METHOD OF VACUUM MEMBRANE FILTRATION

Abstract

A method of vacuum membrane filtration including placing a membrane filter between a filtration base and a pouring funnel, an upper side of the filtration base having a membrane bearing area with a bearing structure and a supporting contour surrounding the bearing structure and the supporting contour having at least one notch in flow connection with a bottom side of the membrane bearing area, detachably mounting the pouring funnel on the filtration base thereby clamping the membrane filter between the filtration base and the pouring funnel, applying suction to the filtration base such that the membrane filter is pulled against the bearing structure and comes into contact with the supporting contour, and dismounting the pouring funnel from the filtration base while still applying the suction, causing an outer rim of the membrane filter to bulge upward from the supporting contour and uncover the at least one notch.

Claims

1. A method of vacuum membrane filtration, comprising steps of: placing a membrane filter between a filtration base and a pouring funnel, an upper side of the filtration base having a membrane bearing area with a bearing structure and a supporting contour surrounding the bearing structure for the membrane filter placed in the membrane bearing area, the supporting contour having at least one notch in flow connection with a bottom side of the membrane bearing area; detachably mounting the pouring funnel on the filtration base, thereby clamping the membrane filter between the filtration base and the pouring funnel; applying suction to the filtration base such that the membrane filter is pulled against the bearing structure and comes into contact with the supporting contour; and dismounting the pouring funnel from the filtration base while still applying the suction, causing an outer rim of the membrane filter to bulge upward from the supporting contour and uncover the at least one notch.

2. The method according to claim 1, further comprising a step of filling the funnel with a liquid volume after detachably mounting the pouring funnel on the filtration base, wherein as the suction is applied to the filtration base the liquid volume is filtered.

3. The method according to claim 2, wherein as the outer rim of the membrane filter is bulged upward from the supporting contour, and the at least notch is uncovered, residual liquid present below the membrane filter is sucked off.

4. The method according to claim 1, wherein the membrane filter covers the at least one notch when the membrane filter is clamped between the filtration base and the pouring funnel and the suction is applied to the membrane filter via a lower side of the filtration base.

5. The method according to claim 1, wherein the at least one notch interrupts a circumferential edge between the bearing structure and the supporting contour.

6. The method according to claim 5, wherein the at least one notch is delimited by sharp edges.

7. The method according to claim 6, wherein the at least one notch extends into the supporting contour.

8. The method according to claim 1, wherein an outside of the supporting contour adjoins a sealing face onto which a rim of the membrane filter is pressed by the pouring funnel being mounted onto the filtration base.

9. The method according to claim 8, wherein the at least one notch does not extend into the sealing face.

10. The method according to claim 8, wherein the bearing structure and the sealing face are arranged offset to each other and in that a difference in height between the bearing structure and the sealing face is bridged by the supporting contour being at an incline.

11. The method according to claim 1, wherein the membrane bearing area has an outer diameter of 15 to 55 mm and the at least one notch is formed at a distance of 2 to 10 mm from the outer diameter.

12. The method according to claim 1, wherein the supporting contour is annular and the at least one notch is a plurality of notches spaced apart from each other in a circumferential direction.

13. The method according to claim 12, wherein each angular distance between the notches is of equal size.

14. The method according to claim 12, wherein the notches have a width of 0.1 to 4 mm in the circumferential direction.

15. The method according to claim 12, wherein the notches have a depth of 0.1 to 1.5 mm.

16. The method according to claim 1, wherein the at least one notch is a prolongation of a discharge groove formed in the bearing structure.

17. The method according to claim 1, wherein the filtration base is made of a sterilizable plastic material.

18. The method according to claim 1, wherein the membrane filter is clamped between a sealing face surrounding the supporting contour and a bulge of the pouring funnel.

19. The method according to claim 1, further comprising a step of mounting the filtration base on a suction device for applying the suction to the filtration base.

20. The method according to claim 19, wherein the filtration base, the pouring funnel, and/or the suction device are made of a sterilizable plastic material.

Description

BRIEF DESCRIPTION OF THE DRAWINGS

[0026] Further features and advantages of the invention will become apparent from the description below and from the accompanying drawings to which reference is made and in which:

[0027] FIG. 1 shows a side view of a filtration device according to the invention;

[0028] FIG. 2 shows a perspective view of the filtration base according to the invention of the filtration device of FIG. 1;

[0029] FIG. 3 shows a side sectional view of the filtration base of FIG. 2;

[0030] FIG. 4 shows a perspective view of a boundary area of the filtration base of FIG. 3;

[0031] FIG. 5 shows a top view of a boundary area of the filtration base of FIG. 3; and

[0032] FIG. 6 is a cutaway detailed view of the clamping area of the filtration device of FIG. 1.

DETAILED DESCRIPTION OF THE INVENTION

[0033] FIG. 1 shows a filtration device 10 intended for vacuum membrane filtration applications. A pouring funnel 14 is detachably mounted on a filtration base 12. The filtration base 12 and the funnel 14 are typically reusable stainless steel units. However, in the present case, designs made of plastic material which are adapted to be pre-sterilized and which are intended for a single use are preferred.

[0034] A membrane filter 16 (see sectional view in FIG. 6) is clamped between the filtration base 12 and the funnel 14.

[0035] The filtration device 10 can be mounted on a suction strip or on another suction device made of stainless steel (multiple use) or of plastic material (single use). To this end, a recess 18 is provided in the filtration base 12, which together with a matching projection on a connection piece of the suction device forms a bayonet lock. The fixation may also be realized by means of a plug-in connection in which no rotary movement as with the bayonet lock is required.

[0036] The filtration base 12 is shown separately in FIGS. 2 and 3. The basic circular filtration base 12 has an upper first cylindrical portion 20 having a preferred outer diameter of 49 mm and a lower second cylindrical portion 22 below the shoulder. The funnel 14 is pushed onto the first cylindrical portion 20, a circumferential shoulder 24 serving as a bearing surface for the front side of the funnel 14. The lower cylindrical portion 22 is connected to the connection piece of the suction device via the bayonet lock or the plug-in connection such that the connection piece is pressed against a sealing contour 26 and/or a limiting wall 38 of the filtration base 12, which will be explained in more detail later. A tight connection to a vacuum (negative pressure) provided by the suction device is thus ensured.

[0037] As can be seen in FIGS. 3 to 5, the filtration base 12 has on its upper side a membrane bearing area 30, which is divided into an annular sealing face 28 adjoining the upper cylindrical portion 20, a supporting contour 32 adjoining the sealing face 28, and a profiled bearing structure 34 surrounded by the supporting contour 32. Both the sealing face 28 and the profiled bearing structure 34 extend substantially in a plane which is perpendicular to the central axis of the filtration base 12. However, the profiled bearing structure 34 is offset downwards with respect to the sealing face 28, the supporting contour 32 extending between the profiled bearing structure 34 and the raised annular sealing face 28.

[0038] On the one hand, the supporting contour 32 constitutes a defined delimitation to the annular sealing face 28, on the other hand, it may be designed as a prolongation of the profiled bearing structure 34 or as another profiled structure (e.g., with steps) or as a flat surface. In either case, the supporting contour 32 bridges the axial height difference between the profiled bearing structure 34 and the sealing face 28.

[0039] The membrane bearing area 30 is interrupted in the middle by a central discharge 36 which creates a flow connection to the area below the membrane bearing area 30 and thus to the suction device. The downward projecting limiting wall 38 of the discharge 36 can be used as a sealing face 28 for the connection to the suction device in addition or alternatively to the sealing contour 26.

[0040] The profiled bearing structure 34 of the membrane bearing area 30 has a multitude of concentric grooves, other structures being however also possible. Several discharge grooves 40, 42 ensure that the liquid that has passed through the membrane filter 16 can reach the discharge 36. The discharge grooves 40, 42 are evenly distributed in the circumferential direction and run straight in a radial direction. In the example embodiment shown, four large discharge grooves 40 are provided at 90° intervals and 12 small discharge grooves 42 are provided at 30° intervals.

[0041] As can be seen in the detailed views of FIGS. 4 and 5, the large discharge grooves 40 extend outwards not completely up to the inclined supporting contour 32, while the small discharge grooves 42 each end in a notch 44 in the supporting contour 32. The notch 44 interrupts a circumferential edge 46 between the supporting contour 32 and the profiled bearing structure 34. The contour 32 supporting the membrane filter 16 is thus interrupted in the circumferential direction at an angular distance of respectively 30° by a notch 44.

[0042] The notches 44, which are delimited by sharp edges, each have a width of 1.0 mm and a depth of 1.4 mm and are located in an area that is inwardly spaced by 4.6 mm to 5.6 mm from the outer circumference of the upper cylindrical portion 20.

[0043] In the example embodiment shown, the notches 44 extend radially into the supporting contour 32 (see FIGS. 4 and 5). Depending on the material used and the precision of the manufacturing process, this radial extension is not absolutely necessary for the function of the notches 44 as explained further below, but is particularly recommended if the filtration base 12 is manufactured as an injection-molded plastic part.

[0044] The filtration operation of the filtration device 10 and the subsequent aeration are described in the following.

[0045] Prior to the filtration operation, a membrane filter 16 is placed onto the upper side of the filtration base 12, and the pouring funnel 14 is put onto the filtration base 12. An inwardly directed circumferential bulge 48 of the funnel 14 thus presses the outer rim of the membrane filter 16 firmly onto the sealing face 28 of the filtration base 12, as shown in the detailed view of FIG. 6.

[0046] Although, in principle, filtration with overpressure on the side of the funnel 14 is also possible, the filtration device 10 is usually connected to a suction device which creates a vacuum below the filtration base 12 in order to suck the liquid contained in the funnel 14 through the membrane filter 16 clamped between the filtration base 12 and the funnel 14. The membrane filter 16 is thus pulled against the profiled bearing structure 34 of the membrane bearing area 30 and comes into contact with the supporting contour 32. The liquid sucked in by the membrane filter 16 is directed through the profiled bearing structure 34 and the discharge grooves 40, 42 to the discharge 36.

[0047] After filtration, the funnel 14 is removed while the vacuum is still applied. Since the membrane filter 16 is now no longer pressed against the sealing face 28 by the funnel 14, the rim of the wetted membrane filter 16, which is still attracted to the filtration base 12 by the vacuum, may bulge upwards, as shown in the detailed views in FIGS. 5 and 6. However, the membrane filter 16 still rests firmly against the inclined supporting contour 32 and the edge 46 between the supporting contour 32 and the sealing face 28, such that no ambient air can get below the membrane filter 16 in these contact areas.

[0048] However, since the edge 46 between the supporting contour 32 and the profiled bearing structure 34 is interrupted by the notches 44, air is sucked through the notches 44 into the small discharge grooves 42 and thus into the area below the membrane filter 16 at these points due to the vacuum applied.

[0049] As already explained, the notches 44 are very small (width in the circumferential direction and depth) and are delimited by sharp edges. For this reason, in case of a negative pressure typical of a filtration process, a commercially available membrane filter 16 in the wetted state is not drawn into the notches 44 due to its stiffness and does not hinder the suction of air or the removal of the residual liquid. If the notches 44 extend radially into the supporting contour 32, as in the example embodiment shown, the suction of air through the notches 44 is ensured even if the edges of the notches 44 are less sharp, e.g., due to manufacturing tolerances.

[0050] Due to the sucked-in air, the volume of liquid present below the membrane filter 16 can flow off through the discharge 36. Furthermore, due to the aeration, it is relatively easy to lift the membrane filter 16 off the filtration base 12 despite the vacuum applied.