance chamber 33.

(30) Application of the above device in the operation processes of mixing, transfer, reaction and the like in a high-pressure environment adopts the following parameter conditions: a rotating speed of the motor is preferably 20 to 3,000 rpm, an operation temperature in the reaction chamber is preferably −40 to 400° C., and operation pressures in the reaction chamber and in the balance chamber are the same, preferably 0.05 to 50 MPa.

(31) According to a further improved embodiment, the rotating speed of the motor is preferably 500 to 3,000 rpm, the operation temperature in the reaction chamber is preferably 100 to 400° C., and the operation pressures in the reaction chamber and in the balance chamber are the same, preferably 1 to 50 MPa.

(32) According to a much further improved embodiment, the rotating speed of the motor is preferably 2,000 to 3,000 rpm, the operation temperature in the chamber is preferably 300 to 400° C., and the operation pressures in the reaction chamber and in the balance chamber are the same, preferably 20 to 50 MPa.

(33) Embodiment 3

(34) With reference to FIG. 3, mixing of suspension and latex under a high pressure in the preparation of a rubber composite material is taken as an example:

(35) 1), firstly, polyurethane latex is pumped into a reaction chamber by a pump, then suspension is pumped into the reaction chamber, with concentration of the suspension being 55% (on the basis of percentage by mass of suspended substances in the suspension); and

(36) 2), a rotating speed of a motor is regulated to 2,000 rpm, which results in that a flowing Reynolds number of the suspension is enabled not to be smaller than 1,000, finally nitrogen is introduced into the reaction chamber through a gas inlet, a system is pressurized to 20 MPa, latex with the suspension is obtained after a period of sufficient mixing, the latex with the suspension is conveyed to a next process, and finally, the rubber composite material is prepared.

(37) Embodiment 4

(38) With reference to FIG. 3, in the measurement of phase equilibrium data of a biodiesel preparation system, mixing of raw materials methanol and soybean oil is taken as an example:

(39) different initial alcohol-to-oil molar ratios are adopted to measure liquid-liquid phase equilibrium data of a methanol and soybean oil system at a high temperature and under a high pressure, firstly, a vacuum pump is started to vacuumize the system, and the methanol and the soybean oil at a certain molar ratio are added into the reaction chamber by a high-pressure pump; a rotating speed of a motor is regulated to 550 rpm to start to stir and a heating system is started; stirring is stopped when a temperature in a high-gravity rotating bed device is constant at 160° C. and the methanol and the soybean oil are uniformly mixed, standing is carried out for 4 h, at the moment, the pressure is 10.11 Mpa, and then upper layer equilibrium liquid and lower layer equilibrium liquid are respectively collected and are analyzed by gas chromatography.

(40) Embodiment 5

(41) With reference to FIG. 3, mass transfer of triethylene glycol dehydration is taken as an example:

(42) 1), natural gas with free liquid and solid impurities being removed is introduced into the reaction chamber by a gas inlet, wherein content of water vapor in the natural gas is 0.092%;

(43) 2), triethylene glycol with a pressure of 7.95 Mpa, a temperature of 42° C. and barren mass fraction of 98.5% is pumped into the reaction chamber by a pump in a storage tank, water vapor in the natural gas is adsorbed by the triethylene glycol, and a rotating speed is regulated to 800 rpm; and

(44) 3), protective gas is introduced into a balance chamber of a high-gravity rotating bed device by an external pipeline, both pressures in the reaction chamber and in the balance chamber are guaranteed to be 7.95 Mpa, and after sufficient reaction, content of the water vapor at a gas outlet is 0.008696%.

(45) Embodiment 6

(46) With reference to FIG. 3, mass transfer of calcium chloride dehydration is taken as an example:

(47) 1), a desiccant calcium chloride is filled into the position of packing, and a temperature and a pressure of natural gas introduced into a housing are respectively 35° C. and 6.42 Mpa, wherein content of water vapor in the natural gas is 0.105%;

(48) 2), protective gas is introduced into a balance chamber of a high-gravity rotating bed device through an external pipeline, and both pressures in a reaction chamber and in the balance chamber are guaranteed to be 6.42 Mpa; and

(49) 3), a rotating speed is regulated to 1,050 rpm, and after sufficient adsorption of calcium chloride, content of the water vapor at a gas outlet is 0.009787%.

(50) Embodiment 7

(51) With reference to FIG. 3, reaction of hydrogen sulfide in natural gas and diethanol amine is taken as an example:

(52) 1), the natural gas with a pressure of 1.85 Mpa and a temperature of 50° C. is introduced into a reaction chamber through the gas inlet, the natural contains 1,960 ppm of harmful gas hydrogen sulfide, and the diethanol amine is pumped into the reaction chamber by a pump in a storage tank to react with the hydrogen sulfide;

(53) 2), a rotating speed of a rotating bed is regulated to 600 rpm, the type of packing is SiC, and a specific surface area of the packing is 600 m.sup.2/m.sup.3;

(54) 3), protective gas is introduced into a balance chamber of a high-gravity rotating bed device through an external pipeline, and both pressures in the reaction chamber and in the balance chamber are guaranteed to be 1.85 Mpa; and

(55) 4), after sufficient reaction in the reaction chamber, content of the harmful gas hydrogen sulfide in gas at an outlet of the rotating bed is 20 ppm.

(56) Embodiment 8

(57) With reference to FIG. 3, reaction of sulfur dioxide in natural gas and ammonium sulfite solution is taken as an example:

(58) 1), the natural gas with a pressure of 1.5 Mpa and a temperature of 45° C. is introduced into a reaction chamber ghrough a gas inlet, the natural gas contains 2,185 ppm of harmful gas sulfur dioxide, and the ammonium sulfite solution is pumped into the reaction chamber by a pump in a storage tank to react with the sulfur dioxide;

(59) 2), a rotating speed of a rotating bed is regulated to 750 rpm, the type of packing is sintered ceramic, and a specific surface area of the packing is 850 m.sup.2/m.sup.3;

(60) 3), protective gas is introduced into a balance chamber of a high-gravity rotating bed device through an external pipeline, and both pressures in the reaction chamber and in the balance chamber are guaranteed to be 1.5 Mpa; and

(61) 4), after sufficient reaction in the reaction chamber, content of the harmful gas sulfur dioxide in gas at an outlet of the rotating bed is 53 ppm.

(62) Obviously, the described embodiments of the invention are merely examples for clearly illustrating the invention, but not intended to limit embodiments of the invention. A person of ordinary skill in the art can make other different forms of variations or modifications based on the illustrations above. All embodiments cannot be exhausted herein. Any obvious variations or modifications derived from the technical solution of the invention shall fall within the scope of protection of the invention.