The present invention relates to a method for producing a modified polymerization initiator, and more particularly, to a method for preparing a modified polymerization initiator, wherein the method includes the steps of: (S1) introducing a first fluid and a second fluid into a reactor, and reacting the compounds included in the fluids, and (S2) obtaining the modified polymerization initiator prepared by the reaction of the step (S1) through an outlet of the reactor, wherein the step (S1) and step (S2) are continuously performed, wherein in the step (S1), the flow amount of the first fluid and the second fluid is maintained constant at the time when the first fluid and the second fluid are mixed, and the flow rate of the first fluid is increased. Also, the present invention provides an apparatus for producing a modified polymerization initiator for performing the same.

Methods and systems for temperature-controlled, on-site generation of peracids, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions are disclosed. In particular, methods for using an adjustable biocide formulator or generator system overcome the limitations of temperature on the kinetics of the peracid generation and/or peracid decomposition inside an adjustable biocide formulator or generator system. The methods include the controlling of the temperature of at least one raw starting material, namely water, to improve upon methods of on-site generation of peracids. The methods allow for the generation of user-selected chemistry without regard to the ambient temperatures of the raw starting materials and/or the biocide formulator or generator system.

Methods and systems for temperature-controlled, on-site generation of peracids, namely peroxycarboxylic acids and peroxycarboxylic acid forming compositions are disclosed. In particular, methods for using an adjustable biocide formulator or generator system overcome the limitations of temperature on the kinetics of the peracid generation and/or peracid decomposition inside an adjustable biocide formulator or generator system. The methods include the controlling of the temperature of at least one raw starting material, namely water, to improve upon methods of on-site generation of peracids. The methods allow for the generation of user-selected chemistry without regard to the ambient temperatures of the raw starting materials and/or the biocide formulator or generator system.

A reactor according to an embodiment of the present invention, the reactor including: a mixing chamber formed as a circular tube; a first injection nozzle connected to the mixing chamber while maintaining a predetermined spacing along a circumferential direction and configured to inject a first mixture; an annular chamber disposed spaced apart from an outer side of the mixing chamber; a second injection nozzle configured to connect the annular chamber to the mixing chamber to inject a second mixture supplied to the annular chamber in a direction intersecting the injection of the first mixture; and an outlet pipe connected to the mixing chamber to discharge a reactant produced by mixing the first and second mixtures in the mixing chamber, in which the second injection nozzle is spaced apart from the first injection nozzle by a predetermined angle in the circumferential direction.

A reactor according to an embodiment of the present invention, the reactor including: a mixing chamber formed as a circular tube; a first injection nozzle connected to the mixing chamber while maintaining a predetermined spacing along a circumferential direction and configured to inject a first mixture; an annular chamber disposed spaced apart from an outer side of the mixing chamber; a second injection nozzle configured to connect the annular chamber to the mixing chamber to inject a second mixture supplied to the annular chamber in a direction intersecting the injection of the first mixture; and an outlet pipe connected to the mixing chamber to discharge a reactant produced by mixing the first and second mixtures in the mixing chamber, in which the second injection nozzle is spaced apart from the first injection nozzle by a predetermined angle in the circumferential direction.

The present invention relaters to a method for continuously preparing a nano zinc oxide with a membrane reactor. A zinc salt solution and a precipitator solution required for the preparation of a zinc oxide are respectively used as dispersion phases, and under the action of a certain pressure, the two reaction solutions respectively penetrate through a membrane tube at a certain rate and disperse quickly under the action of a shear force and react, producing a precursor precipitate. A precursor suspension penetrates through the membrane tube continuously and circularly after being pressurized by a pump, and at the same time, deionized water as a washing fluid is added to a suspension storage tank, wherein impurity ions penetrate through membrane pores and are discharged along with the liquid medium; after the concentration of the impurity ions meets requirements, the concentrated solution is discharged continuously and then spray-dried to obtain a basic zinc carbonate precursor powder. The basic zinc carbonate powder is calcined under certain conditions to obtain the nanostructured zinc oxide powder. The continuous preparation and washing of a powder can be achieved by coupling a membrane washing technique with a membrane dispersion technique. The procedure is simple, the structure of zinc oxide is easy to control and the yield is high.

The present invention relaters to a method for continuously preparing a nano zinc oxide with a membrane reactor. A zinc salt solution and a precipitator solution required for the preparation of a zinc oxide are respectively used as dispersion phases, and under the action of a certain pressure, the two reaction solutions respectively penetrate through a membrane tube at a certain rate and disperse quickly under the action of a shear force and react, producing a precursor precipitate. A precursor suspension penetrates through the membrane tube continuously and circularly after being pressurized by a pump, and at the same time, deionized water as a washing fluid is added to a suspension storage tank, wherein impurity ions penetrate through membrane pores and are discharged along with the liquid medium; after the concentration of the impurity ions meets requirements, the concentrated solution is discharged continuously and then spray-dried to obtain a basic zinc carbonate precursor powder. The basic zinc carbonate powder is calcined under certain conditions to obtain the nanostructured zinc oxide powder. The continuous preparation and washing of a powder can be achieved by coupling a membrane washing technique with a membrane dispersion technique. The procedure is simple, the structure of zinc oxide is easy to control and the yield is high.

The disclosure provides a short-process separation system for separating ionic liquid from alkylation reaction effluent, comprising an alkylation reactor, an ionic liquid storage tank, a primary coalescence separator, a secondary coalescence separator, a flash tank, a low-temperature fine coalescence separator and a fractionating tower that are linked in order. The inlet of the ionic liquid storage tank communicates with the bottom flow ports of the primary coalescence separator, the secondary coalescence separator and the low-temperature fine coalescence separator through delivery lines, and the outlet of the ionic liquid storage tank communicates with the return port of the alkylation reactor through a delivery pump. The alkylated oil collected from this system has a high degree of cleanliness, and can be used directly as a component for formulating clean gasoline. The ionic liquid catalyst collected therefrom may be directly returned to the alkylation reactor for cycle use.

The disclosure provides a short-process separation system for separating ionic liquid from alkylation reaction effluent, comprising an alkylation reactor, an ionic liquid storage tank, a primary coalescence separator, a secondary coalescence separator, a flash tank, a low-temperature fine coalescence separator and a fractionating tower that are linked in order. The inlet of the ionic liquid storage tank communicates with the bottom flow ports of the primary coalescence separator, the secondary coalescence separator and the low-temperature fine coalescence separator through delivery lines, and the outlet of the ionic liquid storage tank communicates with the return port of the alkylation reactor through a delivery pump. The alkylated oil collected from this system has a high degree of cleanliness, and can be used directly as a component for formulating clean gasoline. The ionic liquid catalyst collected therefrom may be directly returned to the alkylation reactor for cycle use.

A system and method for preparing a vanadium battery high-purity electrolyte, comprising preparing a low-valence vanadium oxide with a valence of 3.5 with liquid phase hydrolysis and fluidization reduction with vanadium oxytrichloride, adding clean water and sulfuric acid for dissolution, and further performing ultraviolet activation to obtain the vanadium electrolyte, for use in an all-vanadium redox flow battery stack. The high-temperature tail gas in the reduction fluidized bed is combusted for preheating the vanadium powder material, to recover the sensible heat and latent heat of the high-temperature tail gas, and the sensible heat of the reduction product is recovered through heat transfer between the reduction product and the fluidized nitrogen gas. An internal member is arranged in the reduction fluidized bed to realize the precise regulation of the valence state of the reduction product, and ultraviolet is used to activate the vanadium ions, improving the activity of the electrolyte.